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Home My WebLink About2015 SOIL REPORTDecember 9, 2015 Project No. 1143 -15 Ms. Diane Lopez Franzen -Hill Corporation 1100 North "J" Street Tulare, California 93274 SITE: Texaco Station, Panama Lane and Colony Street, Bakersfield, California SUBJECT: Soil Sample Analytical Results, November 6, 2015 Dear Ms. Lopez, This letter - report presents the. results of soil sampling associated with the upgrade of a fuel dispensing system at the above - referenced site on November 6, 2015. An Associated Soils Analysis; Inc. (Associated) field technician performed the sampling procedures under the direction of Mr. Shane Gardner, Fire Prevention Officer, Bakersfield Fire Department. PURPOSE AND SCOPE The purpose of the soil sampling was to provide information regarding a potential unauthorized release of fuel hydrocarbons, if any, into the subsurface beneath the former dispensers. The scope of work consisted of the following: • As requested by Mr. Shane Gardner, an Associated field technician collected eight soil samples at four locations. Two samples were collected below each of four fuel dispensers, one sample at approximately two feet and a deeper sample at five feet below ground surface (BGS); 1141 E. Batavia Court, Tulare, CA 93274 • P.O. Box 88, Tulare, CA 93275 Toll Free (800) ASA -1278 (272 -1278) ! Phone: (559) 688 -1011 • Fax (559) 688 -1195 E -Mail: Info@asaenv.com Texaco Station, Panama Lane and Colony Street, Bakersfield, California 1143-15.001 December 9, 2015 Page 2 • Transported the soil samples to ASSET Laboratories, Las Vegas, Nevada, a California - certified analytical laboratory. Soil samples were analyzed for benzene, toluene, ethylbenzene, and xylenes (BTEX); methyl tert -butyl ether (MTBE); total petroleum hydrocarbons, gasoline -range constituents (TPH -G); and a suite of volatile organic compounds that included 1,2- dichloroethane (1,2 -DCA), dibromoethane (1,2 -DBA), and naphthalene; • Prepared a vicinity map and soil sample location map; and • Prepared this letter - report. SITE INFORMATION The site is near the northwest corner of Panama Lane and Colony Street, Bakersfield, California. The site may also be found at latitude 36.317906 degrees north and longitude 119.032778 degrees east. Figure 1 is a vicinity map. Figures are attached. HYDROLOGICAL CONDITIONS Based on a cursory review of groundwater information available from the California Department of Water Resources' website, depth to groundwater in 2014 appears- to exceed 150 feet BGS in the vicinity of the site. SAMPLING AND ANALYTICAL PROCEDURES Figure 2 is a soil sample location map utilizing GoogleOR earth imagery. Sampling procedures and analytical testing are summarized in the following subsections. Texaco Station, Panama Lane and Colony Street, Bakersfield, California 1143 - 15.001 December 9, 2015 Page 3 Sampling Procedures: Two soil samples were collected from each of four hand -auger soil borings. Soil samples were collected at approximately two and five feet BGS utilizing a manually - operated slide - hammer. Discrete soil samples were collected in 1.5- inch - diameter by six- inch -long stainless steel sample sleeves. The samples were collected such that no headspace was allowed at either end of the sleeve. Field observations were made at the time of sampling to assess whether or not fuel hydrocarbon odors or -discoloration was present at the sample locations. The soil sample sleeves were each covered with Teflon® tape and fitted with plastic end caps immediately upon collection. The sample sleeves were labeled with information regarding the project number, soil sample number, sample depth, time, date, and name of the field technician. The sample sleeves were promptly placed into a zip locked bag in a precooled ice chest containing a bag of crushed ice. Chain -of- custody documentation was prepared for the samples retained for analytical testing. The chain -of- custody recorded the sampling date, sample depth, time, sample identification number, project name and address, field technician, project manager, and the requested analytes. Analytical Testing: Soil samples were transported to ASSET Laboratories, Las Vegas, Nevada, a California- certified laboratory. Soil samples were analyzed for BTEX, MTBE, and a suite of volatile organic compounds that included 1,2 -DBA, 1,2 -DCA, and naphthalene using United States Environmental Protection Agency's (U.S. EPA's) method 8260B. In addition, each sample was analyzed for TPH -G using U.S. EPA method 8015B. The laboratory report and chain -of- custody documentation are attached. Fd -111, ME 0 Soil sample .analytical results are summarized in Table l . Texaco Station, Panama Lane and Colony Street, Bakersfield, California ..1143- 15.001 December 9, 2015 Page 4 TABLE 3 SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS November 6, 2015 Soils encountered consisted of fine- grained brown silty sand. No fuel hydrocarbon odors or discoloration were noted during the drilling of the soil boring or during the discrete soil sampling. None of the constituents of concern were detected in any of the soil samples submitted for analytical testing. Approximate Ethyl - Sample Depth, Benzene, Toluene, benzene, Xylenes, MTBE, TPH -G, VOCs, Number Feet BGS m /glkg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg S1 2.0 ND ND ND ND ND ND ND S2 5.0 ND ND ND ND ND ND ND S3 2.0 ND ND ND ND ND ND ND S4 5.0 ND ND ND ND ND ND ND S5 2.0 ND ND ND ND ND ND ND S6 5.0 ND ND ND ND ND ND ND S7 2.0 ND ND ND ND ND ND ND S8 5.0 ND ND ND ND ND ND ND PQL 0.0050 0.0050 0.0050 0.0050- 0.0050 1.0 0.0050- 0.010 0.050 BGS Below ground surface MTBE Methyl tert -butyl ether mg/kg Milligrams per kilogram PQL Practical quantitation limit VOCs Volatile organic compounds ND Not detected at or above the PQL TPH -G Total petroleum hydrocarbons, gasoline -range constituents Soils encountered consisted of fine- grained brown silty sand. No fuel hydrocarbon odors or discoloration were noted during the drilling of the soil boring or during the discrete soil sampling. None of the constituents of concern were detected in any of the soil samples submitted for analytical testing. Texaco Station, Panama Lane and Colony Street, Bakersfield, California 1143- 15.001. December 9, 2015 Page 5 CONCLUSIONS Based upon the procedures and findings, the following conclusion is presented: • The presence of fuel hydrocarbons was not detected in any samples collected to a maximum depth of five feet below the fuel dispensers. RECOMMENDATIONS Based upon the findings and conclusions, the following recommendation is presented: • No further assessment appears warranted. LIMITATIONS This letter -report is for the sole use of Associated's client and involved regulatory agencies. Others who seek to rely on information presented herein have a duty to determine its adequacy for their intended use, time, and location. No assessment can eliminate uncertainty regarding the potential for recognized environmental conditions. This letter - report is intended to reduce, but not eliminate this uncertainty, recognizing reasonable limits of time and cost. Subsurface variations cannot be known, nor entirely accounted for, in spite of exhaustive testing. This letter -report should not be regarded as a guarantee that no further recognized environmental conditions are present on or beneath the site, beyond that which could have been reasonably detected within the scope of work. Associated's geologists and technicians perform their services only in areas of their competence, and under the guidance of a licensed PG, registered in the State of California. To the best of the PG's knowledge, all work was performed consistent with the California Business and Professions Code, Sections 7800 et seq., also known as the Geologist and Geophysicist Act. If any part of the work scope was not performed by a licensed PG, or by others working under Texaco Station, Panama. Lane and Colony Street, Bakersfield, .California 1143 - 15.001 December 9, 2015 Page 6 his/her guidance, that part, and any related parts thereof, may be unreliable. Parts of the work scope not performed under the direct supervision of a licensed PG will be identified in the text of the letter - report. The licensed PG shall be held faultless for any scope of work not performed under his/her direct supervision consistent with the Geologist and Geophysicist Act. This limitation is an integral part of all Associated reports (or workplans) subsequent to May 1, 2005. The findings, conclusions, and recommendations rendered in this letter - report are solely professional opinions based on information obtained during the assessment. Changes in existing conditions at the site due to time lapse, natural causes, or operations on adjoining properties, may deem the conclusions and recommendations inappropriate. Associated's staff strive to perform its services in a proper and professional manner with reasonable care and competence, but are not infallible. Associated is unable to eliminate all risks or to provide insurance, thus, is unable to guarantee or warrant the results of this work. Associated does not warrant the accuracy of work performed or information supplied by others, including any of its subcontractors, or any segregated portions of this letter - report. Associated's professional services were performed consistent with generally accepted environmental assessment principles and practices in California at the time the services were performed. This warranty is in lieu of all other warranties, either expressed or implied. Texaco .Station, Panama Lane and Colony Street, Bakersfield, California December 9, 2015 CLOSING If you have any questions, please contact Associated at (559) 688 -1011. Respectfully submitted, ASSOCIATED SOILS ANALYSIS, INC. Prepared by: S%wAAL G�r�� No. 7714 Exp.a3l_211.' Mark D. Edwards, PG OF CA�-� Professional Geologist No. 7714 MDE/kr 1143 - 15.001 Page 7 cc: Mr. Shane Gardner, Bakersfield Fire Department, 2101 H Street, Bakersfield, California 93301 ATTACHMENTS Figure 1 - Vicinity Map Figure 2 - Soil Sample Location Map Laboratory Report and Chain -of- Custody Documentation Approximate Location of the Project Site California Location of Kern County Portion of Section 24, Township 30 South, Range 27 East, Mount Diablo .Baseline and Meridian. Source: United States Geological Surrey, "Gosford, California," 7.5- minute Quadrangle, 1954; photorevised 1973. 0 2,000 Feet Approximate Scale in Feet ! VICINITY MAP FIGURE 1 I Texaco Station NORTH.. Panama Lane and Colony Street . &�° � Associated Soils Analysis, Inc. Bakersfield, California 1141 East Batavia Court,'Fulare, California 93274 Project No, 1143 -15 # r (559) G$8 -1011 F.Ak (5S9) 688 -1196 ago. " Drive -i J igh : ch Theate e =_ - - -- .��. ....< 99�—I •I� - BIV a'� • - Fairview Sch `_• ° ° 19. ° • 366 • ■r FAIRviEW (Aban'd) Lg 368 .... ( {S Q!I �oRD ' ■•. ROAD 1 ' � •�I 35 6 Trailer ° - Park IEiLi SITE • PANAMA •�i i• LANE • v Q •• ■ BIN .::. , r = 'king Plant 26 35 25a BERKSHIRE • ROAD C c`w, 358 30 • • a 'o 355 Source: United States Geological Surrey, "Gosford, California," 7.5- minute Quadrangle, 1954; photorevised 1973. 0 2,000 Feet Approximate Scale in Feet ! VICINITY MAP FIGURE 1 I Texaco Station NORTH.. Panama Lane and Colony Street . &�° � Associated Soils Analysis, Inc. Bakersfield, California 1141 East Batavia Court,'Fulare, California 93274 Project No, 1143 -15 # r (559) G$8 -1011 F.Ak (5S9) 688 -1196 November 19, 2015 Mark Edwards Associated Soils Analysis, Inc. P.O. Box 88 1141 Batavia Court Tulare, CA 93274 TEL: (559) 688 -1011 FAX: (559) 688 -1195 RE: Texaco Fueling Facility, 1143 -15 CA -ELAP No.: 2676 NV Cert. No.: NV -00922 Workorder No.: N017593 Enclosed are the results for sample(s) received on November 11, 2015 by ASSET Laboratories . The sample(s) are tested for the parameters as indicated in the enclosed chain of custody in accordance with the applicable laboratory certifications. Thank you for the opportunity to service the needs of your company. Please feel free to call me at (702) 307 -2659 or Molky Brar at (562) -881 -3622 if we can be of further assistance to your company. Sincerely, Molky Brar Project Manager aaj ...ice Glen Gesmundo QA Manager i CALIFORNIA NEVADA ASSET LABORATORIES 11060 Artesia Blvd., Ste C, Cerritos, CA 90703 3151 W. Post Rd., Las Vegas, NV 89118 .� =rl� <•sz*++7a P: 562.219.7435 F: 562.219.7436 P :702.307.2659 F: 702.307.2691 "Serving Clients with Passion and Professionalism" 01 of 32 aL , ASSET Laboratories CLIENT: Associated Soils Analysis, Inc. Project: Texaco Fueling Facility, 1143 -15 Lab Order: N017593 Date: 19 -Nov -15 CASE NARRATIVE SAMPLE RECEIVING /GENERAL COMMENTS: Samples were received intact with proper chain of custody documentation. Cooler temperature and sample preservation were verified upon receipt of samples if applicable. Information on sample receipt conditions including discrepancies can be found in attached Sample Receipt Checklist Form. Samples were analyzed within method holding time. Analytical Comments for EPA 8260B: Laboratory Control Sample Duplicate (LCSD) recovery biased high for some analytes. Sample results were non - detect (ND) for these analytes therefore reanalysis of the samples was not necessary. CALIFORNIA kagm2 Of 31 ASSET LABORATORIES 11060 Artesia 6LA., Ste C. Cerritos, CA 90703 3151 W. Post Rd., Las Vegas, NV 89118 P P: 562.219.7435 F: 562.219.7436 : 702.307.2659 F: 702.307.2691 "Serving Clients with Passion and Professionalism" 02 of 32 ASSET Laboratories Date: 19 -Nov -I5 CLIENT: Associated Soils Analysis, Inc. Project: Texaco Fueling Facility, 1143 -15 Lab Order: N017593 Contract No: Work Order Sample Summary Lab Sample ID Client Sample ID Matrix Collection Date Date Received Date Reported N017593 -OOIA S1 Soil 11/6/2015 1:00:00 PM 11/11/2015 11/19/2015 N017593 -002A S2 Soil 11/6/2015 1:06:00 PM 11/11/2015 11/19/2015 N017593 -003A S3 Soil 11/6/2015 1:10:00 PM 11/11/2015 11/19/2015 N017593 -004A S4 Soil 11/6/2015 1:15:00 PM 11/11/2015 11/19/2015 N017593 -005A S5 Soil 11/6/2015 1:19:00 PM 11/11/2015 11/19/2015 N017593 -006A S6 Soil 11/6/2015 1:25:00 PM 11/11/2015 11/19/2015 N017593 -007A S7 Soil 11/6/2015 1:29:00 PM 11/11/2015 11/19/2015 N017593 -008A S8 Soil 11/6 /2015 1:36:00 PM 11/11/2015 11/19/2015 CALIFORNIA Page 1 oVENAOA ,,,�kj IAB AT IE- 3151 W. Post Rd., Las Vegas, NV 89118 11060 Artesia 13M., Ste C, Cerritos, CA 90703 P: 562.219.7435 F: 562.219.7436 P: 702.307.2659 F: 702.307.2691 "Serving Clients with Passion and Professionalism" 03 of 32 ASSET Laboratories ANALYTICAL RESULTS Print Date: 19- Nov -15 CLIENT: Associated Soils Analysis, Inc. Client Sample ID: S1 Lab Order: N017593 Collection Date: 11/6/2015 1:00:00 PM Project: Texaco Fueling Facility, 1143 -15 Matrix: SOIL Lab ID: N017593 -OOIA Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC /MS EPA 8260B RunlD: MS8_151113B QC Batch: R15VS025 PrepDate: Analyst: QBM 1,1,1,2 - Tetrachloroethane ND 5.0 pg /Kg 1 11113/2015 09:55 PM 1,1,1 - Trichloroethane ND 5.0 pg /Kg 1 11/13/2015 09:55 PM 1,1,2,2 - Tetrachloroethane ND 5.0 pg /Kg 1 11/13/2015 09:55 PM 1,1,2 - Trichloroethane ND 5.0 pg /Kg 1 11/13/2015 09:55 PM 1,1- Dichioroethane ND 5.0 pg /Kg 1 11/13/2015 09:55 PM 1,1- Dichloroethene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM 1,1- Dichloropropene ND 5.0 pg /Kg 1 11113/2015 09:55 PM 1,2,3 -T rich lorobenzen e ND 5.0 pg /Kg 1 11/13/2015 09:55 PM 1,2,3- Trichloropropane ND 5.0 pg /Kg 1 11/13/2015 09:55 PM 1,2,4- Tdchlorobenzene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM 1,2,4 -Trim ethyl benzene ND 5.0 pg /Kg 1 11/13/2015 09 :55 PM 1,2- Dibromo- 3- chloropropane ND 10 pg /Kg 1 11/13/2015 09:55 PM 1,2- Dibromoethane ND 5.0 pg /Kg 1 11/13/2015 09:55 PM 1,2- Dichlorobenzene ND 5.0 pg /Kg 1 11/1312015 09:55 PM 1,2- Dichloroethane ND 5.0 pg /Kg 1 11/13/2015 09:55 PM 1,2- Dichloropropane ND 5.0 pg /Kg 1 11/13/2015 09:55 PM 1,3,5 -Trim ethyl benzene ND 5.0 pg /Kg 1 11113/2015 09:55 PM 1,3- Dichlorobenzene ND 5.0 pg /Kg 1 .11/13/2015 09:55 PM 1,3- Dichloropropane ND 5.0 pg /Kg 1 11/13/2015 09:55 PM 1,4- Dichlorobenzene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM 2,2- Dichloropropane ND 5.0 pg /Kg 1 11/13/2015 09:55 PM 2- Butanone ND 50 pg /Kg 1 11113/2015 09:55 PM 2- Chlorotoluene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM 4- Chlorotoluene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM 4- Isopropyltoluene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Benzene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Bromobenzene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Bromodichloromethane ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Bromoform ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Bromomethane ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Carbon tetrachloride ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Chlorobenzene ND 5.0 pg /Kg 1 11113/2015 09:55 PM Chloroethane ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Chloroform ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Chloromethane ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike /Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out ft,_ - ' * CALIFORNIA NEVADA ASSET LABORATORIES 11060 Artesia Btvd., Ste C, Cerritos, CA 90703 3151 W. Post Rd., Las Vegas; NV 89118 P: 562.219.7435 F: 562.219.7436 P: 702.307.2659 F: 702.307.2691 0 °Serving Clients with Passion and Professionalism" 04 of 32 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike /Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out CALIFORNIA NEVADA ASSET LABORATORIES 11060 Artesia Blvd., Ste C, Cerritos, CA 90703 3151 W. Post Rd., Las Vegas; NV 89118 AIMI,-:rk%i - A.. P:5fiZ.219.7435 F: 562.219.7436 P: 702.307.2659 F: 702.307.2691 G°Serving Clients with Passion and Professionalism /" 05 of 32 ANALYTICAL RESULTS ASSET Laboratories Print Date: 19- Nov -15 CLIENT: Associated Soils Analysis, Inc. Client Sample ID: S1 Lab Order: N017593 Collection Date: 11/6/2015 1:00:00 PM Project: Texaco Fueling Facility, 1143 -15 Matrix: SOIL Lab ID: N017593 -001A Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC /MS EPA 82608 RunID: MS8_151113B QC Batch: R15VS025 PrepDate: Analyst: QBM cis -1,2- Dichloroethene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM cis- 1,3- Dichloropropene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Dibromochloromethane ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Dibromomethane ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Dichlorodifluoromethane ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Ethylbenzene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Freon -113 ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Hexachlorobutadiene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Isopropylbenzene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM m,p- Xylene ND 10 pg /Kg 1 11/13/2015 09:55 PM Methylene chloride ND 5.0 pg /Kg 1 11/13/2015 09:55 PM MTBE ND 5.0 pg /Kg 1 11/13/2015 09:55 PM n- Butylbenzene ND 5.0 pg /Kg 1 11/1312015 09:55 PM n- Propylbenzene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Naphthalene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM o- Xylene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM sec-Butyl benzene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Styrene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM tert-B utyl benzene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Tetrachloroethene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Toluene ND 5.0 pg /Kg 1 11/1312015 09:55 PM trans -1,2- Dichloroethene ND 5.0 pg /Kg 1 .11/13/2015 09:55 PM Trichloroethene ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Trichlorofluoromethane ND 5.0 pg /Kg 1 11/1312015 09:55 PM Vinyl chloride ND 5.0 pg /Kg 1 11/13/2015 09:55 PM Surr: 1,2- Dichloroethane -d4 127 75 -140 %REC 1 11/13/2015 09:55 PM Surr: 4- Bromofluorobenzene 98.6 73- 128 %REC 1 11/13/2015 09:55 PM Surr: Dibromofluoromethane 119 78 -133 %REC 1 11/13/2015 09:55 PM Surr: Toluene -d8 105 80 -120 %REC 1 11/13/2015 09:55 PM GASOLINE RANGE ORGANICS BY GC /FID EPA 8016B RUnlD: GC4_151112A QC Batch: El5VS130 PrepDate: Analyst: QBM GRO ND 1.0 mg /Kg 1 11/12/2015 12:40 PM Surr: Chlorobenzene - d5 113 46 -154 %REC 1 11/12/2015 12:40 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike /Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out CALIFORNIA NEVADA ASSET LABORATORIES 11060 Artesia Blvd., Ste C, Cerritos, CA 90703 3151 W. Post Rd., Las Vegas; NV 89118 AIMI,-:rk%i - A.. P:5fiZ.219.7435 F: 562.219.7436 P: 702.307.2659 F: 702.307.2691 G°Serving Clients with Passion and Professionalism /" 05 of 32 ASSET Laboratories ANALYTICAL RESULTS Print Date: 19 -Nov -15 CLIENT: Associated Soils Analysis, Inc. Client Sample ID: S2 Lab Order: NO 17593 Collection Date: 11/6/2015 1:06:00 PM Project: Texaco Fueling Facility, 1143 -15 Matrix: SOIL Lab ID: N017593 -002A Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC /MS EPA 82608 RunlD: MS8_151113B QC Batch: R15VS025 PrepDafe: Analyst: QBM 1,1,1,2 - Tetrachloroethane ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 1, 1, 1 -Trichloroethane ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 1,1,2,2- Tetrachloroethane ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 1,1,2 - Trichloroethane ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 1,1- Dichloroethane ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 1,1- Dichloroethene ND 5.0 lag /Kg 1 11/13/2015 10:21 PM 1,1- Dichloropropene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 1,2,3 - Trichlorobenzene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 1,2,3- Trichloropropane ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 1,2,4 - Trichlorobenzene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 1,2,4 -Trim ethyl benzene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 1,2- Dibromo- 3- chloropropane ND 10 pg /Kg 1 11/13/2015 10:21 PM 1,2- Dibromoethane ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 1,2- Dichlorobenzene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 1,2- Dichloroethane ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 1,2- Dichloropropane ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 1,3,5 -Trim ethyl benzene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 1,3- Dichlorobenzene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 1,3- Dichloropropane ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 1,4- Dichlorobenzene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 2,2- Dichloropropane ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 2- Butanone ND 50 pg /Kg 1 11/13/2015 10:21 PM 2- Chlorotoluene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM 4- Chlorotoluene ND 5.0 pg /Kg 1 11113/2015 10:21 PM 4- Isopropyltoluene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Benzene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Bromobenzene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Bro modich lorom ethane ND . 5.0 pg /Kg 1 11/13/2015 10:21 PM Bromoform ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Bromomethane ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Carbon tetrachloride ND 5.0 pg /Kg 1 11113/2015 10:21 PM Chlorobenzene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Chloroethane ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Chloroform ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Chloromethane ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out CLCALIFORNIA NEVADA ASSET LABORATORIES 11060 Artesia B(A., Ste C, Cerritos, CA 90703 3151 W. Post Rd., Las Vegas; NV 89118 0�;�v:RC -a P: 562.219.7435 F: 562.219.7436 P: 702.307.2659 F: 702.307.2691 ...:. "Serving Clients with Passion and Professionalism" 06 of 32 ASSET Laboratories .ANALYTICAL RESULTS Print Date: 19- Nov -15 CLIENT: Associated Soils Analysis, Inc. Client Sample ID: S2 Lab Order: N017593 Collection Date: 11/6/2015 1:06:00 PM Project: Texaco Fueling Facility, 1143 -15 Matrix: SOIL Lab ID: N017593 -002A Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC /MS EPA 8260E RunID: MS8_151113B QC Batch: R15VS025 PrepDate: Analyst: QBM cis -1,2- Dichloroethene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM cis -1,3- Dichloropropene ND 5.0 pg /Kg 1 11113/2015 10:21 PM Dibromochloromethane ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Dibromomethane ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Dichlorodifluoromethane ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Ethylbenzene ND 5.0 pg /Kg 1 11/1312015 10:21 PM Freon -113 ND 5.0 pg /Kg 1 11113/2015 10:21 PM Hexachlorobutadiene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Isopropylbenzene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM m,p- Xylene ND 10 pg /Kg 1 11/13/2015 10:21 PM Methylene chloride ND 5.0 pg /Kg 1 11/13/2015 10:21 PM MTBE ND 5.0 pg /Kg 1 11/13/2015 10:21 PM n- Butylbenzene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM n- Propylbenzene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Naphthalene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM o- Xylene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM sec-Butyl benzene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Styrene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM tert-B utyl benzene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Tetrachloroethene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Toluene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM trans -1,2- Dichloroethene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Trichooroethene ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Trichlorofluoromethane ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Vinyl chloride ND 5.0 pg /Kg 1 11/13/2015 10:21 PM Surr: 1,2- Dichloroethane -d4 116 75 -140 %REC 1 11/13/2015 10:21 PM Surr: 4- Bromofluorobenzene 96.8 73 -128 %REC 1 11/13/2015 10:21 PM Surr: Dibromofluoromethane 110 78 -133 %REC 1 11/13/2015 10:21 PM Surr: Toluene -d8 102 80 -120 %REC 1 11/13/2015 10:21 PM GASOLINE RANGE ORGANICS BY GC /PID EPA 80158 RunID: GC4_151112A QC Batch: E15VS130 PrepDate: Analyst: QBM GRO ND 1.0 mg /Kg 1 11/12/2015 01:16 PM Surr: Chlorobenzene - d5 100 46 -154 %REC 1 11/12/2015 01:16 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out CALIFORNIA NEVADA ET BATIJES 11060 Artesia Blvd., Ste C, Cerritos, CA 90703 3151 W. Post Rd., Las Vegas, NV 89118 P P: 562.219,7435 F; 562.219.7436 : 702.307.2659 F: 702.307.2591 "Serving Clients with Passion and Professionalism" 07 of 32 ASSET Laboratories ANALYTICAL RESULTS Print Date: 19-Nov-15 CLIENT: Associated Soils Analysis, Inc. Client Sample ID: S3 Lab Order: NO 17593 Collection Date: 11/6/2015 1:10:00 PM Project: Texaco Fueling Facility, 1143 -15 Matrix: SOIL Lab ID: N017593 -003A Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC /MS EPA 8260B RunlD: MS8_151113B 1,1,1, 2- Tetrach loroethane 1,1,1- Trichloroetha ne 1,1, 2, 2- Tetrach loroethane 1,1,2- Trichloroethane 1,1- Dichloroethane 1,1- Dichloroethene 1,1- Dichloropropene 1,2,3- Trichlorobenzene 1,2,3- Trichloropropane 1,2,4- Trichlorobenzene 1, 2,4 -Trim ethyl benzene 1,2- Dibromo- 3- chloropropane 1,2- Dibromoeihane 1,2- Dichlorobenzene 1,2- Dichloroethane 1,2- Dichloropropane 1,3,5 -Trim ethyl benzene 1,3- Dichlorobenzene 1,3- Dichloropropane 1,4- Dichlorobenzene 2,2- Dichloropropane 2- Butanone 2- Chlorotoluene 4- Chlorotoluene 4- Isopropyltoluene Benzene Bromobenzene Bro mod ich lorom ethane Bra moform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane QC Batch: R15VS025 PrepDate ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 p9/K9 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 10 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 50 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 ND 5.0 pg /Kg 1 Analyst: QBM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10 :47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11113/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11/13/2015 10:47 PM 11113/2015 10:47 PM 11/13/2015 10:47 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out CALIFORNIA NEVADA ASSET LABORATORIES 3151 W, Post Rd., Las Vegas; NV 89118 11060 Artesia 5tvd., Ste C. Cerritos, CA 90703 A�.:�%V- 01. <ssv«^�� -Y:*w P: 562.219.7435 F: 562.219.7436 P: 702.307.2659 F: 702.307.2691 G°Serving Clients with Passion and Professionalism" 08 of 32 "Serving Clients with Passion and Professionalism" 09 of 32 ANALYTICAL RESULTS ASSET Laboratories Print Date: 19- Nov -15 CLIENT: Associated Soils Analysis, Inc. Client Sample ID: S3 Lab Order: N017593 Collection Date: 11/6/2015 1:10:00 PM Project: Texaco Fueling Facility, 1143 -15 Matrix: SOIL Lab ID: N017593 -003A Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC /MS EPA 8260B RunID: MS8_151113B QC Batch: R15VS025 PrepDate: Analyst: QBM cis- 1,2- Dichloroethene ND 5.0 pg /Kg 1 11/13/2015 10:47 PM cis -1,3- Dichloropropene ND 5.0 pg /Kg 1 11/13/2015 10:47 PM Dibromochloromethane ND 5.0 pg /Kg 1 11/13/2015 10:47 PM Dibromomethane ND 5.0 pg /Kg 1 11/13/2015 10:47 PM Dichlorodifluoromethane ND 5.0 pg /Kg 1 11/13/2015 10:47 PM Ethylbenzene ND 5.0 pg /Kg 1 11/13/2015 10:47 PM Freon -113 ND 5.0 pg /Kg 1 11/13/2015 10:47 PM Hexachlorobutadiene ND 5.0 pg /Kg 1 11/13/2015 10:47 PM Isopropylbenzene ND 5.0 pg /Kg 1 11/13/2015 10:47 PM m,p- Xylene ND 10 pg /Kg 1 11/13/2015 10:47 PM Methylene chloride ND 5.0 pg /Kg 1 11/13/2015 10:47 PM MTBE ND 5.0 pg /Kg 1 11/13/2015 10:47 PM n- Butylbenzene ND 5.0 pg /Kg . 1 11/13/2015 10:47 PM n- Propylbenzene ND 5.0 pg /Kg 1 11/13/2015 10:47 PM Naphthalene ND 5.0 pg /Kg 1 11113/2015 10:47 PM o- Xylene ND 5.0 pg /Kg 1 11/13/2015 10:47 PM sec - Butylbenzene ND 5.0 pg /Kg 1 11/13/2015 10:47 PM Styrene ND 5.0 pg /Kg 1 11/13/2015 10:47 PM tert-B utyl benzene ND 5.0 pg /Kg 1 11/13/2015 10:47 PM Tetrachloroethene ND 5.0 pg /Kg 1 11/13/2015 10:47 PM Toluene ND 5.0 pg /Kg 1 11/13/2015 10:47 PM trans -1,2- Dichloroethene ND 5.0 pg /Kg 1 11/13/2015 10:47 PM Trichloroethene ND 5.0 pg /Kg 1 11/1312015 10:47 PM Trichlorofluoromethane ND 5.0 pg /Kg 1 11/13/2015 10:47 PM Vinyl chloride ND 5.0 pg /Kg 1 11/13/2015 10:47 PM Surr: 1,2- Dichloroethane -d4 124 75 -140 %REC 1 11/13/2015 10:47 PM Surr: 4- Bromofluorobenzene 99.8 73 -128 %REC 1 11/1312015 10:47 PM Surr: Dibromofluorom ethane 115 78- 133 %REC 1 11/13/2015 10:47 PM Surr: Toluene -d8 105 80- 120 %REC 1 11/13/2015 10:47 PM GASOLINE RANGE ORGANICS BY GC /FID EPA 8016B RunID: GC4_151112A QC Batch: E15VS130 PrepDate: Analyst: QBM GRO ND 1.0 mg /Kg 1 11/12/2015 01:52 PM Surr: Chlorobenzene - d5 116 46 -154 %REC 1 11/1212015 01:52 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out ASSET LABORATORIES 11060 Artesia CALIFORNIA Blvd., Ste C. Cerritos, CA 90703 NEVADA 3151 W. Post Rd., Las Vegas, NV 89118 - ::,w�A f -�. =�..:ae�y,.WI �wa�azcdl,m ao � oa P: 562.219.7435 F: 562.219.7436 P: 702.307.2659 F: 702.307.2691 "Serving Clients with Passion and Professionalism" 09 of 32 ASSET Laboratories ANALYTICAL RESULTS Print Date: 19- Nov -15 CLIENT: Associated Soils Analysis, Inc. Client Sample ID: S4 Lab Order: NO 17593 Collection Date: 11/6/2015 1:15:00 PM Project: Texaco Fueling Facility, 1143 -15 Matrix: SOIL Lab ID: N017593 -004A Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC /MS EPA 8260B RunID: MS8_151113B QC Batch: R15VS025 PrepDate: Analyst: QBM 1,1,1,2- Tetrachloroethane ND 5.0 pg /Kg 1 11/1312015 11:13 PM 1,1,1 - Trichloroethane ND 5.0 pg /Kg 1 11/13/2015 11:13 PM 1,1,2,2 - Tetrachloroethane ND 5.0 pg /Kg 1 11/1312015 11:13 PM 1,1,2 - Trichloroethane ND 5.0 pg /Kg 1 11/13/2015 11:13 PM 1,1- Dichloroethane ND 5.0 pg /Kg 1 11/13/2015 11:13 PM 1,1- Dichloroethene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM 1,1- Dichloropropene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM 1,2,3 - Trichlorobenzene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM 1,2,3- Trichloropropane ND 5.0 pg /Kg 1 11/13/2015 11:13 PM 1,2,4 - Trichlorobenzene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM 1,2,4 -T rim ethyl benzene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM 1,2- Dibromo- 3- chloropropane ND 10 pg /Kg 1 11/13/2015 11:13 PM 1,2- Dibromoethane ND 5.0 pg /Kg 1 11/13/2015 11:13 PM 1,2- Dichlorobenzene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM 1,2- Dichloroethane ND 5.0 pg /Kg 1 11/13/2015 11:13 PM 1,2- Dichloropropane ND 5.0 pg /Kg 1 11/13/2015 11:13 PM 1,3,5 -Trim ethyl benzene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM 1,3- Dichlorobenzene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM 1,3- Dichloropropane ND 5.0 pg /Kg 1 11/13/2015 11:13 PM 1,4- Dichlorobenzene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM 2,2- Dichloropropane ND 5.0 pg /Kg 1 11/13/2015 11:13 PM 2- Butanone ND 50 pg /Kg 1 11/13/2015 11:13 PM 2- Chlorotoluene ND 5.0 pg /Kg 1 11113/2015 11:13 PM 4- Chlorotoluene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM 4- Isopropyltoluene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Benzene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Bromobenzene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Bro modich lorom ethane ND 5.0 pg /Kg 1 11113/2015 11:13 PM Bromoform ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Bromomethane ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Carbon tetrachloride ND 5.0 pg /Kg 1 11/13/201511:13 PM Chlorobenzene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Chloroethane ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Chloroform ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Chloromethane ND 5.0 pg /Kg 1 11/13/2015 11 :13 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike /Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out CALIFORNIA NEVADA ASSET LABORATORIES 11060 Artesia Blvd., Ste C, Cerritos, CA 90743 3151 W. Post Rd., Las Vegas, NV 89118 a;;PWW-14. 1rAW10L0&f P: 562.219, 7435 F: Sb2.219.7436 P: 702.307.2659 F: 702.307.2691 _....,...... "Serving Clients with Passion and Professionalism" 10 of 32 ASSET Laboratories ANALYTICAL RESULTS Print Date: 19- Nov -15 CLIENT: Associated Soils Analysis, Inc. Client Sample ID: S4 Lab Order: N017593 Collection Date: 11/6/2015 1:15:00 PM Project: Texaco Fueling Facility, 1143 -15 Matrix: SOIL Lab ID: N017593 -004A Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC /MS EPA 82608 RunlD: MS8_151113B QC Batch: R15VS025 PrepDate: Analyst: QBM cis -1,2- Dichloroethene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM cis- 1,3- Dichloropropene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Dibromochloromethane ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Dibromomethane ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Dichlorodifluoromethane ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Ethylbenzene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Freon -113 ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Hexachlorobutadiene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Isopropylbenzene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM m,p- Xylene ND 10 pg /Kg 1 11/13/2015 11:13 PM Methylene chloride ND 5.0 pg /Kg 1 11/13/2015 11:13 PM MTBE ND 5.0 pg /Kg 1 11/13/2015 11:13 PM n- Butylbenzene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM n- Propylbenzene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Naphthalene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM o- Xylene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM sec - Butylbenzene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Styrene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM tert-B utyl benzene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Tetrachloroethene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Toluene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM trans -1,2- Dichloroethene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Trichloroethene ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Trichlorofluoromethane ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Vinyl chloride ND 5.0 pg /Kg 1 11/13/2015 11:13 PM Sun': 1,2- Dichloroethene -d4 114 75 -140 %REC 1 11/13/2015 11:13 PM Surr: 4- Bromofluorobenzene 95.5 73- 128 %REC 1 11/13/2015 11:13 PM Surr: Dibromofluoromethane 108 78 -133 %REC 1 11/13/2015 11:13 PM Surr: Toluene -d8 101 80 -120 %REC 1 11/13/2015 11:13 PM GASOLINE RANGE ORGANICS BY GC /FID EPA 8016B RunlD: GC4_151112A QC Batch: E15VS130 PrepDate: Analyst: QBM GRO ND 1.0 mg /Kg 1 11/12/2015 02:28 PM Surr: Chlorobenzene - d5 117 46 -154 %REC 1 11/12/2015 02:28 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike /Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out CALIFORNIA NEVADA ASSET LABOR ORIE 11060 Artesia Blvd., Ste C, Cerritos, CA 90703 3151 W. Post. Rd., Las Vegas, NV 89118 a` + "c'x r*r r s'i'r" t�ae� ^'r Mn€'„"i' rrF,"1 ^� P: 562.219.7435 F: 562.219.7436 P: 702.307.2659 F: 702.307.2691 .............._ "Serving Clients with Passion and Professionalism" 11 of 32 A%h CALIFORNIA NEVADA ' `�ET LAB T RIES 11060 Artesia slur!., Ste C, Cerritos, CA 90703 3151 W. Post Rd., Las Vegas; NV 89118 P P: 562.219.7435 F. 562.219.7436 : 702.307.2659 F: 702.307.2691 "Serving Clients with Passion and Professionalism" 12 of 32 ANALYTICAL RESULTS ASSET Laboratories Print Date: 19 -Nov -15 CLIENT: Associated Soils Analysis, Inc. Client Sample ID: S5 Lab Order: N017593 Collection Date: 11/6/2015 1:19:00 PM Project: Texaco Fueling Facility, 1143 -15 Matrix: SOIL Lab ID: N017593 -005A Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC /MS EPA 82608 RunID: MS8_151113B QC Batch: R15VS025 PrepDate: Analyst: QBM 1,1,1,2 - Tetrachloroethane ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 1,1,1 - Trichloroethane ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 1,1,2,2 - Tetrachloroethane ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 1,1,2 - Trichloroethane ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 1,1- Dichloroethane ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 1,1- Dichloroethene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 1,1- Dichloropropene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 1,2,3 - Trichlorobenzene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 1,2,3 - Trichloropropane ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 1,2,4 -T rich lorobenzene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 1,2,4 -Trim ethyl benzene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 1,2- Dibromo- 3- chloropropane ND 10 pg /Kg 1 11/13/2015 11:39 PM 1,2- Dibromoethane ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 1,2- Dichlorobenzene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 1,2- Dichloroethane ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 1,2- Dichloropropane ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 1,3,5 -Trim ethyl benzene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 1,3- Dichlorobenzene ND 5.0 pg /Kg 1 11113/2015 11:39 PM 1,3- Dichloropropane ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 1,4- Dichlorobenzene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 2,2- Dichloropropane ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 2- Butanone ND 50 pg /Kg 1 11/13/2015 11:39 PM 2- Chlorotoluene ND 5.0 pg /Kg 1 11/1312015 11:39 PM 4- Chlorotoluene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM 4- Isopropyltoluene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Benzene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Bromobenzene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Bro mod ichloromethane ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Bromoform ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Bromomethane ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Carbon tetrachloride ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Chlorobenzene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Chloroethane ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Chloroform ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Chloromethane ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike /Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out A%h CALIFORNIA NEVADA ' `�ET LAB T RIES 11060 Artesia slur!., Ste C, Cerritos, CA 90703 3151 W. Post Rd., Las Vegas; NV 89118 P P: 562.219.7435 F. 562.219.7436 : 702.307.2659 F: 702.307.2691 "Serving Clients with Passion and Professionalism" 12 of 32 ASSET Laboratories .ANALYTICAL RESULTS Print Date: 19 -Nov -15 CLIENT: Associated Soils Analysis, Inc. Client Sample ID: S5 Lab Order: N017593 Collection Date: 11/6/2015 1:19:00 PM Project: Texaco Fueling Facility, 1143 -15 Matrix: SOIL Lab ID: N017593 -005A Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC /MS EPA 8260B RunID: MS8_151113B QC Batch: R15VS025 PrepDate: Analyst: QBM cis -1,2- Dichloroethene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM cis- 1,3- Dichloropropene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Dibromochlororn ethane ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Dibromomethane ND 5.0 pg /Kg 1 11113/2015 11:39 PM Dichlorodifluoromethane ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Ethylbenzene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Freon -113 ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Hexachlorobutadiene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Isopropylbenzene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM m,p- Xylene ND 10 pg /Kg 1 11/13/2015 11:39 PM Methylene chloride ND 5.0 pg /Kg 1 11/13/2015 11:39 PM MTBE ND 5.0 pg /Kg 1 11/13/2015 11:39 PM n- Butylbenzene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM n- Propylbenzene ND 5.0 pg /Kg 1 11113/2015 11:39 PM Naphthalene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM o- Xylene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM sec-Butyl benzene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Styrene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM tert-B utyl benzene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Tetrachloroethene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Toluene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM trans -1,2- Dichloroethene ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Trichooroethene ND 5.0 pg /Kg 1 11113/2015 11:39 PM Trichlorofluoromethane ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Vinyl chloride ND 5.0 pg /Kg 1 11/13/2015 11:39 PM Surr: 1,2- Dichloroethane -d4 126 75 -140 %REC 1 11/13/2015 11:39 PM Surr: 4- Bromofluorobenzene 101 73 -128 %REC 1 11/13/2015 11:39 PM Surr: Dibromofluorom ethane 118 78 -133 %REC 1 11113/2015 11:39 PM Surr: Toluene -d8 107 80 -120 %REC 1 11/13/2015 11:39 PM GASOLINE RANGE ORGANICS BY GC /FID EPA 8016B RunID: GC4_151112A QC Batch: E15VS130 PrepDate: Analyst: QBM GRO ND 1.0 mg /Kg 1 11/12/2015 03:04 P.M Surr: Chlorobenzene - d5 117 46 -154 %REC 1 11/12/2015 03:04 PM Qualifiers: B . Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out CALIFORNIA NEVADA ASSET LABORATORIES 11060 Artesia Blvd., Ste C, Cerritos, CA 90703 3151 W. Post Rd., Las Vegas, NV 89118 ova s- s+ ;.vsrxas:rievrauecvua;c <:� +eta P:5b2.219.7435 F: 562.219.7436 P: 702.307.2659 F: 702.307.2691 ...,........ "Serving) Clients with Passion and Professionalism" 13 of 32 ASSET Laboratories ANALYTICAL RESULTS Print Date: 19- Nov -I5 CLIENT: Associated Soils Analysis, Inc. Client Sample ID: S6 Lab Order: N017593 Collection Date: 11/6/2015 1:25:00 PM Project: Texaco Fueling Facility, 1143 -15 Matrix: SOIL Lab ID: NO 17593 -006A Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC /MS EPA 8260B RunID: MSS_151113B QC Batch: R15VS025 PrepDate: Analyst: QBM 1,1,1,2 - Tetrachloroethane ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 1,1,1 - Trichloroethane ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 1,1,2,2 - Tetrachloroethane ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 1,1,2 - Trichloroethane ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 1,1- Dichloroethane ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 1,1- Dichloroethene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 1,1- Dichloropropene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 1,2,3 - Trichlorobenzene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 1,2,3- Trichloropropane ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 1,2,4 - Trichlorobenzene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 1,2,4 - Trimethylbenzene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 1,2- Dibromo -3- chloropropane ND 10 pg /Kg 1 11/14/2015 12:05 AM 1,2- Dibromoethane ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 1,2- Dichlorobenzene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 1,2- Dichloroethane ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 1,2- Dichloropropane ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 1,3,5 - Trim ethyl benzene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 1,3- Dichlorobenzene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 1,3- Dichloropropane ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 1,4- Dichlorobenzene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 2,2- Dichloropropane ND 5.0 pg /Kg 1 11114/2015 12:05 AM 2- Butanone ND 50 pg /Kg 1 11/14/2015 12:05 AM 2- Chlorotoluene ND 5.0 pg /Kg 1 11/1412015 12:05 AM 4- Chlorotoluene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM 4- Isopropyltoluene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Benzene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Bromobenzene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Bromodichloromethane ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Bromoform ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Bromomethane ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Carbon tetrachloride ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Chlorobenzene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Chloroethane ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Chloroform ND 5.0 pg /Kg 1 11114/2015 12:05 AM Chloromethane ND 5.0 pg /Kg 1 11/1412015 12:05 AM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike /Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out CALIFORNIA NEVADA ASSET LABORATORIES 11060 Artesia Blvd., Ste C, Cerritos, CA 90703 3151 W. Post Rd., Las Vedas; NV 89118 -eZW:�w t: -Aa xnll A � +T^ � P: 562.219.7435 F: 562.219.7436 P: 702.307.2659 F: 702.307.2691 _. .............. "Serving Clients with Passim and Professionalism" 14 of 32 ASSET Laboratories ANALYTICAL RESULTS Print Date: 19- Nov -15 CLIENT: Associated Soils Analysis, Inc. Client Sample ID: S6 Lab Order: N017593 Collection Date: 11/6/2015 1:25:00 PM Project: Texaco Fueling Facility, 1143 -15 Matrix: SOIL Lab ID: N017593 -006A Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC /MS EPA 8260B RUnlD: MS8_151113B QC Batch: R15VS025 PrepDate: Analyst: QBM cis -1,2- Dichloroethene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM cis- 1,3- Dichloropropene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Dibromochloromethane ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Dibromomethane ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Dichlorodifluoromethane ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Ethylbenzene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Freon -113 ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Hexachlorobutadiene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Isopropylbenzene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM m,p- Xylene ND 10 pg /Kg 1 11/14/2015 12:05 AM Methylene chloride ND 5.0 pg /Kg 1 11/14/2015 12:05 AM MTBE ND 5.0 pg /Kg 1 11/14/2015 12:05 AM n- Butylbenzene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM n- Propylbenzene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Naphthalene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM o- Xylene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM sec-Butyl benzene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Styrene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM tert-B utyl benzene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Tetrachloroethene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Toluene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM trans -1,2- Dichloroethene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Trichloroethene ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Trichlorofluoromethane ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Vinyl chloride ND 5.0 pg /Kg 1 11/14/2015 12:05 AM Surr: 1,2- Dichloroethene -d4 125 75 -140 %REC 1 11/14/2015 12:05 AM Surr: 4- Bromofluorobenzene 102 73 -128 %REC 1 11/14/2015 12:05 AM Surr: Dibromofluoromethane 119 78- 133 %REC 1 11/14/2015 12:05 AM Surr: Toluene -d8 107 80 -120 %REC 1 11/14/2015 12:05 AM GASOLINE RANGE ORGANICS BY GC /FID EPA 80168 RunlD: GC4_151112A QC Batch: E15VS130 PrepDate: Analyst: QBM GRO ND 1.0 mg /Kg 1 11/12/2015 03:40 PM Surr Chlorobenzene - d5 105 46 -154 %REC 1 11/12/2015 03:40 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out CALIFORNIA NEVADA i T RIE 3151 W. Post Rd., Las Vegas; NV 89118 11060 Artesia Blvd., Ste C, Cerritos, CA 90703 P: 562.219.7435 F: 562.219.7436 P: 702.307.2659 F: 702.307.2691 "Serving Clients with Passion and Professionalism" 15 of 32 ASSET Laboratories ANALYTICAL RESULTS Print Date: 19-Nov-15 CLIENT: Associated Soils Analysis, Inc. Client Sample ID: S7 Lab Order: NO 17593 Collection Date: 11/6/2015 1:29:00 PM Project: Texaco Fueling Facility, 1143 -15 Matrix: SOIL Lab ID: N017593 -007A Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC /MS EPA 8260B RunID: MS8_151113B QC Batch: R15VS025 PrepDate: Analyst: QBM 1,1,1,2 - Tetrachloroethane ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 1,1,1 - Trichloroethane ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 1,1,2,2 - Tetrachloroethane ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 1,1,2 - Trichloroethane ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 1,1- Dichloroethane ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 1,1- Dichloroethene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 1,1- Dichloropropene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 1,2,3 - Trichlorobenzene ND 5.0 pg /Kg 1 11/1412015 12:31 AM 1,2,3 - Trichloropropane ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 1,2,4 - Trichlorobenzene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 1,2,4 - Trimethylbenzene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 1,2- Dibromo- 3- chloropropane ND 10 pg /Kg 1 11114/2015 12:31 AM 1,2- Dibromoethane ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 1,2- Dichlorobenzene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 1,2- Dichloroethane ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 1,2- Dichloropropane ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 1,3,5 - Trimethylbenzene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 1,3- Dichlorobenzene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 1,3- Dichloropropane ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 1,4- Dichlorobenzene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 2,2- Dichloropropane ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 2- Butanone ND 50 pg /Kg 1 . 11/1412015 12:31 AM 2- Chlorotoluene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 4- Chlorotoluene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM 4- Isopropyltoluene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Benzene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Bromobenzene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Bro modich lorom ethane ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Bromoform ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Bromomethane ND 5.0 pg /Kg 1 11/1412015 12:31 AM Carbon tetrachloride ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Chlorobenzene ND 5.0 pg /Kg 1 11/1412015 12:31 AM Chloroethane ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Chloroform ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Chloromethane ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike /Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out CALIFORNIA NEVADA ASSET LABORATORIES 3151 W. Post Rd., Las Vegas, NV 89118 11060 Artesia BI.vd., Ste C, Cerritos, CA 90703 cwwrc+ : srr. . wwe m rev a sir r uR P: 562.219.7435 F: 562.219.7436 P: 702.307.2659 F: 702.307.2691 :...._.... "Serving Clients with Passion and Professionalism " 16 of 32 ASSET Laboratories ANALYTICAL RESULTS Print Date: 19- Nov -15 CLIENT: Associated Soils Analysis, Inc. Client Sample ID: S7 Lab Order: N017593 Collection Date: 11/6/2015 1:29:00 PM Project: Texaco Fueling Facility, 1143 -15 Matrix: SOIL Lab ID: N017593 -007A Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC /MS EPA 8260B RunID: MS8_151113B QC Batch: R15VS025 PrepDate: Analyst: QBM cis -1,2- Dichloroethene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM cis- 1,3- Dichloropropene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Dibromochloromethane ND. 5.0 pg /Kg 1 11/14/2015 12:31 AM Dibromomethane ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Dichlorodifluoromethane ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Ethylbenzene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Freon -113 ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Hexachlorobutadiene ND 5.0 pg /Kg 1 11114/2015 12:31 AM Isopropylbenzene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM m,p- Xylene ND 10 pg /Kg 1 11/14/2015 12:31 AM Methylene chloride ND 5.0 pg /Kg 1 11/14/2015 12:31 AM MTBE ND 5.0 pg /Kg 1 11/14/2015 12:31 AM n- Butylbenzene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM n- Propylbenzene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Naphthalene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM o- Xylene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM sec- Butyl benzene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Styrene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM tert-B utyl benzene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Tetrachloroethene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Toluene ND 5.0 pg /Kg 1 11/1412015 12:31 AM trans -1,2- Dichloroethene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Trichooroethene ND 5.0 pg /Kg 1 11/14/2015 12:31 AM T rich lorofl uoromethan e ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Vinyl chloride ND 5.0 pg /Kg 1 11/14/2015 12:31 AM Surr: 1,2- Dichloroethane -d4 122 75 -140 %REC 1 11/14/2015 12:31 AM Surr: 4- Bromofluorobenzene 100 73 -128 %REC 1 11/14/2015 12:31 AM Surr: Dibromofluoromethane 117 78- 133 %REC 1 11/1412015 12:31 AM Surr: Toluene -d8 105 80 -120 %REC 1 11/14/2015 12:31 AM GASOLINE RANGE ORGANICS BY GC /FID EPA 8015B RunID: GC4_151112A QC Batch: E15VS130 PrepDate: Analyst: QBM GRO ND 1.0 mg /Kg 1 11/12/2015 04:16 PM Surr: Chlorobenzene - d5 114 46 -154 %REC 1 11/12/2015 04:16 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike /Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out CALIFORNIA NEVADA ASSET LABORATORIES 11060 Artesia Blvd., Ste C, Cerritos, CA 90703 3151 W. Post Rd., Las Vegas, NV 89118 z�kwhc. %Xoo i.�4� ,.r�;6�f�� 1+�.� � P: 562.219.7435 F: 562.219.7436 P: 702.307.2659 F: 702.307.2691 .............. "Serving Clients with Passion and Professionalism " 17 of 32 ASSET Laboratories ANALYTICAL RESULTS Print Date: 19-Nov-15 CLIENT: Associated Soils Analysis, Inc. Client Sample ID: S8 Lab Order: N017593 Collection Date: 11/6/2015 1:36:00 PM Project: Texaco Fueling Facility, 1143 -15 Matrix: SOIL Lab ID: N017593 -008A Analyses Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC /MS EPA 8260B RunID: MS8_151113B QC Batch: R15VS025 PrepDate: Analyst: QBM 1,1,1,2 - Tetrachloroethane ND 5.0 pg /Kg 1 11/14/2015 12:57 AM 1,1,1- Trichloroethane ND 5.0 pg /Kg 1 11/14/2015.12:57 AM 1,1,2,2 - Tetrachloroethane ND 5.0 pg /Kg 1 11114/2015 12:57 AM 1,1,2 - Trichloroethane ND 5.0 pg /Kg 1 11/14/2015 12:57 AM 1,1- Dichloroethane ND 5.0 pg /Kg 1 11/14/2015 12:57 AM 1,1- Dichloroethene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM 1,1- D.ichloropropene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM 1,2,3 -T rich loeobe nzen e ND 5.0 pg /Kg 1 11/14/2015 12:57 AM 1,2,3- Trichloropropane ND 5.0 pg /Kg 1 11/14/2015 12:57 AM 1,2,4 - Trichlorobenzene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM 1,2,4 -Trim ethyl benzene ND 5.0 pg /Kg 1 11114/2015 12:57 AM 1,2- Dibromo -3- chloropropane ND 10 pg /Kg 1 11/14/2015 12:57 AM 1,2- Dibromoethane ND 5.0 pg /Kg 1 11/14/2015 12:57 AM 1,2- Dichlorobenzene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM 1,2- Dichloroethane ND 5.0 pg /Kg 1 11/14/2015 12:57 AM 1,2- Dichloropropane ND 5.0 pg /Kg 1 11/14/2015 12:57 AM 1,3,5 - Trimethylbenzene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM 1,3- Dichlorobenzene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM 1,3- Dichloropropane ND 5.0 pg /Kg 1 11/14/2015 12:57 AM 1,4- Dichlorobenzene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM 2,2- Dichloropropane ND 5.0 pg /Kg 1 11/14/2015 12:57 AM 2- Butanone ND 50 pg /Kg 1 11/14/2015 12:57 AM 2- Chlorotoluene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM 4- Chlorotoluene ND 5.0 pg /Kg 1 11114/2015 12:57 AM 4- isopropyltoluene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Benzene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Bromobenzene ND 5.0 pg /Kg 1 11/1412015 12:57 AM Bromodichloromethane ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Bromoform ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Bromomethane ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Carbon tetrachloride ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Chlorobenzene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Chloroethane ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Chloroform ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Chloromethane ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out CALIFORNIA NEVADA ASSET LABORATORIES 3151 W. Post Rd., Las Vegas; NV 89118 11060 Artesia Blvd., Ste C. Cerritos, CA 90703 � OItM. ; � -' 4� AkohW + L 9= P: 702.307.2659 F: 702.307.2691 .........._ P: 562.219.7435 F: 562.219.7436 "Serving Clients with Passion and Professionalism" 18 of 32 ASSET Laboratories ANALYTICAL RESULTS Print Date: 19- Nov -15 CLIENT: Associated Soils Analysis, Inc. Client Sample ID: S8 Lab Order: N017593 Collection Date: 11/6/2015 1:36:00 PM Project: Texaco Fueling Facility, 1143 -15 Matrix: SOIL Lab ID: N017593 -008A Analyses. Result PQL Qual Units DF Date Analyzed VOLATILE ORGANIC COMPOUNDS BY GC /MS EPA 8260B RunID: MS8_151113B QC Batch: R15VS025 PrepDate: Analyst: QBM cis- 1,2- Dichloroethene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM cis -1,3- Dichloropropene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Dibromochlorom ethane ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Dibromomethane ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Dichlorodifluoromethane ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Ethylbenzene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Freon -113 ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Hexachlorobutadiene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Isopropylbenzene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM m,p- Xylene ND 10 pg /Kg 1 11/14/2015 12:57 AM Methylene chloride ND 5.0 pg /Kg 1 11/14/2015 12:57 AM MTBE ND 5.0 pg /Kg 1 11/14/2015 12:57 AM n- Butylbenzene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM n- Propylbenzene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Naphthalene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM o- Xylene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM sec-Butyl benzene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Styrene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM tert-B utyl benzene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Tetrachloroethene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Toluene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM trans- 1,2- Dichloroethene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Trichloroethene ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Trichlorofluoromethane ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Vinyl chloride ND 5.0 pg /Kg 1 11/14/2015 12:57 AM Surr: 1,2- Dichloroethane -d4 121 75 -140 %REC 1 11/14/2015 12:57 AM Surr: 4- Bromofluorobenzene 98.2 73 -128 %REC 1 11/14/2015 12:57 AM Surr: Dibromofluoromethane 117 78 -133 %REC 1 11/14/2015 12:57 AM Surr: Toluene -d8 105 80-120' %REC 1 11/14/2015 12:57 AM GASOLINE RANGE ORGANICS BY GC /FID EPA 8015B RunlD: GC4_151112A QC Batch: E15VS130 PrepDate: Analyst: QBM GRO ND 1.0 mg /Kg 1 11/12/2015 05:23 PM Surr: Chlorobenzene - d5 117 46- 154 %REC 1 11/12/2015 05:23 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out CALIFORNIA NEVADA ASSET LABORATORIES 11060 Artesia Blvd., Ste C. 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Any NO signifies non - compliance. Any non - compliance will be noted and must be understood as having an impact on the quality of the data. All tests will be performed as requested regardless of any compliance issues. If you have any questions or further instruction, please contact our Project Coordinator at (702) 307 -2659. Cooler Received /Opened On: Rep sample Temp (Deg C): Temp Blank: Carrier name: Last 4 digits of Tracking No.: Cooling process: 11/11/2015 3.6 ❑ Yes 0 No Golden State Overnight 2017 V Ice ❑ Ice Pack Workorder: N017593 IR Gun ID: 2 Packing Material Used: Bubble Wrap ❑ Dry Ice ❑ Other ❑ None Sample Receipt Checklist 1. Shipping container /cooler in good condition? Yes No ❑ Not Present ❑ 2. Custody seals intact, signed, dated on shippping container /cooler? Yes ❑ No ❑ Not Present FV-1 3. Custody seals intact on sample bottles? Yes ❑ No ❑ Not Present R 4. Chain of custody present? Yes No ❑ 5. Sampler's name present in COC? Yes No ❑ 6. Chain of custody signed when relinquished and received? Yes 0 No ❑ 7. Chain of custody agrees with sample labels? Yes R No ❑ 8. Samples in proper container /bottle? Yes R No ❑ 9. Sample containers intact? Yes R No ❑ 10. Sufficient sample volume for indicated test? Yes W] No ❑ 11. All samples received within holding time? Yes 0 No ❑ 12. Temperature of rep sample or Temp Blank within acceptable limit? Yes V No ❑ NA ❑ 13. Water - VOA vials have zero headspace? Yes ❑ No ❑ NA R 14. Water - pH acceptable upon receipt? Yes ❑ No ❑ NA 0 Example: pH > 12 for (CN,S); pH <2 for Metals 15. Did the bottle labels indicate correct preservatives used? Yes ❑ No ❑ NA FV 16. Were there Non - Conformance issues at login? Yes ❑ No ❑ NA 0 Was Client notified? Yes ❑ No ❑ NA V Comments Checklist Completed B far MBC ILA 11 /1212015 Reviewed By: 11/18/15 ao e� r° vn 3 CIO 3 cq 3 v) 3 v3 3 yr rn 3 0 3 cn 3 cn 3 cn 3 va 3 cn 3 U 3 cn 3 cn 3 � LO N ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ T ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ Q Q y ?, Q ?a Q > A Q Q } Q ?, A Z 9 CG cq z at z Cti1 z W z as z m z W z 4 +� U p O O O �z O O O �z O zU zu zuz z�z O z�z O C7 O C7 u: O U 0 04 O U C7 04 O U C7 C4 O U C7 O U C7 u; C7 U O U O U O U O U O U O U O U O U Q Q Q Q Q O O © n" O �" O aj W a W W W W W W W W W W W W W W W W U3 z a � a o a o a a Q U O U 60 O 60 O U Q U O U Q U 60 O U O Q O U >0 c H C7 C7 > >0 >0 C) 0 >0 00 >0 >U O >a 00 w t� �n as O as to fx1 o av In CA O cq In as O ca u) Ga a rA v) as o xl 1n ca O wa In 0.1 O z O 00 N O 00 �c N 00 .-� O 00 \o N 00 O 00 w N 00 .-, O 00 \0 N 00 O 00 \a N 00 I- O 00 \ N 00 O 00 �10 N 00 m Q 00 Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q b H a w a w a w a w a w a w a w a w a w a w a w a w a w a w a w a w o w w o z CC A 0 N o N O N O N O N o N 0 N o N O N O N O N o N 0 N o N O N O N O N 00 00 00 00 00 00 00 00 00 QO 00 d0 DD 00 00 a a a a a a a a y °o °o o° o 0 0 ° o ° o O O in In ' N N m 0 h Y7 V'1 V1 V"1 In V1 �n try U O O O O O O O O U w Q cv 5 •�, v Im •�•� o � a b w A W a o H x o Q o 0 0 0 0 0 0 W A O M o m O M o M o M O o O o cn o� 4 �� vi z °z °z zz C °z °z N 4,. 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