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closure report part 2
Client Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-165703-1 Project/Site: Valero Lab Sample ID: 440-165703-11 Date Collected: 11/10116 13:10 Client Sample ID: D-4-4' ---- - - - - -------- Lab Sample ID: 446465703-10 Date Collected: 11/10/16 12:05 Date Received: 11/12/16 10:15 ................................................................................................................................................................................................................................................................................. Matrix: Solid Date Received: 11/12/16 10:15 I ............................ ......................................... ............................................................................................. Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Toluene-d8 (Surr) 108 79-123 11115116 12:56 1 I 4-Bromofluoroberizene (Surr) 103 79-120 11115116 12:56 1 Dibromofluoromethane (Surr) 101 60-120 11115116 12:56 1 Method: 6020 - Metals (lCP/MS) ug/Kg 11/15/1613:22 1 Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Lead 9.8 0.50 0.25 mg/Kg 11!19/1612:00 11/22/1613:43 20 Client Sample ID: D-1 -2' Lab Sample ID: 440-165703-11 Date Collected: 11/10116 13:10 Matrix: Solid Date Received: 11/12/16 10:15 ................................................................................................................................................................................................................................................................................. ..................................................................................... I ............................ ......................................... ............................................................................................. Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/Kg 11/15/1613:22 1 1,1,1-Trichloroethane ND 2.0 1.0 ug/Kg 11/15/1613:22 1 1, 1,2,2-Tetrachloroethane ND 2.0 1.0 ug/Kg 11/15/16 13:22 1 1, 1,2-Trichloroethane ND 2.0 1.0 ug/Kg 11/15/16 13:22 1 1,1-Dichloroethane ND 2.0 1.0 ug/Kg 11/15/1613:22 1 1,1-Dichloroethene ND 5.0 1.0 ug/Kg 11/15/1613:22 1 1,1-Dichloropropene ND 2.0 1.0 ug/Kg 11/15/1613:22 1 1,2,3--Trichlorobenzene ND 5.0 1.0 ug/Kg 11/15/1613:22 1 1,2,3-Trichloropropane ND 10 1.0 ug/Kg 11/15/16 13:22 1 1 2,4-Trichlorobenzene ND 5.0 1.0 u g/Kg 11/15/16 1 13:22 1 1,2,4-Trimethyl benzene ND 2.0 1.0 ug/Kg 11/15/1613:22 1 1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 11/15/1613:22 1 1,2-Dibromoethane (EDB) ND 2.0 1.0 ug/Kg 11/15/16 13:22 1 1,2-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/15/16 13:22 1 1,2-Dichloroethane ND 2.0 1.0 ug/Kg 11/15/16 13:22 1 1,2-Dichloropropane ND 2.0 1.0 ug/Kg 11/15/16 13:22 1 1,3,5-Tdmethylbenzene ND 2.0 1.0 ug/Kg 11/15!1613:22 1 1,3-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/15/16 13:22 1 113-bichloropro I pane ND 2.0 1.0 u g/Kg 11 /15/ 1 6 13:22 1 1,4-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/15/16 13:22 1 2,2-Dichloropropane ND 2.0 1.0 ug/Kg 11/15/1613:22 1 2-Chlorotoluene .. . ND ....... 5.0 1.0 ug/Kg 11/15/1613:22 1 4-Chlorotoluene ND 5.0 1.0 ug/Kg 11/15/1613:22 1 Benzene ND 2.0 1.0 ug/Kg 11/15/1613:22 1 Bromobenzene ND 5.0 1.0 ug/Kg 11/15/1613:22 1 Bromochloromethane ND 5.0 1.0 ug/Kg 11/15/1613:22 1 Bromodichloromethane ND 2.0 1.0 ug/Kg 11/15/1613:22 1 Bromoform ND 5.0 2.0 ug/Kg 11/15/1613:22 1 Bromomethane ND 5.0 1.0 ug/Kg 11/15/1613:22 1 Carbon tetrachloride ND 5.0 1.0 ug/Kg 11/15/16 13:22 1 Chiorobenzene N . D 2.0 1.0 u I g/Kg -.. 11/15/16 1 1 . 3:22 1 Chloroethane ND 5.0 2.0 ug/Kg 11/15/1613:22 1 Chloroform ND 2.0 1.0 ug/Kg 11/15/1613:22 1 Chloromethane ND 5.0 1.0 ug/Kg 11/15/1613:22 1 cis-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 11/15/1613:22 1 cis-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 11/15116 13:22 1 TestAmerica Irvine Page 25 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-165703-1 Project/Site: Valero ---- ---------- - - - --------------------- - --- -------------------------------- - - - - -- - - - ----------- Client Sample ID: D-1 -2' Lab Sample ID: 440-165703-11 Date Collected: 11/10116 13:10 Matrix: Solid Date Received: 11/12/16 10:15 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Dibromochloromethane ND 2.0 1.0 ug/Kg 11/15/1613:22 1 Dibromomethane N . D 2.0 1.0 ug /Kg 11/15/1613:22 1 Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 11/15/1613:22 1 lsopropyl Ether (DIPE) ND 5.0 1.0 ug/Kg 11/15/16 13:22 1 Ethanol ND 300 100 ug/Kg 11/15116 13:22 1 Ethyl-t-butyl ether (ETBE) ND 5.0 1.0 ug/Kg 11/15/16 13:22 1 Ethylbenzene .. ... .. ..... ... ND 2.0 .......... 1.0 ug/Kg ... 11/15/1613:22 1 Hexachlorobutadiene ND 5.0 1.0 ug/Kg 11/15/1613:22 1 lsopropylbenzene ND 2.0 1.0 ug/Kg 11/15/1613:22 1 m,p-Xylene ND 4.0 2.0 ug/Kg 11/15/1613:22 1 Methylene Chloride ND 20 5.0 ug/Kg 11/15/16 13:22 1 Methyl-t-Butyl Ether (MTBE) ND 5.0 1.0 ug/Kg 11/15/16 13:22 1 Naphthalene ND 5.0 2.0 ug/Kg 11/15/16 13:22 1 n-Butylbenzene 1.3 J 5.0 1.0 ug/Kg 11/15/1613:22 1 N-Propylbenzene ND 2.0 1.0 ug/Kg 11/15/1613:22 1 O-Xylene ND 2.0 1.0 ug/Kg 11/15/1613:22 1 sec-Butylbenzene ND 5.0 1.0 ug/Kg 11/15/1613 :22 1 Styrene ND 2.0 1.0 ug/Kg 11/15/1613:22 1 Tert-amyl-methyl ether (TAME) ND 5.0 1.0 ug/Kg 11/15/16 13:22 1 tent -Butyl alcohol (TBA) ND. 100 10 ug/Kg 11/15/16 13:22 1 tert-Butylbenzene ND 5.0 1.0 ug/Kg 11/15/1613:22 1 Tetrachloroethene ND 2.0 1.0 ug/Kg 11/15/1613 :22 1 Toluene ND 2.0 1.0 ug/Kg 11/15/1613:22 1 trans-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 11/15/1613:22 1 trans-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 11/15/16 13:22 1 Trichloroethene ND 2.0 1.0 ug/Kg 11/15/16 13:22 1 Trichlorofluorornethane ND 5.0 1.0 ug/Kg 11/15/1613:22 1 Vinyl chloride ND 5.0 1.0 ug/Kg 11/15/16 13:22 1 Xylenes, Total ND 4.0 2.0 ug/Kg 11/15/16 13:22 1 p-lsopropyltoluene ND 2.0 1.0 ug/Kg 11/15/1613:22 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Toluene-d8 (Surr) 112 79-123 11115116 13:22 1 4-Bromofluorobenzene (Surr) 101 79-120 11115116 13:22 1 Dibromofluoromethane (Surr) 103 60-120 11115116 13:22 1 Method: 8015E - Diesel Range Organics(DRO)/Oil Range Organics (ORO) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac C13 -C22 17 9.9 4.9 mg/Kg 5/16 16:37 11/16/16 04:17 1 C23-C40 82 9.9 4.9 mg/Kg 11 /15/16 16:37 11/16/16 04:17 1 Surrogate n-Octacosane %Recovery Qualifier Limits 102 40-140 Prepared Analyzed Dil Fac 11115116 16:37 11116116 04:17 1 TestAmerica Irvine Page 26 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-165703-1 Project/Site: Valero -- - - -- - - ------ - --- - - - ------------------------ ----------- - ----- - - ------------ - -- - -- - ----- - -------- - ------ - ------ - - ----- Client Sample ID: D-1 -51 Lab Sample ID: 440-165703-12 Date Collected: 11/10/16 13:15 Matrix: Solid Date Received: 11112/16 10:15 Method: 82608 - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane ND 5.0 0.99 ug/Kg 11/15/1616:38 1 1,1,1-Trichloroethane ND 2.0 0.99 ug/Kg 11/15/1616:38 1 1, 1,2,2-Tetrachloroethane ND 2.0 0.99 ug/Kg 11/15/16 16:38 1 1,1,2-Trichloroet I h I a I ne ND 2.0 0.99 u g/Kg 11/15/1616:38 1 1,1-Dichloroethane ND 2.0 0.99 ug/Kg 11/15/1616:38 1 1,1-Dichloroethene ND 5.0 0.99 ug/Kg 11/15/1616:38 1 1,1-Dichloropropene N I D 2.6 0.99 U*g*6 11/15/1616:38 1 1,2,3-Trichlorobenzene ND 5.0 0.99 ug/Kg 11/15/16 16:38 1 1,2,3-Trichloropropane ND 9.9 0.99 ug/Kg 11/15/16 16:38 1 1,2,4-Trichlorobenzene ND 5.0 0.99 ug/Kg 11/15/1616:38 1 1,2,4-Trimethylbenzene ND 2.0 0.99 ug/Kg 11/15/16 16:38 1 1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 11/15/1616:38 1 1,2-Dibromoethane (EDB) ND 2.0 0.99 ug/Kg 11/15/16 16:38 1 1,2-Dichlorobenzene ND 2.0 0.99 ug/Kg 11/15/16 16:38 1 1,2-Dichloroethane ND 2.0 0.99 ug/Kg 11/15/16 16:38 1 1,2-Dichloropropane ND 2.0 0.99 ug/Kg 11/15/16 16:38 1 1,3,5-Trimethylbenzene ND 2.0 0.99 ug/Kg 11/15/1616:38 1 1,3-Dichlorobenzene ND 2.0 0.99 ug/Kg 11/15/1616:38 1 1 3-bichloropropane ND 2.0 0.99 ug/Kg 11/15/1616:38 1 1,4-Dichlorobenzene ND 2.0 0.99 ug/Kg 11/15/16 16:38 1 2,2-Dichloropropane ND 2.0 0.99 ug/Kg 11/15/1616:38 1 2-Chlorotoluene ND 5.0 0.99 ug/Kg 11/15/1616:38 1 4-Chlorotoluene ND 5.0 0.99 ug/Kg 11/15/1616:38 1 Benzene ND 2.0 0.99 ug/Kg 11/15/16 16:38 1 Bromobenzene ND 5.0 0.99 ug/Kg 11/15/16 16:38 1 Bromochloromethane ND 5.0 0.99 ug/Kg 11/15/1616:38 1 Bromodichloromethane ND 2.0 0.99 ug/Kg 11/15/1616:38 1 Brom , ofo . rm N I D 5.0 M ug/Kg 11/15/1616:38 1 Bromomethane ND 5.0 0.99 ug/Kg 11/15/1616:38 1 Carbon tetrachloride ND 5.0 0.99 ug/Kg 11/15/16 16:38 1 Chlorobenzene ND 2.0 0.99 ug/Kg 11/15/1616:38 1 Chloroethane ND 5.0 2.0 ug/Kg 11/15/1616:38 1 Chloroform ND 2.0 0.99 ug/Kg 11/15/1616:38 1 Chloromethane ND 5.0 0.99 ug/Kg 11/15/1616:38 1 cis-1,2-Dichloroethene ND 2.0 0.99 ug/Kg 11/15/16 16:38 1 cis-1,3-Dichloropropene ND 2.0 0.99 ug/Kg 11/15/16 16:38 1 Dibromochloromethane ND 2.0 0.99 ug/Kg 11/15/16 16:38 1 Dibromomethane ND 2.0 0.99 ug/Kg 11/15/1616:38 1 Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 11/15/1616:38 1 Isopropyl Ether (DIPE) ND 5.0 0.99 ug/Kg 11/15/16 16:38 1 Ethanol ND 300 99 ug/Kg 11/15/1616:38 1 Ethyl-t-butyl ether (ETBE) ND 5.0 0.99 ug/Kg 11/15/16 16:38 1 Ethylbenzene ND 2.0 0.99 ug/Kg 11/15/1616:38 1 Hexachlorobutadiene ND 5.0 0.99 ug/Kg 11/15/1616:38 1 lsopropylbenzene ND 2.0 0.99 ug/Kg 11/1511616:38 1 m,p-Xylene ND 4.0 2.0 ug/Kg 11/15/1616:38 1 Methylene Chloride ND 20 5.0 ug/Kg 11/15/16 16:38 1 Methyl-t-Butyl Ether (MTBE) ND 5.0 0.99 ug/Kg 11/15116 16:38 1 Naphthalene ND 5.0 2.0 ug/Kg 11/15/1616:38 1 TestAmerica Irvine Page 27 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440 - 165703 -1 Project/Site: Valero -- - - - - -- - -- -- - -- -- -- -- ----- - - - - -- - - - -- - -- _..__.___ ------- - ----- - --- - - -- -- -- --- - - - - -- - - - -- -- -- - - -- _ - -_ -- - - - - - -- - -- -- - - - - C lent e : - - Lab Sample : 440-165703-12 Date Collected: 11/10/16 1 :15 Matrix: Solid Date Received: 11/12/16 10 :15 Method: 8260B - Volatile Organic Compounds (GC /MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac n- Butylbenzene ND 5.0 0.99 ug /Kg 11/15/1616:38 1 N- Propylbenzene ND 2.0 0.99 ug /Kg 11/15/1616:38 1 o- Xylene ND 2.0 0.99 ug /Kg 11/15/1616:38 1 sec - Butylbenzene ND 5.0 0.99 ug /Kg 11/15/16 16:38 1 Styrene ND 2.0 0.99 ug /Kg 11/15/1616:38 1 Tert- amyl - methyl ether (TAME) ND 5.0 0.99 ug /Kg 11/15/16 16:38 1 tert-Butyl alcohol (TBA) ND 99 9.9 ug /Kg 11/15/16 16:38 1 tert - Butylbenzene ND 5.0 0.99 ug /Kg 11/15/1616:38 1 Tetrachloroethene ND 2.0 0.99 ug /Kg 11/15/1616:38 1 Toluene ND 2.0 0.99 ug /Kg 11/15/1616:38 1 trans -1,2- Dichloroethene ND 2.0 0.99 ug /Kg 11/15/16 16:38 1 trans- 1,3- Dichloropropene ND 2.0 1. 0.99 ug /Kg 11/15/1616:38 1 Trichloroethene ND 2.0 0.99 ug /Kg 11/15/1616:38 1 Trichlorofluoromethane ND 5.0 0.99 ug /Kg 11/15/16 16:38 1 Vinyl chloride ND 5.0 0.99 ug /Kg 11/15/16 16:38 1 Xylenes, Total ND 4.0 2.0 ug /Kg 11/15/16 16:38 1 p- Isopropyltoluene ND 2.0 0.99 ug /Kg 11/15/1616:38 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Toluene -d8 (Surr) 107 79-123 11/15/16 16 :38 1 4- Bromofluorobenzene (Surr) 101 79-120 11/15/16 16 :38 1 Dibromofluoromethane (Surr) 103 60 -120 11/15/16 16 :38 1 Method: 8015B - Diesel Range Organics(DRO) /Oil Range Organics (ORO) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac C13 -C22 26 9.9 4.9 mg /Kg 11/15/16 16 :37 11/16/16 05:00 1 C23 -C40 100 9.9 4.9 mg /Kg 11/15/16 16:37 11/16/16 05:00 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac n- Octacosane 81 40-140 11/15116 16 :37 11/16/16 05 :00 1 Client Sample : -2 -2' Lab Sample ID: 440-165703-13 Date Collected: 11/10116 13 :20 Matrix: Solid Date Received: 11/12/16 1 :15 Method: 82608 /CA_LUFTMS - Volatile Organic Compounds by GC /MS Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Volatile Fuel Hydrocarbons (C4 -C12) ND 0.099 0.069 mg /Kg 11/16/16 15:01 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 105 60-120 11/16/16 15 :01 1 4- Bromofluorobenzene (Surr) 102 79-120 11/16/16 15 :01 1 Toluene -d8 (Surr) 108 79-123 11/16/16 15 :01 1 Method: 8260B - Volatile Organic Compounds (GCIMS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2- Tetrachloroethane ND 5.0 1.0 ug /Kg 11/15/16 17:04 1 1,1,1 - Trichloroethane ND 2.0 1.0 ug /Kg 11/15/1617:04 1 1,1,2,2 - Tetrachloroethane ND 2.0 1.0 ug /Kg 11/15/1617:04 1 1,1,2 - Trichloroethane ND 2.0 1.0 ug /Kg 11/15/1617 :04 1 1,1- Dichloroethane ND 2.0 1.0 ug /Kg 11/15/1617 :04 1 Page 28 of 87 TestAmerica Irvine 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-165703-1 Project/Site: Valero - - - - ----------------------- - ------ - Client Sample ID: D-2-2' Lab Sample ID: 440-165703-13 Date Collected: 11/10/16 13:20 Matrix: Solid Date Received: 11/12/16 10:15 Method: 8260B - `Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1-Dichloroethene ND 5.0 1.0 11115/1617 :04 1 1, 1 -Dichloropropene ND 2.0 1.0 u g . /K I g 11/15/1617:04 1 1,2,3-Trichlorobenzene ND 5.0 1.0 ug/Kg 11/15/16 17:04 1 1,2,3-Trichloropropane ND 10 1.0 ug/Kg 11/15/1617:04 1 1,44-Trichlorobenzene ND 5.0 1.0 u g/Kg 11/15/1617:04 1 1,2,4-Trimethyl benzene ND 2.0 1.0 ug/Kg 11/15/1617:04 1 1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 11/15/1617:04 1 1,2-Dibromoethane (EDB) ND 2.0 1.0 ug/Kg 11/15/16 17:04 1 1,2-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/15/16 17:04 1 1,2-Dichloroethane ND 2.0 1.0 ug/Kg 11/15/1617:04 1 1,2-Dichloropropane ND 2 1 .0 1.0 - u . g /K I g 11 /15/1 . 6 1 1 1 7:04 1 1,3,5-Trimethylbenzene ND 2.0 1.0 ug/Kg 11/15/1617:04 1 1,3-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/15/1617:04 1 1,3-bichloropropane ND 2.0 1.0 ug/Kg 11/15/16 17:04 1 1,4-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/15/16 17:04 1 2,2-Dichloropropane ND 2.0 1.0 ug/Kg 11/15/1617:04 1 2-Chlorotoluene ND 5.0 1.0 ug/Kg 11/15/1617:04 1 4-Chlorotoluene ND 5.0 1.0 ug/Kg 11/15/1617:04 1 Benzene ND 2.0 1.0 ug/Kg 11/15/16 17:04 1 Bromobenzene ND 5.0 1.0 ug/Kg 11115/1617:04 1 Bromochloromethane ND 5.0 1.0 ug/Kg 11/15/1617:04 1 Bromodichloromethane ND 2.0 1.0 ug/Kg 11/15/1617:04 1 Bromoform ND 5.0 2.0 ug/Kg 11115/16 17:04 1 Bromomethane ND 5.0 1.0 ug/Kg 11/15/1617:04 1 Carbon tetrachloride ND 5.0 1.0 ug/Kg 11/15/16 17:04 1 Chiorobenzene ND 2.0 1.0 ug/Kg 11/15/1617:04 1 Chloroethane ND 5.0 2.0 ug/Kg 11/15/1617:04 1 Chloroform ND 2.0 1.0 ug/Kg 11/15/16 17:04 1 Chloromethane ND 5.0 1.0 ug/Kg 11/15/1617:04 1 cis-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 11/15/1617:04 1 cis-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 11/15/1617:04 1 Dibromochloromethane N . D 2.0 1.0 1 ug/Kg 11/15/1617:04 1 Dibromomethane ND 2.0 1.0 ug/Kg 11/15/16 17:04 1 Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 11/15/1617:04 1 Isopropyl Ether (DIPE) ND 5.0 1.0 ug/Kg 11/15/16 17:04 1 Ethanol ND 300 100 ug/Kg 11/15/16 17:04 1 Ethyl-t-butyl ether (ETBE) ND 5.0 1.0 ug/Kg 11/15/16 17:04 1 Ethylbenzene ND 2.0 1.0 ug/Kg 11/15/1617 :04 1 Hexachlorobutadiene ND 5.0 1.0 ug/Kg 11/15/1617:04 1 lsopropylbenzene ND 2.0 1.0 ug/Kg 11/15/1617:04 1 m,p-Xylene ND 4.0 2.0 ug/Kg 11/15/1617 :04 1 Methylene Chloride ND 20 5.0 ug/Kg 11/15/16 17:04 1 Methyl-t-Butyl Ether (MTBE) ND 5.0 1.0 ug/Kg 11/15/16 17:04 1 Naphthalene ND 5.0 2.0 ug/Kg 11/15/1617:04 1 n-Butylbenzene ND 5.0 1.0 ug/Kg 11/15/1617:04 1 N-Propylbenzene ND 2.0 1.0 ug/Kg 11/15/16 17:04 1 0-Xylene ND 2.0 1.0 ug/Kg 11/15/1617:04 1 sec-Butylbenzene ND 5.0 1.0 ug/Kg 11/15/1617 :04 1 Styrene ND 2.0 1.0 ug/Kg 11/15/16 17:04 1 TestAmerica Irvine Page 29 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440 - 165703 -1 Project/Site: Valero - -- _ _ -- - - - - -- ----------------------------- - - - - -- Client le I -2 -2' - -- ------ - - - - -- - - _ _ -- - - - - -- _ __ - -- -- - - - - -- - - - - -- - - - -- -- Lab Sample ID: 440-165703-13 Date Collected: 11/10116 13:20 Matrix: Solid Date Received: 11/12/16 10:15 Method: 8260B - Volatile Organic Compounds (GC /MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Tert -amyl- methyl ether (TAME) ND 5.0 1.0 ug /Kg 1 11/15/16 17:04 1 tert -Butyl alcohol (TBA) ND 100 10 ug /Kg 1,1,2,2- Tetrachloroethane 11/15/16 17:04 1 tent- Butylbenzene ND 5.0 1.0 ug /Kg ND 11/15/1617:04 1 Tetrachloroethene ND 2.0 1.0 ug /Kg 2.0 11/15/1617:04 1 Toluene ND 2.0 1.0 ug /Kg 1.0 11/15/1617:04 1 trans -1,2- Dichloroethene ND 2.0 1.0 ug /Kg ug /Kg 11/15/1617:04 1 trans -1,3- Dichloropropene ND 2.0 1.0 ug /Kg . . . 11/15/1617:04 1 Trichloroethene ND 2.0 1.0 ug /Kg 1 11/15/1617:04 1 Trichlorofluoromethane ND 5.0 1.0 ug /Kg 1,2,4- Trimethylbenzene 11/15/1617:04 1 Vinyl chloride ND 5.0 1.0 ug /Kg ND 11/15/16 17:04 1 Xylenes, Total ND 4.0 2.0 ug /Kg 2.0 11/15/16 17:04 1 p- Isopropyltoluene ND 2.0 1.0 ug /Kg 1.0 11/15/1617:04 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac Toluene -d8 (Surr) 105 79-123 11/15/96 97:04 1 4- Bromofluorobenzene (Surr) 100 79-120 11/15/16 17:04 1 Dibromof/uoromethane (Surr) 104 60 -120 11/15/16 17:04 1 Method: 6020 - Metals (ICP /MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Lead 5.8 0.49 0.25 mg /Kg 11 /15/16 12:27 11116/16 15:10 20 Client Sample -2 -6' Lab Sample :440- 165703 -'14 Date Collected: 11/10116 13:25 Matrix: Solid Date Deceived: 11/12/16 10:15 Method: 8260B /CA_LUFTMS - Volatile Organic Compounds by GC /MS Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Volatile Fuel Hydrocarbons (C4 -C12) ND 0.10 0.070 mg /Kg 11/16/16 15:30 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed DU Fac Dibromof/uoromethane (Surr) 103 60-120 11/16/16 15 :30 1 4- Bromofluorobenzene (Surr) 111 79-120 11/16/16 15 :30 1 Toluene -d8 (Surr) 114 79-123 11/16/16 15 :30 1 Method: 8260B - Volatile Organic Compounds (GC /MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2- Tetrachloroethane ND 5.0 1.0 ug /Kg 11/15/16 17:30 1 1,1,1 - Trichloroethane ND 2.0 1.0 ug /Kg 11/15/1617:30 1 1,1,2,2- Tetrachloroethane ND 2.0 1.0 ug /Kg 11/15/16 17:30 1 1,1,2- Trichloroethane ND 2.0 1.0 ug /Kg 11/15/16 17:30 1 1,1- Dichloroethane ND 2.0 1.0 ug /Kg 11/15/1617:30 1 1,1- Dichloroethene ND 5.0 1.0 ug /Kg 11/15/1617:30 1 1,1- Dichloropropene ND 2.0 1.0 ug /Kg 11/15/1617:30 1 1,2,3- Trichlorobenzene ND 5.0 1.0 ug /Kg 11/15/16 17:30 1 1,2,3- Trichloropropane ND 10 1.0 ug /Kg 11/15/16 17:30 1 1,44- frichlorobenzene ND 5.0 1.0 ug /Kg ... . 11/15/1617:30 1 1,2,4- Trimethylbenzene ND 2.0 1.0 ug /Kg 11/15/16 17:30 1 1,2- Dibromo -3- Chloropropane ND 5.0 2.0 ug /Kg 11/15/16 17:30 1 1,2- Dibromoethane (EDB) ND 2.0 1.0 ug /Kg 11/15/16 17:30 1 1,2- Dichlorobenzene ND 2.0 1.0 ug /Kg 11/15/1617:30 1 TestAmerica Irvine Page 30 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc Project/Site: Valero TestAmerica Job ID: 440-165703-1 Client Sample ID: D-2-6' Lab Sample ID: 440-165703-14 Date Collected: 11110/16 13:25 Matrix: Solid Date Received: 11/12/16 10:15 Method: 8260B - Volatile Organic Compounds (GCIMS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,2-Dichloroethane ND 2.0 1.0 ug/Kg 11/15/1617:30 1 1,2-Dichloropropane ND 2.0 . ...... 1.0 u . g . /K . g . . ..... 11/15/16 vm I 1,3,5-Trimethylbenzene ND 2.0 1.0 ug/Kg 11/15/1617:30 1 1,3-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/15/16 17:30 1 1,3-bichloropropane ND 2.0 1.0 ug/Kg 11/15/1617:30 1 1,4-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/15/1617:30 1 2,2-Dichloropropane ND 2.0 1.0 ug/Kg 11/15/1617:30 1 2-Chlorotoluene ND 5.0 1.0 ug/Kg 11/15/1617:30 1 4-Chlorotoluene ND 5.0 1.0 ug/Kg 11/15/1617:30 1 Benzene ND 2.0 1.0 ug/Kg 11/15/1617:30 1 Bromobenzene ND 5.0 1.0 ug/Kg 11/15/1617:30 1 Bromochloromethane ND 5.0 1.0 ug/Kg 11/15/1617:30 1 Bromodichloromethane ND 2.0 1.0 ug/Kg 11/15/1617:30 1 Bromoform ND 5.0 2.0 ug/Kg 11/15116 17:30 1 Bromomethane ND 5.0 1.0 ug/Kg 11/15/1617:30 1 Carbon tetrachloride ND 5.0 1.0 ug/Kg 11/15/16 17:30 1 Chlorobenzene ND 2.0 1.0 ug/Kg 11/15/1617:30 1 Chloroethane ND 5.0 2.0 ug/Kg 11/15/1617:30 1 Chloroform ND 2.0 1.0 ug/Kg 11/15/16 17:30 1 Chloromethane ND 5.0 1.0 ug/Kg 11/15/1617 :30 1 cis-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 11/15/16 17:30 1 cis-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 11/15/1617:30 1 Dibromochloromethane ND 2.0 1.0 ug/Kg 11/15/1617:30 1 Dibromomethane ND 2.0 1.0 ug/Kg 11/15/1617:30 1 Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 11/15/1617:30 1 Isopropyl Ether (DIPE) ND 5.0 1.0 ug/Kg 11/15/16 17:30 1 Ethanol ND 300 100 ug/Kg 11/15/16 17:30 1 Ethyl-t-butyl ether (ETBE) ND 5.0 1.0 ug/Kg 11/15/16 17:30 1 Ethylbenzene ND 2.0 1.0 ug/Kg 11/15/1617 :30 1 Hexachlorobutadiene ND 5.0 1.0 ug/Kg 11/15/1617:30 1 Isopropylbenzene ND 2.0 1.0 ug/Kg 11/15/1617:30 1 m . p-Xylene ND 4.0 2.0 ug/Kg 11/15/1617:30 1 Methylene Chloride ND 20 5.0 ug/Kg 11/15/16 17:30 1 Methyl-t-Butyl Ether (MTBE) ND 5.0 1.0 ug/Kg 11/15/16 17:30 1 Naphthalene ND 5.0 2.0 ug/Kg 11/15/16 17:30 1 n-Butylbenzene ND 5.0 1.0 ug/Kg 11/15/1617:30 1 N-Propylbenzene ND 2.0 1.0 ug/Kg 11/15/1617:30 1 o-Xylene ND 2.0 1.0 ug/Kg 11/15/1617:30 1 sec-Butylbenzene ND 5.0 1.0 ug/Kg 11/15/1617:30 1 Styrene ND 2.0 1.0 ug/Kg 11/15/16 17:30 1 Tert-amyl-methyl ether (TAME) ND 5.0 1.0 ug/Kg 11/15/16 17:30 1 tert-Butyl alcohol (TBA) ND 100 10 ug/Kg 11/15/16 17:30 1 tert-Butylbenzene ND 5.0 1.0 ug/Kg 11/15/1617:30 1 Tetrachlor o*ethene ND 2.6 1.0 ug/Kg 11/15/1617:30 1 Toluene ND 2.0 1.0 ug/Kg 11/15/1617:30 1 trans-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 11/15/16 17:30 1 trans-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 11/15/16 17:30 1 Trichloroethene ND 2.0 1.0 ug/Kg 11/15/1617:30 1 Trichlorofluoromethane ND 5.0 1.0 ug/Kg 11/15/1617:30 1 TestAmerica Irvine Page 31 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-165703-1 Project/Site: Valero - - - --- - --- - ------ - ---------------- - - - ----- - ------- - - - ------- - - - ------ - - ------------ - ----- - - - - -- Client Sample ID: D-2-6' Lab Sample ID: 440-165703-14 Date Collected: 11/10116 13:25 Matrix: Solid Date Received: 11/12/16 10:15 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Vinyl chloride ND 5.0 1.0 ug/Kg 11/15/16 17:30 1 Xylenes, Total ND 4.0 2.0 ug/Kg 11/15/16 17:30 1 p-Isopropyltoluene ND 2.0 1.0 ug/Kg 11/15/1617:30 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Toluene-d8 (Surr) 108 79-123 1111511617 1 4-Bromofluorobenzene (Surr) 103 79-120 11115116 17:30 1 Dibromofluoromethane (Surr) 101 60-120 11115116 17:30 1 Method: 6020 - Metals (ICP/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Lead 36 0.50 0.25 mg/Kg 11/15/16 12:27 11/16/16 15:13 20 Client Sample ID: D-3-21 Lab Sample ID: 440-165703-15 Date Collected: 11/10/16 13.30 Matrix- Solid Date Received: 11/12/16 10:15 - --- - -------- - ------ ---- Method: 8260B/CA LUFTMS - Volatile Organic Compounds by GC/MS Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Volatile Fuel Hydrocarbons (C4-C12) ND 0.099 0.070 mg/Kg 11/16/16 16:00 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 101 60-120 11116116 16:00 1 4-Bromofluorobenzene (Surr) 104 79-120 11116116 16:00 1 Toluene-d8 (Surr) 109 79-123 11116116 16:00 1 Method: 82608 - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/Kg 11/15/1617:57 1 1, 1, 1 -Trichloroethane ND 2.0 1.0 ug/Kg 11/15/16 17:57 1 1, 1,2,2-Tetrachloroethane ND 2.0 1.0 ug/Kg 11/15/1617:57 1 1, 1,2-Trichloroethane ND 2.0 1.0 ug/Kg 11/15/16 17:57 1 1,1-Dichloroethane ND 2.0 1.0 ug/Kg 11/15/1617:57 1 1,1-Dichloroethene ND 5.0 1.0 ug/Kg 11/15/16,17:57 1 1,1-Dichloropropene ND 2.0 1.0 ug/Kg 11/15/16 17:57 1 1,2,3-Trichlorobenzene ND 5.0 1.0 ug/Kg 11/15/16 17:57 1 1,2,3-Trichloropropane ND 10 1.0 ug/Kg 11 /15/16 17:57 1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/Kg 11/15/1617:57 1 1,2,4-Trimethylbenzene ND 2.0 1.0 ug/Kg 11/15/1617:57 1 1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 11/15/16 17:57 1 1,2-Dibromoethane (EDB) ND 2.0 1.0 ug/Kg 11/15/16 17:57 1 1,2-Dichlorobenzene ND 2.0 1.0 ug/Kg 11 /15/16 17:57 1 1,2-Dichloroethane ND 2.0 1.0 ug/Kg 11115/16 17.57 1 1,2-Dichloropropane ND 2.0 1.0 ug/Kg 11/15/16 17:57 1 1,3,5-Trimethylbenzene ND 2.0 1.0 ug/Kg 11/15/16 17:57 1 1,3-Dichlorobenzene ND 2.0 1.0 ug/Kg 11 /15/16 17:57 1 1,3-bichioropropane ND 2.0 1.0 ug/Kg 11/15/1617:57 1 1,4-Dichlorobenzene ND 2.0 1.0 ug/Kg 11 /15/16 17:57 1 2,2-Dichloropropane ND 2.0 1.0 ug/Kg 11/15/1617:57 1 2-Chlorotoluene ND 5.0 1.0 ug/Kg 11/15/1617:57 1 4-Chlorotoluene ND 5.0 1.0 ug/Kg 11/15/1617:57 1 TestAmerica Irvine Page 32 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-165703-1 Project/Site: Valero -------------- - - - - -- - - ------------------ - - - ------- - ------- Client Sample ID: D-3-2' Lab Sample ID: 440-165703-15 Date Collected: 11/10/16 13:30 Matrix: Solid Date Received: 11/12/°16'10:15 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Benzene ND 2.0 1.0 ug/Kg 11/15/1617:57 1 Bromobenzene ND 5.0 1.0 ug/K9 11/15/1617:57 1 Bromochloromethane ND 5.0 1.0 ug/Kg 11/15/16 17:57 1 Bromodichloromethane ND 2.0 1.0 ug/Kg 11/15/1617:57 1 Bromof6rm* ND 5.0 2.0 ug/Kg 11/15/1617:57 1 Bromomethane ND 5.0 1.0 ug/Kg 11/15/1617:57 1 Carbon tetrachloride ND 5.0 1.0 ug/Kg 11/15/16 17:57 1 Chlorobenzene ND 2.0 1.0 ug/Kg 11/15/1617:57 1 Chloroethane ND 5.0 2.0 ug/Kg 11/15/1617:57 1 Chloroform ND 2.0 1.0 ug/Kg 11/15/1617:57 1 Chloromethane ND 5.0 1.0 ug/Kg 11/15/1617:57 1 cis-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 11/15/1617:57 1 cis-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 11/15/1617:57 1 Dibromochioromethane ND 2.0 1.0 ug/Kg 11/15/1617:57 1 Dibromomethane ND 2.0 1.0 ug/Kg 11/15/1617:57 1 Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 11/15/1617:57 1 Isopropyl Ether (DIPS) ND 5.0 1.0 ug/Kg 11/15/16 17:57 1 Ethanol ND 300 100 ug/Kg 11/15/1617:57 1 Ethyl-t-butyl ether (ETBE) ND 5.0 1.0 ug/Kg 11/15/16 17:57 1 Ethylbenzene ND 2.0 1.0 ug/Kg 11/15/1617:57 1 Hexachlorobutadiene ND 5.0 1.0 ug/Kg 11/15/1617:57 1 lsopropylbenzene ND 2.0 1.0 ug/Kg 11/15/1617:57 1 m I p-Xylene ND 4.0 2.0 u g/Kg 11/15/16 17:57 1 Methylene Chloride ND 20 5.0 ug/Kg 11/15/16 17:57 1 Methyl-t-Butyl Ether (MTBE) ND 5.0 1.0 ug/Kg 11/15/16 17:57 1 Naphthalene ND 5.0 2.0 ug/Kg 11/15/1617:57 1 n-Butylbenzene ND 5.0 1.0 ug/Kg 11/15/1617:57 1 N-Propylbenzene ND 2.0 1.0 ug/Kg 11/15/16 17:57 1 o-Xylene ND 2.0 1.0 ug/Kg 11/15/1617:57 1 see-Butylbenzene ND 5.0 1.0 ug/Kg 11/15/1617:57 1 Styrene ND 2.0 1.0 ug/Kg 11/15/1617:57 1 Tert-amyl-methyl ether (TAME) N . D 5.0 1.0 ug/Kg 11/15/16 17:57 1 tert-Butyl alcohol (TBA) ND 100 10 ug/Kg 11/15/16 17:57 1 tert-Butylbenzene ND 5.0 1.0 ug/Kg 11/15/1617:57 1 Tetrachloroethene ND 2.6 1.0 ug/kg 11/15/1617:57 1 Toluene ND 2.0 1.0 ug/Kg 11/15/1617:57 1 trans- 1,2-Dichloroethene ND 2.0 1.0 ug/Kg 11/15/16 17:57 1 trans-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 11/15/1617:57 1 Trichloroethene ND 2.0 1.0 ug/Kg 11/15/1617:57 1 Trichlorofluorornethane ND 5.0 1.0 ug/Kg 11/15/1617:57 1 Vinyl chloride ND 5.0 1.0 ug/Kg 11/15/16 17:57 1 Xylenes, Total ND 4.0 2.0 ug/Kg 11/15/16 17:57 1 p-Isopropyltoluene ND 2.0 1.0 ug/Kg 11/15/1617:57 1 Surrogate %Recovety Qualifier Limits Prepared AnaWed Dit Fac -1 Toluene-d8 (Surr) 106 79-123 11115116 17:57 4-Bromofluoroberizene (Surr) 96 79-120 11115116 17:57 1 Dibromofluoromethane (Surr) 101 60-120 11115116 17:57 1 TestAmerica Irvine Page 33 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc Project/Site: Valero -- -- ------- - ------ - - - - - --- - - - -- - -- - -- - - ------- - - - ---- - ---- - ---------------- - - - - - -- Client Sample ID: D-3-2' Date Collected: 11/10116 13:30 Date Received: 11/12116 10:15 Method: 6020 - Metals (ICP/MS) Analyte, Result Qualifier RL Lead 2.9 0.50 ............... .......................................................................................... ................................... .............................................................. .............. ...................... Client Sample ID: D-3-6' Date Collected: 11/10116 13:35 Date Received: 11/12/16 10:15 MDL Unit 0.25 mg/Kg r Method: 8260B/CA LUFTMS - Volatile Organic Compounds by GC/MS Analyte Result Qualifier RL MDL Unit Volatile Fuel Hydrocarbons (C4-C12) ND 0.10 0.070 mg/Kg Surrogate %Recovery Qualifier Limits Dibromofluoromethane (Surr) 101 60-120 4-Bromofluorobenzene (Surr) 104 79-120 Toluene -d8 (Surr) 111 79-123 Method: 8260B - Volatile Organic Compounds (GC /MS) Analyte Result Qualifier 1,1,1,2-Tetrachloroethane ND 1,1,1-Trichloroethane ND 1, 1,2,2-Tetrachloroethane ND 1, 1,2-Trichloroethane ND 1,1-Dichloroethane ND 1,1-Dichloroethene ND 1 7 1 -bichloropropene ND 1,2,3-Trichlorobenzene ND 1,2,3-Trichloropropane ND 1,2,4-Trichlorobenzene ND 1,2,4-Trimethylbenzene ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane (EDB) ND 1,2-Dichlorobenzene ND 1,2-Dichloroethane ND 1,2-bichloropropane ND 1, 3,5-Trimethyl benzene ND 1,3-Dichlorobenzene ND 1,3-Dichloropropane ND 1,4-Dichlorobenzene ND 2,2-Dichloropropane ND 2-Chlorotoluene ND 4-Chlorotoluene ND Benzene ND Bromobenzene .... ND Bromochloromethane ND Bromodichloromethane ND Brornof6rm ND Brornornethane ND Carbon tetrachloride ND Chlorobenzene ND Chloroethane ND Chloroform ND TestAmerica Job ID: 440-165703-1 5-ab Sample ID: 440-165703-1 Matrix: Solii D Prepared Analyzed Dil Fac 11/15/16 12:27 11/16/16 15:15 20 Lab Sample ID: 440-165703-16 Matrix: Solid D Prepared Analyzed Dil Fac 11/16/16 16:29 1 Prepared Analyzed Dil Fac 11116116 16:29 1 11116116 16:29 1 11116116 16:29 1 RL MDL Unit D Prepared Analyzed Dil Fac 5.0 1.0 ug/Kg 11/15/16 18:23 1 2.0 1.0 ug/Kg 11/15/16 18:23 1 2.0 1.0 ug/Kg 11/15/16 18:23 1 2.0 1.0 ug/Kg 11/15/16 18:23 1 2.0 1.0 ug/Kg 11/15/16 18:23 1 5.0 1.0 ug/Kg 11/15/16 18:23 1 2.0 1.0 ug/Kg 11/15/16 18:23 1 5.0 1.0 ug/Kg 11/15/1618:23 1 10 1.0 ug/Kg 11/15/16 18:23 1 5.0 1.0 ug/Kg 11/15/16 18:23 1 2.0 1.0 ug/Kg 11/15/16 18:23 1 5.0 2.0 ug/Kg 11/15/16 18:23 1 2.0 1.0 ug/Kg 11/15/16 18:23 1 2.0 1.0 ug/Kg 11 /15/16 18:23 1 2.0 1.0 ug/Kg 11/15/16 18:23 1 2.0 1.0 ug/Kg 11/15/16 18:23 1 2.0 1.0 ug/Kg 11/15/16 18:23 1 2.0 1.0 ug/Kg 11/15/16 18:23 1 2.0 1.0 ug/Kg 11/15/16 18:23 1 2.0 1.0 ug/Kg 11/15/16 18:23 1 2.0 1.0 ug/Kg 11/15/16 18:23 1 5.0 1.0 ug/Kg 11/15/16 18:23 1 5.0 1.0 ug/Kg 11115/16 18:23 1 2.0 1.0 ug/Kg 11/15/16 18:23 1 5.0 1.0 u9/K9 11/15/16 18:23 1 5.0 1.0 ug/Kg 11/15/16 18:23 1 2.0 1.0 ug/Kg 11/15/16 18:23 1 5.0 2.0 ug/Kg 11/15/16 18:23 1 5.0 1.0 ug/Kg 11/15/16 18:23 1 5.0 1.0 ug/Kg 11/15/16 18:23 1 2.0 1.0 ug/Kg 11/15/1618:23 1 5.0 2.0 ug/Kg 11/15/16 18:23 1 2.0 1.0 ug/Kg 11/15/16 18:23 1 Page 34 of 87 TestAmerica Irvine 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID-. 440-165703-1 Project/Site: Valero, - - - - ----- - -------- ------ ------ - ------------- - -- - --- - ---- Client Sample ID: D-3-6" Lab Sample ID: 440-165703-16 Date Collected: 11/10116 13:35 Matrix: Solid Date Received: 11/12116 10:15 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloromethane ND 5.0 1.0 ug/Kg 11/15/1618:23 1 cis-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 11/15/16 18:23 1 cis-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 11/15/16 18:23 1 Dibromochloromethane ND 2.0 1.0 ug/Kg 11/15/1618:23 1 Dibromornethane ND 2.0 1.0 ug/Kg 11/15/1618:23 1 Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 11/15/1618:23 1 Isopropyl Ether (biPE) ND 5.0 1.0 ug/Kg 11/15/16 18:23 1 Ethanol ND 300 100 ug/Kg 11/15/1618:23 1 Ethyl-t-butyl ether (ETBE) ND 5.0 1.0 ug/Kg 11/15/16 18:23 1 i Ethylbenzene ND 2.0 1.0 ug/Kg 11/15/16 18:23 1 Hexachlorobutadiene ND 5.0 1.0 ug/Kg 11/15/16 18:23 1 lsopropylbenzene ND 2.0 1.0 ug/Kg 11/15/1618:23 1 rn,p-Xylene ND 4.0 2.0 ug/Kg 11/15/16 18:23 1 Methylene Chloride ND 20 5.0 ug/Kg 11/15/16 18:23 1 Methyl-t-Butyl Ether (MTBE) ND 5.0 1.0 ug/Kg 11/15/16 18:23 1 Naphthalene ND 5.0 2.0 ug/Kg 11/15/1618:23 1 n-Butylbenzene ND 5.0 1.0 ug/Kg 11/15/1618:23 1 N-Propylbenzene ND 2.0 1.0 ug/Kg 11/15/1618:23 1 o-Xylene ND 2.0 1.0 ug/Kg 11/15/1618:23 1 sec-Butylbenzene ND 5.0 1.0 ug/Kg 11/15/1618:23 1 Styrene ND 2.0 1.0 ug/Kg 11/15/16 18:23 1 Tert-amyl-methyl ether (TAME) ND 5.0 1.0 ug/Kg 11/15/16 18:23 1 tert-Butyl alcohol (TBA) ND 100 10 ug/Kg 11/15/16 18:23 1 tert-Butylbenzene ND 5.0 1.0 ug/Kg 11/15/1618:23 1 -1 etrachloroethene ND 2.0 1.0 ug/Kg 11/15/1618:23 1 Toluene ND 2.0 1.0 ug/Kg 11/15/1618:23 1 trans-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 11/15/1618:23 1 trans- 1, 3-Dichloropropene ND 2.0 1.0 ug/Kg 11/15/16 18:23 1 Trichloroethene ND 2.0 1.0 ug/Kg 11/15/16 18:23 1 Trichlorofluorornethane ND 5.0 1.0 ug/Kg 11/15/1618:23 1 Vinyl chloride ND 5.0 1.0 ug/Kg 11/15/16 18:23 1 Xylenes, Total ND 4.0 2.0 ug/Kg 11/15/16 18:23 1 p-Isopropyltoluene ND 2.0 1.0 ug/Kg 11/15/16 18:23 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Toluene-d8 (Surr) 107 79-123 11115116 18:23 1 4-Bromofluorobenzene (Surr) 101 79-120 11115116 18:23 1 Dibromofluoromethane (Surr) 103 60-120 11115116 18:23 1 Method: 6020 - Metals (ICP/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Lead 2.4 0.50 0.25 mg/Kg 11/15/16 12:27 11/16/16 15:18 20 Client Sample ID: 10K-E-2' Lab Sample ID: 440-165703-17 Date Collected: 11/10/16 13:37 Matrix: Solid Date Received: 11/12/16 10:15 Method: 8260B/CA LUFTMS - Volatile Organic Compounds by GC/MS Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Volatile Fuel Hydrocarbons (C4-C12) ND 0.099 0.070 mg/Kg 11/16/16 16:59 1 TestAmerica Irvine Page 35 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-165703-1 Project/Site: Valero --------------- - - - - -- - Client Sample ID: I OK-E-2' Lab Sample ID: 440-165703-17 Date Collected: 11/10/16 13:37 Matrix: Solid Date Received: 11/12116 10:15 ............. ........... .... Surrogate %Recovety Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 107 60-120 11116116 16:59 1 4-Bromofluorobenzene (Surr) 101 79-120 11116116 16:59 1 Toluene-d8 (Surr) 110 79-123 11116116 16:59 1 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane ND 5.0 0.99 ug/Kg 11/16/1616:59 1 1,1,1-Trichloroethane ND 2.0 0.99 ug/Kg 11/16/1616:59 1 1,1,2,2-Tetrachloroethane ND 2.0 0.99 ug/Kg 11/16/16 16:59 1 I 1,2 -Trichloroethane ND 2.0 0.99 ug/Kg 11/16/1616:59 1 1,1-Dichloroethane ND 2.0 0.99 ug/Kg 11/16/1616:59 1 1,1-Dichloroethene ND 5.0 0.99 ug/Kg 11/16/1616:59 1 1,1-Dichloropropene ND 2.0 0.99 ug/Kg 11/16/1616:59 1 1,2,3-Trichlorobenzene ND 5.0 0.99 ug/Kg 11/16/1616:59 1 1,2,3-Trichloropropane ND 9.9 0.99 ug/Kg 11/16/16 16:59 1 1,2,4-Tdchlorobenzene ND 5.0 0.99 ug/Kg 11/16/1616:59 1 1,2,4-Trimethylbenzene ND 2.0 0.99 ug/Kg 11/16/1616:59 1 1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 11/16/1616:59 1 1,2-bibromoethane (EDB) ND 2.0 0.99 ug/Kg 11/16/16 16:59 1 1,2-Dichlorobenzene ND 2.0 0.99 ug/Kg 11/16/16 16:59 1 1,2-Dichloroethane ND 2.0 0.99 ug/Kg 11/16/16 16:59 1 1,2-Dichloropropane ND 2.0 0.99 ug/Kg 11/16/16 16:59 1 1,3,5-Trimethylbenzene ND 2.0 0.99 ug/Kg 11/1611616:59 1 1,3-Dichlorobenzene ND 2.0 0.99 ug/Kg 11/16/16 16:59 1 1,3-Dichloropropane ND 2.0 0.99 ug/Kg 11/16/1616:59 1 1,4-Dichlorobenzene ND 2.0 0.99 ug/Kg 11116/16 16:59 1 2,2-Dichloropropane ND 2.0 0.99 ug/Kg 11/16/1616:59 . . 1 2 Chlorotoluene ND 5.6 0.66 ug/Kg ........ . .... 11/16/1616:59 1 4-Chlorotoluene ND 5.0 0.99 ug/Kg 11/16/1616:59 1 Benzene ND 2.0 0.99 ug/Kg 11/16/1616:59 1 Brornobenzene ND 5.0 6.99 ug/Kg 11 /16/1 6 16:59 1 Brornochloromethane ND 5.0 0.99 ug/Kg 11/16/16 16:59 1 Bromodichloromethane ND 2.0 0.99 ug/Kg 11/16/16 16:59 1 Brornoform ND 5.0 1 2.0 ug/Kg 11/16/1616:59 1 Brornornethane ND 5.0 0.99 ug/Kg 11/16/1616:59 1 Carbon tetrachloride ND 5.0 0.99 ug/Kg 11/16/16 16:59 1 Chlorobenzene ND 2.0 0.99 ug/Kg 11/16/16 16:59 1 Chloroethane ND 5.0 2.0 ug/Kg 11/16/1616:59 1 Chloroform ND 2.0 0.99 ug/Kg 11/16/1616:59 1 Chioromethane ND 5.0 0.99 ug/Kg 11/16/1616:59 1 cis-1,2-Dichloroethene ND 2.0 0.99 ug/Kg 11/16/16 16:59 1 cis-1,3-Dichloropropene ND 2.0 0.99 ug/Kg 11/16/1616:59 1 Dibromochloromethane ND 2.0 0.99 ug/Kg 11/16/1616:59 1 Dibromornethane ND 2.0 0.99 ug/Kg 11/16/1616:59 1 Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 11/16/1616 :59 1 Isopropyl Ether (DIPE) ND 5.0 0.99 ug/Kg 11/16/16 16:59 1 Ethanol ND 300 99 ug/Kg 11/16/16 16:59 1 Ethyl-t-butyl ether (ETBE) ND 5.0 0.99 ug/Kg 11/16/16 16:59 1 Ethylbenzene ND 2.0 0.99 ug/Kg 11/16/16 16:59 1 Hexachlorobutadiene ND 5.0 0.99 ug/Kg 11/16/1616:59 1 TestAmerica Irvine Page 36 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-165703-1 Project/Site: Valero _--------- a---------------- - - - - -- ---- - ------------- - ------------------------ - - - - -- Client Sample ID: I OK-E-2 Lab Sample ID: 440-165703-17 Date Collected: 11/10/16 13:37 Matrix: Solid Date Received: 11/12/16 10:15 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac lsopropylbenzene ND 2.0 0.99 ug/Kg 1 11/16/1616:59 1 m,p-Xylene ND 4.0 2.0 ug/Kg 1,1,2,2-Tetrachloroethane 11/16/1616:59 2.0 Methylene Chloride ND 20 5.0 ug/Kg ND 11/16/16 16:59 1 Methyl-t-Butyl Ether (MTBE) ND 5.0 0.99 ug/Kg 11/16/16 16:59 1 Naphthalene ND 5.0 2.0 ug/Kg 11/16/1616:59 1 n-Butylbenzene ND 5.0 0.99 ug/Kg 11/16/1616:59 1 N-Propylbenzene ND 2.0 0.99 ug/Kg 11/16/1616:59 1 o-Xylene ND 2.0 0.99 ug/Kg 11/16/16 16:59 1 sec-Butylbenzene ND 5.0 0.99 ug/Kg 11/16/1616:59 1 Styrene ND 2.0 0.99 ug/Kg 11/16/16 16:59 1 Tert-amyl-methyl ether (TAME) ND 5.0 0.99 ug/Kg ........ ..... 11/16/16 16:59 1 tert-Butyl alcohol (TBA) ND 99 9.9 ug/Kg 11/16/16 16:59 1 tert-Butylbenzene ND 5.0 0.99 ug/Kg 11/16/1616:59 1 Tetrachloroethene ND 2.0 0.99 ug/Kg 11/16/1616:59 1 Toluene ND 2.0 0.99 uglKg 11/16/1616:59 1 trans-1,2-Dichloroethene ND 2.0 0.99 ug/Kg 11/16/16 16:59 1 trans-1,3-Dichloropropene ND 2.0 0.99 ug/Kg 11/16/16 16:59 1 Trichloroethene ND 2.0 0.99 ug/Kg 11/16/1616:59 1 Trichlorofluoromethane ND 5.0 0.99 ug/Kg 11/16/1616:59 1 Vinyl chloride ND 5.0 0.99 ug/Kg 11/16/16 16:59 1 Xylenes, Total ND 4.0 2.0 ug/Kg 11/16/16 16:59 1 p-lsopropyltoluene ND 2.0 0.99 ug/Kg 11/16/1616:59 1 Surrogate %Recovety Qualifier Limits Prepared Analyzed Dil Fac Toluene -d8 (Surr) 110 79-123 11116116 16:59 1 4-Bromofluorobenzene (Surr) 101 79-120 11116116 16:59 1 Dibromofluoromethane (Surr) 107 60-120 11116116 16:59 1 Method: 6020 - Metals (ICP/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Lead 2.3 0.50 0.25 mg/Kg 5/16 12:27 11/16/16 15:20 20 ............................................................... ........................................................ -- ....................................... Client Sample ID: 1OK-E-6" ....................................................... ............. ............ ................................................................................................................................... ...................................................................... . ........................................ ---- .......... .............................. Lab Sample ID: 440-165703-18 Date Collected: 11/10/16 13:40 Matrix: Solid Date Received: 11/12/16 10:15 Method: 8260B/CA LUFTMS - Volatile Organic Compounds by GC/MS Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Volatile Fuel Hydrocarbons (C4-C12) ND 0.099 0.070 mg/Kg 11/16/16 17:29 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac Dibrornofluoromethane (Surr) 106 60-120 11116116 17:29 1 4-Bromofluorobenzene (Surr) 102 79-120 11116116 17. -29 1 Toluene -d8 (Surr) 109 79-123 11116116 17:29 1 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1, 1, 1,2-Tetrachloroethane ND 5.0 0.99 ug/Kg 11/16/16 17:29 1 1,1,1-Trichloroethane ND 2.0 0.99 ug/Kg 11/16/1617:29 1 1,1,2,2-Tetrachloroethane ND 2.0 0.99 ug/Kg 11/16/1617:29 1 1, 1,2-Trichloroethane ND 2.0 0.99 ug/Kg 11/16/16 17:29 1 TestAmerica Irvine Page 37 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-165703-1 Project/Site: Valero ----------------------------- - - - - - - -- - -- - --------- - ------------------ - ---------------- - -- - - - ----- - -- - -------- Client Sample ID: I OK-E-61 Lab Sample ID: 440-165703-18 Date Collected: 11/10/16 13:40 Matrix: Solid Date Received: 11/12/16 10:15 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1-Dichloroethane ND 2.0 0.99 11/16/1617:29 1 1,1-Dichloroethene ND 5.0 0.99 ug/Kg 11/16/1617:29 1 1,1-Dichloropropene ND 2.0 0.99 ug/Kg 11/16/1617:29 1 1,2,3-Trichlorobenzene ND 5.0 0.99 ug/Kg 11/16/16 17:29 1 1,2,3-Trichloropropane ND 9.9 0.99 ug/Kg 11/16/1617:29 1 1,2,4-Trichlorobenzene ND 5.0 0.99 ug/Kg 11/16/16 17:29 1 1,2,4-Trimethylbenzene ND 2.0 0.99 ug/Kg 11/16/16 17:29 1 1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 11/16/1617:29 1 1,2-bibromoethane (LbB) ND 2.0 0.99 ug/Kg 11/16/16 17:29 1 1,2-Dichlorobenzene ND 2.0 0.99 ug/Kg 11/16/1617:29 1 1,2-Dichloroethane ND 2.0 0.99 ug/Kg 11/16/1617:29 1 1,2-Dichloropropane ND 2.0 0.99 ug/Kg 11/16/16 17:29 1 1,3,5-Trimethylbenzene ND 2.0 0.99 ug/Kg 11/16/1617:29 1 1,3-Dichlorobenzene ND 2.0 0.99 ug/Kg 11/16/16 17:29 1 1,3-Dichloropropane ND 2.0 0.99 ug/Kg 11/16/1617:29 1 1,4-Dichlorobenzene ND 2.0 0.99 ug/Kg 11/16/1617:29 1 2,2-Dichloropropane ND 2.0 0.99 ug/Kg 11/16/1617:29 1 2-Chlorotoluene ND 5.0 0.99 ug/Kg 11/16/16 17:29 1 4-Chlorotoluene ND 5.0 0.99 ug/Kg 11/16/1617:29 1 Benzene ND 2.0 0.99 ug/Kg 11/16/1617 :29 1 Bromobenzene ND 5.0 0.99 ug/Kg 11/16/1617:29 1 Bromochloromethane ND 5.0 0.99 ug/Kg 11/16/1617:29 1 Bromodichloromethane ND 2.0 0.99 ug/Kg 11/16/1617:29 1 Bromoform ND 5.0 2.0 ug/Kg 11/16/1617:29 1 Bromomethane ND 5.0 0.99 ug/Kg 11/16/1617:29 1 Carbon tetrachloride ND 5.0 0.99 ug/Kg 11/16/16 17:29 1 Chlorobenzene ND 2.0 0.99 ug/Kg 11/16/1617:29 1 Chloroethane ND 5.0 2.0 ug/Kg 11/16/1617:29 1 Chloroform ND 2.0 0.99 ug/Kg 11/16/1617:29 1 Chloromethane ND 5.0 0.99 ug/Kg 11/16/1617:29 1 cis-1,2-Dichloroethene ND 2.0 0.99 ug/Kg 11/16/1617:29 1 cis-1,3-Dichloropropene ND 2.0 0.99 ug/Kg 11/16/16 17:29 1 Dibromochloromethane ND 2.0 0.99 ug/Kg 11/16/1617:29 1 Dibromomethane ND 2.0 0.99 ug/Kg 11/16/1617:29 1 Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 11/16/1617:29 1 Isopropyl Ether (DIPE) ND 5.0 0.99 ug/Kg 11/16/16 17:29 1 Ethanol ND 300 99 ug/Kg 11/16/1617:29 1 Ethyl-t-butyl ether (ETBE) ND 5.0 0.99 ug/Kg 11/16/16 17:29 1 Ethylbenzene* ND 2.0 0.99 ug/Kg 11/16/1617:29 1 Hexachlorobutadiene ND 5.0 0.99 ug/Kg 11/16/1617:29 1 lsopropylbenzene ND 2.0 0.99 ug/Kg 11/16/16 17:29 1 m . p-Xylene ND 4.0 2.0 ug/Kg 11/16/1617:29 1 Methylene Chloride ND 20 5.0 ug/Kg 11/16/16 17:29 1 Methyl-t-Butyl Ether (MTBE) ND 5.0 0.99 ug/Kg 11/16/16 17:29 1 Naphthalene ND 5.0 2.0 ug /Kg 11/16/1617:29 1 n-Butylbenzene ND 5.0 0.99 ug/Kg 11/16/1617:29 1 N-Propylbenzene ND 2.0 0.99 ug/Kg 11/16116 17:29 1 o-Xylene ND 2.0 0.99 ug/Kg 11/16/1617:29 1 sec-Butylbenzene ND 5.0 0.99 ug/Kg 11/16/16 17:29 1 TestAmerica Irvine Page 38 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc Result Qualifier RL MDL Unit D Prepared Analyzed TestAmerica Job ID: 440-165703-1 Project/Site: Valero ND 0.10 0.070 mg/Kg 11/16/16 17:58 1 Surrogate - - - - - ---- - - ------- - ------ ---------- - - - - - --- Client Sample ID: 10K-E-6' - -- - -------- - ---- - - - - - --- - ---------------------- ------- DR Fac Dibromofluoromethane (Surr) Lab Sample ID: 440-165703-18 Date Collected: 11/10/16 13:40 11116116 17:58 1 4-Bromofluorobenzene (Surr) 104 Matrix: Solid Date Received: 11/12/16 10:15 1 Toluene -d8 (Surr) 108 79-123 ----------- Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) 1.0 ug/Kg 11/16/1617:58 Analyte, Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Styrene ND 2.0 0.99 ug/Kg 11/16/1617:29 1 Tert-amyl-methyl ether (TAME) ND 5.0 0.99 ug/Kg 11/16/16 17:29 1 tert-Butyl alcohol (TBA) ND 99 9.9 ug/Kg 11/16/16 17:29 1 tert-Butylbenzene ND 5.0 0.99 ug/Kg 11/16/16 17:29 1 Tetrachloroethene ND 2.0 0.99 ug/Kg 11/16%1617:29 1 Toluene ND 2.0 0.99 ug/Kg 11/16/1617:29 1 trans-1,2-Dichloroethene ND 2.0 0.99 ug/Kg 11/16/1617:29 1 trans-1,3-Dichloropropene ND 2.0 0.99 ug/Kg 11/16/16 17:29 1 Trichloroethene ND 2.0 0.99 ug/Kg 11/16/1617:29 1 Trichlorofluoromethane ND 5.0 0.99 ug/Kg 11/16/1617:29 1 ... ..... . . Vinyl chloride ND 5.0 0.99 ug/Kg 11/16/16 17:29 1 Xylenes, Total ND 4.0 2.0 ug/Kg 11/16/16 17:29 1 p-isopropyltoluene ND 2.0 0.99 ug/Kg 11/16/1617:29 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed DR Fac Toluene -d8 (Surr) 109 79-123 11116116 17:29 1 4-Bromofluorobenzene (Surr) 102 79-120 11116116 17:29 1 Dibromofluoromethane (Surr) 106 60-120 11116116 17:29 1 Method: 6020 - Metals (ICP/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Lead 1.9 0.50 0.25 mg/Kg 5/16 12:27 11/16/16 15:23 20 Client Sample ID: 1 OK-W-2 . .... . .......... - -------- Lab Sample ID: 440-165703-19 Date Collected: 11/10/16 13:42 Matrix: Solid Date Received: 11/12/16 10:14 Method: 8260B/CA-LUFTMS - Volatile Organic Compounds by GC /MS Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Volatile Fuel Hydrocarbons (C4-C12) ND 0.10 0.070 mg/Kg 11/16/16 17:58 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed DR Fac Dibromofluoromethane (Surr) 106 60-120 11116116 17:58 1 4-Bromofluorobenzene (Surr) 104 79-120 11116116 17:58 1 Toluene -d8 (Surr) 108 79-123 11116116 17:58 1 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/Kg 11/16/16 17:58 1 1,1,1-Trichloroethane ND 2.0 1.0 ug/Kg 11/16/1617:58 1 1, 1,2,2-Tetrachloroethane ND 2.0 1.0 ug/Kg 11/16/16 17:58 1 1, 1,2-Trichloroethane ND 2.0 1.0 ug/Kg 11/16/1617:58 1 1,1-Dichloroethane ND 2.0 1.0 ug/Kg 11/16/1617:58 1 1,1-Dichloroethene ND 5.0 1.0 ug/Kg 11/16/1617:58 1 1,1-Dichloropropene ND 2.0 1.0 ug/Kg 11/16/1617:58 1 1,2,3-Trichlorobenzene ND 5.0 1.0 ug/Kg 11/16/16 17:58 1 1,2,3-Tdchloropropane ND 10 1.0 ug/Kg 11/16/16 17:58 1 1,2,4-Tdchlorobenzene ND 5.0 1.0 ug/Kg 11/16/16 17:58 1 1,2,4-Trimethylbenzene ND 2.0 1.0 ug/Kg 11/16/16 17:58 1 1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 11/16/16 17:58 1 1,2-bibromoethane (EbB) ND 2.0 1.0 ug/Kg 11/16/16 17:58 1 TestAmerica Irvine Page 39 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-165703-1 Project/Site: Valero - - -- - -- - -- - --- - ---- - ------ - ------ - ----------- Client Sample ID: 10K-W-21 Lab Sample ID: 440-165703-19 Date Collected: 11/10/16 13:42 Matrix: Solid Date Received: 11/12/16 10:15 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte, Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,2-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/16/16 17:58 1 1,2-Dichloroethane ND 2.0 1.0 ug/Kg 11/16/16 17:58 1 1,2-Dichloropropane ND 2.0 1.0 ug/Kg 11/16/1617:58 1 1,3,5-Thmethylbenzene ND 2.0 1.0 ug/Kg 11/16/1617:58 1 1,3-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/16/1617:58 1 1,3-Dichloropropane ND 2.0 1.0 ug/Kg 11/16/1617:58 1 1,4-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/16/1617 :58 1 2,2-Dichloropropane ND 2.0 1.0 ug/Kg 11/16/16 17:58 1 2-Chlorotoluene ND 5.0 1.0 ug/Kg 11/16/16 17:58 1 4-Chlorotoluene ND 5.0 1.0 ug/Kg 11/16/1617:58 1 Benzene ND 2.0 1.0 ug/Kg 11/16/1617:58 1 Bromobenzene ND 5.0 1.0 ug/Kg 11/16/1617:58 1 Bromochloromethane ND 5.0 1.0 ug/Kg 11/16/1617:58 1 Bromodichloromethane ND 2.0 1.0 ug/Kg 11/16/16 17:58 1 Bromoform ND 5.0 2.0 ug/Kg 11/16/16 17:58 1 Bromomethane ND 5.0 1.0 ug/Kg 11/16/1617:58 1 Carbon tetrachloride ND 5.0 1.0 ug/Kg 11/16/16 17:58 1 Chlorobenzene ND 2.0 1.0 ug/Kg 11/16/1617:58 1 Chloroethane ND 5.0 2.0 ug/Kg 11/16/1617 :58 1 Chloroform ND 2.0 1.0 ug/Kg 11/16/1617:58 1 Chioromethane ND 5.0 1.0 ug/Kg 11/16/1617:58 1 cis-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 11/16/16 17:58 1 cis-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 11/16/16 17:58 1 Dibromochloromethane ND 2.0 1.0 ug/Kg 11/16/1617 :58 1 Dibromomethane ND 2.0 1.0 ug/Kg 11/16/1617:58 1 Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 11/16/1617:58 1 Isopropyl Ether (DIPE) ND 5.0 1.0 ug/Kg 11116/16 17:58 1 Ethanol ND 300 100 ug/Kg 11/16/1617:58 1 Ethyl-t-butyl ether (ETBE) ND 5.0 1.0 ug/Kg 11/16/16 17:58 1 Ethylbenzen'e ND 2.0 1.0 ug/Kg 11/16/1617:58 1 Hexachlorobutadiene ND 5.0 1.0 ug/Kg 11/16/1617:58 1 lsopropylbenzene ND 2.0 1.0 ug/Kg 11/16/16 17:58 1 m'p-Xylene ND 4.0 2.0 ug/Kg 11/16/1617:58 1 Methylene Chloride ND 20 5.0 ug/Kg 11/16/16 17:58 1 Methyl-t-Butyl Ether (MTBE) ND 5.0 1.0 ug/Kg 11/16/16 17:58 1 Naphthalene ND 5.0 2.0 ug/Kg 11/16/1617:58 1 n-Butylbenzene ND 5.0 1.0 ug/Kg 11/16/16 17:58 1 N-Propylbenzene ND 2.0 1.0 ug/Kg 11/16/16 17:58 1 o4ylene ND 2.0 1.0 ug/Kg 11/16/1617:58 1 sec-Butylbenzene ND 5.0 1.0 ug/Kg 11/16/1617 :58 1 Styrene ND 2.0 1.0 ug/Kg 11/16/16 17:58 1 Tert-amyl-methyl ether (TAME) ND 5.0 1.0 ug/Kg 11/16/16 17:58 1 tert-Butyl alcohol (TBA) ND 100 10 ug/Kg 11/16/16 17:58 1 tert-Butylbenzene ND 5.0 1.0 ug/Kg 11/16/1617:58 1 Tetrachloroethene ND 2.0 1.0 ug/Kg 11/16/1617:58 1 Toluene ND 2.0 1.0 ug/Kg 11/16/1617:58 1 trans-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 11/16/1617:58 1 trans-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 11/16/16 17:58 1 Trichloroethene ND 2.0 1.0 ug/Kg 11/16/1617:58 1 TestAmerica Irvine Page 40 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc Project/Site: Valero It #. Method: 8260B - Volatile Organic Compounds (GC /MS) (Continued) Analyte Result Qualifier RL MDL Unit Trichlorofluoromethane ND 5.0 1.0 ug /Kg Vinyl chloride ND 5.0 1.0 ug /Kg Xylenes, Total ND 4.0 2.0 ug /Kg p- Isopropyltoluene ND 2.0 1.0 ug /Kg TestAmerica Job ID: 440 - 165703 -1 .,ar - ! 1T 0 Prepared Analyzed Dil Fac 11/16/16 17:58 1 11/16/16 17:58 1 11/16/16 17:58 1 11/16/16 17:58 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Toluene -d8 (Surr) 108 79-123 11/16/16 17:58 1 4- Bromofluorobenzene (Surr) 104 79-120 11/16/16 17:58 1 Dibromofluoromethane (Surr) 106 60-120 11/16/16 17:58 1 Method: 6020 - Metals (ICP /MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Lead 1.5 0.50 0.25 mg /Kg 11/15/16 12:27 11/16/16 15:25 20 .__.._._..._....__.__._ -__ -- Client Sample : 10K-W-6' _ ......... _.-------- Lab Sample ID: 440-165703-20 Date Collected: 11/10/16 13 :45 Matrix: Solid Date Deceived: 11/12/16 10:15 Method: 8260B /CA_LUFTMS - Volatile Organic Compounds by GC /MS Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Volatile Fuel Hydrocarbons (C4 -C12) ND 0.10 0.070 mg /Kg 11/16/16 18:28 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Dibromofluoromethane (Surr) 108 60-120 11/16/16 18 :28 1 4- Bromofluorobenzene (Surr) 104 79-120 11/16/16 18 :28 1 Toluene -d8 (Surr) 109 79-123 11/16/16 18 :28 1 Method: 8260B - Volatile Organic Compounds (GC /MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2- Tetrachloroethane ND 5.0 1.0 ug /Kg 11/16/1618 :28 1 1,1,1 - Trichloroethane ND 2.0 1.0 ug /Kg 11/16/1618:28 1 1,1,2,2- Tetrachloroethane ND 2.0 1.0 ug /Kg 11/16/1618:28 1 1,1,2- Trichloroeth ane ND 2.0 1.0 ug /Kg 11/16/16 18:28 1 1,1- Dichloroethane ND 2.0 1.0 ug /Kg 11/16/1618:28 1 1,1- Dichloroethene ND 5.0 1.0 ug /Kg 11/16/1618:28 1 1,1- Dichloropropene ND 2.0 1.0 ug /Kg 11/16/1618:28 1 1,2,3- Trichlorobenzene ND 5.0 1.0 ug /Kg 11116/16 18:28 1 1,2,3- Trichloropropane ND 10 1.0 ug /Kg 11/16/16 18:28 1 1,2,4- Trichlorobenzene ND 5.0 1.0 ug /Kg 11/16116 18:28 1 1,2,4- Trimethylbenzene ND 2.0 1.0 ug /Kg 11/16/16 18:28 1 1,2- Dibromo- 3- Chloropropane ND 5.0 2.0 ug /Kg 11/16/1618:28 1 1,2- Dibromoethane (EDB) ND 2.0 1.6 ug /Kg 11/16/16 18:28 1 1,2- Dichlorobenzene ND 2.0 1.0 ug /Kg 11/16/16 18:28 1 1,2- Dichloroethane ND 2.0 1.0 ug /Kg 11/16/16 18:28 1 1,2- Dichloropropane ND 2.0 1.0 ug /Kg 11/16/1618:28 1 1,3,5- Trimethylbenzene ND 2.0 1.0 ug /Kg 11/16/1618:28 1 1,3- Dichlorobenzene ND 2.0 1.0 ug /Kg 11/16/1618:28 1 1,3- Dichloropropane ND 2.0 1.0 ug /Kg 11/16/1618:28 1 1,4- Dichlorobenzene ND 2.0 1.0 ug /Kg 11/16/16 18.28 1 2,2- Dichloropropane ND 2.0 1.0 ug /Kg 11/16/1618:28 1 2- Chlorotoluene ND 5.6 1.0 ug /Kg 11/16/ 1 6 18 :28 1 TestAmerica Irvine Page 41 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440 - 165703 -1 Project/Site: Valero _- .----- --------- - --- - - - -- - - - - - -- -- --- - - - - -- ---------- - - - - -- --- _____------- - - - - -- --------------- - - - - -- - -- - - -- - -- - -_ -_ _ - -- __ __ Client : 10K-W-6' Lab} Sample ! D: 440-165703-20 Date Collected: 11/10116 13:45 Matrix: Solid Date Deceived: 11/12/16 10 :15 Method: 82608 - Volatile Organic Compounds (GC /MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 4- Chlorotoluene ND 5.0 1.0 ug /Kg 11/16/1618:28 1 Benzene ND 2.0 1.0 ug /Kg 11/16/1618:28 1 Bromobenzene ND 5.0 1.0 ug /Kg 11/16/1618:28 1 Bromochloromethane ND 5.0 1.0 ug /Kg 11/16/1618:28 1 Bromodichloromethane ND 2.0 1.0 ug /Kg 11/16/1618:28 1 Bromoform ND 5.0 2.0 ug /Kg 11/16/1618:28 1 Bromomethane ND 5.0 1.0 ug /Kg 11/16/1618:28 1 Carbon tetrachloride ND 5.0 1.0 ug /Kg 11/16/16 18:28 1 Chlorobenzene ND 2.0 1.0 ug /Kg 11/16/1618:28 1 Chloroethane ND 5.0 2.0 ug /Kg 11/16/16 18:28 1 Chloroform ND 2.0 1.0 ug /Kg 11/16/1618:28 1 Chloromethane ND.. 5.0 1.0 ug /Kg 11/16/1618:28 1 cis -1,2- Dichloroethene ND 2.0 1.0 ug /Kg 11/16/16 18:28 1 cis -1,3- Dichloropropene ND 2.0 1.0 ug /Kg 11/16/16 18:28 1 Dibromochloromethane ND 2.0 1.0 ug /Kg 11/16/1618:28 1 Dibromomethane ND 2.0 1.0 ug /Kg 11/16/1618:28 1 Dichlorodifluoromethane ND 5.0 2.0 ug /Kg 11/16/1618:28 1 Isopropyl Ether (DIPE) ND 5.0 1.0 u9/K9 .. 11/16/16 18:28 1 Ethanol ND 300 100 ug /Kg 11/16/1618:28 1 Ethyl -t -butyl ether (ETBE) ND 5.0 1.0 ug /Kg 11/16/16 18:28 1 Ethylbenzene ND 2.0 1.0 ug /Kg 11/16/16 18:28 1 Hexachlorobutadiene ND 5.0 1.0 ug /Kg 11/16/1618:28 1 Isopropylbenzene ND 2.0 1.0 ug /Kg 11/16/16 18:28 1 m,p- Xylene ND 4.0 2.0 ug /Kg 11/16/16 18:28 1 Methylene Chloride ND 20 5.0 ug /Kg 11/16/16 18:28 1 Methyl -t -Butyl Ether (MTBE) ND 5.0 1.0 ug /Kg 11/16/16 18:28 1 Naphthalene ND 5.0 2.0 ug /Kg 11/16/1618:28 1 n- Butylbenzene ND 5.0 1.0 ug /Kg 11/16/1618:28 1 N- Propylbenzene ND 2.0 1.0 ug /Kg 11/16/1618:28 1 o- Xylene ND 2.0 1.0 ug /Kg 11/16/1618 :28 1 see Butylbenzene ND 5.0 1.0 ug /Kg 11/16/16 18:28 1 Styrene ND 2.0 1.0 ug /Kg 11/16/1618:28 1 Tert- amyl- methyl ether (TAME) ND 5.0 1.0 ug /Kg 11%16/16 18:28 1 tert-Butyl alcohol (TBA) ND 100 10 ug /Kg 11/16116 18:28 1 tert- Butylbenzene ND 5.0 1.0 ug /Kg 11/16/16 18:28 1 Tetrachloroethene ND 2.0 1.0 ug /Kg 11/16/16 18:28 1 Toluene ND 2.0 1.0 ug /Kg 11/16/16 18:28 1 trans -1,2- Dichloroethene ND 2.0 1.0 ug /Kg 11/16/16 18:28 1 trans -1,3- Dichloropropene ND 2.0 1.0 ug /Kg 11/16/16 18:28 1 Trichloroethene ND 2.0 1.0 ug /Kg 11/16/1618 :28 1 Trichlorofluoromethane ND 5.0 1.0 ug /Kg 11/16/1618:28 1 Vinyl chloride ND 5.0 1.0 u /K 9 9 11/16/16 18:28 1 Xylenes, Total ND 4.0 2.0 ug /Kg 11/16/16 18:28 1 p4sopropyltoluene ND 2.0 1.0 ug /Kg 11/16/1618:28 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Toluene -d8 (Surr) 109 79-123 11/16/16 18 :28 1 4- Bromofluorobenzene (Surr) 104 79-120 11/16/16 18 :28 1 Dibromof/uoromethane (Surr) 108 60-120 11/16/16 18 :28 1 TestAmerica Irvine Page 42 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc Project/Site: Valero - - - -- --------- -- - - - - - -- - --- - - - ------------------ Client Sample ID: 10K-W-6' Date Collected: 11110/16 13:45 Date Received: 11/12/16 10:15 Method: 6020 - Metals (ICP/MS) Analyte Result Qualifier Lead 1.7 ................................................ .... .......................................................... ............ ............................................................... ............................................................. ............................................................................................... Client Sample ID: 4K-S-E-2' Date Collected: 11/10116 14:02 Date Received: 11/12/16 10:15 RL 0.50 MDL 0.25 Unit mg/Kg ................................................................................................ TestAmerica Job ID: 440-165703-1 Lab Sample ID: 440-165703-20 Matrix: Solid D Prepared Analyzed Dil Fac 11/15/16 12:27 11/16/16 15:28 20 .............................................................................................. Lab Sample ID: 440-165703-21 Matrix: Solid Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane ND 13 2.5 ug/Kg 11/16/16 11:33 1 1, 1, 1 -Trichloroethane ND 5.0 2.5 ug/Kg 11/16/16 11:33 1 1,1,2,2-Tetrachloroethane ND 5.0 2.5 ug/Kg 11/16/16 11:33 1 1, 1,2-Trichloroethane ND 5.0 2.5 U91K9 11/16/16 11:33 1 1,1-Dichloroethane ND 5.0 2.5 ug/Kg 11/16/1611:33 1 1,1-Dichloroethene ND 13 2.5 ug/Kg 11/16/1611:33 1 1,1-Dichloropropene ND 5.0 2.5 ug/Kg 11/16/1611:33 1 1,2,3-Trichlorobenzene ND 13 2.5 ug/Kg 11/16/1611:33 1 1,2,3-Trichloropropane ND 25 2.5 ug/Kg 11/16/16 11:33 1 1,2,4-Trichlorobenzene ND 13 2.5 ug/Kg 11/16/16 11:33 1 I 1,2,4-Trimethylbenzene ND 5.0 2.5 ug/Kg 11/16/16 11:33 1 1,2-Dibromo-3-Chloropropane ND 13 5.0 ug/Kg 11/16/16 11:33 1 1,2-Dibromoethane (EDB) Nb 5.0 2.5 ug/Kg 11/16/16 11:33 1 1,2-Dichlorobenzene ND 5.0 2.5 ug/Kg 11116/1611:33 1 1,2-Dichloroethane ND 5.0 2.5 ug/Kg 11/16/1611:33 1 1,2-Dichloropropane ND 5.0 2.6 ug/kg 11 /*16/1*6 11:33 1 1,3,5-Trimethylbenzene ND 5.0 2.5 ug/Kg 11/16/1611:33 1 1,3-Dichlorobenzene ND 5.0 2.5 ug/Kg 11 /16/16 11:33 1 1,3-Dichloropropane ND 5.0 2.5 ug/Kg 11/16116 11. -33 1 1,4-Dichlorobenzene ND 5.0 2.5 ug/Kg 11/16/1611:33 1 2,2-Dichloropropane ND 5.0 2.5 ug/Kg 11/16/1611:33 1 2-Chlorotoluene ND 13 2.5 ug/Kg 11/16/1611:33 1 4-Chlorotoluene ND 13 2.5 ug/Kg 11/16/1611:33 1 Benzene ND 5.0 2.5 ug/Kg 11/16/16 11:33 1 Bromobenzene ND 13 2.5 ug/Kg 11/16/1611:33 1 Bromochloromethane ND 13 2.5 ug/Kg 11/16/1611:33 1 Bromodichloromethane ND 5.0 2.5 ug/Kg 11/16/1611:33 1 Bromoform ND 13 5.0 ug/Kg 11/16/1611:33 1 Bromomethane ND 13 2.5 ug/Kg 11/16/16 11:33 1 Carbon tetrachloride ND 13 2.5 ug/Kg 11/16/16 11:33 1 Chlorobenzene ND 5.0 2.5 ug/Kg 11/16/16 11:33 1 Chloroethane ND 13 5.0 ug/Kg 11/16/16 11:33 1 Chloroform ND 5.0 2.5 ug/Kg 11/16/1611:33 1 Chloromethane ND 13 2.5 ug/Kg 11/16/1611:33 1 cis-1,2-Dichloroethene ND 5.0 2.5 ug/Kg 11/16/1611:33 1 cis-1,3-Dichloropropene ND 5.0 2.5 ug/Kg 11/16/1611:33 1 Dibromochloromethane ND 5.0 2.5 ug/Kg 11/16/1611:33 1 Dibromomethane ND 5.0 2.5 ug/Kg 11/16/16 11:33 1 Dichlorodifluoromethane ND 13 5.0 ug/Kg 11/16/1611:33 1 Isopropyl Ether (DIPE) ND 13 2.5 ug/Kg 11/16/16 11:33 1 Ethanol ND 750 250 ug/Kg 11/16/1611 :33 1 Ethyl-t-butyl ether (ETBE) ND 13 2.5 ug/Kg 11/16/16 11:33 1 TestAmerica Irvine Page 43 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-165703-1 Project/Site: Valero Client Sample ID: 4K-S- E-2' Lab Sample ID: 440-165703-21 Date Collected: 11/10116 14.02 Matrix: Solid Date Received: 11/12/16 10:15 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Ethylbenzene ND 5.0 2.5 ug/Kg 11/16/16 11:33 1 Hexachlorobutadiene ND 13 2.5 ug/Kg 11/16/1611:33 1 lsopropylbenzene ND 5.0 2.5 ug/Kg 11/16/1611:33 1 m,P-Xylene ND 10 5.0 ug/Kg 11/16/1611:33 1 Methylene Chloride ND 50 13 ug/Kg 11/16/16 11:33 1 Methyl-t-Butyl Ether (MTBE) ND 13 2.5 ug/Kg 11/16/16 11:33 1 Naphthalene ND 13 5.0 ug/Kg 11/16/1611:33 1 n-Butylbenzene ND 13 2.5 ug/Kg 11116/1611:33 1 N-Propylbenzene ND 5.0 2.5 ug/Kg 11/16/1611:33 1 o-Xylene ND 5.0 2.5 ug/Kg 11/16/16 11:33 1 sec-Butylbenzene ND 13 2.5 ug/Kg 11/16/16 11:33 1 Styrene ND 5.0 2.5 ug/Kg 11/16/16 11:33 1 Tert-amyl-methyl ether (TAME) ND 13 2.5 ug/Kg 11/16/16 11:33 1 tert-Butyl alcohol (TBA) ND 250 25 ug/Kg 11/16/16 11:33 1 tert-Butylbenzene ND 13 2.5 ug/Kg 11/16/1611:33 1 Tetrachloroethene ND 5.0 2.5 ug/Kg 11/16/1611:33 1 Toluene ND 5.0 2.5 ug/Kg 11/16/1611:33 1 trans-1,2-Dichloroethene ND 5.0 2.5 ug/Kg 11/1611611:33 1 trans-1,3-Dichloropropene ND 5.0 2.5 ug/Kg 11/16/16 11:33 1 Trichloroethene ND 5.0 2.5 ug/Kg 11/16/1611:33 1 Trichlorofluorornethane ND 13 2.5 ug/Kg 11/16/1611:33 1 Vinyl chloride ND 13 2.5 ug/Kg 11/16116 11:33 1 Xylenes, Total ND 10 5.0 ug/Kg 11/16/16 11:33 1 p-Isopropyltoluene ND 5.0 2.5 ug/Kg 11/16/1611:33 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Toluene -d8 (Surr) 110 79-123 11116116 11:33 1 4-Bromofluorobenzene (Surr) 103 79-120 11116116 11:33 1 Dibromofluoromethane (Surr) 102 60-120 11116116 11:33 1 Method: 8015B - Diesel Range Organics(DRO)/Oil Range Organics (ORO) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac C13 -C22 100 4.9 2.5 mg/Kg 11/15/1616:37 11116/1603:35 1 C23-C40 25 4.9 2.5 mg/Kg 11/15/1616:37 11/16/1603:35 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac n-Octacosane 69 40-140 11115116 16:37 11116116 03:35 1 .. . ............ . ....... Client Sample ID: 4K-S-E-6' . ....... Lab Sample ID: 440-165703-22 Date Collected: 11/10/16 14:05 Matrix: Solid Date Received: 11/12/16 10:15 Method: 8260B - Volatile Organic Compounds (GC /MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/Kg 11/16/16 12:02 1 1,1,1-Trichloroethane ND 2.0 1.0 ug/Kg 11/16/1612:02 1 1, 1,2,2-Tetrachloroethane ND 2.0 1.0 ug/Kg 11/16/1612:02 1 1,1,2-Trichloroethane ND 2.0 1.0 ug/Kg 11/16/16 12:02 1 1,1-Dichloroethane ND 2.0 1.0 ug/Kg 11/16/1612:02 1 1,1-Dichloroethene ND 5.0 1.0 ug/Kg 11/16/1612:02 1 TestAmerica Irvine Page 44 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc Project/Site: Valero TestAmerica Job ID-. 440-165703-1 Client Sample ID: 4K-S-E-69 Lab Sample ID: 440-165703-22 Date Collected: 11/10/16 14:05 Matrix: Solid Date Received: 11/12/16 10:15 Method: 8260B - Volatile Organic Compounds (GC /MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1-Dichloropropene ND 2.0 1.0 ug/Kg 11/16/1612:02 1 ND 5.0 1.0 u g /K g 11/16/1612:02 1 1,2,3-Trichloropropane ND 10 1.0 ug/Kg 11/16/1612:02 1 1,2+Trichlorobenzene ND 5.0 1.0 ug/Kg 11/16/16 12:02 1 1,2,4-Trimethylbenzene ND 2.0 1.0 ug/Kg 11/16/16 12:02 1 1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 11/16/16 12:02 1 1,2-Dibromoethane (EDB) ND 2.0 1.0 ug/Kg 11/16/16 12:02 1 1,2-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/16/16 12:02 1 1,2-Dichloroethane ND 2.0 1.0 ug/Kg 11/16/16 12:02 1 1,2-Dichloropropane ND 2.0 1.0 ug/Kg 11/16/16 12:02 1 1,3,5-Trimethylbenzene ND 2.0 1.0 ug/Kg 11/16/1612:02 1 1,3-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/16/1612:02 1 1,3-Dichloropropane ND 2.0 1.0 ug/Kg 11/16/1612:02 1 1,4-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/16/16 12:02 1 2,2-Dichloropropane ND 2.0 1.0 ug/Kg 11/16/1612:02 1 2-Chlorotoluene ND 5.0 1.0 ug/Kg 11/16/16 12:02 1 4-Chlorotoluene ND 5.0 1.0 ug/Kg 11/16/16 12:02 1 Benzene ND 2.0 1.0 ug/Kg 11/16/1612:02 1 Bromobenzene ND 5.0 1.0 ug/Kg 11/16/1612:02 1 Bromochloromethane ND 5.0 1.0 ug/Kg 11/16/16 12:02 1 Bromodichloromethane ND 2.0 1.0 ug/Kg 11/16/1612:02 1 Bromoform ND 5.0 2.0 ug/Kg 11/16/1612:02 1 Bromomethane ND 5.0 1.0 ug/Kg 11/16/1612:02 1 Carbon tetrachloride ND 5.0 1.0 ug/Kg 11/16/16 12:02 1 Chlorobenzene ND 2.0 1.0 ug/Kg 11/16/16 12:02 1 Chloroethane ND 5.0 2.0 ug/Kg 11/16/1612:02 1 Chloroform ND 2.0 1.0 ug/Kg 11/16/1612:02 1 Chloromethane ND 5.0 1.0 ug/Kg 11/16116 12:02 1 cis-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 11/16/16 12:02 1 cis-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 11/16/16 12:02 1 Dibromochloromethane ND 2.0 1.0 ug/Kg 11/16/1612:02 1 Dibromomethane ND 2.0 1.0 ug/Kg 11/16/1612:02 1 Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 11/16/1612:02 1 Isopropyl Ether (DIPE) ND 5.0 1.0 ug/Kg 11/16/16 12:02 1 Ethanol ND 300 100 ug/Kg 11/16/1612:02 1 Ethyl-t-butyl ether (ETBE) ND 5.0 1.0 ug/Kg 11/16116 12:02 1 Ethylbenzene ND 2.0 1.0 ug/Kg .. .. . ....... 11/16/16 12:02 1 Hexachlorobutadiene ND 5.0 1.0 ug/Kg 11/16/16 12:02 1 lsopropylbenzene ND 2.0 1.0 ug/Kg 11/16/1612:02 1 m,p-Xyiene ND 4.0 2.0 ug/Kg 11/16/1612:02 1 Methylene Chloride ND 20 5.0 ug/Kg 11/16/16 12:02 1 Methyl-t-Butyl Ether (MTBE) ND 5.0 1.0 ug/Kg 11/16/16 12:02 1 Naphthalene ND 5.0 2.0 ug/Kg 11/16/1612:02 1 n-Butylbenzene ND 5.0 1.0 ug/Kg 11/16/16 12:02 1 N-Propylbenzene ND 2.0 1.0 ug/Kg 11/16/1612:02 1 o-Xylene ND 2.0 1.0 ug/Kg 11/16/1612:02 1 sec-Butylbenzene ND 5.0 1.0 ug/Kg 11/16/1612:02 1 Styrene ND 2.0 1.0 ug/Kg 11/16/16 12:02 1 Tert-amyl-methyl ether (TAME) ND 5.0 1.0 ug/Kg 11/16/16 12:02 1 TestAmerica Irvine Page 45 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440- 165703 -1 -- Project/Site: Valero -------- ---- ------ ---- --- ---- -- --- ---------------------------- - ------ -- - ------ - - - __ - - - -- -- ----------------------------------- - - - - -- - - - - -- - -- - -__ _ --------- - - - - -- _- Client Sample : - Lab Sample : 440-165703-22 Date Collected: 11/14/16 14:05 atria: Solid Date Received: 11/12/16 10 :15 Method: 82606 - Volatile Organic Compounds (GC /MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac tert -Butyl alcohol (TBA) ND 100 10 ug /Kg 11/16/16 12:02 1 tert- Butylbenzene ND 5.0 1.0 ug /Kg 11/16/1612:02 1 Tetrachloroethene ND 2.0 1.0 ug /Kg 11/16/1612:02 1 Toluene ND 2.0 1.0 ug /Kg 11/16/1612:02 1 trans -1,2- Dichloroethene ND 2.0 1.0 ug /Kg 11/16/16 12:02 1 trans -1,3- Dichloropropene ND 2.0 1.0 ug /Kg 11/16/1612:02 1 Trichooroethene ND 2.0 1.0 ug /Kg 11/16/1612:02 1 Trichlorofluoromethane ND 5.0 1.0 ug /Kg 11/16/1612:02 1 Vinyl chloride ND 5.0 1.0 ug /Kg 11/16/16 12:02 1 Xylenes, Total ND 4.0 2.0 ug /Kg 11/16/16 12:02 1 p- Isopropyltoluene ND 2.0 1.0 ug /Kg 11/16/1612:02 1 Surrogate %Recovery Qualifier Limits ug /Kg Prepared Analyzed Dil Fac Toluene -d8 (Surr) 108 79-123 4.8 ug /Kg 11/16/16 12 :02 1 4- Bromofluorobenzene (Surr) 101 79-120 9.5 4.8 11/16/16 12 :02 1 Dibromofluoromethane (Surr) 104 60-120 ND 24 11/16/16 12 :02 1 Method: 80158 - Diesel Range Organics(DRO) /Oil Range Organics (ORO) Analyte Result Qualifier C13 -C22 ND C23 -C40 ND Surrogate %Recovery Qualifier n- Octacosane 83 Client Sample ID: 4 -- -' Date Collected: 11/10/16 14 :07 Date Received: 11/12/16 10 :15 RL 5.0 5.0 Limits 40-140 MDL 2.5 2.5 Unit mg /Kg mg /Kg D Prepared Analyzed Dil Fac 11/15/1616:37 11/16/1601:06 1 11 /15/16 16:37 11116/16 01 :06 1 Prepared Analyzed Dil Fac 11/15/16 16 :37 11/16/16 01 :06 1 Lab Sample ID: 44- 155703 -23 atria: Solid Method: 82608 - Volatile Organic Compounds (GC /MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2- Tetrachloroethane ND 24 4.8 ug /Kg 11/16/16 12:32 1 1,1,1- Tdchloroethane ND 9.5 4.8 ug /Kg 11/16/1612:32 1 1,1,2,2- Tetrachloroethane ND 9.5 4.8 ug /Kg 11/16/1612:32 1 1,1,2- Trichooroethane ND 9.5 4.8 ug /Kg 11/16/1612:32 1 1,1- Dichloroethane ND 9.5 4.8 ug /Kg 11/16/1612:32 1 1,1- Dichloroethene ND 24 4.8 ug /Kg 11/16/1612:32 1 1,1- Dichloropropene ND 9.5 4.8 ug /Kg 11/16/1612:32 1 1,2,3- Trichlorobenzene ND 24 4.8 ug /Kg 11/16/1612:32 1 1,2,3- Trichloropropane ND 48 4.8 ug /Kg 11/16/16 12:32 1 1,2,4- Trichlorobenzene ND 24 4.8 ug /Kg 11/16/1612:32 1 1,2,4- Trimethylbenzene ND 9.5 4.8 ug /Kg 11/16/1612:32 1 1,2- Dibromo- 3- Chloropropane ND 24 9.5 ug /Kg 11/16/1612:32 1 1,2- Dibromoethane (EDB) ND 9.5 4.8 ug /Kg 11/16/16 12:32 1 1,2- Dichlorobenzene ND 9.5 4.8 ug /Kg 11/16/16 12:32 1 1,2- Dichloroethane ND 9.5 4.8 ug /Kg 11/16/16 12:32 1 1,2- Dichloropropane ND 9.5 4.8 ug /Kg 11/16/1612:32 1 1,3,5 - Trimethylbenzene ND 9.5 4.8 ug /Kg 11/16/1612:32 1 1,3- Dichlorobenzene ND 9.5 4.8 ug /Kg 11/16/1612:32 1 1,3- Dichloropropane ND 9.5 4.8 ug /Kg 11/16/1612:32 1 TestAmerica Irvine Page 46 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440 - 165703 -1 Project/Site: Valero __ - - -- - - - - - -- - - - -- -- - -- - - - - - - - -- --- - - - - -- ---- _--- _ ------------------- - -_ - _ _---- - - - - -- - __ _ _ -_- - - - - -- - - - -- -- _ Client Sample ID: 4 - _ -2' Lai Sample ID: 440-165703-23 Date Collected: 11/10/16 14 :07 atria: Solid Date Received: 11/12/16 10 :15 Method: 8260B - Volatile Organic Compounds (GC /IDES) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,4- Dichlorobenzene ND 9.5 4.8 ug /Kg 11/16/1612:32 1 2,2- Dichloropropane ND 9.5 4.8 ug /Kg 11/16/16 12:32 1 2- Chlorotoluene ND 24 4.8 ug /Kg 11/16/1612:32 1 4- Chlorotoluene ND 24 4.8 ug /Kg 11/16/1612:32 1 Benzene ND 9.5 4.8 ug /Kg 11/16/16 12:32 1 Bromobenzene ND 24 4.8 ug /Kg 11/16/1612:32 1 Bromochloromethane ND 24 4.8 ug /Kg 11/16/1612:32 1 Bromodichloromethane ND 9.5 4.8 ug /Kg 11/16/1612:32 1 Bromoform ND 24 9.5 ug /Kg 11/16/1612:32 1 Bromomethane ND 24 4.8 ug /Kg 11/16/1612:32 1 Carbon tetrachloride ND 24 4.8 ug /Kg 11/16/16 12:32 1 Chlorobenzene ND 9.5 4.8 ug /Kg 11/16/1612:32 1 Chloroethane ND 24 9.5 ug /Kg 11/16/16 12:32 1 Chloroform ND 9.5 4.8 ug /Kg 11/16/16 12:32 1 Chloromethane ND 24 4.8 ug /Kg 11/16/1612:32 1 cis -1,2- Dichloroethene ND 9.5 4.8 ug /Kg 11/16/16 12:32 1 cis -1,3- Dichloropropene ND 9.5 4.8 ug /Kg 11/16/1612:32 1 Dibromochloromethane ND 9.5 4.8 ug /Kg 11/16/1612:32 1 Dibromomethane ND 9.5 4.8 ug /Kg 11/16/1612:32 1 Dichlorodifluoromethane ND 24 9.5 ug /Kg 11/16/1612:32 1 Isopropyl Ether (DIPE) ND 24 4.8 u9/Kg 11/16/16 12:32 1 Ethanol ND 1400 480 ug /Kg 11/16/1612:32 1 Ethyl -t -butyl ether (ETBE) ND 24 4.8 ug /Kg 11/16/16 12:32 1 Ethylbenzene ND 9.5 4.8 ug /Kg 11/16/16 12:32 1 Hexachlorobutadiene ND 24 4.8 ug /Kg 11/16/1612:32 1 Isopropylbenzene ND 9.5 4.8 ug /Kg 11/16/16 12:32 1 m,p- Xylene ND 19 9.5 ug /Kg 11/16/1612:32 1 Methylene Chloride ND 95 24 ug /Kg 11/16/16 12:32 1 Methyl -t -Butyl Ether (MTBE) ND 24 4.8 ug /Kg 11/16/16 12:32 1 Naphthalene ND 24 9.5 ug /Kg 11/16/1612:32 1 n- Butylbenzene ND 24 4.8 ug /Kg 11/16/1612:32 1 N- Propylbenzene ND 9.5 4.8 ug /Kg 11/16/16 12:32 1 o- Xylene ND 9.5 4.8 ug /Kg 11/16/16 12:32 1 sec - Butylbenzene ND 24 4.8 ug /Kg 11/16/1612:32 1 Styrene ND 9.5 4.8 ug /Kg 11/16/1612:32 1 Tert- amyl - methyl ether (TAME) ND 24 4.8 ug /Kg 11/16/16 12:32 1 tert -Butyl alcohol (TBA) ND 480 48 ug /Kg 11/16/16 12:32 1 tert- Butylbenzene ND 24 4.8 ug /Kg 11/16/1612:32 1 Tetrachloroethene ND 9.5 4.8 ug /Kg 11/16/1612:32 1 Toluene ND 9.5 4.8 ug /Kg 11/16/1612:32 1 trans- 1,2- Dichloroethene ND 9.5 4.8 ug /Kg 11/16/16 12:32 1 trans- 1,3- Dichloropropene ND 9.5 4.8 ug /Kg 11/16/1612:32 1 Trichloroethene ND 9.5 4.8 ug /Kg 11/16/16 12:32 1 Trichlorofluoromethane ND 24 4.8 ug /Kg 11/16/1612:32 1 Vinyl chloride ND 24 4.8 ug /Kg 11/16/16 12:32 1 Xylenes, Total ND 19 9.5 ug /Kg 11/16/16 12:32 1 p- Isopropyltoluene ND 9.5 4.8 ug /Kg 11/16/1612:32 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Toluene -d8 (Surr) 119 79-123 1 9/96/16 12 :32 1 TestAmerica Irvine Page 47 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc Project/Site: Valero Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Surrogate %Recovery Qualifier Limits 4-Bromofluoroberizene (Surd 117 79-120 Dibromofluoromethane (Surr) 100 60-120 Method: 8015B - Diesel Range Organ ics(D RO)/Oi I Range Organics (ORO) Analyte Result Qualifier RL MDL Unit C13 -C22 1500 99 50 mg/Kg C23-C40 220 99 50 mg/Kg Surrogate %Recovery Qualifier Limits n-Octacosane 81 40-140 Client Sample ID: 4K-S-w- Date Collected: 11/10/16 14:10 Date Received: 11/12116 10:15 1 Method: 82608 - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/Kg 1,1,1-Trichloroethane ND 2.0 1.0 ug/Kg 1, 1,2,2-Tetrachloroethane ND 2.0 1.0 ug/Kg 1, 1,2-Trichloroethane ND 2.0 1.0 ug/Kg 1,1-Dichloroethane ND 2.0 1.0 ug/Kg 1,1-Dichloroethene ND 5.0 1.0 ug/Kg 1,1-Dichloropropene ND 2.0 1.0 ug/Kg 1,2,3-Trichlorobenzene ND 5.0 1.0 ug/Kg 1,2,3-Trichloropropane ND 10 1.0 ug/Kg I 44-Trichlorobenzene ND 5.0 1.0 ug/Kg 1,2,4-Trimethylbenzene ND 2.0 1.0 ug/Kg 1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 1,2-Dibromoethane (Mbj t4b 2.0 1.0 ug/Kg 1,2-Dichlorobenzene ND 2.0 1.0 ug/Kg 1,2-Dichloroethane ND 2.0 1.0 ug/Kg 1,2-Dichloropropane ND 2.0 1.0 ug/Kg 1,3,5-Trimethylbenzene ND 2.0 1.0 ug/Kg 1,3-Dichlorobenzene ND 2.0 1.0 ug/Kg 1,3-Dichloropropane ND 2.0 1.0 ug/Kg 1,4-Dichlorobenzene ND 2.0 1.0 ug/Kg 2,2-Dichloropropane ND 2.0 1.0 ug/Kg 2-thlorotoluene ND 5.0 1.0 ug/Kg 4-Chlorotoluene ND 5.0 1.0 ug/Kg Benzene ND 2.0 1.0 ug/Kg Bromobenzene ND 5.0 1.0 ug/Kg Bromochloromethane ND 5.0 1.0 ug/Kg Bromodichloromethane ND 2.0 1.0 ug/Kg Bromoform ND 5.0 2.0 ug/Kg Bromomethane ND 5.0 1.0 ug/Kg Carbon tetrachloride ND 5.0 1.0 ug/Kg Chlorobenzene ND 2.0 1.0 ug/Kg Chloroethane ND 5.0 2.0 ug/Kg Chloroform ND 2.0 1.0 ug/Kg TestAmerica Job ID: 440-165703-1 Lab Sample ID: 440-165703-23 Matrix: Solid Prepared Analyzed DR Fac 11116116 12:32 1 11116116 12:32 1 D Prepared Analyzed Dil Fac 11/15/1616:37 11/17/1601:20 20 11/15/1616:37 11/17/1601:20 20 Prepared Analyzed DR Fac 11115116 16:37 11117116 01:20 26 Lab Sample ID: 440-165703-24 w Prepared Analyzed Dil Fac 11/16/16 10:04 1 11/16/16 10:04 1 11/16116 10:04 1 11 /16/16 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16116 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16116 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16116 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 11/16/16 10:04 1 TestAmerica Irvine Page 48 of 87 11/23/2016 Client Sample Results Client: Advanced Environmental Concepts Inc Project/Site: Valero TestAmerica Job ID: 440-165703-1 Client Sample ID: 4K-S-W-6' Lab Sample ID: 440-165703-24 Date Collected: 11/10/16 14:10 Matrix: Solid Date Received: 11/12/16 10:15 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloromethane ND 5.0 1.0 ug/Kg 11/16/1610:04 1 cis-1,2-Dich loroet I hene ND ..... 2.0 1.0 u I g /Kg . ....... 11/16M 16:64 1 cis-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 11/16/1610:04 1 Dibromochloromethane ND 2.0 1.0 ug/Kg 11/16/1610:04 1 Dibromomethane ND 2.0 1.0 ug/Kg 11/16/1610:04 1 Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 11/16/1610:04 1 Isopropyl Ether (blPE) ND 5.0 1.0 ug/Kg 11/16/16 10:04 1 Ethanol ND 300 100 ug/Kg 11/16/16 10:04 1 Ethyl-t-butyl ether (ETBE) ND 5.0 1.0 ug/Kg 11/16/16 10:04 1 Ethylbenzene ND 2.0 1.0 ug/Kg 11/16/1610:04 1 Hexachlorobutadiene ND F1 5.0 1.0 ug/Kg 11/16/1610:04 1 lsopropylbenzene ND 2.0 1.0 ug/Kg 11/16/1610:04 1 m,p-Xylene ND 4.0 2.0 ug/Kg 11/16/1610:04 1 Methylene Chloride ND 20 5.0 ug/Kg 11/16/16 10:04 1 Methyl-t-Butyl Ether (MTBE) ND 5.0 1.0 ug/Kg 11/16/16 10:04 1 Naphthalene ND 5.0 2.0 ug/Kg 11/16/1610:04 1 n-Butylbenzene ND 5.0 1.0 ug/Kg 11/16/1610:04 1 N-Propylbenzene ND 2.0 1.0 ug/Kg 11/16/16 10:04 1 O-Xylene ND 2.0 1.0 ug/Kg 11%16/1610:04 1 sec-Butylbenzene ND 5.0 1.0 ug/Kg 11/16/1610:04 1 Styrene ND 2.0 1.0 ug/Kg 11/16/1610:04 1 Tert-amyl-methyl ether (TAME) ND 5.0 1.0 ug/Kg 11/16/16 10:04 1 tert-Butyl alcohol (TBA) ND 100 10 ug/Kg 11/16/16 10:04 1 tert-Butylbenzene ND 5.0 1.0 ug/Kg 11/16/1610:04 1 Tetrachloroethene ND 2.0 1.0 ug/Kg 11 /16/16 10:04 1 Toluene ND 2.0 1.0 ug/Kg 11/16/16 10:04 1 trans-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 11/16/1610:04 1 trans-1,3-bichloropropene ND 2.0 1.0 ug/Kg 11/16/1610:04 1 Trichloroethene ND 2.0 1.0 ug/Kg 11/16/1610:04 1 Trichlorofluoromethane ND 5.0 1.0 ug/Kg 11/16/1610:04 1 Vinyl chloride ND 5.0 1.0 ug/Kg 11/16/16 10:04 1 Xylenes, Total ND 4.0 2.0 ug/Kg 11/16/16 10:04 1 p-lsopropyltoluene ND 2.0 1.0 ug/Kg 11/16/1610:04 1 Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene (Surr) Dibromofluoromethane (Surr) %Recovery Qualifier Limits 114 79-123 109 79-120 101 60-120 Method: 8015B - Diesel Range Organics(DRO)/Oil Range Organics (ORO) Analyte Result Qualifier RL MDL Unit C13 -C22 240 4.9 2.5 mg/Kg C23-C40 64 4.9 2.5 mg/Kg Surrogate %Recovery Qualifier Limits n-Octacosane 90 40-140 Prepared Analyzed Dil Fac 11116116 10:04 1 11116116 10:04 1 11116116 10:04 1 D Prepared Analyzed Dil Fac 11/15/1616:37 11/16/1607:51 1 11/15/1616:37 11/16/1607:51 1 Prepared Analyzed Dil Fac 11115116 16:37 11116116 07:51 1 TestAmerica Irvine Page 49 of 87 11/23/2016 Method Summary Client: Advanced Environmental Concepts Inc Project/Site: Valero TestAmerica Job ID: 440 - 165703 -1 Method Method Description Protocol Laboratory 8260B Volatile Organic Compounds (GC /MS) SW846 TAL IRV 8260B /CA_LUFTN Volatile Organic Compounds by GC /MS SW846 TAL IRV S 8015B Diesel Range Organics(DRO) /Oil Range Organics (ORO) SW846 TAL IRV 6020 Metals (ICP /MS) SW846 TAL IRV Protocol References: SW846 ='Test Methods For Evaluating Solid Waste, Physical /Chemical Methods ", Third Edition, November 1986 And Its Updates. Laboratory References: TAL IRV = TestAmerica Irvine, 17461 Derian Ave, Suite 100, Irvine, CA 92614 -5817, TEL (949)261 -1022 TestAmerica Irvine Page 50 of 87 11/23/2016 Lab Chronicle Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440 - 165703 -1 Project/Site: Valero -- ....._......._.._._...__ __ _ ._---. .____.__......_.....�...__.____ _...__ .__.__......... _ ........- ....... .. _ _.._._ ........................_ Client e ID: _2 _. --____._.................... _....______..._._.._...._....__ . __............................ ___ _...._._. _._._._. -_ - -- --_._ .......... .._._— _____..._.__...-- __ ........... _ Lab Sample : 440-165703-1 Date Collected: 11/10/16 10:15 atria: Solid Date Received: 11/12/16 10:15 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total /NA Analysis 82608 1 2.02 g 10 mL 369133 11/15/16 18:49 ATL TAL IRV Total /NA Prep 3546 15.17 g 1.0 mL 369289 11/15/16 16:37 AP TAL IRV Total /NA Analysis 8015B 20 369684 11/16/1623:56 LMB TAL IRV Client Sample : - - -5' Lab Sample ID: 440-165703-2 13 Date Collected: 11/10/1 10:25 atria: Solid Date Received: 11/12/16 10:15 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total /NA Analysis 8260B 1 2.02 g 10 mL 369451 11/16/16 09:34 ATL TAL IRV Total /NA Prep 3546 15.11 g 1.0 mL 369289 11/15/16 16:37 AP TAL IRV -. Total /NA Analysis 8015B 10 369684 11/17/1600:38 LMB TAL IRV ..................... Lab Sample III: 0- 155703 -3 _ Client Sample III: a -E -2g Crate Collected: 11/10/16 10:30 Matrix: Solid Date Received: 11/12/16 10:15 ............................................................................................................................................................................................................................................................................................................................................................... ............................... Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total /NA Analysis 82606 1 2 g 10 mL 369451 11/16/16 12:12 ATL TAL IRV Total /NA Prep 3546 15.20 g 1.0 mL 369289 11/15/16 16:37 AP TAL IRV Total /NA Analysis 8015B 20 369684 11/17/1600:59 LMB TAL IRV .............................................................................................. ............................... .................................................................................................................................................................................................................................. Client Sample ID: 4K-N-E-6 ............................... Lab Sample ID: 440- 155703 -4 Date Collected: 11/10/16 10 :35 atria: Solid Date Deceived: 11/12/16 10:15 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total /NA Analysis 8260B 1 5.02 g 10 mL 369133 11115/1609:26 ATL TAL IRV Total /NA Prep 3546 15.05 g 1.0 mL 369289 11/15/16 16:37 AP TAL IRV Total /NA Analysis 8015B 1 369368 11116/16 01:48 AMH TAL IRV ---- - ------ -- -- -- ----- - - - - - -_ - -- Client Sample ID: 7K-W-2' - -- -- - - -- Lab Sample IC: 440- 155703 -5 Date Collected: 11/10/16 10:50 Matrix: Solid Crate Received: 11/12/16 10 :15 ........................................................................................................................................................................................................................................................................................................................................................................................ ............................... . .................................................................................................................. ............................... Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total /NA Analysis 82606 1 5.02 g 10 mL 369133 11/15/16 10:44 ATL TAL IRV Total /NA Analysis 8260B /CA_LUFTU 1 5 g 10 mL 369459 11116/16 13:02 ATL TAL IRV S Total /NA Prep 30506 2.02 g 50 mL 369278 11/15/16 12 :27 DT TAL IRV Total /NA Analysis 6020 20 369659 11/16/16 14:26 MQP TAL IRV TestAmerica Irvine Page 51 of 87 11/23/2016 Client: Advanced Environmental Concepts Inc Project/Site: Valero W : r • Date Collected: 11110116 # Date Received: a # a # Lab Chronicle Batch Batch Prep Type Type Method Run Total /NA Analysis 82606 Total /NA Analysis 8260B/CA LUFTN Batch Factor S Total /NA Prep 3050B Total /NA Analysis 6020 a # Lab Chronicle Batch Batch Pre p Type pe Type Method Run Total /NA Analysis 60B Total /NA Analysis 8260B /CA LUFTN Batch Factor S Total /NA Prep 3050B Total /NA Analysis .6020 a # Lab Chronicle Initial Final Dil Initial Final TestAmerica Job ID: 440- 165703 -1........... ........................... ...................................... ....................... ............... ...._ .................. ................._..- l...al�...a 440- Batch Batch Factor Matrix: Solid Amount Number Analyzed Analyst Dil Initial Final Batch Prepared Factor Amount Amount Number or Analyzed Analyst Lab 1 9 10 L 369133 11/15/16 11:11 ATL TAL IRV 1 5.01 g 10 mL 369459 11/16/16 13:32 ATL TAL IRV 10 mL 2.02 g 50 mL 369278 11/15/16 12:27 DT TAL IRV TAL IRV Total /NA Analysis 369659 11/16/16 14:35 MQ P TAL IRV 13 1 20 Lab Sample ID: 440-16 703 -7 2.03 g 50 mL Matrix: Solid .................... Dil Initial Final Batch Prepared Factor Amount Amount Number or Analyzed Analyst Lab 1 -' 5.05 g 10 mL 369133 11/15/1611 :37 ATL TAL IRV 1 5.04 g 10 mL 369459 11116/16 14:01 ATL TAL IRV 20 2.03 g 50 mL 369278 11/15/16 12:27 DT TAL IRV 369659 11/16/16 14:46 MQP TAL IRV 20 i L-ab Sample ID: Solid Client Sample : D-4-2' Date Collected: 11/10/"16 1 :53 Date Deceived: 11/12116 10 :15 Batch Batch Prep Type Type Method Run Y Total /NA Analysis 8260B Total /NA Prep 3050B Total /NA Analysis 6020 Client Sample : D- 44 Date Collected: 11/10/16 12 :05 Date Deceived: 11/12116 10 :15 Batch Batch Prep Type Type Method Total /NA Analysis 8260B Lab Sample ID: 440-165703-9 Solid Dill Initial Final Dil Initial Final Batch Prepare Amount Amount Number Batch Batch Factor Amount Amount Number Analyzed Analyst La Prep Pre Type Type Method Run 1 5. 205. g 10 mL 369133 11/15/16 12.03 l/ ATL TAL IRV Total /NA Analysis 8260B MQP TAL IRV 10 mL 369459 11/16/16 14:31 ATL TAL IRV Total /NA Analysis 82606 /CA_LUFTN 1 5.04 g S 2.03 g 50 mL 369278 11/15/1612:27 DT TAL IRV :Total /NA Prep 30506 369659 11/16/1615:32 MQP TAL IRV Total /NA Analysis 6020 20 Client Sample : D-4-2' Date Collected: 11/10/"16 1 :53 Date Deceived: 11/12116 10 :15 Batch Batch Prep Type Type Method Run Y Total /NA Analysis 8260B Total /NA Prep 3050B Total /NA Analysis 6020 Client Sample : D- 44 Date Collected: 11/10/16 12 :05 Date Deceived: 11/12116 10 :15 Batch Batch Prep Type Type Method Total /NA Analysis 8260B Lab Sample ID: 440-165703-9 Solid Dill Initial Final Batch Prepared Factor Amount Amount Number or Analyzed Analyst Lab 1 5.04 g 10 mL 369133 11/15/16 12:30 ATL TAL IRV 2.04 g 50 mL 369278 11/15116 15:08 DT TAL IRV 369659 11/16/16 15:34 MQP TAL IRV 20 Lab Sample ID: 440-165703-17f * • Dil Initial Final Batch Prepared Run Factor Amount Amount Number or Analyzed Analyst Lab 1 5. g 10 mL 369133 11/15/16 12:56 ATL TAL IRV TestAmerica Irvine Page 52 of 87 11/23/2016 Lab Chronicle Client: Advanced Environmental Concepts Inc Initial Final Batch TestAmerica Job ID: 440 - 165703 -1 Project/Site: Valero Factor Amount Amount ........................................................ ..............................a .................................................................................................................................................................................. Client le m -- or Analyzed ............................... ................................. ............................................................................................ ............................... ............................... . Lab Sample m - 165703.1 Date Collected: 11/10/16 12:05 10 mL 369133 11/15/16 17:04 Matrix: Solid Date Deceived: 11/12/16 10:15 1 5.04 g 10 mL k 11/16/16 15:01 ATL TAL IRV 2.03 g Batch Batch Dil Initial Final Batch Prepared ='.. Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total /NA Prep 3050B TAL IRV 2.02 g 50 mL 370377 11/19/1612:00 DT TAL IRV Total /NA Analysis 6020 20 371024 11/22/16 13:43 EN TAL IRV ___.- ._.__._ __..._ _ _.._.------ ..__._.__...__. _ .__.__ ........_._. Client Sample D-1 -2' — .......... _._......_ �... Lab Sample : 440-165703-11 Matrix: Solid Date Collected: 11/10/16 13:10 Date Deceived: 11/12/16 10 :1 :M: Batch Batch Dil Initial Final Batch Prepared i Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 82606 1 5.01 g 10 mL 369133 11/15/16 13:22 ATL TAL IRV Total/NA Prep 3546 15.18 g 2.0 mL 369289 11/15/16 16:37 AP TAL IRV Total/NA Analysis 80156 1 369368 11/16116 04:17 AMH TAL IRV Client Sample I -1 -6° Lab Sample ID: 440-165703-12 Date Collected: 11/10/16 13:15 Matrix: Solid Date Deceived: 11/12/16 10:15 Batch Batch Dil In Final Batch Prepared im Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total /NA Analysis 82606 1 5.03 g 10 mL 369133 11/15/161 6:38 ATL TAL IRV Total /NA Prep 3546 15.18 g 2.0 mL 369289 11/15/16 16:37 AP TAL IRV Total /NA Analysis 8015E 1 369368 11/16/1605:00 AMH TAL IRV Client Sample ID: D -2 -2' Date Collected: 11/10/16 13:20 Date Deceived: 11/12/16 10:15 ........................... ............................... .......................................................................................................................................................... Batch Batch Prep Type Type Method Run Total /NA Analysis 8260B Total /NA Analysis 8260B /CA LUFTN S Total /NA Prep 3050B Total/NA Analysis 6020 Client Sample ID: -2 -6° Date Collected: 11/10/16 13:25 Date Deceived: 11/12/16 10:15 Batch Batch Prep Type Type Method Run Total/NA Analysis 8260B Total /NA Analysis 8260B /CA_LUFTN S Total /NA Prep 3050B Total /NA Analysis 6020 Lab Sample Matrix S r r Dil Initial Final Batch Prepared Factor Amount Amount Number or Analyzed Analyst Lab 1 5.02 g 10 mL 369133 11/15/16 17:04 ATL TAL IRV 1 5.04 g 10 mL 369459 11/16/16 15:01 ATL TAL IRV 2.03 g 50 mL 369278 11/15/16 12:27 DT TAL IRV 20 369659 11/16/16 15:10 MOP TAL IRV Lab Sample ID: 440-165703-14 17. Dil Initial Final Batch Prepared Factor Amount Amount Number or Analyzed Analyst Lab 1 4.98 g 10 mL 369133 11/15/16 17:30 ATL TAL IRV 1 5 g 10 mL 369459 11/16/16 15:30 ATL TAL IRV 2.00 g 50 mL 369278 11/15/16 12:27 DT TAL IRV 20 369659 11/16/16 15:13 MOP TAL IRV Page 53 of 87 TestAmerica Irvine 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc Project/Site: Valero TestAmerica Job ID: 440-165703-1 Lab Sample ID: MB 440-369133/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 369133 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/Kg 11/15/16 08:33 1 1, 1, 1 -Trichloroethane ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 1, 1,2,2-Tetrachloroethane ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 1, 1,2-Trichloroethane ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 1,1-Dichloroethane ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 1,1-Dichloroethene ND 5.0 1.0 ug/Kg 11/15/16 08:33 1 1,1-Dichloropropene ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 1,2,3-Trichlorobenzene ND 5.0 1.0 ug/Kg 11/15/16 08:33 1 1,2,3-Trichloropropane ND 10 1.0 ug/Kg 11/15/16 08:33 1 1,2,4-Trichlorobenzene .. ND .... .. .. 5.0 1.0 ug/Kg 11/15/16 08:33 1 1,2,4-Trimethylbenzene ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 11/15/16 08:33 1 1,2-Dibromoethane (EDB) ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 1,2-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 1,2-Dichloroethane ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 1,2-Dichloropropane ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 1,3,5-Trimethylbenzene ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 1,3-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 1,3-Dichloropro I pane ND 2.0 1.0 ug/Kg 11/15116 08:33 1 1,4-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 2,2-Dichloropropane ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 2-Chlorotoluene ND 5.0 1.0 ug/Kg 11/15/16 08:33 1 4-Chlorotoluene ND 5.0 1.0 ug/Kg 11/15/16 08:33 1 Benzene ND 2.0 1.0 ug/Kg 11/15116 08:33 1 Bromobenzene ND 5.0 1.0 ug/Kg 11/15/16 08:33 1 Bromochloromethane ND 5.0 1.0 ug/Kg 11/15/16 08:33 1 Bromodichloromethane ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 Bromoform ND 5.0 2.0 ug/Kg 11115/16 08:33 1 Bromomethane ND 5.0 1.0 ug/Kg 11/15/16 08:33 1 Carbon tetrachloride ND 5.0 1.0 ug/Kg 11/15/16 08:33 1 Chlorobenzene ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 Chloroethane ND 5.0 2.0 ug/Kg 11/15/16 08:33 1 Chloroform ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 Chloromethane ND 5.0 1.0 ug/Kg 11/15/16 08:33 1 cis-1,2-Dichloroethene ND 2.0 1.0 uglKg 11/15/16 08:33 1 cis-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 Dibromochloromethane ND 2.0 1.0 ug/Kg 11115/16 08:33 1 Dibromomethane ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 11/15/16 08:33 1 lsopropyl Ether (DIPE) ND D 5.6 1.0 *ug*/Kg 11/15/16 08:33 1 Ethanol ND 300 100 ug/Kg 11/15/16 08:33 1 Ethyl-t-butyl ether (ETBE) ND 5.0 1.0 ug/Kg 11/15/16 08:33 1 Ethylbenzene ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 Hexachlorobutadiene ND 5.0 1.0 ug/Kg 11/15/16 08:33 1 lsopropylbenzene ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 m,p-Xylene ND 4.0 2.0 ug/Kg 11/15/16 08:33 1 Methylene Chloride ND 20 5.0 ug/Kg 11/15/16 08:33 1 Methyl-t-Butyl Ether (MTBE) ND 5.0 1.0 ug/Kg 11/15/16 08:33 1 TestAmerica Irvine Page 57 of 87 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc Project/Site- Valero TestAmerica Job ID: 440-165703-1 Lab Sample ID: MB 440-369133/4 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 369133 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Naphthalene ND 5.0 2.0 ug/Kg 11/15/16 08:33 1 n-Butylbenzene ND 5.0 1.0 ug/Kg 11/15/16 06M 1 N-Propylbenzene ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 o-Xylene ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 sec-Butylbenzene ND 5.0 1.0 ug/Kg 11/15/16 08:33 1 Styrene ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 Tert-amyl-methyl ether (TAME) ND 5.0 1.0 ug/Kg 11/15/16 08:33 1 tert-Butyl alcohol (TBA) ND 100 10 ug/Kg 11/15/16 08.33 1 tert-Butylbenzene ND 5.0 1.0 ug/Kg 11/15/16 08:33 1 Tetrachloroethene ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 Toluene ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 trans-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 11/15116 08:33 1 trans-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 Trichloroethene ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 Trichlorofluoromethane ND 5.0 1.0 ug/Kg 11/15/16 08:33 1 Vinyl chloride ND 5.0 1.0 ug/Kg 11/15/16 08:33 1 Xylenes, Total ND 4.0 2.0 ug/Kg 11/15/16 08:33 1 p4sopropyltoluene ND 2.0 1.0 ug/Kg 11/15/16 08:33 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed DR Fac Toluene-d8 (Surr) 107 79-123 11115116 08:33 1 4-Bromofluoroberizene (Surr) 95 79-120 11115116 08:33 1 Dibromofluoromethane (Surr) 101 60-120 11115116 08:33 1 Lab Sample ID: LCS 440-369133/5 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 369133 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits 1,1,1,2-Tetrachloroethane 50.0 51.5 ug/Kg 103 70-130 1,1,1-Trichloroethane 50.0 52.0 ug/Kg 104 65-135 1,1,2,2-Tetrachloroethane 50.0 55.9 ug/Kg 112 55-140 1, 1,2-Trichloroethane 50.0 56.6 ug/Kg 113 65-135 1,1-Dichloroethane 50.0 52.0 ug/Kg 104 70-130 1,1-Dichloroethene 50.0 50.1 ug/Kg 100 70-125 1,1-Dichloropropene 50.0 51.3 ug/Kg 103 70-130 1,2,3-Trichlorobenzene 50.0 54.1 ug/Kg 108 60-130 1,2,3-Trichloropropane 50.0 54.2 ug/Kg 108 60-135 1,2,4-Trichlorobenzen , e 50.0 53.8 ug/Kg 108 70-135 1,2,4-Trimethylbenzene 50.0 49.7 ug/Kg 99 70-125 1,2-Dibromo-3-Chloropropane 50.0 59.6 ug/Kg 119 50-135 1 2-bibromoethane (EDB) 50.0 58.0 ug/Kg 116 70-130 1,2-Dichlorobenzene 50.0 51.8 ug/Kg 104 75-120 1,2-Dichloroethane 50.0 57.3 ug/Kg 115 60-140 1,2-Dichloropropane 50.0 54.6 ug/Kg 109 70-130 1,3,5-Trimethylbenzene 50.0 51.2 ug/Kg 102 70-125 1,3-Dichlorobenzene 50.0 50.6 ug/Kg 101 75-125 1,3-Dichloropropane 50.0 53.3 ug/Kg 107 70-125 TestAmerica Irvine Page 58 of 87 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440- 165703 -1 Project/Site: Valero .►, Lab Sample ID: LCS 440 - 369133/5 Client Sample 1D: Lab Control Sample Matrix: Solid Prep Type: Total /NA Analysis Batch: 369133 TestAmerica Irvine Page 59 of 87 11/23/2016 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits 1,4- Dichlorobenzene 50.0 50.1 ug /Kg 100 75-120 2,2- Dichloropropane 50.0 55.6 ug /Kg 111 60-145 2- Chlorotoluene 50.0 49.4 ug /Kg 99 70-125 4- Chlorotoluene 50.0 49.6 ug /Kg 99 75-125 Benzene 50.0 51.3 ug /Kg 103 65-120 Bromobenzene 50.0 49.8 ug /Kg 100 75-120 Bromochloromethane 50.0 54.6 ug /Kg 109 70-135 Bromodichloromethane 50.0 56.5 ug /Kg 113 70-135 Bromoform 50.0 57.1 ug /Kg 114 55-135 Bromomethane 50.0 55.2 ug /Kg 110 60-145 Carbon tetrachloride 50.0 53.2 ug /Kg 106 65-140 Chlorobenzene 50.0 51.9 ug /Kg 104 75-120 Chloroethane 50.0 53.3 ug /Kg 107 60-140 Chloroform 50.0 55.6 ug /Kg 111 70-130 Chloromethane 50.0 52.3 ug /Kg 105 45-145 cis -1,2- Dichloroethene 50.0 53.2 ug /Kg 106 70-125 cis -1,3- Dichloropropene 50.0 55.9 ug /Kg 112 75-125 Dibromochloromethane 50.0 53.2 ug /Kg 106 65 _ 140 Dibromomethane 50.0 57.4 ug /Kg 115 70-130 Dichlorodifluoromethane 50.0 50.7 ug /Kg 101 35-160 Isopropyl Ether (DIPE) 50.0 59.0 ug /Kg 118 60-140 Ethanol 2000 2180 ug /Kg 109 35-160 Ethyl -t -butyl ether (ETBE) 50.0 55.3 ug /Kg 111 60-140 Ethylbenzene 50.0 50.4 ug /Kg 101 70-125 Hexachlorobutadiene 50.0 51.2 ug /Kg 102 60-135 Isopropylbenzene 50.0 51.6 ug /Kg 103 75-130 m,p- Xylene 50.0 52.2 ug /Kg 104 70 -125 Methylene Chloride 50.0 52.9 ug /Kg 106 55-135 Methyl -t -Butyl Ether (MTBE) 50.0 55.5 ug /Kg 111 60.140 Naphthalene 50.0 55.4 ug /Kg 111 66-135 n- Butylbenzene 50.0 52.1 ug /Kg 104 70-130 N- Propylbenzene 50.0 51.0 ug /Kg 102 70-130 o- Xylene 50.0 49.1 ug /Kg 98 70-125 sec - Butylbenzene 50.0 50.8 ug /Kg 102 70-125 Styrene 50.0 49.3 ug /Kg 99 75-130 Tert- amyl - methyl ether (TAME) 50.0 54.1 ug /Kg 108 60-145 tert-Butyl alcohol (TBA) 500 547 ug /Kg 109 70-135 tert- Butylbenzene 50.0 49.7 ug /Kg 99 70-125 Tetrachloroethene 50.0 51.1 ug /Kg 102 70-125 Toluene 50.0 49.7 ug /Kg 99 70-125 trans- 1,2- Dichloroethene 50.0 53.5 ug /Kg 107 70-125 trans -1,3- Dichloropropene 50.0 53.4 ug /Kg 107 70-135 Trichloroethene 50.0 51.3 ug /Kg 103 70-125 Trichlorofluoromethane 50.0 51.2 ug /Kg 102 60-145 Vinyl chloride 50.0 59.3 ug /Kg 119 55-135 p- Isopropyltoluene 50.0 50.3 ug /Kg 101 75-125 TestAmerica Irvine Page 59 of 87 11/23/2016 Client: Advanced Environmental Concepts Inc Project/Site: Valero !!111111111151 1!,11 J�lil 11 Lab Sample ID: LCS 440-369133/5 Matrix: Solid Analysis Batch: 369133 Surrogate Toluene-d8 (Surr) 4-Bromofluorobenzene (Surr) Dibromofluoromethane (Surr) QC Sample Results LCS LCS Sample Sample %Recovery Qualifier Limits 100 79-123 92 79-120 104 60-120 Lab Sample ID: 440-165703-4 MS Matrix: Solid Analysis Batch: 369133 TestAmerica Job ID: 440-165703-1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Client Sample ID: 4K-N-E-61 Prep Type: Total/NA TestAmerica Irvine Page 60 of 87 11/23/2016 Sample Sample Spike MS MS %Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits 1, 1, 1,2-Tetrachloroethane ND 49.7 52.4 ug/Kg 106 65-145 1, 1, 1 -Trichloroethane ND 49.7 52.6 ug/Kg 106 65-145 1, 1,2,2-Tetrachloroethane ND 49.7 57.8 ug/Kg 116 40-160 1, 1,2-Trichloroethane ND 49.7 58.1 ug/Kg 117 65-140 1,1-Dichloroethane ND 49.7 52.1 ug/Kg 105 65-135 1,1-Dichloroethene ND 49.7 48.7 ug/Kg 98 65-135 1,1-Dichloropropene ND 49. . 7 5 1 1.4 . ug /Kg 103 65 . -135 1,2,3-Trichlorobenzene ND 49.7 45.3 ug/Kg 91 45-145 1,2,3-Trichloropropane ND 49.7 57.4 ug/Kg 115 50-150 I 44-Trichlorobenzene ND 49.7 47. . 6 ug . /K . g 96 5 . 0 140 1,2,4-Trimethylbenzene 1.3 J 49.7 51.7 ug/Kg 101 65-140 1,2-Dibromo-3-Chloropropane ND 49.7 60.2 ug/Kg 121 40-150 1,2-Dibromoethane (EDB) ND 49.7 57.8 ug/Kg 116 65-140 1,2-Dichlorobenzene ND 49.7 51.1 ug/Kg 103 70-130 1,2-Dichloroethane ND 49.7 55.1 ug/Kg 111 60-150 1,2-Dichloropropane ND 49.7 53.8 u . g I /Kg 10 1 8 65 130 1,3,5-Trimethylbenzene ND 49.7 51.7 ug/Kg 104 65-135 1,3-Dichlorobenzene ND 49.7 51.3 ug/Kg 103 70-130 1,3-bichioropropane ND 49.7 54.0 ug/Kg 109 6 . 5 140 1,4-Dichlorobenzene ND 49.7 51.6 ug/Kg 104 70-130 2,2-Dichloropropane ND 49.7 57.2 ug/Kg 115 65-150 2-Chlorotoluene ND 49.7 52.6 ug/Kg 106 60-135 4-Chlorotoluene ND 49.7 53.3 ug/Kg 107 65-135 Benzene ND 49.7 50.3 ug/Kg 101 65-130 Bromobenzene ND 49.7 52.7 ug/Kg 106 65-140 Bromochloromethane ND 49.7 52.9 ug/Kg 106 65-145 Bromodichloromethane ND 49.7 52.8 ug/Kg 106 65-145 Bromoforrn ND 49.7 54.5 ug/Kg 110 50-145 Bromomethane ND 49.7 53.0 ug/Kg 107 60-155 Carbon tetrachloride ND 49.7 52.5 ug/Kg 106 60-145 Chiorobenzene ND 49. . 7 . 52.4 u . g . /Kg 105 70 130 Chloroethane ND 49.7 51.0 ug/Kg 103 60-150 Chloroform ND 49.7 54.0 ug/Kg 109 65-135 Chloromethane ND 49.7 51.9 ug/Kg 104 40-145 cis-1,2-Dichloroethene ND 49.7 53.0 ug/Kg 107 65-135 cis-1,3-Dichloropropene ND 49.7 55.7 ug/Kg 112 70-135 Dibromochloromethane ND 49.7 52.7 ug/Kg 106 60-145 Dibromomethane ND 49.7 54.8 ug/Kg 110 65-140 Dichlorodifluoromethane ND 49.7 49.3 ug/Kg 99 30-160 TestAmerica Irvine Page 60 of 87 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc Project/Site: Valero STRINTIOMI !I TestAmerica Job ID: 440 - 165703 -1 Lab Sample ID: 440- 165703 -4 MS MSD MSD Client Sample ID: 4K- N -E -6' Matrix: Solid RPD Added Result Qualifier Unit D %Rec Prep Type: Total /NA Analysis Batch: 369133 Limit 50.0 51.2 ug /Kg 102 65-145 2 Sample Sample Spike MS MS ug /Kg 103 %Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits Isopropyl Ether (DIPE) ND 49.7 56.3 ug /Kg 113 60-150 Ethanol ND 1990 2090 ug /Kg 105 30 -165 Ethyl -t -butyl ether (ETBE) ND 49.7 51.9 ug /Kg 104 60-145 Ethylbenzene ND 49.7 50.6 ug /Kg 102 70-135 Hexachlorobutadiene ND 49.7 28.6 ug /Kg 57 50-145 Isopropylbenzene ND 49.7 50.9 ug /Kg 102 70-145 m,p- Xylene ND 49.7 53.8 ug /Kg 108 70-130 Methylene Chloride ND 49.7 51.0 ug /Kg 103 55-145 Methyl -t -Butyl Ether (MTBE) ND 49.7 52.9 ug /Kg 106 55-155 Naphthalene ND 49.7 54.5 ug /Kg 110 40-150 n- Butylbenzene ND 49.7 47.3 ug /Kg 95 55-145 N- Propylbenzene ND 49.7 51.8 ug /Kg 104 65-140 o- Xylene ND 49.7 50.5 ug /Kg 102 65 -130 sec - Butylbenzene ND 49.7 48.5 ug /Kg 97 60-135 Styrene ND 49.7 48.8 ug /Kg 98 70-140 Tert- amyl - methyl ether (TAME) ND 49.7 50.9 ug /Kg 103 60 -150 tent -Butyl alcohol (TBA) ND 497 540 ug /Kg 109 65-145 tert- Butylbenzene ND 49.7 50.1 ug /Kg 101 60-140 Tetrachloroethene ND 49.7 51.6 ug /Kg 104 65-135 Toluene ND 49.7 52.4 ug /Kg 105 70-130 trans -1,2- Dichloroethene ND 49.7 54.5 ug /Kg 110 70-135 trans -1,3- Dichloropropene ND 49.7 55.4 ug /Kg 111 60-145 Trichloroethene ND 49.7 51.5 ug /Kg 104 65-140 Trichlorofluoromethane ND 49.7 50.7 ug /Kg 102 55-155 Vinyl chloride ND 49.7 58.8 ug /Kg 118 55-140 p- Isopropyltoluene ND 49.7 46.2 ug /Kg 93 60-140 MS MS Surrogate %Recovery Qualifier Limits Toluene -d8 (Surr) 105 79-123 4- Bromofluorobenzene (Surr) 96 79-120 Dibromofluoromethane (Surr) 99 60-120 Lab Sample ID: 440- 165703 -4 MSD Matrix: Solid Analysis Batch: 369133 Analyte 1, 1, 1,2-Tetrachloroethane 1,1,1- Trichloroethane 1,1,2,2- Tetrachloroethane 1,1,2- Trichloroethane 1,1- Dichloroethane 1,1- Dichloroethene 1,1- Dichloropropene 1,2,3- Trichlorobenzene 1,2,3- Trichloropropane 1,44- Trichlorobenzene 1,2,4- Trimethylbenzene Sample Sample Result Qualifier ND ND ND ND ND ND ND ND ND ND 1.3 J Client Sample ID: 4K- N -E -6' Prep Type: Total /NA Spike MSD MSD %Rec. RPD Added Result Qualifier Unit D %Rec Limits RPD Limit 50.0 51.2 ug /Kg 102 65-145 2 20 50.0 51.7 ug /Kg 103 65-145 2 20 50.0 56.9 ug /Kg 114 40-160 2 30 50.0 59.3 ug /Kg 119 65-140 2 30 50.0 50.2 ug /Kg 100 65-135 4 25 50.0 47.6 ug /Kg 95 65-135 2 25 50.0 50.6 ug /Kg 101 65-135 2 20 50.0 48.6 ug /Kg 97 45-145 7 30 50.0 56.1 ug /Kg 112 50-150 2 30 50.0 48.8 ug /Kg 98 50-140 3 30 50.0 48.5 ug /Kg 94 65-140 6 25 Page 61 of 87 TestAmerica Irvine 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc Project/Site: Valero TestAmerica Job ID: 440- 165703 -1 Lab Sample ID: 440- 165703 -4 MSD Client Sample ID: 4K- N -E -6' Matrix: Solid Prep Type: Total /NA Analysis Batch: 369133 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit 1,2- Dibromo -3- Chloropropane ND 50.0 61.2 ug /Kg 122 40-150 2 30 1,2- Dibromoethane (EDB) ND 50.0 58.5 ug /Kg 117 65 -140 1 25 1,2- Dichlorobenzene ND 50.0 50.4 ug /Kg 101 70-130 2 25 1,2- Dichloroethane ND 50.0 55.5 ug /Kg 111 60-150 1 25 1,2- Dichloropropane ND 50.0 53.9 ug /Kg 108 65-130 0 20 1,3,5- Trimethylbenzene ND 50.0 49.2 ug /Kg 98 65-135 5 25 1,3- Dichlorobenzene ND 50.0 49.2 ug /Kg 98 70-130 4 25 1,3- Dichloropropane ND 50.0 54.2 ug /Kg 108 65-140 0 25 1,4- Dichlorobenzene ND 50.0 48.7 ug /Kg 97 70-130 6 25 2,2- Dichloropropane ND 50.0 55.4 ug /Kg 111 65-150 3 25 2- Chlorotoluene ND 50.0 49.8 ug /Kg 100 60 -135 6 25 4- Chlorotoluene ND 50.0 49.3 ug /Kg 99 65-135 8 25 Benzene ND 50.0 49.6 ug /Kg 99 65-130 1 20 Bromobenzene ND 50.0 50.4 ug /Kg 101 65-140 4 25 Bromochloromethane ND 50.0 53.2 ug /Kg 106 65-145 0 25 Bromodichloromethane ND 50.0 52.3 ug /Kg 105 65-145 1 20 Bromoform ND 50.0 58.2 ug /Kg 116 50-145 7 30 Bromomethane ND 50.0 51.1 ug /Kg 102 60-155 4 25 Carbon tetrachloride ND 50.0 51.4 ug /Kg 103 60-145 2 25 Chiorobenzene ND 50.0 51.5 ug /Kg 103 70 -130 2 25 Chloroethane ND 50.0 48.5 ug /Kg 97 60-150 5 25 Chloroform ND 50.0 52.0 ug /Kg 104 65-135 4 20 Chloromethane ND 50.0 49.3 ug /Kg 99 40-145 5 25 cis -1,2- Dichloroethene ND 50.0 50.9 ug /Kg 102 65-135 4 25 cis -1,3- Dichloropropene ND 50.0 56.0 ug /Kg 112 70-135 1 25 Dibromochloromethane ND 50.0 54.9 ug /Kg 110 60-145 4 25 Dibromomethane ND 50.0 56.1 ug /Kg 112 65-140 2 25 Dichlorodifluoromethane ND 50.0 46.8 ug /Kg 94 30-160 5 35 Isopropyl Ether (DIPE) ND 50.0 56.2 ug /Kg 112 60-150 0 25 Ethanol ND 2000 2050 ug /Kg 102 30-165 2 40 Ethyl -t -butyl ether (ETBE) ND 50.0 54.1 ug /Kg 108 60-145 4 30 Ethylbenzene ND 50.0 49.8 ug /Kg 100 70-135 2 25 Hexachlorobutadiene ND 50.0 34.5 ug /Kg 69 50-145 19 35 Isopropylbenzene ND 50.0 48.9 ug /Kg 98 70-145 4 25 m,p- Xylene ND 50.0 51.3 ug /Kg 103 . . . .. 70-130 ...... 5 25 Methylene Chloride ND 50.0 50.2 ug /Kg 100 55 -145 2 25 Methyl -t -Butyl Ether (MTBE) ND 50.0 55.6 ug /Kg 111 55-155 5 35 Naphthalene ND 50.0 57.4 ug /Kg 115 40-150 5 40 n- Butylbenzene ND 50.0 46.8 ug /Kg 94 55 -145 1 30 N- Propylbenzene ND 50.0 48.7 ug /Kg 97 65-140 6 25 o- Xylene ND 50.0 49.6 ug /Kg 99 65-130 2 25 sec - Butylbenzene ND 50.0 46.3 ug /Kg 93 60-135 5 25 Styrene ND 50.0 49.3 ug /Kg 99 70-140 1 25 Tert-amyl- methyl ether (TAME) ND 50.0 53.9 ug /Kg 108 60- 1 150 6 25 tert -Butyl alcohol (TBA) ND 500 508 ug /Kg 102 65-145 6 30 tert- Butylbenzene ND 50.0 47.6 ug /Kg 95 60-140 5 25 Tetrachloroethene ND 50.0 49.6 ug /Kg 99 65-135 4 25 Toluene ND 50.0 49.8 ug /Kg 100 70-130 5 20 TestAmerica Irvine Page 62 of 87 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440 - 165703 -1 Project/Site: Valero Tt ;. Lab Sample 1D: 440 - 165703 -4 MSD Matrix: Solid Analysis Batch: 369133 Surrogate Toluene -d8 (Surr) 4- Bromofluorobenzene (Surr) Dibromofluoromethane (Surr) Client Sample ID: 4K- N -E -6' Prep Type: Total /NA Spike Sample Sample Analyte Result Qualifier trans -1,2- Dichloroethene ND trans -1,3- Dichloropropene ND Trichloroethene ND Trichlorofluoromethane ND Vinyl chloride ND p- Isopropyltoluene ND Surrogate Toluene -d8 (Surr) 4- Bromofluorobenzene (Surr) Dibromofluoromethane (Surr) Client Sample ID: 4K- N -E -6' Prep Type: Total /NA Spike MSD MSD %Recovery Qualifier Limits %Rec. 79-123 RPD Added Result Qualifier Unit D %Rec Limits RPD Limit 50.0 52.2 ug /Kg 104 70-135 4 25 50.0 56.0 ug /Kg 112 60 -145 1 25 50.0 49.8 ug /Kg 100 65-140 3 25 50.0 48.9 ug /Kg 98 55-155 4 25 50.0 57.7 ug /Kg 115 55-140 2 30 50.0 45.2 ug /Kg 90 60-140 2 25 MSD MSD %Recovery Qualifier Limits 105 79-123 95 79-120 101 60-120 Lab Sample ID: MB 440 - 369451/6 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total /NA Analysis Batch: 369451 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2- Tetrachloroethane ND 5.0 1.0 ug /Kg 11/16/16 08:41 1 1,1,1 - Trichloroethane ND 2.0 1.0 ug /Kg 11/16/16 08:41 1 1,1,2,2- Tetrachloroethane ND 2.0 1.0 ug /Kg 11/16/16 08:41 1 1,1,2- Trichloroethane ND 2.0 1.0 ug /Kg 11/16/16 08:41 1 1,1- Dichloroethane ND 2.0 1.0 ug /Kg 11/16/16 08:41 1 1,1- Dichloroethene ND 5.0 1.0 ug /Kg 11/16/16 08:41 1 1,1- Dichloropropene ND 2.0 1.0 ug /Kg 11/16/16 08:41 1 1,2,3 - Trichlorobenzene ND 5.0 1.0 ug /Kg 11/16/16 08:41 1 1,2,3- Tiichooropropane ND 10 1.0 ug /Kg 11/16/16 08:41 1 1,2,4 - Trichlorobenzene ND 5.0 1.0 ug /Kg 11/16/16 08:41 1 1,2,4- Trimethylbenzene ND 2.0 1.0 ug /Kg 11/16/16 08:41 1 1,2- Dibromo- 3- Chloropropane ND 5.0 2.0 ug /Kg 11/16/16 08:41 1 1,2- Dibromoethane (EDB) ND 2.0 1.0 ug /Kg 11/1 6/1 6 08:41 1 1,2- Dichlorobenzene ND 2.0 1.0 ug /Kg 11/16/16 08:41 1 1,2- Dichloroethane ND 2.0 1.0 ug /Kg 11/16/16 08:41 1 1,2- Dichloropropane ND 2.0 .. .... 1.0 ...... ug /Kg .. 11/16/16 08:41 1 1,3,5- Trimethylbenzene ND 2.0 1.0 ug /Kg 11/16/16 08:41 1 1,3- Dichlorobenzene ND 2.0 1.0 ug /Kg 11/16/16 08:41 1 1,3- Dichloropropane ND 2.0 1.0 ug /Kg 11/16/16 08:41 1 1,4- Dichlorobenzene ND 2.0 1.0 ug /Kg 11/16/16 08:41 1 2,2- Dichloropropane ND 2.0 1.0 ug /Kg 11/16/16 08:41 1 2- Chlorotoluene ND 5.0 1.0 ug /Kg 11/16/16 08:41 1 t- Chlorotoluene ND 5.0 1.0 ug /Kg 11/16/16 08:41 1 3enzene ND 2.0 1.0 ug /Kg 11/16/16 08:41 1 3romobenzene ND 5.0 1.0 ug /Kg 11/16/16 08:41 1 3romochloromethane ND 5.0 1.0 ug /Kg 11/16/16 08:41 1 3romodichloromethane ND 2.0 1.0 ug /Kg 11/16/16 08:41 1 3romoform ND 5.0 2.0 ug /Kg 11/16/16 08:41 1 3romomethane ND 5.0 1.0 ug /Kg 11/16/16 08:41 1 :arbon tetrachloride ND 5.0 1.0 ug /Kg 11/16/16 08:41 1 ,hlorobenzene ND 2.0 1.0 ug /Kg 11/16/16 08:41 1 TestAmerica Irvine Page 63 of 87 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc - Project/Site: Valero, Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 440-36945116 Matrix: Solid Analysis Batch: 369451 TestAmerica Job ID: 440-165703-1 Client Sample ID: Method Blank Prep Type: Total /NA Lab Sample ID: LCS 440-369451/7 Matrix: Solid Analysis Batch: 369451 Analyte 1, 1, 1,2-Tetrachloroethane 1, 1, 1 -Trichloroethane Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits 50.0 54.0 ug/Kg 108 70-130 50.0 52.2 ug/Kg 104 65-135 TestAmerica Irvine Page 64 of 87 11/23/2016 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloroethane ND 5.0 2.0 11116/16 08:41 1 Chloroform ND 2.0 1.0 ug/Kg 11/16116 08:41 1 Chloromethane ND 5.0 1.0 ug/Kg 11/16116 08:41 1 cis-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 11/16/16 08:41 1 cis-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 11/16/16 08:41 1 Dibromochloromethane .... N . D 2.0 1.0 u . g . /K I g .... ........ 11 /16/1 6 08:41 1 Dibromomethane ND 2.0 1.0 ug/Kg 11/16/16 08:41 1 Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 11/16/16 08:41 1 Isopropyl Ether (DIPS) ND 5.0 1.0 ug/Kg 11/16116 08:41 1 Ethanol ND 300 100 ug/Kg 11/16/16 08:41 1 Ethyl-t-butyl ether (ETBE) ND 5.0 1.0 ug/Kg 11/16/16 08:41 1 Ethylbenzene ND 2.0 1.0 ug/Kg 11/16/16 08:41 1 Hexachlorobutadiene ND 5.0 1.0 ug/Kg 11/16/16 08:41 1 lsopropylbenzene ND 2.0 1.0 ug/Kg 11/16/16 08:41 1 m,p-Xylene ND 4.0 2.0 ug/Kg 11/16/16 08:41 1 Methylene Chloride ND 20 5.0 ug/Kg 11/16/16 08:41 1 Methyl-t-Butyl Ether (MTBE) ND 5.0 1.0 ug/Kg 11/16/16 08:41 1 Naphthalene ND 5.0 2.0 ug/Kg 11/16/16 08:41 1 n-Butylbenzene ND 5.0 1.0 ug/Kg 11/16/16 08:41 1 N-Propylbenzene ND 2.0 1.0 ug/Kg 11/16/16 08:41 1 o-Xylene ND 2.0 1.0 ug/Kg 11/16/16 08:41 1 see-Butylbenzene ND 5.0 1.0 ug/Kg 11/16/16 08:41 1 Styrene ND 2.0 1.0 ug/Kg 11/16116 08:41 1 Tert-amyl-methyl ether (TAME) ND 5.0 1.0 ug/Kg 11/16/16 08:41 1 tert-Butyl alcohol (TBA) ND 100 10 ug/Kg 11/16/16 08:41 1 tert-Butylbenzene ND 5.0 1.0 ug/Kg 11/16/16 08:41 1 Teirachloroethene ND ...... 2.0 ... .... 1.0 . . . ug/Kg . .. 11/16/16 08:41 1 Toluene ND 2.0 1.0 ug/Kg 11/16/16 08:41 1 trans-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 11/16/16 08:41 1 trans-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 11/16/16 08:41 1 Trichloroethene ND 2.0 1.0 ug/Kg 11/16/16 08:41 1 Trichlorofluoromethane ND 5.0 1.0 ug/Kg 11/16116 08:41 1 Vinyl chloride ND 5.0 1.0 ug/Kg 11/16/16 08:41 1 Xylenes, Total ND 4.0 2.0 ug/Kg 11/16/16 08:41 1 p-lsopropyltoluene ND 2.0 1.0 ug/Kg 11/16/16 08:41 1 MB MB Surrogate %Recovety Qualifier Limits Prepared Analyzed Dil Fac Toluene -d8 (Surr) 104 79-123 11116116 08:41 1 4-Bromofluorobenzene (Surr) 100 79-120 11116116 08:41 1 Dibromofluoromethane (Surr) 102 60-120 11116116 08:41 1 Lab Sample ID: LCS 440-369451/7 Matrix: Solid Analysis Batch: 369451 Analyte 1, 1, 1,2-Tetrachloroethane 1, 1, 1 -Trichloroethane Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits 50.0 54.0 ug/Kg 108 70-130 50.0 52.2 ug/Kg 104 65-135 TestAmerica Irvine Page 64 of 87 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc Project/Site: Valero Z1.11 Bill'' TestAmerica Job ID: 440 - 165703 -1 Lab Sample ID: LCS 440 - 36945117 Client Sample ID: Lab Control Sample Matrix: Saud Prep Type: Total /IAA Analysis Batch: 369451 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits 1,1,2,2- Tetrachloroethane 50.0 55.1 ug /Kg 110 55 -140 1,1,2- Trichloroethane 50.0 57.4 ug /Kg 115 65-135 1,1- Dichloroethane 50.0 51.4 ug /Kg 103 70 -130 1,1- Dichloroethene 50.0 50.0 ug /Kg 100 70 -125 1,1- Dichloropropene 50.0 52.3 ug /Kg 105 70 -130 1,2,3- Trichlorobenzene 50.0 52.8 ug /Kg 106 60-130 1,2,3- Trichooropropane 50.0 54.6 ug /Kg 109 60-135 1,2,4- Trichlorobenzene 50.0 53.8 ug /Kg 108 70-135 1,2,4- Trimethylbenzene 50.0 49.9 ug /Kg 100 70-125 1,2- Dibromo- 3- Chloropropane 50.0 57.7 ug /Kg 115 50-135 1,2- Dibromoethane (EDB) ..... 50.0 .... ..... 59.7 ug /Kg 119 70-130 1,2- Dichlorobenzene 50.0 50.2 ug /Kg 100 75-120 1,2- Dichloroethane 50.0 55.0 ug /Kg 110 60-140 1,2- Dichloropropane 50.0 53.7 ug /Kg 107 70-130 1,3,5- Trimethylbenzene 50.0 51.3 ug /Kg 103 70-125 1,3- Dichlorobenzene 50.0 51.1 ug /Kg 102 75-125 1,3- Dichloropropane 50.0 54.7 ug /Kg 109 70-125 1,4- Dichlorobenzene 50.0 50.2 ug /Kg 100 75-120 2,2- Dichloropropane 50.0 54.6 ug /Kg 109 60-145 . . ...... ....... 2- Chlorotoluene 50.0 ...... 51.1 ug /Kg 102 70-125 4- Chlorotoluene 50.0 50.7 ug /Kg 101 75-125 Benzene 50.0 51.6 ug /Kg 103 65-120 Bromobenzene 50.0 51.2 ug /Kg 102 75-120 Bromochloromethane 50.0 57.7 ug /Kg 115 70-135 Bromodichloromethane 50.0 54.5 ug /Kg 109 70-135 Bromoform 50.0 60.7 ug /Kg 121 55-135 Bromomethane 50.0 53.8 ug /Kg 108 60-145 Carbon tetrachloride 50.0 54.0 ug /Kg 108 65-140 Chlorobenzene 50.0 54.1 ug /Kg 108 75-120 Chloroethane 50.0 50.6 ug /Kg 101 60-140 Chloroform 50.0 53.8 ug /Kg 108 70-130 Chloromethane 50.0 43.2 ug /Kg 86 45-145 cis -1,2- Dichloroethene 50.0 53.0 ug /Kg 106 70-125 cis- 1,3- Dichloropropene 50.0 57.8 ug /Kg 116 75-125 Dibromochloromethane 50.0 57.3 ug /Kg 115 65-140 Dibromomethane 50.0 57.2 ug /Kg 114 70-130 Dichlorodifluoromethane 50.0 43.5 ug /Kg 87 35-160 Isopropyl Ether (DIPE) 50.0 51.9 ug /Kg 104 60-140 Ethanol 2000 1890 ug /Kg 94 35-160 Ethyl -t -butyl ether (ETBE) 50.0 56.4 ug /Kg 113 60-140 Ethylbenzene 50.0 50.7 ug /Kg 101 70-125 Hexachlorobutadiene 50.0 51.4 ug /Kg 103 60-135 Isopropylbenzene 50.0 51.8 ug /Kg 104 75-130 m,p- Xylene 50.0 54.2 ug /Kg 108 70-125 Methylene Chloride 50.0 51.7 ug /Kg 103 55-135 Methyl -t -Butyl Ether (MTBE) 50.0 57.1 ug /Kg 114 60-140 Naphthalene 50.0 54.4 ug /Kg 109 55-135 n- Butylbenzene 50.0 48.6 ug /Kg 97 70-130 TestAmerica Irvine Page 65 of 87 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc Project/Site: Valero Method: 8260B - Volatile Organic Compounds (GCIMS) (Continued) Lab Sample ID: LCS 440 - 369451/7 Matrix: Solid Analysis Batch: 369451 Analyte N- Propylbenzene o- Xylene sec - Butylbenzene Styrene Tert- amyl - methyl ether (TAME) tert -Butyl alcohol (TBA) tert- Butylbenzene Tetrachloroethene Toluene trans -1,2- Dichloroethene trans -1,3- Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride p- Isopropyltoluene Spike Added 50.0 50.0 50.0 50.0 50.0 500 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 LCS LCS Surrogate %Recovery Qualifier Limits Toluene -d8 (Surr) 102 79-123 4- Bromofluorobenzene (Surr) 93 79-120 Dibromof/uoromethane (Surr) 105 60-120 Lab Sample ID: 440 - 165849 -A -5 MS Matrix: Solid Analysis Batch: 369451 TestAmerica Job ID: 440 - 165703 -1 Client Sample ID: Lab Control Sample Prep Type: Total /NA LCS LCS Sample Sample Spike %Rec. Result Qualifier Unit D %Rec Limits 48.6 ug /Kg 97 70-130 52.8 ug /Kg 106 70-125 49.0 ug /Kg 98 70-125 51.0 ug /Kg 102 75-130 56.4 ug /Kg 113 60-145 533 ug /Kg 107 70-135 51.4 ug /Kg 103 70-125 52.7 ug /Kg 105 70-125 50.6 ug /Kg 101 70-125 54.9 ug /Kg 110 70-125 55.5 ug /Kg 111 70-135 54.2 ug /Kg 108 70-125 49.8 ug /Kg 100 60-145 45.2 ug /Kg 90 55-135 49.6 ug /Kg 99 75-125 Client Sample ID: Matrix Spike Prep Type: Total /NA Page 66 of 87 TestAmerica Irvine 11/23/2016 Sample Sample Spike MS MS %Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits 1,1,1,2- Tetrachloroethane ND 50.0 52.0 ug /Kg 104 65-145 1,1,1 - Trichloroethane ND 50.0 52.5 ug /Kg 105 65 -145 1,1,2,2- Tetrachloroethane ND 50.0 51.5 ug /Kg 103 40-160 1,1,2- Trichloroethane ND 50.0 53.9 ug /Kg 108 65-140 1,1- Dichloroethane ND 50.0 50.3 ug /Kg 101 65 -135 1,1- Dichloroethene ND 50.0 51.0 ug /Kg 102 65 -135 1,1- Dichloropropene ND 50.0 51.2 ug /Kg 102 65-135 1,2,3 - Trichlorobenzene ND 50.0 50.1 ug /Kg 100 45 -145 1,2,3- Trcchloropropane ND 50.0 52.8 ug /Kg 106 50-150 1,2,4- Trichlorobenzene ND 50.0 52.2 ug /Kg 104 50-140 1,2,4- Trimethylbenzene ND 50.0 51.2 ug /Kg 102 65-140 1,2- Dibromo- 3- Chloropropane ND 50.0 50.9 ug /Kg 102 40-150 1,2- Dibromoethane (EDB) ND 50.0 53.8 ug /Kg .. ... .. .. 108 .... 65-140 1,2- Dichlorobenzene ND 50.0 50.3 ug /Kg 101 70-130 1,2- Dichloroethane ND 50.0 50.8 ug /Kg 102 60-150 1,2- Dichloropropane ND 50.0 52.9 ug /Kg 106 65-130 1,3,5- Trimethylbenzene ND 50.0 52.2 ug /Kg 104 65-135 1,3- Dichlorobenzene ND 50.0 50.3 ug /Kg 101 70-130 1,3- Dichloropropane ND 50.0 50.8 ug /Kg 102 65-140 1,4- Dichlorobenzene ND 50.0 51.3 ug /Kg 103 70-130 2,2- Dichloropropane ND 50.0 56.1 ug /Kg 112 65-150 2- Chlorotoluene ND 50.0 51.4 ug /Kg 103 60-135 Page 66 of 87 TestAmerica Irvine 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-165703-1 Project/Site: Valero Lab Sample ID: 440-165849-A-5 MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA Analysis Batch: 369451 Sample Sample Spike MS MS %Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits 4-Chlorotoluene ND 50.0 52.1 ug/Kg 104 65-135 Benzene ND 50.0 50.7 ug/Kg 101 65-130 Bromobenzene ND 50.0 52.9 ug/Kg 106 65-140 Bromochloromethane ND 50.0 55.2 ug/Kg 110 65-145 Bromodichloromethane ND 50.0 52.6 ug/Kg 105 65-145 Bromoform ND ... ... 50. . 0 55 . .6 - u I g . /Kg 11 . 1 50 145 Bromomethane ND 50.0 51.3 ug/Kg 103 60-155 Carbon tetrachloride ND 50.0 54.8 ug/Kg 110 60-145 Chlorobenzene ND 50.0 53.2 ug/Kg 106 70-130 Chloroethane ND 50.0 49.9 ug/Kg 100 60-150 Chloroform ND 50.0 52.5 ug/Kg 105 65-135 Chloromethane ND 50.0 40.4 ug/Kg 81 40-145 cis-1,2-Dichloroethene ND 50.0 52.5 ug/Kg 105 65-135 cis-1,3-Dichloropropene ND 50.0 55.1 ug/Kg 110 70-135 Dibromochloromethane ND 50.0 53.4 ug/Kg 107 60-145 Dibromomethane ND 50.0 51.1 ug/Kg 102 65-140 Dichlorodifluoromethane ND 50.0 40.4 ug/Kg 81 30-160 Isopropyl Ether (NPE) ND 50.0 . . . 49.7 u . g/Kg 99 60 150 Ethanol ND 2000 1890 ug/Kg 94 30-165 Ethyl-t-butyl ether (ETBE) ND 50.0 53.2 ug/Kg 106 60-145 Ethylbenzene ND 50.0 49.5 ug/Kg 99 70-135 Hexachlorobutadiene ND 50.0 47.6 ug/Kg 95 50-145 lsopropylbenzene ND 50.0 51.1 ug/Kg 102 70-145 m,p-Xylene ND 50.0 52.7 ug/Kg 105 70-130 Methylene Chloride ND 50.0 52.3 ug/Kg 105 55-145 Methyl-t-Butyl Ether (MTBE) ND 50.0 52.8 ug/Kg 106 55-155 Naphthalene ........ ND . .... 50.0 52.6 ug/Kg 105 40-150 n-Butylbenzene ND 50.0 48.5 ug/Kg 97 55-145 N-Propylbenzene ND 50.0 50.4 ug/Kg 101 65-140 o4ylene ND 50. 1 0 5 . 1.1 . u I g I /Kg 102... 65 130 sec-Butylbenzene ND 50.0 50.0 ug/Kg 100 60-135 Styrene ND 50.0 49.4 ug/Kg 99 70-140 Tert-amyl-methyl ether (TAME) ND 50.0 53.2 ug/Kg 106 60-150 tert-Butyl alcohol (TBA) ND 500 505 ug/Kg 101 65-145 tert-Butylbenzene ND 50.0 53.3 ug/Kg 107 60-140 Tetrachloroethene ND 50.0 52.3 ug/Kg 105 65-135 Toluene ND 50.0 50.5 ug/Kg 101 70-130 trans-1,2-Dichloroethene ND 50.0 54.7 ug/Kg 109 70-135 trans-!, 3-Dichloropropene ND 50.0 52 . .8 1 u I g . /Kg 106 60 145 ........ Trichloroethene ND 50.0 54.6 ug/Kg 109 65-140 Trichlorofluoromethane ND 50.0 49.9 ug/Kg 100 55-155 Vinyl chloride ND 50.0 44.1 ug/Kg 88 55-140 p-Isopropyltoluene ND 50.0 50.0 ug/Kg 100 60-140 MS MS Surrogate %Recovery Qualifier Limits Toluene-o`8 (Surr) 100 79-123 4-Bromofluorobenzene (Surr) 100 79-120 Dibromofluoromethane (Surr) 101 60-120 TestAmerica Irvine Page 67 of 87 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440 - 165703 -1 Project/Site: Valero Lab Sample ID: 440 - 165849 -A -5 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total /NA Analysis Batch: 369451 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit 1,1,1,2- Tetrachloroethane ND 50.0 52.8 ug /Kg 106 65-145 2 20 1,1,1- Trichloroethane ND 50.0 53.2 ug /Kg 106 65-145 1 20 1,1,2,2- Tetrachloroethane ND 50.0 52.6 ug /Kg 105 40-160 2 30 1,1,2- Trichloroethane ND 50.0 56.6 ug /Kg 113 65-140 5 30 1,1- Dichloroethane ND 50.0 51.1 ug /Kg 102 65 -135 2 25 1,1- Dichloroethene ND 50.0 51.6 ug /Kg 103 65-135 1 25 1,1- Dichloropropene ND 50.0 52.0 ug /Kg 104 65 -135 2 20 1,2,3- Trichlorobenzene ND 50.0 48.7 ug /Kg 97 45-145 3 30 1,2,3- Trichooropropane ND 50.0 55.0 ug /Kg 110 50-150 4 30 1,2,4- Trichlorobenzene ND 50.0 50.8 ug /Kg 102 50-140 3 30 1,2,4- Trimethylbenzene ND 50.0 48.6 ug /Kg 97 65-140 5 25 1,2- Dibromo -3- Chloropropane ND 50.0 57.1 ug /Kg 114 40-150 11 30 1,2- Dibromoethane (Ebb) ND 50.0 58.4 ug /Kg 117 65 -140 8 25 1,2- Dichlorobenzene ND 50.0 48.8 ug /Kg 98 70-130 3 25 1,2- Dichloroethane ND 50.0 52.5 ug /Kg 105 60-150 3 25 1,2- Dichloropropane ND 50.0 53.9 ug /Kg 108 65-130 2 20 1,3,5- Trimethylbenzene ND 50.0 50.0 ug /Kg 100 65-135 4 25 1,3- Dichlorobenzene ND 50.0 50.4 ug /Kg 101 70-130 0 25 1,3- Dichloropropane ND 50.0 53.4 ug /Kg 107 65-140 5 25 1,4- Dichlorobenzene ND 50.0 49.3 ug /Kg 99 70-130 4 25 2,2- Dichloropropane ND 50.0 55.1 ug /Kg 110 65-150 2 25 2- Chlorotoluene ND 50.0 49.6 ug /Kg 99 60-135 4 25 4- Chlorotoluene ND 50.0 50.3 ug /Kg 101 65-135 4 25 Benzene ND 50.0 49.5 ug /Kg 99 65-130 2 20 Bromobenzene ND 50.0 51.7 ug /Kg 103 65-140 2 25 Bromochloromethane ND 50.0 55.8 ug /Kg 112 65.145 1 25 Bromodichloromethane ND 50.0 52.7 ug /Kg 105 65-145 0 20 Bromoform ND 50.0 61.4 ug /Kg 123 50-145 10 30 Bromomethane ND 50.0 51.4 ug /Kg 103 60-155 0 25 Carbon tetrachloride ND 50.0 54.3 ug /Kg 109 60-145 1 25 Chlorobenzene ND 50.0 53.1 ug /Kg 106 70-130 0 25 Chloroethane ND 50.0 50.4 ug /Kg 101 60-150 1 25 Chloroform ND 50.0 54.0 ug /Kg 108 65-135 3 20 Chloromethane ND 50.0 40.3 ug /Kg 81 40-145 0 25 cis -1,2- Dichloroethene ND 50.0 54.8 ug /Kg 110 65-135 4 25 cis -1,3- Dichloropropene ND 50.0 57.1 ug /Kg 114 70-135 4 25 Dibromochloromethane ND 50.0 56.2 ug /Kg 112 60-145 5 25 Dibromomethane ND 50.0 55.3 ug /Kg 111 65-140 8 25 Dichlorodifluoromethane ND 50.0 40.7 ug /Kg 81 30-160 1 35 Isopropyl Ether (DIPE) ND 50.0 51.9 ug /Kg 104 60-150 4 25 Ethanol ND 2000 1790 ug /Kg 90 30-165 5 40 Ethyl -t -butyl ether (ETBE) ND 50.0 55.0 ug /Kg 110 60-145 3 30 Ethylbenzene ND 50.0 51.2 ug /Kg 102 70-135 3 25 Hexachlorobutadiene ND 50.0 44.6 ug /Kg 89 50-145 6 35 Isopropylbenzene ND 50.0 51.0 ug /Kg 102 70-145 0 25 m,p- Xyiene ND 50.0 54.1 ug /Kg 108 70-130 2 25 Methylene Chloride ND 50.0 52.6 ug /Kg 105 55-145 1 25 Methyl -t -Butyl Ether (MTBE) ND 50.0 56.5 ug /Kg 113 55-155 7 35 Naphthalene ND 50.0 53.1 ug /Kg 106 40-150 1 40 n- Butylbenzene ND 50.0 46.5 ug /Kg 93 55-145 4 30 TestAmerica Irvine Page 68 of 87 11/23/2016 11 QC Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID-. 440-165703-1 Project/Site: Valero Lab Sample ID: 440-165849-A-5 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA Analysis Batch: 369451 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit N-Propylbenzene ND 50.0 48.9 ug/Kg 98 65-140 3 25 O-xylene ... ND 50. . 0 5 1 0.5 1 u I g/Kg 10 . 1 65 1 1 30 1 25 sec-Butylbenzene ND 50.0 47.1 ug/Kg 94 60-135 6 25 Styrene ND 50.0 50.0 ug/Kg 100 70-140 1 25 Tert-amyl-methyl ether (TAME) ND 50.0 55.9 ug/Kg 112 60-150 5 25 tert-Butyl alcohol (TBA) ND 500 496 ug/Kg 99 65-145 2 30 tert-Butylbenzene ND 50.0 49.8 ug/Kg 100 60-140 7 25 Tetrachloroethene ND 50.0 52.8 ug/Kg 106 65-135 1 25 Toluene ND 50.0 51.8 ug/Kg 104 70-130 3 20 trans-1,2-Dichloroethene ND 50.0 54.7 ug/Kg 109 70-135 0 25 trans-1,3-Dichloropropene ND 50.0 55.8 ug/Kg 112 60-145 5 25 Trichloroethene ND 50.0 56.0 ug/Kg 112 65-140 3 25 Trichlorofluoromethane ND 50.0 50.1 ug/Kg 100 55-155 0 25 Vinyl chloride ND 50.0 44.7 ug/Kg 89 55-140 1 30 p-isopropyltoluene ND 50.0 48.0 ug/Kg 96 60-140 4 25 MSD MSD Surrogate %Recovefy Qualifier Limits Toluene -d8 (Surr) 102 79-123 4-Bromofluoroberizene (Surr) 101 79-120 Dibromofluoromethane (Surr) 104 60-120 Lab Sample ID: MB 440-369458/7 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 369458 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1, 1, 1,2-Tetrachloroethane ND 5.0 1.0 ug/Kg 11/16/16 08:35 1 1, 1, 1 -Trichloroethane ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 1, 1,2,2-Tetrachloroethane ND 2.0 1.0 ug/Kg 11116/16 08:35 1 1, 1,2-Trichloroethane ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 1,1-Dichloroethane ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 1,1-Dichloroethene ND 5.0 1.0 ug/Kg 11/16/16 08:35 1 1 1 1 -bichloropropene ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 1,2,3-Trichlorobenzene ND 5.0 1.0 ug/Kg 11/16/16 08:35 1 1,2,3-Trichloropropane ND 10 1.0 ug/Kg 11/16/16 08:35 1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/Kg 11/16/16 08:35 1 1,2,4-Trimethylbenzene ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 1,2-Dibromo-3-Chloropropane ND 5.0 2.0 ug/Kg 11/16/16 08:35 1 1,2-Dibrornoethane (ED13) ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 1,2-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 1,2-Dichloroethane ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 1,2-bichioropropane ND 2.0 1.0 u . g/Kg 11/16/16 08:35 1 1,3,5-Trimethylbenzene ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 1,3-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 1,3-Dichloropropane ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 1,4-Dichlorobenzene ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 2,2-Dichloropropane ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 2-Chlorotoluene ND 5.0 1.0 ug/Kg 11/16/16 08:35 1 TestAmerica Irvine Page 69 of 87 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc Project/Site: Valero OFF' Lab Sample ID: MB 440-36945817 Matrix: Solid Analysis Batch: 369458 Analyte MB MB Result Qualifie TestAmerica Job ID: 440-165703-1 Client Sample ID: Method Blank Prep Type: Total/NA r RL MDL Unit D Prepared Analyzed Dil Fac 4-Chlorotoluene ND 5.0 1.0 ug/Kg 11/16/16 08:35� 1 Benzene ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 Bromobenzene ND 5.0 1.0 ug/Kg 11/16116 08:35 1 Bromochloromethane ND 5.0 1.0 ug/Kg 11/16/16 08:35 1 Bromodichloromethane ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 Bromoform ND 5.6 2.0 ug/Kg 11/16/16 08:35 1 Bromomethane ND 5.0 1.0 ug/Kg 11/16/16 08:35 1 Carbon tetrachloride ND 5.0 1.0 ug/Kg 11/16/16 08:35 1 Chlorobenzene ND 2.0 1.0 ug/Kg 11/16/16 68:35 1 Chloroethane ND 5.0 2.0 ug/Kg 11/16/16 08:35 1 Chloroform ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 Chloromethane ND 5.0 1.0 ug/Kg 11/16/16 08:35 1 cis-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 cis-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 Dibromochloromethane ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 Dibromomethane ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 Dichlorodifluoromethane ND 5.0 2.0 ug/Kg 11/16/16 08:35 1 Isopropyl Ether (DOE) .... ND 5.0 1.0 u I g/K I g 11/16/16 1 08:35 1 Ethanol ND 300 100 ug/Kg 11/16/16 08:35 1 Ethyl-t-butyl ether (ETBE) ND 5.0 1.0 ug/Kg 11/16/16 08:35 1 Ethylbenzene ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 Hexachlorobutadiene ND 5.0 1.0 ug/Kg 11116/16 08:35 1 lsopropylbenzene ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 m,p-Xylene ND 4.0 2.0 ug/Kg 11/16116 08:35 1 Methylene Chloride ND 20 5.0 ug/Kg 11/16/16 08:35 1 Methyl-t-Butyl Ether (MTBE) ND 5.0 1.0 ug/Kg 11/16/16 08:35 1 Naphthalene ND 5.0 2.0 ug/Kg 11%16/16 08:35 1 n-Butylbenzene ND 5.0 1.0 ug/Kg 11/16/16 08:35 1 N-Propylbenzene ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 O-Xylene ND 2.0 1.0 ug/Kg 11/16/16 mm 1 sec-Butylbenzene ND 5.0 1.0 ug/Kg 11/16/16 08:35 1 Styrene ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 Tert-amyl-methyl ether (TAME) ND 5.0 1.0 ug/Kg 11/16/16 08:35 1 tert-Butyl alcohol (TBA) ND 100 10 ug/Kg 11/16/16 08:35 1 tert-Butylbenzene ND 5.0 1.0 ug/Kg 11/16/16 08:35 1 Tetrachloroethene ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 Toluene ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 trans-1,2-Dichloroethene ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 trans-1,3-Dichloropropene ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 Trichloroethene ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 Trichlorofluoromethane ND 5.0 1.0 ug/Kg 11/16/16 08:35 1 Vinyl chloride ND 5.0 1.0 ug/Kg 11/16/16 08:35 1 Xylenes, Total ND 4.0 2.0 ug/Kg 11/16/16 08:35 1 p-isopropyltoluene ND 2.0 1.0 ug/Kg 11/16/16 08:35 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac Toluene -d8 (Surr) 106 79-123 11116116 08:35 1 4-Bromofluorobenzene (Surr) 102 79-120 11116116 08:35 1 Page 70 of 87 TestAmerica Irvine 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440 - 165703 -1 Project/Site: Valero 73 V Lab Sample ID: LCS 440 - 369458/5 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total /NA Analysis Batch: 369458 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits 1,1,1,2- Tetrachloroethane 50.0 54.7 ug /Kg 109 70-130 1,1,1- Trichloroethane 50.0 50.8 ug /Kg 102 65-135 1,1,2,2- Tetrachloroethane 50.0 58.8 ug /Kg 118 55-140 1,1,2- Trichloroethane 50.0 56.0 ug /Kg 112 65-135 1,1- Dichloroethane 50.0 51.6 ug /Kg 103 70-130 1,1- Dichloroethene 50.0 46.6 ug /Kg 93 70-125 1,1- Dichloropropene 50.0 48.5 ug /Kg 97 7 0- 130 1,2,3- Trchlorobenzene 50.0 56.6 ug /Kg 113 60-130 1,2,3 - Trichloropropane 50.0 57.9 ug /Kg 116 60 -135 1,2,4- Trichlorobenzene 50.0 57.9 ug /Kg 116 70-135 1,2,4- Trimethylbenzene 50.0 51.5 ug /Kg 103 70-125 1,2- Dibromo -3- Chloropropane 50.0 55.3 ug /Kg 111 50-135 1,2- Dibromoethane (EDB) 50.0 58.1 ug /Kg 116 70-130 1,2- Dichlorobenzene 50.0 56.4 ug /Kg 113 75-120 1,2- Dichloroethane 50.0 61.1 ug /Kg 122 60-140 1,2- Dichloropropane 50.0 59.1 ug /Kg 118 70 -130 1,3,5- Trimethylbenzene 50.0 52.8 ug /Kg 106 70-125 1,3- Dichlorobenzene 50.0 54.5 ug /Kg 109 75-125 1,3- Dichloropropane 50.0 53.8 ug /Kg 108 70-125 1,4- Dichlorobenzene 50.0 54.5 ug /Kg 109 75-120 2,2- Dichloropropane 50.0 52.5 ug /Kg 105 60-145 2- Chlorotoluene 50.0 51.3 ug /Kg 103 70-125 4- Chlorotoluene 50.0 53.0 ug /Kg 106 75-125 Benzene 50.0 52.6 ug /Kg 105 65-120 Bromobenzene 50.0 56.7 ug /Kg 113 75-120 Bromochloromethane 50.0 61.4 ug /Kg 123 70-135 Bromodichloromethane 50.0 60.8 ug /Kg 122 70-135 Bromoform 50.0 63.0 ug /Kg 126 55-135 Bromomethane 50.0 55.0 ug /Kg 110 60-145 Carbon tetrachloride 50.0 51.8 ug /Kg 104 65-140 Chlorobenzene 50.0 49.8 ug /Kg 100 75-120 Chloroethane 50.0 493 ug /Kg 99 60-140 Chloroform 50.0 55.9 ug /Kg 112 70-130 Chloromethane 50.0 42.1 ug /Kg 84 45-145 cis -1,2- Dichloroethene 50.0 57.7 ug /Kg 115 70-125 cis- 1,3- Dichloropropene 50.0 57.0 ug /Kg 114 75-125 Dibromochloromethane 50.0 56.5 ug /Kg 113 65-140 Dibromomethane 50.0 61.3 ug /Kg 123 70-130 Dichlorodifluoromethane 50.0 30.5 ug /Kg 61 35-160 Isopropyl Ether (DIPS) 50.0 60.3 ug /Kg 121 60-140 Ethanol 2000 2310 ug /Kg 116 35-160 TestAmerica Irvine Page 71 of 87 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-165703-1 Project/Site: Valero Lab Sample ID: LCS 440-369458/5 Sample Sample Spike Client Sample ID: Lab Control Sample Matrix: Solid %Rec. Analyte Result Qualifier Prep Type: Total/NA Analysis Batch: 369458 Unit D %Rec Limits 1,1,1,2-Tetrachloroethane ND 50.0 Spike LCS LCS 106 65-145 %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Ethyl-t-butyl ether (ETBE) 50.0 61.9 ug/Kg 124 --60---140 Ethylbenzene 50. . 0 4 . 7.3 u I g/Kg 9 . 5 70 125 Hexachlorobutadiene 50.0 50.4 ug/Kg 101. 60-135 lsopropylbenzene 50.0 47.4 ug/Kg 95 75-130 rn,p-Xylene 50.0 47.9 ug/Kg 96 70-125 Methylene Chloride 50.0 54.3 ug/Kg 109 55-135 Methyl-t-Butyl Ether (MTBE) 50.0 63.8 ug/Kg 128 60-140 Naphthalene 50.0 57.0 ug/Kg 114 55-135 n-Butylbenzene 50.0 50.7 ug/Kg 101 70-130 N-Propylbenzene 50.0 49.9 ug/Kg 100 70-130 O-Xylene 50.0 48.4 ug/Kg 97 70-125 sec-Butylbenzene 50.0 47.8 ug/Kg 96 70-125 Styrene 50.0 48.3 ug/Kg 97 75-130 Tert-amyl-methyl ether (TAME) 50.0 60.8 ug/Kg 122 60-145 tert-Butyl alcohol (TBA) 500 575 ug/Kg 115 70-135 tert-Butylbenzene 50.0 50.6 ug/Kg 101 70-125 Tetrachloroethene 50.0 45.2 ug/Kg 90 70-125 Toluene 50.0 47.8 ug/Kg 96 70-125 trans-1,2-Dichloroethene 50.0 54.2 ug/Kg 108 70-125 trans- 1, 3-bichloropropene 50.0 57.2 ug/Kg 114 70-135 Trichloroethene 50.0 54.0 ug/Kg 108 70-125 Trichlorofluoromethane 50.0 45.3 ug/Kg 91 60-145 Vinyl chloride 50.0 42.0 ug/Kg 84 55-135 p-Isopropyltoluene 50.0 49.6 ug/Kg 99 75-125 LCS LCS Surrogate %Recovery Qualifier Limits Toluene-d8 (Surr) 97 79-123 4-Bromofluorobenzene (Surr) 100 79-120 Dibromotluoromethane (Surr) 109 60-120 Lab Sample ID: 440-165703-A-24 MS Matrix: Solid Analysis Batch: 369458 Client Sample ID: 4K-S-W-6' Prep Type: Total/NA TestAmerica Irvine Page 72 of 87 11/23/2016 Sample Sample Spike ms ms %Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits 1,1,1,2-Tetrachloroethane ND 50.0 52.8 ug/Kg 106 65-145 1, 1, 1 -Trichloroethane ND 50.0 55.3 ug/Kg Ill 65-145 1, 1,2,2-Tetrachloroethane ND 50.0 60.3 ug/Kg 121 40-160 1,1,2-Trichloroethane ND 50.0 52.9 ug/Kg 106 65-140 1,1-Dichloroethane ND 50.0 52.0 ug/Kg 104 65-135 1,1-Dichloroethene ND 50.0 52.2 ug/Kg 104 65-135 1,1-bichloropropene ND 50.0 51.7 ug/Kg 103 65-135 1,2,3-T(ichlorobenzene ND 50.0 38.1 ug/Kg 76 45-145 1,2,3-Trichloropropane ND 50.0 60.9 ug/Kg 122 50-150 1,2,4-Tdchlorobenzene ND 50.0 42.2 ug/Kg 84 50-140 1,2,4-Trimethylbenzene ND 50.0 51.2 ug/Kg 102 65-140 1,2-Dibromo-3-Chloropropane ND 50.0 58.9 ug/Kg 118 40-150 1,2-Dibromoethane (EDB) ND 50.0 54.5 ug/Kg 109 65-140 TestAmerica Irvine Page 72 of 87 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440 - 165703 -1 Project/Site: Valero Method: 826 - Volatile Organic Compounds (GCS (Continued) Lab Sample ID: 440- 165703 -A -24 MS Client Sample ID: 4K- S -W -6' Matrix: Solid Prep Type: Total /PIA Analysis Batch: 368458 TestAmerica Irvine Page 73 of 87 11/23/2016 Sample Sample Spike MS MS %Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits 1,2- Dichlorobenzene ND 50.0 54.3 ug /Kg 109 70-130 1,2- Dichloroethane ND 50.0 51.8 ug /Kg 104 60 -150 1,2- Dichloropropane ND 50.0 53.5 ug /Kg 107 65-130 1,3,5- Trimethylbenzene ND 50.0 52.0 ug /Kg 104 65-135 1,3- Dichlorobenzene ND 50.0 52.9 ug /Kg 106 70-130 1,3- Dichloropropane ND 50.0 50.6 ug /Kg 101 65-140 1,4- Dichlorobenzene ND 50.0 53.5 ug /Kg 107 70-130 2,2- Dichloropropane ND 50.0 59.3 ug /Kg 119 65-150 2- Chlorotoluene ND 50.0 53.5 ug /Kg 107 60 -135 4- Chlorotoluene ND 50.0 55.5 ug /Kg 111 65-135 Benzene ND 50.0 50.8 ug /Kg 102 65-130 Bromobenzene ND 50.0 58.7 ug /Kg 117 65-140 Bromochloromethane ND 50.0 53.9 ug /Kg 108 65-145 Bromodichloromethane ND 50.0 52.9 ug /Kg 106 65-145 Bromoform ND 50.0 58.1 ug /Kg 116 50-145 Bromomethane ND 50.0 55.3 ug /Kg 111 60-155 Carbon tetrachloride ND 50.0 55.2 ug /Kg 110 60-145 Chlorobenzene ND 50.0 48.5 ug /Kg 97 70 -130 Chloroethane ND 50.0 52.7 ug /Kg 105 60-150 Chloroform ND 50.0 52.7 ug /Kg 105 65-135 Chloromethane ND 50.0 46.5 ug /Kg 93 40-145 cis -1,2- Dichloroethene ND 50.0 54.3 ug /Kg 109 65 -135 cis -1,3- Dichloropropene ND 50.0 54.5 ug /Kg 109 70-135 Dibromochloromethane ND 50.0 53.1 ug /Kg 106 60-145 Dibromomethane ND 50.0 53.6 ug /Kg 107 65-140 Dichlorodifluoromethane ND 50.0 43.6 ug /Kg 87 30-160 Isopropyl Ether (DIPS) ND 50.0 54.1 ug /Kg .. 108 . ......... 60-150 Ethanol ND 2000 2090 ug /Kg 104 30-165 Ethyl -t -butyl ether (ETBE) ND 50.0 54.7 ug /Kg 109 60-145 Ethylbenzene ND 50.0 48.4 ug /Kg 97 70-135 Hexachlorobutadiene ND F1 50.0 18.4 F1 ug /Kg 37 50-145 Isopropylbenzene ND 50.0 45.6 ug /Kg 91 70-145 m,p- Xylene ND 50.0 48.3 ug /Kg 97 70-130 Methylene Chloride ND 50.0 50.3 ug /Kg 101 55-145 Methyl -t -Butyl Ether (MTBE) ND 50.0 55.9 ug /Kg 112 55-155 Naphthalene ND 50.0 48.7 ug /Kg 97 40-150 n- Butylbenzene ND 50.0 40.6 ug /Kg 81 55-145 N- Propylbenzene ND 50.0 50.9 ug /Kg 102 65-140 o- Xylene ND 50.0 47.8 ug /Kg 96 65-130 sec - Butylbenzene ND 50.0 42.6 ug /Kg 85 60-135 Styrene ND 50.0 47.6 ug /Kg 95 70-140 Tert- amyl - methyl ether (TAME) ND 50.0 52.8 ug /Kg 106 60-150 tert-Butyl alcohol (TBA) ND 500 548 ug /Kg 110 65-145 tert- Butylbenzene ND 50.0 48.1 ug /Kg 96 60-140 Tetrachloroethene ND 50.0 48.2 ug /Kg 96 65-135 Toluene ND 50.0 50.3 ug /Kg 101 70-130 trans- 1,2- Dichloroethene ND 50.0 56.8 ug /Kg 114 70-135 trans -1,3- Dichloropropene ND 50.0 54.1 ug /Kg 108 60-145 TestAmerica Irvine Page 73 of 87 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440 - 165703 -1 Project/Site: Valero Lab Sample ID: 440- 165703 -A -24 MS Client Sample ID: 4K- S -W -6' Matrix: Solid Prep Type: Total /NA Analysis Batch: 369458 Sample Sample Spike MS MS Spike MSD MSD %Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits Trichooroethene ND 50.0 55.4 ug /Kg 111 65 -140 Trichlorofluoromethane ND 50.0 53.9 ug /Kg 108 55-155 Vinyl chloride ND 50.0 49.6 ug /Kg 99 55-140 p- isopropyltoluene ND 50.0 43.3 ug /Kg 87 60-140 ug /Kg MS MS 40 -160 7 30 1,1,2- Trcchloroethane ND Surrogate %Recovery Qualifier Limits 104 65-140 2 30 Toluene -d8 (Surr) 104 79-123 50.9 ug /Kg 102 65 -135 4- Bromofluorobenzene (Surr) 109 79-120 ND 49.7 51.6 ug /Kg Dibromofluoromethane (Surr) 102 60-120 25 1,1- Dichloropropene ND 49.7 Lab Sample ID: 440- 165703 -A -24 MSD Client Sample ID: 4K- S -W -6' Matrix: Solid Prep Type: Total /NA Analysis Batch: 369458 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit 1,1,1,2- Tetrachloroethane ND 49.7 52.1 ug /Kg 105 65-145 1 20 1,1,1- Tiichooroethane ND 49.7 519 ug /Kg 108 65-145 3 20 1,1,2,2 - Tetrachloroethane ND 49.7 56.1 ug /Kg 113 40 -160 7 30 1,1,2- Trcchloroethane ND 49.7 51.8 ug /Kg 104 65-140 2 30 1,1- Dichloroethane ND 49.7 50.9 ug /Kg 102 65 -135 2 25 1,1- Dichloroethene ND 49.7 51.6 ug /Kg 104 65 -135 1 25 1,1- Dichloropropene ND 49.7 51.4 ug /Kg 103 65 -135 1 20 1,2,3 - Trichlorobenzene ND 49.7 37.1 ug /Kg 75 45 -145 3 30 1,2,3- Trichloropropane ND 49.7 57.9 ug /Kg 116 50-150 5 30 1,2,4- Trichlorobenzene ND 49.7 41.5 ug /Kg 84 50-140 1 30 1,2,4- Trimethylbenzene ND 49.7 49.2 ug /Kg 99 65-140 4 25 1,2- Dibromo -3- Chloropropane ND 49.7 53.0 ug /Kg 107 40-150 10 30 1,2- Dibromoethane (EDB) ND 40 53.2 ug /Kg 107 65 _ 140 2 25 1,2- Dichlorobenzene ND 49.7 51.6 ug /Kg 104 70-130 5 25 1,2- Dichloroethane ND 49.7 50.9 ug /Kg 102 60-150 2 25 1,2- Dichloropropane ND 49.7 52.5 ug /Kg 106 65-130 2 20 1,3,5 - Trimethylbenzene ND 49.7 50.4 ug /Kg 101 65 -135 3 25 1,3- Dichlorobenzene ND 49.7 51.1 ug /Kg 103 70-130 3 25 1,3- Dichloropropane ND 49.7 49.8 ug /Kg 100 65-140 2 25 1,4- Dichlorobenzene ND 49.7 51.4 ug /Kg 103 70-130 4 25 2,2- Dichloropropane ND 49.7 57.3 ug /Kg 115 65-150 3 25 2- Chlorotoluene ND 49.7 51.4 ug /Kg 103 60-135 4 25 4- Chlorotoluene ND 49.7 52.7 ug /Kg 106 65-135 5 25 Benzene ND 49.7 50.6 ug /Kg 102 65-130 0 20 Bromobenzene ND 49.7 55.5 ug /Kg 112 65-140 6 25 Bromochloromethane ND 49.7 53.9 ug /Kg 108 65-145 0 25 Bromodichloromethane ND 49.7 53.4 ug /Kg 107 65-145 1 20 Bromoform ND 49.7 56.7 ug /Kg 114 50-145 2 30 Bromomethane ND 49.7 54.2 ug /Kg 109 60-155 2 25 Carbon tetrachloride ND 49.7 54.9 ug /Kg 110 60-145 1 25 Chlorobenzene ND 49.7 48.6 ug /Kg 98 70-130 0 25 Chloroethane ND 49.7 53.3 ug /Kg 107 60-150 1 25 Chloroform ND 49.7 52.5 ug /Kg 106 65 -135 0 20 TestAmerica Irvine Page 74 of 87 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440 - 165703 -1 Project/Site: Valero 111111q 11111111111111 111111q liq 1111111 11�11iii Lab Sample ID: 440-165703-A-24 MSD Matrix: Solid Analysis Batch: 369458 Sample Sample Analyte Result Qualifier Chloromethane ND cis -1,2- Dichloroethene ND cis -1,3- Dichloropropene ND Dibromochloromethane ND Dibromomethane ND Dichlorodifluoromethane ND Isopropyl Ether (DIPE) ND Ethanol ND Ethyl -t -butyl ether (ETBE) ND Ethylbenzene ND Hexachlorobutadiene ND F1 Isopropylbenzene ND m,p- Xylene ND Methylene Chloride ND Methyl -t -Butyl Ether (MTBE) ND Naphthalene ND n- Butylbenzene ND N- Propylbenzene ND o- Xylene ND sec - Butylbenzene ND Styrene ND Tert- amyl - methyl ether (TAME) ND tert-Butyl alcohol (TBA) ND tent- Butylbenzene ND Tetrachloroethene ND Toluene ND trans -1,2- Dichloroethene ND trans -1,3- Dichloropropene ND Trichloroethene ND Trichlorofluoromethane ND Vinyl chloride ND p- Isopropyltoluene ND Client Sample ID: 4K- S -W -6' Prep Type: Total /NA Spike MSD MSD %Rec. RPD Added Result Qualifier Unit D %Rec Limits RPD Limit 49.7 46.4 ug /Kg 93 40 -145 0 25 493 515 ug /Kg 108 65-135 1 25 49.7 54.5 ug /Kg 110 70-135 0 25 49.7 52.4 ug /Kg 105 60 -145 1 25 49.7 53.0 ug /Kg 107 65-140 1 25 49.7 42.3 ug /Kg 85 30-160 3 35 49.7 54.7 ug /Kg 110 60 -150 1 25 1990 2200 ug /Kg 111 30 -165 5 40 49.7 54.3 ug /Kg 109 60-145 1 30 49.7 47.6 ug /Kg 96 70-135 2 25 49.7 19.1 F1 ug /Kg 38 50-145 4 35 49.7 46.3 ug /Kg 93 70-145 2 25 49.7 47.4 ug /Kg 95 70-130 2 25 49.7 50.2 ug /Kg 101 55-145 0 25 49.7 54.2 ug /Kg 109 55-155 3 35 49.7 46.1 ug /Kg 93 40-150 6 40 49.7 40.3 ug /Kg 81 55-145 1 30 49.7 49.7 ug /Kg 100 65-140 2 25 49.7 48.2 ug /Kg 97 65-130 1 25 49.7 42.2 ug /Kg 85 60-135 1 25 49.7 47.4 ug /Kg 95 70-140 0 25 49.7 53.1 ug /Kg 107 60-150 1 25 497 561 ug /Kg 113 65 -145 2 30 49.7 46.8 ug /Kg 94 60-140 3 25 49.7 47.4 ug /Kg 95 65-135 2 25 49.7 49.5 ug /Kg 100 70-130 2 20 49.7 55.9 ug /Kg 112 70-135 2 25 49.7 53.6 ug /Kg 108 60-145 1 25 49.7 55.0 ug /Kg 111 65-140 1 25 49.7 52.9 ug /Kg 106 55-155 2 25 49.7 48.6 ug /Kg 98 55-140 2 30 49.7 42.5 ug /Kg 85 60-140 2 25 MSD MSD Surrogate %Recovery Qualifier Limits Toluene -d8 (Surr) 103 79-123 4- Bromofluorobenzene (Surr) 107 79-120 Dibromofluoromethane (Surr) 102 60-120 Lab Sample ID: MB 440 - 36945917 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total /NA Analysis Batch: 369459 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Volatile Fuel Hydrocarbons (C4 -C12) ND 0.10 0.070 mg /Kg 11/16/16 08:35 1 Page 75 of 87 TestAmerica Irvine 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440 - 165703 -1 Project/Site: Valero ..... ............................... .............................. ............................... . Method: 2 IC LUFT - Volatile Organic Compounds by C (Continued) Lab Sample ID: MB 440 - 369459/7 MSD MSD Client Sample ID: Method Blank Matrix: Solid Limits Prep Type: Total /NA ::.......... Analysis Batch: 369459 107 79-120 MB MB 79-123 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 13 Dibromofluoromethane (Surr) 110 60-120 11/16/16 08:35 1 4- Bromofluorobenzene (Surr) 102 79-120 11/16/16 08 :35 1 Toluene -d8 (Surr) 106 79-123 11/16/16 08 :35 1 Lab Sample ID: LCS 440- 369459/6 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total /NA Analysis Batch: 369459 El Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Volatile Fuel Hydrocarbons 1.00 0.893 mg /Kg 89 60 -135 (C4-C12) LCS LCS Surrogate %Recovery Qualifier Limits Dibromofluoromethane (Surr) 109 60-120 4- Bromofluorobenzene (Surr) 102 79-120 Toluene -d8 (Surr) 106 79-123 Lab Sample ID: 440 - 165703 -A -24 MS Client Sample ID: 440 - 165703 -A -24 MS Matrix: Solid Prep Type: Total /NA Analysis Batch: 369459 Sample Sample Spike MS MS %Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits Volatile Fuel Hydrocarbons 0.31 3.45 3.45 mg /Kg 91 55-140 (C4 -C12) MS MS Surrogate %Recovery Qualifier Limits Dibromofluoromethane (Surr) 102 60-120 4- Bromofluorobenzene (Surr) 109 79-120 Toluene -d8 (Surr) 104 79-123 Lab Sample ID: 440 - 165703 -A -24 MSD Matrix: Solid Analysis Batch: 369459 Analyte Volatile Fuel Hydrocarbons (C4 -C12) Surrogate Dibromofluoromethane (Surr) 4- Bromofluorobenzene (Surr) Toluene -d8 (Surr) Sample Sample Spike Result Qualifier Added 0.31 3.43 MSD MSD %Recovery Qualifier Limits 102 60-120 107 79-120 103 79-123 Client Sample ID: 440 - 165703 -A -24 MSD Prep Type: Total /NA MSD MSD %Rec. RPD Result Qualifier Unit D %Rec Limits RPD Limit 3.39 mg /Kg 90 55-140 2 25 TestAmerica Irvine Page 76 of 87 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440-165703-1 Project/Site: Valero . . . .. .. . .......... *"*"*"*"* .......................................... . ......... * ..................... ... -------- --- * ................. . ................. ..... . .. . ......... Method: 8015B - Diesel Range Organ ics(DRO)/Oil Range Organics (ORO) Lab Sample ID: MB 440-369289/1-A Matrix: Solid Analysis Batch: 369369 MB MB Analyte Result Qualifier C13 -C22 ND C23-C40 ND Surrogate n-Octacosane Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 369289 RL MDL Unit D Prepared Analyzed Dil Fac 5--0 2.5 mg/Kg 11/15/1613:00 11/15/1622:26 1 5.0 2.5 mg/Kg 11/15/1613:00 11/15/1622:20 1 MB MB %Recovery Qualifier Limits 74 40-140 Lab Sample ID: LCS 440-36928912-A Matrix: Solid Analysis Batch: 369369 Analyte C10 -C28 LCS LCS Surrogate %Recovery Qualifier n-Octacosane 83 Lab Sample ID: 440-165457-A-1-B MS Matrix: Solid Analysis Batch: 369368 Sample Sample Analyte Result Qualifier C10 -C28 140 F1 MS MS Surrogate %Recovery Qualifier n-Octacosane 69 Prepared Analyzed DY Fac 11115116 13:00 11115116 22:20 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 369289 Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits 66.7 53.4 mg/Kg 80 45-115 Limits 40-146 Client Sample ID: Matrix Spike Prep Type: Total/NA Prep Batch: 369289 Spike MS IVIS %Rec. Added Result Qualifier Unit D %Rec Limits 66.5 29-7 f-1— img /Kg — —238 ---40 --120 Limits 40-146 Lab Sample ID: 440-165457-A-1-C MSD Matrix: Solid Analysis Batch: 369368 Sample Sample Spike Analyte Result Qualifier Added C10-C28 140 F1 66.5 MSD MSD Surrogate %Recovery Qualifier Limits n-Octacosane 69 40-140 Method: 6020 - Metals (ICP/MS) Lab Sample ID: MB 440 - 369278/1 -A Matrix: Solid Analysis Batch: 369659 MB MB Analyte Result Qualifier Lead ND Client Sample ID: Matrix Spike Duplicate Prep Type: Total/NA Prep Batch: 369289 MSD MSD %Rec. RPD Result Qualifier Unit D %Rec Limits RPD Limit 259 F1 mg/Kg 182 40-120 13 30 Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 369278 RL MDL Unit D Prepared Analyzed Dil Fac 0.025 0.012 mg/Kg 5/16 12:27 11/16/16 14:26 1 Page 77 of 87 TestAmerica Irvine 11/23/2016 QC Sample Results Client: Advanced Environmental Concepts Inc Project/Site: Valero Lab Sample ID: LCS 440-369278/2-A "20 Matrix: Solid Analysis Batch: 369659 1 Analyte Lead Lab Sample ID: 440-165703-5 MS Matrix: Solid Analysis Batch: 369659 TestAmerica, Job ID: 440-165703-1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 369278 Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits - - 49.5 47.3 mg/Kg 96 ---80 -120 Client Sample ID: 7K-W-2' Prep Type: Total/NA Prep Batch: 369278 Sample Sample Spike ms ms %Rec. I Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits Lead 3.4 50.0 55.3 mg/Kg 104 80-120 Lab Sample ID: 440-165703-5 MSD Matrix: Solid Analysis Batch: 369659 Lead Lab Sample ID: 440-165573-A-1-D MS '20 Matrix: Solid Analysis Batch: 371024 . Spike Added 49.3 Client Sample ID: 7K-W-2' Prep Type: Total/NA Prep Batch: 369278 MSD MSD %Rec. RPD Result Qualifier Unit D %Rec Limits RPD Limit 56.6 mg/Kg 108 80-120 2 20 Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 370377 RL MDL Unit D Prepared Analyzed Dil Fac 0.50 0.25 mg/Kg 11 /19/16 12:00 11/22/16 13:26 20 Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 370377 Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits 50.0 44.9 mg/Kg 90 80-120 Sample Sample Spike MS Ms Analyte Result Qualifier Added Result Qualifier Unit Lead 18 49.8 62.8 mg/Kg Lab Sample ID: 440-165573-A-1 -E MSD A20 Matrix: Solid Analysis Batch: 371024 Sample Sample Analyte Result Qualifier Lead 18 Client Sample ID: Matrix Spike Prep Type: Total/NA Prep Batch: 370377 %Rec. D %Rec Limits 91 80-120 Client Sample ID: Matrix Spike Duplicate Prep Type: Total/NA Prep Batch: 370377 Spike MSD MSD %Rec. RPD Added Result Qualifier Unit D %Rec Limits RPD Limit 49.0 60.2 mg/Kg 87 80-120 4 20 Page 78 of 87 TestAmerica Irvine 11/23/2016 Sample Sample Analyte Result Qualifier Lead 3.4 Lab Sample ID: MB 440-37037711-A ^20 Matrix: Solid Analysis Batch: 371024 MB MB Analyte Result Qualifier Lead ND Lab Sample ID: LCS 440-370377/2-A 120 Matrix: Solid Analysis Batch: 371024 Analyte Lead Lab Sample ID: 440-165573-A-1-D MS '20 Matrix: Solid Analysis Batch: 371024 . Spike Added 49.3 Client Sample ID: 7K-W-2' Prep Type: Total/NA Prep Batch: 369278 MSD MSD %Rec. RPD Result Qualifier Unit D %Rec Limits RPD Limit 56.6 mg/Kg 108 80-120 2 20 Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 370377 RL MDL Unit D Prepared Analyzed Dil Fac 0.50 0.25 mg/Kg 11 /19/16 12:00 11/22/16 13:26 20 Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 370377 Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits 50.0 44.9 mg/Kg 90 80-120 Sample Sample Spike MS Ms Analyte Result Qualifier Added Result Qualifier Unit Lead 18 49.8 62.8 mg/Kg Lab Sample ID: 440-165573-A-1 -E MSD A20 Matrix: Solid Analysis Batch: 371024 Sample Sample Analyte Result Qualifier Lead 18 Client Sample ID: Matrix Spike Prep Type: Total/NA Prep Batch: 370377 %Rec. D %Rec Limits 91 80-120 Client Sample ID: Matrix Spike Duplicate Prep Type: Total/NA Prep Batch: 370377 Spike MSD MSD %Rec. RPD Added Result Qualifier Unit D %Rec Limits RPD Limit 49.0 60.2 mg/Kg 87 80-120 4 20 Page 78 of 87 TestAmerica Irvine 11/23/2016 QC Association Summary Client: Advanced Environmental Concepts Inc Project/Site: Valero Analysis Batch: 369133 Lab Sample ID Client Sample ID 440 - 165703 -1 4K -N -W 2' 440- 165703 -4 4 K- N -E -6' 440 - 165703 -5 7K-W-2' 440 - 165703 -6 7K -W -6' 440 - 165703 -7 7K -E -2' 440 - 165703 -8 7K-E-6' 440 - 165703 -9 D-4 -2' 440 - 165703 -10 D-4-4' 440 - 165703 -11 D -1 -2' 440 - 165703 -12 D -1 -5' 440 - 165703 -13 D -2 -2' 440 - 165703 -14 D -2 -6' 440 - 165703 -15 D -3 -2' 440 - 165703 -16 D -3 -6' MB 440 - 369133/4 Method Blank LCS 440 - 369133/5 Lab Control Sample 440 - 165703 -4 MS 4K- N -E -6' 440 - 165703 -4 MSD 4K- N -E -6' Analysis Batch: 369451 Lab Sample ID Client Sample ID 440 - 165703 -2 4K-WW-6' 440 - 165703 -3 4K- N -E -2' MB 440 - 369451/6 Method Blank ...................... LCS 440- 369451/7 ............ . ......... Lab Control Sample 440 - 165849 -A -5 MS Matrix Spike 440 - 165849 -A -5 MSD Matrix Spike Duplicate Analysis Batch: 369458 I ah Samnla In Miant Samnla In 440 - 165703 -17 440 - 165703 -18 440 - 165703 -19 ........ .. ......... 440 - 165703 -20 440 - 165703 -21 440- 165703 -22 440 - 165703 -23 440 - 165703 -24 MB 440 - 369458/7 LCS 440 - 36945815 440 - 165703 -A -24 MS 440 - 165703 -A -24 MSD Analysis Batch: 369459 Lab Sample ID 440- 165703 -5 440 - 165703 -6 440- 165703 -7 10K -E -2' 10K -E -6' 10K -W 2' 10K -W 6' 4K- S -E -2' 4K- S -E -6' 4K -S -W 2' 4K -S -W 6' Method Blank Lab Control Sample 4K -S -W 6' 4K- S -W-6' TestAmerica Job ID: 440 - 165703 -1 Prep Type M Matrix M Method P Prep Batch Total /NA S Solid 8 82608 Solid Total /NA S Solid 8 8260E 8260B Total/NA S Solid 8 8260B Total /NA Total /NA S Solid 8 82606 Solid Total /NA S Solid 8 8260B 82606 Total /NA S Solid 8 8260B Total /NA Total /NA S Solid 8 8260B Solid Total /NA S Solid 8 8260B 8260B Total /NA S Solid 8 8260B Total /NA S Solid 8 82606 Total /NA S Solid 8 8260B Prep Type Matrix Method Prep Batch Total /NA Solid 8260B Total /NA Solid 8260B Total /NA Solid 8260B Total/NA Solid 8260B Total /NA Solid 8260B Total /NA Solid 8260B Total /NA Solid 82606 Total /NA Solid 82606 Total /NA Solid 8260B Total /NA Solid 8260B Total /NA Solid 8260B Total /NA Solid 8260B Client Sample ID Prep Type Matrix Method Prep Batch 7K-W-2' Total /NA Solid 8260B /CA_LUFT MS 7K-W-6' Total /NA Solid 8260B /CA_LUFT MS 7K -E -2' Total /NA Solid 8260B /CA_LUFT MS TestAmerica Irvine Page 79 of 87 11/23/2016 QC Association Summary Client: Advanced Environmental Concepts Inc Project/Site: Valero V (Continued) Analysis Batch: 369459 (Continued) Lab Sample ID Client Sample ID 440- 165703 -8 7K -E -6' 440 - 165703 -13 D -2 -2' 440 - 165703 -14 D -2 -6' 440 - 165703 -15 D -3 -2' 440 - 165703 -16 D -3 -6' 440 - 165703 -17 10K -E -2' 440- 165703 -18 10K -E -6' 440 - 165703 -19 10K -W 2' 440 - 165703 -20 10K -W -6' MB 440 - 369459/7 Method Blank LCS 440 - 369459/6 440 - 165703 -A -24 MS Lab Control Sample 440 - 165703 -A -24 MS 440- 165703 -A -24 MSD 440- 165703 -A -24 MSD GC Semi VOA ........................... ------.....-...... ............................... Prep Batch: 369289 Prep Type Matrix Method Prep Batch Total /NA Solid 82606 /CA_LUFT 440 - 165703 -1 4K -N -W 2' MS Total /NA Solid 8260B /CA LUFT 440- 165703 -2 4K -N -W 6' MS Total /NA Solid 8260B/CA LUFT 440 - 165703 -3 4K- N -E -2' MS Total /NA Solid 8260B/CA—LUFT 440 - 165703 -4 4K- N -E -6' MS Total /NA Solid 8260B/CA LUFT 440- 165703 -11 D -1 -2' MS Total /NA Solid 8260B /CA LUFT 440 - 165703 -12 D -1 -5' MS Total /NA Solid 82606/CA LUFT � •� E�c 440- 165703 -21 4K- S -E -2' MS Total /NA Solid 8260B /CA LUFT 440- 165703 -22 4K- S -E -6' MS Total /NA Solid 82606 /CA LUFT 440- 165703 -23 4K -S -W 2' MS Total/NA Solid 8260B/CA—LUFT 440- 165703 -24 4K- S -W-6' MS Total /NA Solid 8260B /CA_LUFT 4v=> MB 440 - 369289/1 -A Method Blank MS Total /NA Solid 8260B /CA_LUFT LCS 440 - 369289/2 -A Lab Control Sample MS Total /NA Solid 82606 /CA—LUFT 440- 165457 -A -1 -B MS Matrix Spike MS Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440 - 165703 -1 4K -N -W 2' Total /NA Solid 3546 440- 165703 -2 4K -N -W 6' Total /NA Solid 3546 440 - 165703 -3 4K- N -E -2' Total /NA Solid 3546 440 - 165703 -4 4K- N -E -6' Total /NA Solid 3546 440- 165703 -11 D -1 -2' Total /NA Solid 3546 440 - 165703 -12 D -1 -5' Total /NA Solid 3546 440- 165703 -21 4K- S -E -2' Total /NA Solid 3546 440- 165703 -22 4K- S -E -6' Total /NA Solid 3546 440- 165703 -23 4K -S -W 2' Total /NA Solid 3546 440- 165703 -24 4K- S -W-6' Total /NA Solid 3546 MB 440 - 369289/1 -A Method Blank Total /NA Solid 3546 LCS 440 - 369289/2 -A Lab Control Sample Total /NA Solid 3546 440- 165457 -A -1 -B MS Matrix Spike Total /NA Solid 3546 440 - 165457 -A -1 -C MSD Matrix Spike Duplicate Total/NA Solid 3546 Analysis Batch: 369368 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440 - 165703 -4 4K- N -E -6' Total /NA Solid 8015B 369289 440- 165703 -11 D -1 -2' Total /NA Solid 8015B 369289 440- 165703 -12 D -1 -5' Total /NA Solid 80156 369289 440- 165703 -21 4K- S -E -2' Total /NA Solid 8015B 369289 440 - 165703 -22 4K- S -E-6' Total /NA Solid 8015B 369289 440 - 165703 -24 4K -S -W 6' Total /NA Solid 80156 369289 TestAmerica Irvine Page 80 of 87 11/23/2016 QC Association Summary Client: Advanced Environmental Concepts Inc Project/Site: Valero �: • T� Analysis Batch: 369368 (Continued) Lab Sample ID Client Sample ID 440- 165457 -A -1 -B MS Matrix Spike 440- 165457 -A -1 -C MSD Matrix Spike Duplicate Analysis Batch: 369369 Total /NA Lab Sample ID Client Sample ID MB 440 - 369289/1 -A Method Blank LCS 440 - 369289/2 -A Lab Control Sample Analysis Batch: 369684 TestAmerica Job ID: 440 - 165703 -1 Prep Type Matrix Method Total /NA Solid 8015B Total /NA Solid 8015B Prep Type Matrix Method Total /NA Solid 8015B Total /NA Solid 8015B Pren Batch 3oaZoa 369289 Prep Batch 369289 369289 ? Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440- 165703 -1 4K-WW-2' Total /NA Solid 8015B 369289 440 - 165703 -2 4K -N -W 6' Total/NA Solid 80156 369289 440 - 165703 -3 4K- N -E -2' Total /NA Solid 8015B 369289 440 - 165703 -23 4K- S -W -2' Total /NA Solid 8015B 369289 Prep Batch: 369278 Lab Sample ID 440 - 165703 -5 440 - 165703 -6 440 - 165703 -7 440 - 165703 -8 440 - 165703 -9 440 - 165703 -13 440 - 165703 -14 440 - 165703 -15 440 - 165703 -16 440 - 165703 -17 440 - 165703 -18 440- 165703 -19 440 - 165703 -20 M B 440 - 369278/1 -A LCS 440 - 369278/2 -A ^20 440 - 165703 -5 MS 440 - 165703 -5 MSD Analysis Batch: 369659 Lab Sample ID 440 - 165703 -5 440 - 165703 -6 440 - 165703 -7 440 - 165703 -8 440 - 165703 -9 440 - 165703 -13 440 - 165703 -14 440 - 165703 -15 440 - 165703 -16 440 - 165703 -17 440 - 165703 -18 Client Sample ID Prep Type Matrix Method Prep Batch 7K-W-2' Total /NA Solid 3050B 7K-W-6' Total /NA Solid 3050B 7K -E -2' Total /NA Solid 3050B 7K -E -6' Total /NA Solid 3050B D-4 -2' Total /NA Solid 3050B D -2 -2' Total /NA Solid 3050B D -2 -6' Total /NA Solid 30508 D -3 -2' Total /NA Solid 30506 D -3 -6' Total /NA Solid 3050B 10K -E -2' Total /NA Solid 3050B 10K -E -6' Total /NA Solid 3050B 10K -W 2' Total /NA Solid 30506 10K -W 6' Total /NA Solid 3050B Method Blank Total /NA Solid 3050B Lab Control Sample Total /NA Solid 3050B 7K -W -2' Total /NA Solid 3050B 7K-W-2' Total /NA Solid 3050B Client Sample ID 7K-W-2' 7K-W-6' 7K -E -2' 7K -E -6' D-4 -2' D -2 -2' D -2 -6' D -3 -2' D -3 -6' 10K -E -2' 10K -E -6' Prep Type Matrix Method Prep Batch Total /NA Solid 6020 369278 Total /NA Solid 6020 369278 Total /NA Solid 6020 369278 Total /NA Solid 6020 369278 Total /NA Solid 6020 369278 Total /NA Solid 6020 369278 Total /NA Solid 6020 369278 Total /NA Solid 6020 369278 Total /NA Solid 6020 369278 Total /NA Solid 6020 369278 Total /NA Solid 6020 369278 TestAmerica Irvine Page 81 of 87 11/23/2016 QC Association Summary Client: Advanced Environmental Concepts Inc TestAmerica Job ID: 440 - 165703 -1 Project/Site: Valero Metals (Continued) ..................... Analysis Batch: 369659 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440 - 165703 -19 10K -W -2' Total /NA Solid 6020 369278 440 - 165703 -20 10K -W 6' Total/NA Solid 6020 369278 MB 440 - 369278/1 -A Method Blank Total /NA Solid 6020 369278 LCS 440 - 369278/2 -A "20 Lab Control Sample Total /NA Solid 6020 369278 440- 165703 -5 MS 7K-W-2' Total /NA Solid 6020 369278 440- 165703 -5 MSD 7K -W -2' Total /NA Solid 6020 369278 Prep Batch: 370377 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440- 165703 -10 D-4-4' Total /NA Solid 30508 MB 440 - 370377/1 -A ^20 Method Blank Total /NA Solid 30506 LCS 440 - 370377/2 -A ^20 Lab Control Sample Total /NA Solid 3050B LID, 440- 165573 -A -1 -D MS ^20 Matrix Spike Total /NA Solid ....... 3050B .......... 440 - 165573 -A -1 -E MSD ^20 Matrix Spike Duplicate Total /NA Solid 3050B Analysis Batch: 371024 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 440- 165703 -10 D-4-4' Total /NA Solid 6020 370377 MB 440 - 370377/1 -A ^20 Method Blank Total /NA Solid 6020 370377 - -' LCS 440-370377/2-AA 20 Lab Control Sample Total /NA Solid 6020 370377 440 - 165573 -A -1 -D MS ^20 Matrix Spike Total /NA Solid 6020 370377 440 - 165573 -A -1 -E MSD ^20 Matrix Spike Duplicate Total /NA Solid 6020 370377 TestAmerica Irvine Page 82 of 87 11/23/2016 Definitions /Glossary `. Client: Advanced Environmental Concepts Inc Project/Site: Valero TestAmerica Job ID: 440 - 165703 -1 GC /IVIS VOA Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. F1 MS and /or MSD Recovery is outside acceptance limits. GC Semi VOA Qualifier Qualifier Description F1 MS and /or MSD Recovery is outside acceptance limits. Glossary Abbreviation These commonly used abbreviations may or may not be present in this report XX Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference) Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re- analysis, Re- extraction, or additional Initial metals /anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TestAmerica Irvine Page 83 of 87 11/23/2016 Z 0 vI 0 0 cc$ m L-61 ammi go cl ;fir r tN Page 85 of 87 or 2 0. E "a 0 c 6= Oe 0 r .0 3 11/23/2016 a ri E E E 0 U II cd C (D cts z Al ON M > 'a :3 ED zs LO m CO aL a vi 0 �r —0 CO 6 LLJ . c m E 0 Z c 0 0 co D 0 Z M a) E cr < cr) m .9 cts z Z Ir D cr Z ca a iD cu CL U) a. w rt 0 CM ci UJ rZ iu cc E F- Cd z OL Ix Z 0 ai N 2 cc %q Cc -W LL z 0 E C.) A J2 .0 uj 10 ai ca cc to ;z —mw m �ncc—:) 65 iti z 6s 03 C LU CL E 0 cc uj m D ir 0 d CL WOW Cl) 0 a. z 1: _0 O 10 .0— Z 0 --..i b 0 > Ol Iz 0O xd .dw I LL z cr w r4 N ZZI CA CL E Cl) E I 7:S- cc Cl) 0 V ai IL Z E Cz, g aw- Z Cl 12 cr c d ct 05 is :E cm co 17 1!�2 1!�2 Page 85 of 87 or 2 0. E "a 0 c 6= Oe 0 r .0 3 11/23/2016 a 0 O Z mc 0 —j tts a_ co Im Lm 0 0 4) 0 Yl 0 cc 0 apswit oat o�� Page 86 of 87 11/23/2016 t CA CL E I 10 0 W IL 0 4 40 r- 4.1 • co cu • • z LO • z • ■ NNEMEMEM MENEM MOMMOMEM ■■M■M■■■■E■■■■.I cm �.N.■MUNEW■■■■■■ • • lat 1- El It `v, tit _ - Fin- 904 9 Ira" Page 86 of 87 11/23/2016 t CA CL E I 10 0 W IL 0 4 40 r- Client: Advanced Environmental Concepts Inc Login Number: 165703 List Number: 1 Creator: Chavez, Yonny 1 Question Login Sample Receipt Checklist Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey True meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. False Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date /times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS /MSDs Containers requiring zero headspace have no headspace or bubble is True <6mm (1/4 "). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A TestAmerica Irvine Page 87 of 87 11/23/2016