The URL can be used to link to this page

Home My WebLink About1415 truxtun soil report 2014am TT I NAME M. LO ED SER710E ADDRESS 4750 BURR STRUT CITY, STATE, ZIP BAKERSIFIELD CA 93309 PHONE NO. 661 588-6410 <Zre, "7 TRUCK, UNIT, I.D. NO. TYPED OR PR FULL NAME &goTA_fb_ RE' SERVICE ORDER NO. PICK UP DATE NAME MMT TRICK WASTE LAMIUL Pmfile id; SM414 CA DISPOSAL METHOD ADDRESS M533 HIGHWAY 2 MST DISPOSAL LANDFILL ❑ OTHER CITY, STATE, ZIP McMTTRJCK CA 93251 PHONE NO. -27- DATE k 4 tq OR PRINTED FULL NAME & Si NATURE DATE GEN OLD/NEW 098875 TONS NON-HAZARDOUS WASTE DATA FORM s B C/Q KERN COUNTY Attn: DENNIS BOLENDER HWDF NONE NAME 1116 TRU)(TON AVE., 3RD FL. ADDRESS BAKERSFIELD, CA 93301 CITY, STATE, ZIP PHONE NO. 661 8&-3 000 It '1 0 1 CONTAINERS: NO. VOLUME WEIGHT Tons Lli Z TANK TYPE: Ei TRUCK ❑ TEWUMCPK ❑ DRUMS ❑ CARTONS ❑ OTHER Lli WASTE DESCRIPTION DOTY UNDMROUND STORAGE TMK GENERATING PROCESS PMAOVAL OF CLEUM UST COMPONENTS OF WASTE PPM % COMPONENTS OF WASTE PPM % UJI 1. PMERGLASS 100 5. Lu .j 2. 6. CL 2 o 3. 7. 0 Lu 4. 8. Im 0 PROPERTIES: pH ❑ StLID ❑ LIQUID ❑ SLUDGE ❑ SLURRY ❑ OTHER HANDLING INSTRUCTIONS: AVOID EYE CONTACT & VVEAR RUBBER GLOVES Fadhi-a- ERG 126 KBU�OUNTY GENERAL WAYNE PERRY CONTRACTOR: SERVICES % qlZ-71 1415 TRUXTUN MENU BAKERSFIELD, CA 93301 TYPED OR PRINTED FL�L NAME 81SIGNATUR EK / D am TT I NAME M. LO ED SER710E ADDRESS 4750 BURR STRUT CITY, STATE, ZIP BAKERSIFIELD CA 93309 PHONE NO. 661 588-6410 <Zre, "7 TRUCK, UNIT, I.D. NO. TYPED OR PR FULL NAME &goTA_fb_ RE' SERVICE ORDER NO. PICK UP DATE NAME MMT TRICK WASTE LAMIUL Pmfile id; SM414 CA DISPOSAL METHOD ADDRESS M533 HIGHWAY 2 MST DISPOSAL LANDFILL ❑ OTHER CITY, STATE, ZIP McMTTRJCK CA 93251 PHONE NO. -27- DATE k 4 tq OR PRINTED FULL NAME & Si NATURE DATE GEN OLD/NEW L A TONS TRANS s B C/Q RT/CD HWDF NONE DISCREPANCY RDICDEEIVING SITE (DOPY, Laboratories Inc. Environmental Testing Laboratory Since 1949 Date of Report: 05/27/2016 Janet Crane Crane's Waste Oil Inc. 15412 Hwy 178 Weldon, CA 93283 Client Project: KCOS BCL Project: Misc Samples BCL Work Order: 1613800 Invoice ID: 6236412 Enclosed are the results of analyses for samples received by the laboratory on 5/17/2016. If you have any questions concerning this report, please feel free to contact me. Sincerely, Contact Person: Vanessa Sandoval Client Service Rep 000000, Authorized Signature Certifications: CAELAP#1186; NV#CA00014; OR ELAP #4032 -001; AKUST101 The results in. this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 - 1 . 1 4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 1 of 33 Laboratories Inc. Iiul, Environmental Testing Laboratory Since 1949 Chain of Custody and Cooler Receipt Form for 1613800 Page 1 of 3 i i f g R O U I ctS � 3 .fl , I 00 MEN MENNEMENEEN N M �O w 1 � I �j N r ri cc � I GU ®rNMONEEMENNEEN 01 M KINNOMENNEEMEN MMEENNOMEMOMEN cn CL w f y I 0 I W U fr pot d ftS a +p 0 a i The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.bclabs.com page 3 of 33 s ■ - I i i f g R O U I ctS � 3 .fl , I 00 MEN MENNEMENEEN N M �O w 1 � I �j N r ri cc � I GU ®rNMONEEMENNEEN 01 M KINNOMENNEEMEN MMEENNOMEMOMEN cn CL w f y I 0 I W U fr pot d ftS a +p 0 a i The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.bclabs.com page 3 of 33 Laboratories Inc. I. t Environmental Testing Laboratory Since 1949 Chain of Custody and Cooler Receipt Form for 1613800 Page 3 of 3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.bclabs.com Page 5 of 33 Ln 57 a ru M a O C. M Mi. rip, G xs; a n n 3 N "mot Y v V < 0 ; n a n C T�Ywb't' "yi ID TL > Cj N N iY 7 77 10 Cr N V .]nary 3 n S Sal O tU C O M (A H < N ♦�'��rt��ri'i+.�J g' y. .4?�., .'. f s �w y1 m m < S ae Ln d: 1 fix 4 ? x M yy� a � +r w c`�i � � {• t, Ott { a [PA. r+w. , . , a L a' C rfi O ! r'Nrs f,,: 2. " G { N '^ L C n i ' ip �7 vii D Q. n C uroi SM "' •� A S O a V 1 t4k�ti 'G ar in A o ^ 2 n= �, n 3 rb z O c T w o, w LI 1 H a P yR.:�n0 t i ytt. Ftt:: k]' it fii." )�j�•4F �S,WAfRS.t T t�K' A ]'le i Y} 11 i f ;rl}l - -.A CC! F� Z,!'S .f' }t,y �CiM+� The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.bclabs.com Page 5 of 33 in Laboratories Inc. Environmental Testing Laboratory Since 1949 Crane's Waste Oil Inc. Reported: 05/27/2016 16:52 15412 Hwy 178 Project: Misc Samples Weldon, CA 93283 Project Number: KCOS Project Manager: Janet Crane Total Petroleum Hydrocarbons BCL Sample ID: 1613800 -01 Client Sample Name: Waste Water, 5/17/2016 11:50:OOAM, Chris G. MB Lab Constituent Result Units PQL MDL Method Bias Qualls Run # TPH - Light Naptha ND ug /L 500 200 EPA -8015B /FFP ND TPH - Aviation Gas ND ug /L 500 200 EPA -80158 /FFP ND TPH - Stoddard Solvent ND ug /L 200 100 EPA - 80158 /FFP ND TPH - Heavy Naptha ND ug /L 200 100 EPA - 8015E /FFP ND TPH - Gasoline ND ug /L 500 200 EPA -80158 /FFP ND 1 TPH - Jet Fuel (JP4) ND ug /L 200 100 EPA -80158 /FFP ND 1 TPH - Jet Fuel (JP5) ND ug /L 200 130 EPA -8015B /FFP ND TPH - Jet Fuel (JP8) ND ug /L 200 100 EPA -80158 /FFP ND TPH - Kerosene ND ug /L 200 57 EPA -80158 /FFP ND TPH - Diesel (FFP) ND ug /L 200 34 EPA -8015B /FFP ND TPH - Fuel Oil #6 ND ug /L 50 25 EPA -80158 /FFP ND TPH - Crude Oil 8800 ug /L 500 140 EPA -80158 /FFP ND A56 1 TPH - Hydraulic Oil / Motor Oil ND ug /L 500 66 EPA -80158 /FFP ND TPH - WD -40 ND ug /L 200 100 EPA -80158 /FFP ND 1 Tetracosane (Surrogate) 85.0 % 40-140 (LCL - UCL) EPA -8015B /FFP Run # Method Prep Date Run Date/Time Analyst Instrument Dilution QC Batch ID 1 EPA -80158 /FFP 05/18/16 05/20/16 11:43 AS1 GC -2 1 BZE1980 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.bclabs.com Page 7 of 33 :Z& Laboratories Inc. Environmental Testing Laboratory Since 1949 Crane's Waste Oil Inc. Reported: 05/27/2016 16:52 15412 Hwy 178 Project: Misc Samples Weldon, CA 93283 Project Number: KCOS Project Manager: Janet Crane Water Analysis (General Chemistry) BCL Sample ID: 1613800 -01 Client Sample Name: Waste Water, 5/17/2016 11:50:OOAM, Chris G. MB Lab Constituent Result Units PQL MDL Method Bias Quals Run # Total Calcium 69 mg /L 0.10 0.015 EPA -6010B 0.031 1 Total Magnesium 7.2 mg /L 0.050 0.019 EPA -6010B ND Total Sodium 69 mg /L 0.50 0.051 EPA -6010B ND 1 Total Potassium 6.5 mg /L 1.0 0.13 EPA -60108 ND 1 EPA -6010B 05/24/16 05/24/16 20:08 JCC PE -OP3 1 BZE2275 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.belabs.com Page 9 of 33 Laboratories Inc. Environmental Testing Laboratory Since 1949 Crane's Waste Oil Inc. Reported: 05/27/2016 16:52 15412 Hwy 178 Project: Misc Samples Weldon, CA 93283 Project Number: KCOS Project Manager: Janet Crane Volatile Organic Analysis (EPA Method 82608) BCL Sample ID: 1613800 -02 Client Sample Name: Solids W /Sludge, 5/17/2016 11:55:OOAM, Chris G. MB Lab Constituent Result Units PQL MDL Method Bias Quals Run # Benzene ND mg /kg 0.0050 0.0013 EPA -8260B ND Bromobenzene ND mg /kg 0.0050 0.0013 EPA -82606 ND 1 Bromochloromethane ND mg /kg 0.0050 0.00092 EPA -8260B ND 1 Bromodichloromethane ND mg /kg 0.0050 0.00084 EPA -8260B ND Bromoform ND mg /kg 0.0050 0.0015 EPA -8260B ND Bromomethane ND mg /kg 0.0050 0.0016 EPA -8260B ND 1 n- Butylbenzene 0.0074 mg /kg 0.0050 0.0015 EPA -8260B ND sec - Butylbenzene ND mg/kg 0.0050 0.0012 EPA -82606 ND tert - Butylbenzene ND mg /kg 0.0050 0.0012 EPA -8260B ND Carbon tetrachloride ND mg /kg 0.0050 0.0011 EPA -8260B ND 1 Chlorobenzene ND mg /kg 0.0050 0.0013 EPA -82606 ND 1 Chloroethane ND mg/kg 0.0050 0.0014 EPA -8260B ND 1 Chloroform ND mg /kg 0.0050 0.00063 EPA -8260B ND Chloromethane ND mg /kg 0.0050 0.0014 EPA -8260B ND 2- Chlorotoluene ND mg /kg 0.0050 0.0018 EPA -8260B ND 4- Chlorotoluene ND mg /kg 0.0050 0.0014 EPA -8260B ND Dibromochloromethane ND mg /kg 0.0050 0.00099 EPA -82606 ND 1,2- Dibromo- 3- chloropropane ND mg /kg 0.0050 0.0017 EPA -8260B ND 1,2- Dibromoethane ND mg /kg 0.0050 0.0010 EPA -82608 ND Dibromomethane ND mg /kg 0.0050 0.0018 EPA -8260B ND 1,2- Dichlorobenzene ND mg /kg 0.0050 0.00081 EPA -82606 ND 1,3- Dichlorobenzene ND mg /kg 0.0050 0.0014 EPA -8260B ND 1,4- Dichlorobenzene ND mg /kg 0.0050 0.0015 EPA -82606 ND Dichlorodifluoromethane ND mg /kg 0.0050 0.0013 EPA -8260B ND 1, 1 -Dichloroethane ND mg /kg 0.0050 0.0014 EPA -8260B ND 1,2- Dichloroethane ND mg /kg 0.0050 0.00085 EPA -8260B ND 1, 1 -Dichloroethene ND mg /kg 0.0050 0.0012 EPA -8260B ND cis -1,2- Dichloroethene ND mg /kg 0.0050 0.0013 EPA -8260B ND trans -1,2- Dichloroethene ND mg /kg 0.0050 0.0014 EPA -8260B ND 1,2- Dichloropropane ND mg /kg 0.0050 0.00081 EPA -82606 ND 1,3- Dichloropropane ND mg /kg 0.0050 0.0011 EPA -8260B ND 2,2- Dichloropropane ND mg /kg 0.0050 0.0013 EPA -8260B ND 1,1- Dichloropropene ND mg /kg 0.0050 0.0012 EPA -8260B ND The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.bclabs.com Page 11 of 33 :Z& Laboratories Inc. Environmental Testing Laboratory Since 1949 Crane's Waste Oil Inc. Reported: 05/27/2016 16:52 15412 Hwy 178 Project: Misc Samples Weldon, CA 93283 Project Number: KCOS Project Manager: Janet Crane Volatile Organic Analysis (EPA Method 826013) BCL Sample ID: 1613800 -02 Client Sample Name: Solids W /Sludge, 5/17/2016 11:55:OOAM, Chris G. Run QC Run # Method Prep Date Date/Time Analyst Instrument Dilution Batch ID 1 EPA -82608 05/18116 05/18/16 12:55 MRF MS -V3 1 BZE1354 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.bc[abs.com Page 13 of 33 :Z& Laboratories Inc. Environmental Testing Laboratory Since 1949 Crane's Waste Oil Inc. Reported: 05/27/2016 16:52 15412 Hwy 178 Project: Misc Samples Weldon, CA 93283 Project Number: KCOS Project Manager: Janet Crane EPA Method 1664 BCL Sample ID: 1613800 -02 Client Sample Name: Solids W /Sludge, 5/17/2016 11:55:OOAM, Chris G. MB Lab Constituent Result Units PQL MDL Method Bias Qualls Run # Oil and Grease 68000 mg /kg 1700 470 EPA -1664A HEM ND 1 Run QC Run # Method Prep Date Date/Time Analyst Instrument Dilution Batch ID 1 EPA -1664A HEM 05/19/16 05/19/16 14:00 MAM MAN -SV 33.333 BZE2387 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.bclabs.com Page 15 of 33 :I& Laboratories Inc. Ulu, Environmental Testing Laboratory Since 1949 Crane's Waste Oil Inc. Reported: 05/27/2016 16:52 15412 Hwy 178 Project: Misc Samples Weldon, CA 93283 Project Number: KCOS Project Manager: Janet Crane Volatile Organic Analysis (EPA Method 826013) Quality Control Report - Method Blank Analysis Constituent QC Sample ID MB Result Units PQL MDL Lab Quals QC Batch ID: BZE1354 trans- 1,3- Dichloropropene BZE1354 -BLK1 ND mg /kg 0.0050 0.0012 Ethylbenzene BZE1354 -BLK1 ND mg /kg 0.0050 0.0015 Hexachlorobutadiene BZE1354 -BLK1 ND mg /kg 0.0050 0.0017 Isopropylbenzene BZE1354 -BLK1 ND mg /kg 0.0050 0.0013 p- Isopropyltoluene BZE1354 -BLK1 ND mg /kg 0.0050 0.0013 Methylene chloride BZE1354 -BLK1 ND mg /kg 0.010 0.0024 Methyl t -butyl ether BZE1354 -BLK1 ND mg /kg 0.0050 0.00050 Naphthalene BZE1354 -BLK1 ND mg /kg 0.0050 0.0014 n- Propylbenzene BZE1354 -BLK1 ND mg /kg 0.0050 0.0013 Styrene BZE1354 -BLK1 ND mg /kg 0.0050 0.0014 1, 1, 1,2-Tetrachloroethane BZE1354 -BLK1 ND mg /kg 0.0050 0.0011 1,1,2,2 - Tetrachloroethane BZE1354 -BLK1 ND mg /kg 0.0050 0.0011 Tetrachloroethene BZE1354 -BLK1 ND mg /kg 0.0050 0.0013 Toluene BZE1354 -BLK1 ND mg /kg 0.0050 0.0012 1,2,3 - Trichlorobenzene BZE1354 -BLK1 ND mg /kg 0.0050 0.0021 1,2,4 - Trichlorobenzene BZE1354 -BLK1 ND mg/kg 0.0050 0.0020 1, 1, 1 -Trichloroethane BZE1354 -BLK1 N D mg /kg 0.0050 0.0011 1,1,2 - Trichloroethane BZE1354 -BLK1 ND mg /kg 0.0050 0.00077 Trichloroethene BZE1354 -BLK1 ND mg /kg 0.0050 0.0011 Trichlorofluoromethane BZE1354 -BLK1 ND mg /kg 0.0050 0.0011 1,2,3- Trichloropropane BZE1354 -BLK1 ND mg /kg 0.0050 0.0016 1,1,2 - Trichloro- 1,2,2- trifluoroethane BZE1354 -BLK1 ND mg /kg 0.0050 0.0013 1,2,4 - Trimethylbenzene BZE1354 -BLK1 ND mg /kg 0.0050 0.0013 1,3,5- Trimethylbenzene BZE1354 -BLK1 ND mg /kg 0.0050 0.0015 Vinyl chloride BZE1354 -BLK1 ND mg /kg 0.0050 0.0016 Total Xylenes BZE1354 -BLK1 ND mg /kg 0.010 0.0034 p- & m- Xylenes BZE1354 -BLK1 ND mg /kg 0.0050 0.0022 o- Xylene BZE1354 -BLK1 ND mg /kg 0.0050 0.0012 1,2- Dichloroethane -d4 (Surrogate) BZE1354 -BLK1 106 % 70 -121 (LCL - UCL) Toluene -d8 (Surrogate) BZE1354 -BLK1 106 % 81 -117 (LCL - UCL) 4- Bromofluorobenzene (Surrogate) BZE1354 -BLK1 99.2 % 74 -121 (LCL - UCL) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.bclabs.com Page 17 of 33 :Z& Laboratories Inc. Environmental Testing Laboratory Since 1949 Crane's Waste Oil Inc. Reported: 05/27/2016 16:52 15412 Hwy 178 Project: Misc Samples Weldon, CA 93283 Project Number: KCOS Project Manager: Janet Crane Volatile Organic Analysis (EPA Method 82.608) Quality Control Report - Precision & Accuracy Control Limits Source Source Spike Percent Percent Lab Constituent Type Sample ID Result Result Added Units RPD Recovery RPD Recovery Qualls The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.bclabs.com Page 19 of 33 QC Batch ID: BZE1364 I Used client sample: N Benzene MS 1612122 -09 ND 0.097280 0.12500 mg /kg 77.8 70-130 MSD 1612122 -09 ND 0.10692 0.12500 mg /kg 9.4 85.5 20 70-130 Bromodichloromethane MS 1612122 -09 ND 0.10551 0.12500 mg /kg 84.4 70-130 MSD 1612122 -09 ND 0.12254 0.12500 mg /kg 14.9 98.0 20 70-130 Chlorobenzene MS 1612122 -09 ND 0.10238 0.12500 mg /kg 81.9 70-130 MSD 1612122 -09 ND 0.11244 0.12500 mg /kg 9.4 90.0 20 70-130 Chloroethane MS 1612122 -09 ND 0.095150 0.12500 mg /kg 76.1 70-130 MSD 1612122 -09 ND 0.10436 0.12500 mg /kg 9.2 83.5 20 70-130 1,4- Dichlorobenzene MS 1612122 -09 ND 0.10138 0.12500 mg /kg 81.1 70-130 MSD 1612122 -09 ND 0.11619 0.12500 mg /kg 13.6 93.0 20 70-130 1, 1 -Dichloroethane MS 1612122 -09 ND 0.099540 0.12500 mg /kg 79.6 70-130 MSD 1612122 -09 ND 0.10760 0.12500 mg /kg 7.8 86.1 20 70-130 1,1- Dichloroethene MS 1612122 -09 ND 0.087420 0.12500 mg /kg 69.9 70-130 MSD 1612122 -09 ND 0.096340 0.12500 mg /kg 9.7 77.1 20 70-130 Toluene MS 1612122 -09 ND 0.10411 0.12500 mg /kg 83.3 70-130 MSD 1612122 -09 ND 0.11907 0.12500 mg /kg 13.4 95.3 20 70-130 Trichloroethene MS 1612122 -09 ND 0.10157 0.12500 mg /kg 81.3 70-130 MSD 1612122 -09 ND 0.12067 0.12500 mg /kg 17.2 96.5 20 70-130 1,2- Dichloroethane -d4 (Surrogate) MS 1612122 -09 ND 0.051580 0.050000 mg /kg 103 70-121 MSD 1612122 -09 ND 0.050870 0.050000 mg /kg 1.4 102 70-121 Toluene -d8 (Surrogate) MS 1612122 -09 ND 0.051040 0.050000 mg /kg 102 81-117 MSD 1612122 -09 ND 0.053970 0.050000 mg /kg 5.6 108 81 - 117 4- Bromofluorobenzene (Surrogate) MS 1612122 -09 ND 0.053490 0.050000 mg /kg 107 74-121 MSD 1612122 -09 ND 0.050260 0.050000 mg /kg 6.2 101 74-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.bclabs.com Page 19 of 33 :2& Laboratories Inc. Environmental Testing Laboratory Since 1949 Crane's Waste Oil Inc. Reported: 05/27/2016 16:52 15412 Hwy 178 Project: Misc Samples Weldon, CA 93283 Project Number: KCOS Project Manager: Janet Crane Total Petroleum Hydrocarbons Quality Control Report - Laboratory Control Sample Control Limits Spike Percent Percent Lab Constituent QC Sample ID Type Result Level Units Recovery RPD Recovery RPD Quals QC Batch ID: BZE1980 TPH - Diesel (FFP) BZE1980 -BS1 LCS 2007.6 2500.0 ug /L 80.3 52-128 Tetracosane (Surrogate) BZE1980 -BS1 LCS 74.850 100.00 ug /L 74.8 40-140 QC Batch ID: BZE2145 TPH - Diesel (FFP) BZE2145 -BSI LCS 66.587 81.967 mg /kg 81.2 64-124 Tetracosane (Surrogate) BZE2145 -BS1 LCS 2.8438 3.2787 mg /kg 86.7 30-130 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.bclabs.com Page 21 of 33 Laboratories Inc. Environmental Testing Laboratory Since 1949 Crane's Waste Oil Inc. Reported: 05/27/2016 16:52 15412 Hwy 178 Project: Misc Samples Weldon, CA 93283 Project Number: KCOS Project Manager: Janet Crane EPA Method 1664 Quality Control Report - Method Blank Analysis Constituent QC Sample ID MB Result Units PQL IVIDL Lab Quals QC Batch ID: BZE2187 Oil and Grease BZE2187 -BLK1 ND mg /L 5.0 0.76 QC Batch ID: BZE23$7 Oil and Grease BZE2387 -BLK1 ND mg /kg 50 14 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting parry. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.bolabs.com Page 23 of 33 :Z& Laboratories Inc. Environmental Testing Laboratory Since 1949 Crane's Waste Oil Inc. Reported: 05/27/2016 16:52 15412 Hwy 178 Project: Misc Samples Weldon, CA 93283 Project Number: KCOS Project Manager: Janet Crane EPA Method 1664 Quality Control Report - Precision & Accuracy Control Limits Source Source Spike Percent Percent Lab Constituent Type Sample ID Result Result Added Units RPD Recovery RPD Recovery Qualls QC Batch ID: BZE2187 Used client sample: N Oil and Grease DUP 1612122 -14 ND ND mg /L 18 MS 1612122 -14 ND 39.000 42.700 mg /L 91.3 78-114 MSD 1612122 -14 ND 38.950 42.700 mg /L 0.1 91.2 18 78-114 QC Batch ID: BZE2387 Used client sample: N Oil and Grease DUP 1612122 -42 ND ND mg /kg 30 MS 1612122 -42 ND 788.42 806.39 mg /kg 97.8 56-111 MSD 1612122 -42 ND 773.45 806.39 mg /kg 1.9 95.9 30 56-111 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.bclabs.com Page 25 of 33 :Z& Laboratories, Inc. Environmental Testing Laboratory Since 1949 Crane's Waste Oil Inc. Reported: 05/27/2016 16:52 15412 Hwy 178 Project: Misc Samples Weldon, CA 93283 Project Number: KCOS Project Manager: Janet Crane Water Analysis (General Chemistry) Quality Control Report - Laboratory Control Sample Control Limits Spike Percent Percent Lab Constituent QC Sample ID Type Result Level Units Recovery RPD Recovery RPD Quals QC Batch ID: BZE2275 Total Calcium BZE2275 -BS1 LCS 10.739 10.000 mg /L 107 85-115 Total Magnesium BZE2275 -BS1 LCS 10.855 10.000 mg /L 109 85-115 Total Sodium BZE2275 -BS1 LCS 10.681 10.000 mg /L 107 85-115 Total Potassium BZE2275 -BS1 LCS 10.265 10.000 mg /L 103 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.bclabs.com Page 27 of 33 :Z& Laboratories Inc. Environmental Testing Laboratory Since 1949 Crane's Waste Oil Inc. Reported: 05/27/2016 16:52 15412 Hwy 178 Project: Misc Samples Weldon, CA 93283 Project Number: KCOS Project Manager: Janet Crane The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.bclabs.com Page 29 of 33 Metals Analysis Quality Control Report - Method Blank Analysis Constituent QC Sample ID MB Result Units PQL MDL Lab Quals QC Batch ID: BZE2241 Total Mercury BZE2241 -BLK1 ND ug /L 0.20 0.030 QC Batch ID: BZE2275 Total Iron BZE2275 -BLK2 ND mg /L 0.050 0.030 Total Lithium BZE2275 -BLK1 ND ug /L 20 6.2 Total Tin BZE2275 -BLK1 ND ug /L 50 6.7 QC Batch ID: BZE2368 Total Recoverable Aluminum BZE2368 -BLK1 ND ug /L 40 5.9 Total Recoverable Antimony BZE2368 -BLK1 ND ug /L 4.0 0.58 Total Recoverable Arsenic BZE2368 -BLK1 ND ug /L 4.0 1.7 Total Recoverable Barium BZE2368 -BLK1 ND ug /L 2.0 0.20 Total Recoverable Beryllium BZE2368 -BLK2 ND ug /L 2.0 0.24 Total Recoverable Cadmium BZE2368 -BLK1 ND ug /L 2.0 0.20 Total Recoverable Chromium BZE2368 -BLK1 ND ug /L 6.0 1.9 Total Recoverable Cobalt BZE2368 -BLK1 ND ug /L 2.0 0.20 Total Recoverable Copper BZE2368 -BLK1 ND ug /L 4.0 0.41 Total Recoverable Lead BZE2368 -BLK1 ND ug /L 2.0 0.20 Total Recoverable Manganese BZE2368 -BLK1 ND ug /L 2.0 0.81 Total Recoverable Molybdenum BZE2368 -BLK1 ND ug /L 2.0 0.34 Total Recoverable Nickel BZE2368 -BLK1 ND ug /L 4.0 1.4 Total Recoverable Selenium BZE2368 -BLK1 ND ug /L 4.0 0.57 Total Recoverable Silver BZE2368 -BLK1 ND ug /L 2.0 0.23 Total Recoverable Thallium BZE2368 -BLK1 ND ug /L 2.0 0.20 Total Recoverable Vanadium BZE2368 -BLK1 ND ug /L 6.0 4.7 Total Recoverable Zinc BZE2368 -BLK1 ND ug /L 20 4.4 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.bclabs.com Page 29 of 33 :Z& Laboratories Inc. Environmental Testing Laboratory Since 1949 Crane's Waste Oil Inc. Reported: 05/27/2016 16:52 15412 Hwy 178 Project: Misc Samples Weldon, CA 93283 Project Number: KCOS Project Manager: Janet Crane Metals Analysis Quality Control Report - Precision & Accuracy Control Limits Source Source Spike Percent Percent Lab Constituent Type Sample ID Result Result Added Units RPD Recovery RPD Recovery Quals QC Batch ID: BZE2241 Used client sample: N Total Mercury DUP 1614169 -01 ND ND ug /L 20 MS 1614169 -01 ND 0.97000 1.0000 ug /L 97.0 70-130 MSD 1614169 -01 ND 1.0300 1.0000 ug /L 6.0 103 20 70-130 QC Batch ID: BZE2275 Used client sample: N Total Iron DUP 1613519 -02 0.19217 0.18646 mg /L 3.0 20 MS 1613519 -02 0.19217 1.2517 1.0000 mg /L 106 75-125 MSD 1613519 -02 0.19217 1.2903 1.0000 mg /L 3.0 110 20 75-125 Total Lithium DUP 1613519 -02 12.303 11.939 ug /L 3.0 20 J MS 1613519 -02 12.303 226.28 200.00 ug /L 107 75-125 MSD 1613519 -02 12.303 232.42 200.00 ug /L 2.7 110 20 75-125 Total Tin DUP 1613519 -02 ND ND ug /L 20 MS 1613519 -02 ND 201.46 200.00 ug /L 101 75-125 MSD 1613519 -02 ND 203.18 200.00 ug /L 0.8 102 20 75-125 QC Batch ID: BZE2368 Used client sample: N Total Recoverable Aluminum DUP 1614213 -02 783.12 792.63 ug /L 1.2 20 MS 1614213 -02 783.12 1507.2 600.00 ug /L 121 75-125 MSD 1614213 -02 783.12 1502.9 600.00 ug /L 0.3 120 20 75-125 Total Recoverable Antimony DUP 1614213 -02 ND ND ug /L 20 MS 1614213 -02 ND 79.680 80.000 ug /L 99.6 75-125 MSD 1614213 -02 ND 79.618 80.000 ug /L 0.1 99.5 20 75-125 Total Recoverable Arsenic DUP 1614213 -02 ND ND ug /L 20 MS 1614213 -02 ND 199.81 200.00 ug /L 99.9 75-125 MSD 1614213 -02 ND 198.11 200.00 ug /L 0.9 99.1 20 75-125 Total Recoverable Barium DUP 1614213 -02 74.276 71.070 ug /L 4.4 20 MS 1614213 -02 74.276 141.71 80.000 ug /L 84.3 75-125 MSD 1614213 -02 74.276 142.16 80.000 ug /L 0.3 84.9 20 75-125 Total Recoverable Beryllium DUP 1614213 -02 ND ND ug /L 20 MS 1614213 -02 ND 105.52 80.000 ug /L 132 75-125 Q03 MSD 1614213 -02 ND 107.01 80.000 ug /L 1.4 134 20 75-125 003 Total Recoverable Cadmium DUP 1614213 -02 ND ND ug /L 20 MS 1614213 -02 ND 80.020 80.000 ug /L 100 75-125 MSD 1614213 -02 ND 79.226 80.000 ug /L 1.0 99.0 20 75-125 Total Recoverable Chromium DUP 1614213 -02 9.6760 8.6480 ug /L 11.2 20 MS 1614213 -02 9.6760 80.926 80.000 ug /L 89.1 75-125 MSD 1614213 -02 9.6760 80.402 80.000 ug /L 0.6 88.4 20 75-125 Total Recoverable Cobalt DUP 1614213 -02 1.9320 1.8420 ug /L 4.8 20 J MS 1614213 -02 1.9320 72.650 80.000 ug /L 88.4 75-125 MSD 1614213 -02 1.9320 71.698 80.000 ug /L 1.3 87.2 20 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.bclabs.com Page 31 of 33 Laboratories Inc. Environmental Testing Laboratory Since 1949 Crane's Waste Oil Inc. Reported: 05/27/2016 16:52 15412 Hwy 178 Project: Misc Samples Weldon, CA 93283 Project Number: KCOS Project Manager: Janet Crane Notes And Definitions J Estimated Value (CLP Flag) MDL Method Detection Limit ND Analyte Not Detected PQL Practical Quantitation Limit A01 Detection and quantitation limits are raised due to sample dilution. A52 Chromatogram not typical of diesel. A55 Chromatogram not typical of crude oil. Q03 Matrix spike recovery(s) is(are) not within the control limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Report ID: 1000485515 4100 Atlas Court Bakersfield, CA 93308 (661) 327 -4911 FAX (661) 327 -1918 www.bc[abs.com Page 33 of 33