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HomeMy WebLinkAbout2601 S Chester Ave_ LUCKY 7 Tank Closure ReportAugust 7, 2013 Mr. Ernie Martinez City of Bakersfield Fire Department 2101 H Street Bakersfield, CA 93301 RE: Tank Closure Report Lucky 7 2601 S. Chester Avenue Bakersfield, California Dear Mr. Martinez: Please find enclosed 1 (one) copy of the Tank Closure Report prepared by Advanced Environmental Concepts, Inc. Should you have any questions or require clarification on any aspects of the enclosed, please do not hesitate to contact our office at (661) 395-1646. Respectfully yours, Advanced Environmental Concepts, Inc. April Saceaux Office Manager - ENVIRONMENTAL CONCEPTS WITH DESIGN IN MIND - 220 E. TRUXTUN AVENUE BAKERSFIELD, CA 93305 661/395-1646 FAX 661/395-1616 iI —ADVANCED ENVIRONMENTAL CONCEPTS INC — Advanced Environmental Concepts, Inc. is pleased to present the following: Tank Closure Report for Lucky 7 2601 South Chester Avenue County of Kern - Bakersfield, California This report has been prepared for: Mr. Jerry Hale July 2013 D n J Construction - ENVIRONMENTAL CONCEPTS WITH DESIGN IN MIND - 220 E. TRUXTUN AVENUE BAKERSFIELD, CA 93305 661/395 -1646 FAX 661/395 -1616 _ Tank Closure Report Lucky Table of Contents 1.0 INTRODUCTION 2.0 PROCEDURES 3.0 PHYSICAL CHARACTERISTICS 3.1 Site Description 3.2 GdmHydrogeo|ogy 3.3 Soil Profile 4.0 TANK REMOVAL PROCEDURES 4.1 Soil Sample Location and Collection Procedures 5.0 LABORATORY ANALYSIS and RESULTS 8.0 CONCLUSIONS 7.0 RECOMMENDATIONS 8.0 L|yW|T/T|(]NG 0.0 CLOSING (A) ([) ([) (E) (F) Appendices Figures Uniform Waste Manifest Tank Destruction Certification Dry Ice Receipt City of Bakersfield Fire Department Permit Laboratory Reports and Chain-of-Custody Documents Advanced Environmental Concepts, Inc. ^ ENVIRONMENTAL CONCEPTS WITH DESIGN /wMIND ^ 1 1 1 1 2 2 9 3 3 4 4 5 5 220 E. TRUXTUwmENuE BAKERSF|ELD.CA 93305 661n95-1646 FAX 661/395-161e Tank Closure Report Lucky 7 1.0 INTRODUCTION Advanced Environmental Concepts, Inc. This report presents the results of a tank removal conducted by D n J Construction at 2601 South Chester Avenue, Bakersfield, California on July 11, 2013. The objective was to assess the soil beneath the three gasoline underground storage tanks (USTs), having capacities of 6,000 - gallons and 10,000 - gallons, following excavation and removal (Figure 1). Tank removal procedures were performed under the supervision of the City of Bakersfield Fire Department (Mr. Ernie Martinez) and a permit was obtained from the City for the removal. D n J Construction conducted the UST and dispenser removals and Adams Services cleaned the tank interiors and transported the rinseate and the three USTs for offsite disposal; Mr. Jonathan Buck, Professional Geologist, of Advanced Environmental Concepts, Inc. (AEC), collected the required soil samples. This report includes background information regarding existing site characteristics, local geology and hydrology, tank removal procedures, sample collection procedures, analytical results, and related conclusions and recommendations. Report appendices contain Figures (Appendix A), Uniform Hazardous Waste Manifest (Appendix B), Tank Destruction Certification (Appendix C), Dry Ice Receipt (Appendix D), City of Bakersfield Fire Department Permit (Appendix E), and Laboratory Reports /Chain -of- Custody Documents (Appendix H). 2.0 PROCEDURES The USTs were located at 2601 South Chester Avenue and constructed of single -wall steel that had been lined at a prior date. The following UST removal services were conducted during the course of this project on behalf of Lucky 7: • Excavated the backfill surrounding the USTs; • Decontaminated the interiors of the three USTs with a high - pressure washer and collect, transport, and dispose of the rinseate generated during the tank cleaning process; • Inert the tanks prior to removal using solid Carbon Dioxide (dry ice); • Measure LEL and Oxygen using a recently calibrated meter; • Remove the tanks from the excavation using a crane and transport to a metals recycling facility; Collect soil samples from beneath tank inverts and former dispenser locations; • Backfill the excavation; • Summarize these procedures in the form of a "Tank Closure Report ". 3.0 PHYSICAL CHARACTERISTICS 3.1 Site Description The property is located at 2601 South Chester Avenue in Bakersfield, California. The three USTs were located north of the mini -mart building and the dispensers beneath a corrugated metal roofed canopy. 1 - ENVIRONMENTAL CONCEPTS WITH DESIGN IN MIND - 220 E. TRUXTUN AVENUE BAKERSFIELD, CA 93305 661/395 -1646 FAX 661/395 -1616 Tank Closure Report Lucky 7 3.2 Site Hydrogeology Advanced Environmental Concepts, Inc. The subject property is located in the southeastern end of the San Joaquin Valley where the Sierra Nevada, Great Valley, and Coastal Range physiographic provinces meet. The southern end of the Sierra Nevada province is composed of a massive block of igneous and metamorphic rock of Mesozoic age and older. This Sierran block, 40 to 100 miles wide and 400 miles long, slopes five to seven degrees beneath the San Joaquin Valley. The Coastal Range province on the west consists of tectonically deformed and fractured marine and non - marine sedimentary rocks of Jurassic, Cretaceous, and Tertiary age which dip eastward beneath the San Joaquin Valley. The Great Valley province is a broad asymmetrical synclinal trough, which is known as the Sacramento Valley in the north and the San Joaquin Valley in the south. Beneath the southern San Joaquin Valley floor, the Sierran plutonic and metamorphic rock is overlain by consolidated marine rocks of Jurassic and Cretaceous age. These rocks are overlain by continental marine and non- marine sedimentary rocks of Tertiary age. These continental deposits are consolidated to semi - consolidated, fossilferous sandstone, siltstone, and shale which thicken toward the south and west. The Tertiary rocks are overlain by unconsolidated continental deposits consisting of Pliocene to Holocene river and lake sediments of gravel, sand, silt, and clay. Surface features of the floor of the San Joaquin Valley consist of dissected uplands, alluvial fans, overflow areas, and lake bottoms. Dissected uplands lie between the mountains and the nearly flat Valley floor and are manifest in low lying hills through which perennial and intermittent streams flow. These features consist of reworked older alluvium. The alluvial fans are the sites of active stream deposition of sand and silts derived from the Sierra Nevada and the dissected uplands. The overflow lands and lake bottoms lie in the central part of the Valley where silt and clay accumulate in quiet lake and marsh environments. The Central Valley of California is underlain by a broad and deep hydrogeologic unit consisting of soil and rock of varying porosity and permeability. Physical dimensions are approximately 50 miles wide at the widest point in the Valley, 400 miles long, and as much as 2,000 feet deep. Recharge to regional aquifers consists of infiltration of seasonal precipitation and percolation of surface waters. The Valley aquifer of greatest storage, highest quality, and greatest accessibility for domestic and agricultural use consists of the alluvial and lacustrine continental deposits extending to depths of 1,500 to 2,000 feet beneath the San Joaquin Valley floor. Lithology and hydraulic properties of these sediments are largely the product of the sediment source and the depositional environment. These sediments range in size from clays to boulders and include all mixtures between the extremes. Those of the west side of the Valley are derived largely from the Coastal Ranges, which tend to consist of shales and fine sandstones with limited permeability. The east side sediments are derived mainly from granitic materials of the Sierra Nevada which are generally coarser and much more permeable. The majority of groundwater pumped from beneath the Valley floor occurs within unconsolidated continental deposits. The groundwater flow direction (gradient) beneath the site is estimated to be toward the west. Using data published by the Kern County Water Agency, depth to first unconfined groundwater is estimated range between 100 and 150 -feet below ground surface (bgs) beneath the site area. 3.3 Soil Profile Native soil within the excavation consisted of well graded, moist, sand from below grade level to approximately 17 -feet bgs. • ENVIRONMENTAL CONCEPTS WITH DESIGN IN MIND - 220 E. TRUXTUN AVENUE BAKERSFIELD, CA 93305 661/395 -1646 FAX 661/395 -1616 Tank Closure Report Advanced Environmental Concepts, Inc. Lucky 7 4.0 TANK REMOVAL PROCEDURES AEC witnessed the excavation and removal of the three USTs on July 11, 2013. The three USTs were oriented north -to- south. The concrete and asphalt surface was saw -cut, the surface removed, then the top and sides of the USTs were uncovered. The tanks were triple- rinsed by Adams Services and the rinseate generated during the cleaning was pumped into the vacuum truck for offsite removal. No visually stained soil nor hydrocarbon odor were detected during the removal of the soil surrounding the USTs. After cleaning the tank interiors, the USTs were inerted with 20- pounds of dry ice per 1,000- gallons of capacity. Adams Services supervised the monitoring of the oxygen concentration and lower explosive limit (LEL) within the tank interiors using an RKI Eagle LEL /Oxygen meter and with the Fire Department approved the removal of the underground storage tanks. The three USTs were removed from the excavation using a crane and loaded onto flatbed trailers for disposal at a metal recycler (SA Recycling). The liquid waste and rinseate removed from the USTs was transported for disposal to DeMenno Kerdoon, located in Compton, California, under Uniform Hazardous Waste Manifest #010396450JJK. 4.1 Soil Sample Location and Collection Procedures A total of 20 individual soil samples were collected at the subject site as part of the UST removal procedures from beneath each end of the three USTs and dispenser location (2' and 6' beneath the bottom of the tanks and dispensers). No visual indications of hydrocarbon contamination were observed during the UST removal procedures and subsequent soil sample collection procedures with the exception of gasoline odor in the soil sample collected from the north end of the 6,000- gallon gasoline UST. All sample collection locations and procedures were conducted in accordance with UST removal permit requirements of the BCFD. The following protocol was observed during sampling procedures: • A hand auger was used to excavate a representative sample of native soil from beneath the ends of each UST and beneath the former dispenser locations; An AEC geologist pushed a clean sampling sleeve into an undisturbed portion of the soil within the auger bucket, leaving no head space within the container; The sampling containers were labeled, placed in a sealable plastic bag, and stored in a cooler chilled to approximately 4- degrees Centigrade; • The soil samples were recorded on a Chain -of- Custody document to ensure sample integrity and traceability; • Analytical tests were performed by Associated Laboratories, a California - certified Laboratory located in Orange, California. 5.0 LABORATORY ANALYSIS and RESULTS The analyses specified and performed on the soil samples were in accordance with accepted State of California Department of Health Services (DHS) laboratory procedures for total petroleum hydrocarbons as gasoline (TPH -g), and EPA Method 8021 B for volatile aromatic compounds (MTBE, benzene, toluene, ethylbenzene, and total xylenes). The analytical results are summarized in the following table and the laboratory reports and chain of custody documents are presented in Appendix D of this report. Units of measurement presented in Table 1 are reported in milligrams per kilogram (mg /kg), equivalent to parts per million (ppm) for total gasoline -range hydrocarbons (TPH -g) and volatile organic compounds (benzene, toluene, ethylbenzene, total xylenes, and MTBE). 3 ENVIRONMENTAL CONCEPTS WITH DESIGN IN MIND - 220 E. TRUXTUN AVENUE BAKERSFIELD, CA 93305 661/395 -1646 FAX 661/395 -1616 Tank Closure Report Advanced Environmental Concepts, Inc. Lucky 7 TABLE 1 Analytical Results of Soil Samples July 11, 2013 Sample ID: TPH -g ppm ) Benzene (ppm) Toluene (ppm) Ethyl- Benzene (ppm ) Total Xylenes (ppm) MTBE (p m NE -DIS -2' ND <0.018 ND <0.0006 ND <0.0004 ND <0.0005 ND <0.0012 ND <0.0009 NE -DIS -6' ND <0.018 ND <0.0006 ND <0.0004 ND <0.0005 ND <0.0012 ND <0.0009 SW- Disp -2' ND <0.018 ND <0.0006 ND <0.0004 ND <0.0005 ND <0.0012 ND <0.0009 SW -Dis -6' ND <0.018 ND <0.0006 ND <0.0004 ND <0.0005 ND <0.0012 ND <0.0009 6K -S -2' ND <0.018 ND <0.0006 ND <0.0004 ND <0.0005 ND <0.0012 ND <0.0009 6K -S -6' ND <0.018 ND <0.0006 ND <0.0004 ND <0.0005 ND <0.0012 ND <0.0009 6K -N -2' 1,550 ND <0.0006 7.0 24 360 ND <0.0009 6K -N -6' ND <0.018 ND <0.0006 ND <0.0004 0.008 0.101 ND <0.0009 C- 10K -S -2' ND <0.018 ND <0.0006 ND <0.0004 ND <0.0005 ND <0.0012 ND <0.0009 C- 10K -S -6' ND <0.018 ND <0.0006 ND <0.0004 ND <0.0005 ND <0.0012 ND <0.0009 C- 10K -N -2' 7.41 ND <0.0006 ND <0.0004 ND <0.0005 0.141 ND <0.0009 C- 10K -N -6' ND <0.018 ND <0.0006 ND <0.0004 ND <0.0005 ND <0.0012 ND <0.0009 W- 10K -S -2' ND <0.018 ND <0.0006 ND <0.0004 ND <0.0005 ND <0.0012 ND <0.0009 W- 10K -S -6' ND <0.018 ND <0.0006 ND <0.0004 ND <0.0005 ND <0.0012 ND <0.0009 W- 10K -N -2' ND <0.018 ND <0.0006 ND <0.0004 ND <0.0005 ND <0.0012 ND <0.0009 LW-10K-N-6' ND <0.018 ND <0.0006 ND <0.0004 ND <0.0005 ND <0.0012 ND <0.0009 Note: See Figure 2 for identification of sampling locations. 6.0 CONCLUSIONS Non - detectable to trace concentrations of volatile organic compounds and TPH - gasoline were indicated in the soil samples collected from beneath the three USTs and dispensers with the exception of the soil sample from the north end of the 6,000 - gallon UST at 2 -feet beneath tank invert. This soil sample exhibited 1,550 mg /kg of TPH as gasoline; 7 mg /kg of Toluene; 24 mg /kg of Ethyl Benzene; and 360 mg /kg of Xylenes. The extent of the migration was minimal since the soil sample at 6 -feet below tank invert indicated trace to non - detectable hydrocarbon concentrations. The small area of detection in the soil coupled with the absence of Benzene and MTBE indicates that this release occurred well in the past and was probably from a one -time event. 7.0 RECOMMENDATIONS Based on the "non- actionable" hydrocarbon and VOC concentrations beneath the former USTs and dispensers at 6 -feet below tank invert, AEC recommends no further investigation appears warranted for this site. 4 • ENVIRONMENTAL CONCEPTS WITH DESIGN IN MIND 220 E. TRUXTUN AVENUE BAKERSFIELD, CA 93305 661/395 -1646 FAX 661/395 -1616 —L . _ 4 Radiant -a `i Hovie°S - iy x Trailer G6urt r - �ilisnli�'r � s un T H GATE, ng Center._.. a� _. - i -A, _ . p,. .... .... ,... * iM, Vine -Dr, T � _ 71. � '�IneDr K Lawson 1. "' TD .r dt �., ��� 17 _� 0 rte. > �t Holdlm,Voa . tilllvnan.4_v F D (=aril P,1..__ - Doollmle -Pre . Altus $1' CD custeT Awe + Phop -nix r°� e' Le f °'''e -I T °� Piost `s 6 ark€ F, Sv`uth�,.Union I- 'Clark Ave nrd ' ,11son R Wilson. Rd Dentork Par �� y z-' N:' % -Q a Cleaners Antonia Way Dorian Dr 7, Atoalard Dr- oca �� r Patiicia Ave wood Dr H.�ndTi � I� k:s Lr ::._ Lindsay Eyr �a+�e Belvedere Ave _ Osr, as A'qe Sidney lor � Dayton Ave Sylvia .D ��� tivia Dr r Lacey ° St Beryl Dry r Beryl Dr_ Lela nd Ave Niereduth Di Meredith Dr U r Ranz ., F?Lnz �3*�. PlanzR� l Manoh est er a ��a -;� `Dr: piage ► I �, � e.utr Wile H€ me. .. Car -son Ave High n, + F School f Dodge Ave, � Ernery Ave Falcon Ave Cr rn _ ° Garfield Ave 13.. 1 Hub Ave i an Awe White Ln R C F�I A.� _ _ .. n ti icente Dr . T°idrea .rime, , � 3 aa co 0lybourrn Dr w Holida inn c, Ri Ave 'e 'i'r - i±s' E747[5�i Rikerv:l -. @�SJ ... L.i.�Jd..+i�.. . �, m ns .. t'r ..,+ aJi ,-i i',1 _ W Al =11MMIMMM16 ADVANCED ENVIRONMENTAL CONCEPTS INC z 220 East Truxtun Avenue Bakersfield, California 93305 (661) 395 -1646 Site Location Map Lucky 7 2601 South Chester Avenue Bakersfield, California FIGURE Dorian Drive 0 Sample Location N 0' 10' 20' W E ■ S Scale 1" = 20ft. Site Map FIGURE Lucky 7 .� CEO Elm RONMENTALOONOEPTS[NO 2601 South Chester Avenue 2 220 East Truxtun Avenue Bakersfield, California Bakersfield, California 93305 Canopy port W -10K -N C-1 OK-N S Poles® YP Dispenser g I 6K -N / NE -Disp O O o / O / 10K 10K 6K � / t6- Dispenser W -10K -S C -10K -S m �� SW -Disp 0 Sample Location N 0' 10' 20' W E ■ S Scale 1" = 20ft. Site Map FIGURE Lucky 7 .� CEO Elm RONMENTALOONOEPTS[NO 2601 South Chester Avenue 2 220 East Truxtun Avenue Bakersfield, California Bakersfield, California 93305 Please print or type. (Form designed for use on elite (12- pitch) typewriter.) Form Aooroved. OMB No. 2050.0039 EPA Form 8700 -22 (Rev. 3 -05) Previous editions are obsolete. 1) 00 62..1. 1 t Ar4: :0 V UH I r- K'5 U U r r UNIFORM HAZARDOUS 1• Generator ID Number 2. Page 1 of 3. Emergency Response Phone 4. Manifest Tracking Number WASTE MANIFEST j s 5. Generator's Name and Mailing Address Generator's Site Address (if different than mailing address) ri?�rF-X11.13ViE1XY, C-11". !413.304 26431 !3t- 4 AZVE1VLTY.- Generator's Phone: wAl .'tsViEla -'s f:.%:?; "e` 1= : L� t x;, a-zio4i 6. Transporter 1 Company Name U.S. EPA ID Number V q4{ ��yy } � to PR y .7 �.. IIE 3 , T -C- _ .� k � 44' 7. Transporter 2 Company Name U.S. EPA ID Number 8, Designated Facility Name and Site Address U.S. EPA ID Number tii != §N!' 87e*FV.7 _.,J�. . Ti. 'ry Facility's Phone: 31.0 5-317-71330 9a. 9b. U.S. DOT Description {including Proper Shipping Name, Hazard Class, ID Number, 10. Containers 11. Total 12. Unit 13. Waste Codes No. Type HM and Packing Group (if any)) Quantity W11Ual. � 1. �r... ;� ;_� ti;t %�$d ��1yy�-' ��».,�_:t ".:�':k�it'��y.��''��� ��I�.��jc���k ?r��• t'a.! 'fi ',�¢'� 1�a�rr... �A. ! L� ii...i'.41.��. .Y �•�1 ,,5 �k i i © ,i L'f.J cF f'J ............._...L .._..... -... 2. i i 3. r � 1 i i I i I 4. 14, Special Handling Instructions and Additional Information •• 47 :.:._ . ;.. a'j: �'fiiza:.'S �..'a° .. .T• .�'y..':j�!: "v . "�:S'r:�3"� :c:`:'� 15. GENERATOR'SlOFFEROR`S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by the proper shipping name, and are classified, packaged, 15. marked and labelediplacarded, and are in all respects in proper condition for transport according to applicable international and national governmental regulations. If export shipment and I am the Primary ' Exporter. I certify that the contents of this consignment conform to the terms of the attached EPA Acknowledgment of Consent. I certify that the waste minimization statement identified in 40 CFR 262.27(a) (f I am a large quantity generator) or (b) (if I am a small quantity generator) is true. GeneratoeslOfferorrs PrintedlTyped Name yj , Signature . -,, Month Day Year J 16. Internatlorial Shipment's f, ��--77 ❑ Import to U.S. L.- Export from U.S. Part atentrylexit:� � Transporter signature (for exports only): j Date leaving U.S.: LU 17. Transporter Acknowledgment of Receipt of Materials 1 Pdntedgyped Name Signature 1, Month Day Year Transporter Transporter 2 PdntedlTyped Name Signature '� , .. Month Day Year 18. Discrepancy s' 18a. Discrepancy Indication Space quantity ❑Type ❑Residue ❑ Partial Rejection El Rejection Manifest Reference Number: 18b. Alternate Facility (or Generator) U.S. EPA ID Number U tit Facility's Phone: LL, 180. Signature of Alternate Facility (or Generator) Month Ray Year N19. Hazardous Waste Report Management Method Codes (Le,, codes.5ar hazardous waste freatment, disposal, and recycling: systems) UJ 1 2, 3. 4. 20. Designated Facility Owner or Operator: Cerf rication of receipt of hazardous materials covered by the manifest except as noted in Item 18a PrintediTyped Name Signatun Month Day Year , EPA Form 8700 -22 (Rev. 3 -05) Previous editions are obsolete. 1) 00 62..1. 1 t Ar4: :0 V UH I r- K'5 U U r r I' - a UNDERGROUND STORAGE TANK PERMIT APPLICATION TO CONSTRUCT - INSTALL NEW TANK (NEW FACILITY) /NEW TANK INSTALL (EXISTING FACILITY) /MOD -MINOR MOD Permit # BAKitASIFIELD FIRE DEPARTMENT Prevention Services ,',940 w 2101 H Street r Bakersfield, CA 93301 *'� Phone: 661- 326 -3979 ® Fax: 661- 852 -2171 ARTArAwr Page 1 of 1 TYPE OF APPLICATION: ❑ NEW TANK INSTALL/NEW FACILITY ❑ NEW TANK INSTALL/EXISTING FACILITY ff_ut=f. V riAlm.nhti VNI n Mn1lTGTf`A -rTnN1 nP GAf it T7V r-1 MTNr1R Mr)r)TFT(- ATTr)N OF FA(71 TTY STARTING DATE) PROPOSED COMPLETION DATE FACILITY NAME � � EXISTING FACILITY PERMIT # FACILITY ADDRESS f �f /'7 � �+ C Cr11' r J ZIP CODE TYPE OF BUSINESS � TANK OWNER G PHONE ADDRESS s� . �iJ� /L.+��,r�C..� =� CITY „/a 'F ZIP CODE f� '' CONTRACTOR 11CA4CE//�ii��i/�C ADDRESS CITY ZIP CODE PHONE # BAKERSFIELD CITY BUSIN S LICENSE # WORKMANS COMP # INSU ER BRIEFLY DESCRIBE THE WORK TO BE DONE: s WATER TO FACILITY PROVIDED BY DEPTH TO GROUND WATER �fj SOIL TYPE EXPECTED AT SITE # OF TANKS TO BE INSTALLED ARE THEY FOR MOTOR FUEL? Q YES 0 NO SPILL PREVENTION CONTROL AND COUNTERMEASURES PLAN ON FILE? 0 YES CI_.. NO., THIS SECTION IS FOR STORAGE TANK IDENTIFICATION TANK VBLUMt UNLEADED REGULAR PREMIUM DIESEL OTHER Tank Testing Company NAME OF TESTING COMPANY PHONE NUMBER MAILING ADDRESS NAME OF TESTER ICC# THE APPLICANT HAS RECEIVED, UNDERSTANDS, AND WILL COMPLY WITH THE ATTACHED CONDITIONS OF THIS PERMIT AND ANY OTHER STATE, LOCAL, AND FEDERAL REGULATIONS. THIS FORM HAS BEEN COMPLETED UNDER PENALTY OF PER7URY, AND TO THE BEST OF MY KNOWLEDGE IS TRUE AND CORRECT. NAME OF TESTER ICC# THIS APPLICATION BECOMES A PERMIT WHEN APPROVED FOR OFFICIAL USE ONLY DATE APPROVED APPROVED BY �n�nee :reo:...ne innt BAKERSFIELD CITY FIRE DEPARTMENT -- INSPECTIuN RECORD Post this Card at the Job Site and DO NOT Remove for Duration of Work Inspection Request Phone No. (661) 326 -3979 i UST NEW INSTALL DESCRIPTION DATE SIGNATURE BACKFILL PRIMARY PIPE SECONDARY PIPE .SECONDARY CONTAINMENT SENSORS AUTHORIZATION FOR FUEL ELECTRICAL SEAK -OFF AST NEW INSTALL DESCRIPTION DATE SIGNATURE MODIFICATIONS MINOR /MAJOR AST REMOVAL DESCRIPTION DATE SIGNATURE EAAARKS[. BUILDING ADDRESS: JOB DESCRIPTION: (C ICONTRACTOR OCCUPANCY TYPE: i OWNER: . PERMIT NO. s. ,3.=''E rc�:� =- �•,..�c • PHONE # f ` FD 1743 Associated laboratories 806 N. Batavia - Orange, CA 92868 Tel (794)779 -6900 Fax (774)538 -9209 www.associatedlabs.com lnfo@associatediabs.com Client: Advanced Environmental Concepts Inc. Address: 220 E. Truxtun Ave. _ Bakersfield, CA 93305 Attn: Jonathan Buck Comments: Lucky 7 7601 S. Chester Ave., Bakersfield, CA 04232 .......... Chi. Lab Request: 326052 Report Date: 07/19/2013 Date Received: 07/13/2013 Client ID: 10022 This laboratory request covers the following listed samples which were analyzed for the parameters indicated on the attached Analytical Result Report. All analyses were conducted using the appropriate methods. Methods accredited by NELAC are indicated on the report. This cover letter is an integral part of the final report. Sample # 326052 -001 326052 -002 326052 -003 326052 -004 326052 -005 326052 -006 326052 -007 326052 -008 326052 -009 326052 -010 326052 -011 326052 -012 326052 -013 .326052 -014 326052 -015 326052 -016 Client Sample ID NE- disp -2' NE- disp -6' SW- disp -2' SW- disp -6' 6K-S-2' 6K-S-6' 6K -N -2' 6K -N -6' C-1 OK-S-2' C-1 OK-S-6 C-1 OK-N-2' C- 10K -N -6' W-1 OK-S-2' W-1 OK-S-6' W-1 OK-N-2' W-1 OK-N-6' Thank you for the opportunity to be of service to your company. Please feel free to call if there are any questions regarding this report or if we can be of further service. ASSOCIATED LABORATORIES by, Nina Prasad President NOTE: Unless notified in writing , all samples will be discarded by appropriate disposal protocol 45 days from date reported. The reports of the Associated Laboratories are confidential property of our clients and TESTING & CONSULTING may not be reproduced or used for publication in part or in full without our written Chemical permission. This is for the mutual protection of the public, our clients, and ourselves. Microbiological Page 1 of 17 Environmental am p Sit amp 26052:' CjentSaffiple.A Method: EPA 8015 NE"c Prep Method: EPA 5035 QCBatch]D: QC1 138287 Analyte % Recovery Limits Notes 4-8romofluorobenzene (SUR) 77 60-140 Method: EPA 8021 NEL4C Prep Method: EPA 5035 QCBatchID: QC1138288 Benzene _ _._________________.__wo_.___�_uzmoa_.o�on_..�g»�i__orn�no__�anmh_________. Ethylbenzene ------..___________________.wo____1_u/�ps_.o�o�__��x�__ornan�_.�ao»»_________ �ihbK---___--___--.—_----._--.—wo---.�_'ozmo�—.�o��--��w�--on1ax�—��t�.-----_--- �����--' N- -D, � umx�.—»�»a -------'-------'------'--'----'----' enem�o�V wo 1 umno—'-10--��M�-------����- ��—�- —�gx�i--.on1ans—.���x-------.—.. o7neno mm ' ........ ......... ....... mo= Not Detected n,< MDL MoL= Method Detection Limit noL= Reporting Detection Limit oF= Dilution Factor -IlkASSOCIATED LABORATORIES Analytical Results Report Lab Request 326052 Page 2 of 17 _ Analyte Result DF MDL RDL Units Anal zed By Notes Method: EPA B015 NELAC Prep Method: EPA 5035 QCBatchID: QC1 138287 TpV.oauooma.____._____________'---.-mo_---.�—.uo�a---o--��xg--.o��a/��—'��»�---'-----'-- _ 4-Bromofluorobenzene (SUR) 73 60-140 Method: EPA 8021 ^ELAc Prep Method: EPA 5035 uuu*tcnu' wu/`unzou Benzene ND 1 0.0006 0.005 mg/Kg 07/16/13 rparish - ���—'---'-----'--------'-----���---''i '��k� ���� ��«g--�mv1a/��--��«�----'-----' wIToc____.____________________..mo___..�._�ouu�.__n��/__��w�___o/xa»�__���l__________ Tvmrne_______________.____..wo_.__.�_o�qo*__0�oa__ ---' '- xy�nos(rv�V wo / o�o�u oo�e - . mux« . ���i--_--.---'��—'-------- __on�an�_.mano on1enu ._________ �ono 4-Bromofluorobenzene (SUR) 73 60-140 _ _ � _ mo= Not Detected or< MoL mmL= Method Detection Limit RoL= Reporting Detection Limit op= Dilution Factor ACOnr%IATs=n i APnPATr)t?I)=-4Z Analvtical Results ReDort A Lab Request 326052 Page 3 of 17 4 Cheat A vance6' En' vironmen taI:Qbhdept§. Inc. Collector 4T 6 '3 13:35.. SarripIed.,,,'.,.'07/1'1/`2 .1 site�%;:, . . . . .. . ... �M 14-1, -,S,aMDI,e Type; ypo: Client Sampl Sample #: e 326052-:003 SW -�dis*p . ... . ..... Analyte Result DF MDL RDL Units Analyzed By Notes - Method: EPA 8015 NELAC Prep Method: EPA 5035 QCBatchID: QC1138287 TPH Gasoline ----------------- ---------------------- ND --------------------- ------------------ --------------------------------- 1 0,018 3 mg/Kg ---------- -------------- 07/16/13 ------------------- rparish ----------------------- Analyte 4-Bromofluorobenzene (SUR) % Recovery 70 Limits 60-140 Notes Method: EPA 8021 NELAC Prep Method: EPA 5035 QCBatchID: QC1138288 Benzene ------------------- ............. ---------------------------------- Ethylbenzene Vi:6-E ----------------------------------------------------------- ----------------------------------------------------- Toluene X�Ienes - (Total) - . ........................ ---------------------------------- •..•...... ND -- ----------- ND ---------- ----------- ND --------------------- ------- ------------------------------- ND ND •--------------- --------------------- 1 ------------- 1 --- 1 1 1 0.0006 - ............ 0.0005 ----------- 0.0009 0.0004 0.0012 - 0.005 0.005 ------------- 0.035 0.005 0.015 mg/Kg --- .............................. mg/Kg --------- mg/Kg ---------------- mg/Kg -- ----- m g/Kg 07/16/13 07/16/13 ---- -- ----------------- 07/16/13 — ------------------------------------------ 07116/13 - -------- 07/16/13 -------------------- rparish - .............................. rparish -- ........ rparish rparish r pa rish ----------- -------- ------------------- Anal )de 4-Bromofluorobenzene (SUR) v % Recovery, 70 Limits 60-140 Notes ND = Not Detected or < MDL MDL = Method Detection Limit RDL = Reporting Detection Limit DF = Dilution Factor ft ACCt1r1ATi=n i ARnPATr)j?ij=-,q Analvtical Results Reoort Lab Request 326052 Page 4 of 17 Mi6ix-n15 Oita mo=Not Detected m< MoL MDL=Method Detection Limit RDL = Reporting Detection Limit DF=Dilution Factor ���� Lab Request 326052 Page 5 of 17 Method: EPA 8015 I�f-LAC Prep Method: EPA 5035 QCBatchID: QC1138287 Tp�Gosoom».--_-------.--------_--wo----�—'uo10---y—.-�gx�L--or�ans--��x�------------------ -- Analyte % Recovery Limits Notes 4-Bromofluorobenzene (SUR) 76 60-140 � Mouhuu EPA 8021 N-"-Ac Prep Method: EPA yoos ooaatcom' uc1138288 '- —'-------------'-----------------'---'-����-----'—�u7neno nzene ,pmnsh .----.----.--_--.------wo.---'�—�000a------.��x�---__--'-------.-_----. �i��---'' wo___��_o�nm»—.nosa--��x��_—on�sn�—��n�n---_--_--' �����'-------------------'--''��----�—o�«��—'o�m5--mo»Ku--'or«���—Ip��n---_--.__.. — ----'7om[ — __________.__.__mo___..�.-o�n�.--oo�s_—��ng---o��an�—.�on,x _—_____ Analyte % Recovery Limits Notes 4-Bromofluorobenzene (SUR) 76 60-140 _ -- _ _ _ � � mo=Not Detected m< MoL MDL=Method Detection Limit RDL = Reporting Detection Limit DF=Dilution Factor ���� Lab Request 326052 Page 5 of 17 b6lie or: di t Analyte Result DF MDL RDL Units Analyzed By Notes Method: EPA 8015 NELAC Prep Method: EPA 5035 QCBatchlD: QC1 138287 4-Bromofluorobenzene (SUR) 76 60-140 oxetm,u: sPxaoz1 weuC Prep Method: EPA 5035 QoBatoh|o' oonoazao _ Benzene ND 1 0.0006 0.005 mg/Kg 07/16/13 rparish ---_----__--_------.----.---._--__---___--.-----_.------.------------ -.----------__---.-----mo----�-000us-.«�oo--'��x�'--.on�en�-.��x�_-__--_.___ mrha� --'- ___._____.._.___________.__wo--.-.�-�mzua-.o�ms-.-��x�--o�1ano-��n�!_---.----.' T�����-.---------------.-_-_--'mo----�-u000�-.o�os-''��xg._---_�_.��---.------- on�sn �m -' wo 1 uomn 0o15 ��w� orxsnu .��o�.____._____ 4-8romofluorobenzene (SUR) _ _ -- 76 60-140 � � mo= Not Detected u,^MoL MoL= Method Detection Limit noL= Reporting Detection Limit op= Dilution Factor � ^��� mx»en�IA TrnxA����PATnP��z /mow�o|no�u no�� '��� Lab Request 326052 Page 6 of 17 _ Method: EPA 8015 NELAC Prep Method: EPA 5035 QCBatchID: QC1 138287 _ 4-Bromofluorobenzene (SUR) 75 60-140 Method: EPA 1 wsLAm Prep Method: EPA 5035 ooBetchm ocnouuuo -- ------------------- .......... - ............ Eu�m�����---_---.--------.------m�.----�-�000a--��os.--�gx�_-.-----�-��*� --------------------------------- ---'-'--'���i------------------------ mnnn ----------- --------- .-. «»To�_____________--_-----.-.---wo-_-.-�-uu000-.uoos-.-��w�.---_._�.-���n---------' mn7n Tom���---.----�--�-_---_.-.-_.-.-mo-.--��-o�oVcw-.uoo�-_��w�---onx--..!��am-..------.-' 7na - enau(n�a� wo 1 o.uu10 o.n10 mn«Ku__.pn�n��_ _________. nal)qe % Recovery Limits Notes 4-Bromofluorobenzene (SUR) 75 60-140 _ mo=Not Detected o,<mmL Mcu= Method Detection Limit noL= Reporting Detection Limit or= Dilution Factor ---' - A a��nv�T�iaR���R� �a��|���� Lab Request 326052 Page 7 of 17 IX Analyte Result DF MDL RDL Units Analyzed By Notes Method: EPA 8015 NELAC EPA 5035 un1rn�_��xm-._________. QCBatchID: QC1 138287 �TPH Gasoline ._��� _��� _ __________.__________.1s��_—..�mo--.�.�--�oo--��p�.--mnrn�—��,�.---'—'—'---' nalyte % Recovery Limits Notes ______.__ _ e — �mo«�--'�����—'�on» Method: EPA 8021 NELAC Prep Method: EPA 5035 ____.____.___________-mo--..�Vo--�oo_._.��—.-����--'-----���m.----'----- Toluene QCBatchlD: QC1 138288 Benzene wo 100 umy u5 ��wg un1rn�_��xm-._________. _ —.-------____------------------------ - _____.��_..��� ._��� _��� ''--'------'' ______.__ _ e — �mo«�--'�����—'�on» un�/nn �anw ____.____.___________-mo--..�Vo--�oo_._.��—.-����--'-----���m.----'----- Toluene 7o�uo�p� ����! u��r���n�n — .......... ------- .—.--------------..--..--.--o----.n-' — x���{n��V � 360 ueoo o o7� mox� on1rnn '-'--'----'--—-- �onox nalyte % Recovery Limits Notes 4-Bromofluorobenzene (SUR) 97 60-140 mm= Not Detected o,< MoL MoL= Method Detection Limit RoL= Reporting �Detection Limit oF= Dilution Factor ASSOCIATED ORATORIES Analytical Results Report - _ Analyte Result DF MDL RDL Units - Analyzed By Notes Method: EPA 8015 NELAC Prep Method: EPA 5035 QCBatchID: QC1 138287 _n,*.G000xm*____._._______._._____._.�o____1__uo�o___.a_..��n�.__»7n�n�_.��mm_________.. Analyte % Recovery Limits Notes 4-Bromofluorobenzene (SUR) 102 60-140 Method: EPA 8021 NELAC Prep Method: EPA 5035 QcButcx/ - ---- ... -----'-----------------'---------'---h��|--------'------ enzene -----.----------.—.—.—.«�m�_---�—»000a—.o�os.-_�g»�--.cnnrn�-'!��m�.--------.. xm6 aoh.--'_----.- Tumene________.____.________._mo____1 --- ------------- ---.mo ------ — --1—uu000—.nu3>—_mo»g--.«717nu—!p- ____ ---- _ - --E - xymnea(rnaV --------------------------- 010 ------------- -------- 1 _u0004 _-o0oo_..mq»g 00012 0015 __.mvr/l3_.poro» moog 07n713 !p uh Analyte 4-Bromofluorobenzene (SUR) % Recovery 102 Limits 60-140 Notes _ mo= Not Detected n,< MoL M L = Mamouoeteouonumu moL = menom no �oate:uonumu oF= Dilution Factor -- A m�CfI�xA�n I A��IPA��P�� pma|�oo|R�u|�ma�� Lab Request 326052 Page 9 of 17 ien b` cepi ih lien -Sampled: 07/11/20.13 14:17 in Method: EPA 8015 NELAC Prep Method: EPA 5035 QCBatchlD: OC1 138287 —4-Bromofluoroberizene (SUR) 66 60-140 Method: EPA 8021 IvELAC Prep Method: EPA 5035 QCBatchlD: QC1 138288 ,_ -----------.--.----------.------_-----.--------.---_— '-----'-- _____.________—.---..mo---.�—u000s—'o�oe--��«�'--o7«r»�—���»----'----'' �f6�------------__—.—.–_--_--.mo—.--��—�ono�—'o�oa—_��m�—.–nn1���–'��t�--'----.--. �����--' --on�rna—.��u�--.------- -- ----------'-- -----------.--mo---'�—0000�_-000s—... mo 1 0.0012 0.015 mnxx 07x7113 mmna _.._ ------------- Analyte 4-Bromofluorobenzene (SUR) % Recovery 66 Limits 60-140 Notes _ / mo= Not Detected o,«MoL MoL= Method Detection Limit RoL= Reporting Detection Limit oF= Dilution Factor ASSOCIATED LABORATORIES Analytical Results Report La� Request 326052 Page 10 of 17 _ �_�. _ Analvte Result DF MDL RDL Units Analyzed By Notes Method: EPA 8015 NELAC Prep Method: EPA 5035 QCBatchlD: QC1 138287 _ Analyte % Recovery Limits Notes 4-Bromofluorobenzene (SUR) 74 60-140 Method: EPA 8021 NELAC Prep Method: EPA 5035 ooBotchm' oo1 138288 — '---'------' �n'-----.—'--'.--'-----'-----''Nb----10l�b�—'0�05--mgx�--'��i���—'nono �o�m�����..—_---'---'--------'----------'---'------���---'------' ��----------- �r��-- �� on�rnn �����---' _____.______________.wu__._�_o/�ma._uo»a__.�q»��_______�����.---------.. N 1 0 o004 0;005 mg/Kg on17no—.!9�m�—.--------'' — ----'-----------'---------------'-----''—'��--'------��rnm wn � o�uo �a ��x� �ona !���� ._._.__ Analyte % Recovery Limits Notes 4-Bromofluorobenzene (SUR) _ 74 60-140 wo= Not Detected nr«MoL MoL= Method Detection Limit noL= Reporting Detection Limit oF= Dilution Factor it ASSOCIATED ORATORIES Analytical Results Report c==~ _ Analyte Result DF IVIDL RDL Units Analyzed By Notes Method: EPA 8015 NELAC Prep Method: EPA 5035 QCBatchID: QC1 138287 AA f)7JI 7/11 r,�rioh _ 4-Bromofluorobenzene (SUR) 115 60-140 Method: EPA 8021 NELAC Prep Method: EPA 5035 dooatcmo' oo1138288 — Benzene ND 1 0000a 07/17/13 rpmnsh -- -------------- --------------------------------- �mym�����---_.---.--_------_.—.—wo_—.--�—nzmus—.��--..�gx�.—.----__��nm�----_----- ------- ................... ------------------------- ''6���---�---''b�����'---------'---- �Tee wo Toluene ND ..�..V/�x�—.o�se_--��p�.--un17n�— 1 0.0004 0.005 mg/Kg 07/17/13 ---------' rparish -- «����!{o�m� u,*/ . "",.� 0.015 mg/Kg 07/17/13 rparish ' 4-Bromofluorobenzene (SUR) 115 60-140 -- '~ � wo= Not Detected n,< MoL MnL= Method Detection Limit RoL= Reporting Detection Limit oF= Dilution Factor Lab Request uomosu Page 1o'x17 Analyte Result DF MDL RDL Units Analyzed - By Notes Method: EPA 8015 N,6"c Prep Method: EPA 5035 QCBatchID: QC1 138287 Tp*.Gaaoxma.__________..___.______.mo____�__�o�a'__.o__mo»�___on�r»�_.�a�s»_.___._____ Analyte % Recovery Limits Notes 4-Bromofluorobenzene (SUR) 73 60-140 Method: EPA 8021 Af-LAC Prep Method: EPA 5035 QCBatchl,D: QC1 138288 Benzene ND 1 0.0006 0.005 mg/Kg 07/17/13 rparish Ethylbenzene ND 1 0.0005 0.005 mg/Kg 07/17113 rparish Toluene ND 1 0.0004 0.005 mg/Kg 07/17/13 rparish Xylenes (Total) ND 1 0.0012 0.015 mg/Kg 07/17/13 rparish '^ mo= Not Detected nr< MoL MoL= Method Detection Limit eoL= Reporting Detection Limit oF= Dilution Factor ---- � A Lab Request 326052 Page 13 of 17 amp YP Method. EPA 8015 N-L-4c Prep Method: EPA 5035 QCBatch[D: QC1 138287 Analyte % Recovery Limits Notes 4-Bromofluorobenzene (SUR) 76 60-140 Benzene --orn7os—p axs!—_------- ._._____..___..wD.___�_0oome__o0om--- ---------'-----_____.____._.wo___1 --------- —' -----------'---'' wo ._u000a.__oo»o__mu»«--.m,rxs-'pa«s�— 1 00009 0000 mux« 071713 mons � Toune ___________--.—'-------'ND ---- ___.___._.__._���_____—.--./---_------- 1 oouo+ 000s ��o�...—o7nrnx—�o��l--------''- ----'-------------'-------'-----''��'—'—' — xv�nosTo�V wo 1 0.0 012 10 .��x�.—_—_---!?��n---.----.—_ o7n7nu mono - 4-Bromofluorobenzene (SUR) 76 60-140 wo= Not Detected or < MDL MDL=Method Detection Limit RDL= Reporting Detection Limit DF= Dilution Factor ASSOCIATED LABORATORIES Analytical Results Report- ���� Lab Request 326052 Page 14 of 1-i ( pncep Collector: die'6 Client Matrix lid �,.-1 .2 . 5 sit ffipldd-."Wj1/2013 5 - Site. ; Sa.r6ple,#: 326052 J01 lienV8.amplep'M W-10f 6 .Type s Analyte Result DF MDL RDL Units Analyzed By Notes Method: EPA 8015 NELAc Prep Method: EPA 5035 QCBatchlD: QC1138287 TPH Gasoline ------------------------ 1— ....... I ---------------------------------------------------------------------------------------------------------------------- ND 1 0.018 3 mg/Kg 07/17/13 rparish ------------------------------ F An' alyte 4-Bromofluorobenzene (SUR) % Recovery 72 Limits 60-140 Notes Method: EPA 8021 NELAC Prep Method: EPA 5035 QCBatchlD: QC1138288 Benzene . .......... – ............................... Ethylbenzene ---------------------------------------------------------- MTBE .................. -- ------------------------ Toluene .......... I ....... ........ ........... Xylenes (Total) -------------------- - - - - -- ------ ------------------------ ND ...... ------------------------------- ND ------------ ------ 6 ------------------------------- N ---- ......... ......... .................. ND ------------------------------------------------------------------------------------------------------------------------ ND ---------------- -------- ----------------- 1 1 1 ------------------------------------------------------ 1 1 0.0006 0.0005 0.0009 0.0004 0.0012 ------- 0.005 .................................. 0.005 ------------------------------------------ 0.0 i6 0.005 0.015 mg /Kg mg/Kg mg /Kg mg/Kg mg /Kg --------------------------------- 07/17/13 ................ 07/17/13 07/17/13 .......... 07/17/13 07117/13 rparish ........ --------------- rparish - ------------------------- rparish ..................... rparish ------------------ rparish ------- ------- ------- ------ Analyt 4-Bromofluorobenzene (SUR) % Recovery 72 Limits 60-140 Notes ND = Not Detected or < MDL MDL = Method Detection Limit RDL = Reporting Detection Limit DF = Dilution Factor ASSOCIATED LABORATORIES Analytical Results Report A Lab Request 326052 Page 15 of 17 -- Analyte Result DF MDL RDL Units Analyzed B Notes 5035 - T�*.Goo»xma..'----.—.---.---..------wo---.�—.no��—_-'o--�gx��__-'-----._-----------.. — ornzno mansn -- 4-Bromofluorobenzene (SUR) 73 60-140 Momuu EPA 8021 ^ELAc Prep Method: EPA 503e Qoeatcmo' oc1 138288 _ Benzene ND 1 0.0006 0.005 mg[Kg 07/17113 rparish --.---- --------------------- ------------ -----_--_------.---------.-_--.-.--.------._----_—.— wo � o�uos o�ou o7nzno �ana ............. ----------- ------------------ MroE .......................... ------------d���--------''�����-------------- wo 1..o/�ma_.. f����� -------'-------------''�b -- --.—�go�L._------�/��o�---------- ,— x����i�(Tota� mo '� 1 'o/�o�—�h�b� o�no n�1* —���g--o7nr»�—'�ano»--------- !��^�_ on�7nu ���». _._ -------------- 4-Bromofluorobenzene (SUR) 73 60-140 -- _ ~- _ _ _ - _ — wo Not Detected o,< MoL MoL =Mnmpu ooteounn Limit � � � � � � � � � � � � i RoL = mopumn � Detection Limit op=cxmunn Factor --- ASSOCIATED LABORATORIES Analytical Results Report Lab Request o26ua2 Page 1sor17 110 t oncep Eh Clieht '0711112013 15:35 _ Method: EPA 8015 NELAc Prep Method: EPA 5035 QCBatchlD: QC1 138287 Tp�aauoxm,________________._.___wo___..1 .uu�o__..o__mgo�__.o7n7n�__���n_.................. ngiyLe % Recovery Limits Notes -Bromofluorobenzene (SUR) 74 60-140 Method: EPA 8021 NELAC Prep Method: EPA 5035 ooeatch|c, oc1138288 Benzene ND 1 0.0006 0.005 mg/Kg 07117/13 rparish -- Ethylbenzene --'-------'----------''wo----�—o�oop9—'o/�'o's'--'��x�--'o��rn3�a� wo�_»000a._ �g»�V��r«» '._��«h —;l -._-'._—_—_—_—._'-.—_- Tomane _._____._____mo 1 u000*V�o��gx�on�rxo __ �n�n — x--�-�T—a—s —��'�—{T—�m—»-------'-------'------'��---''�—o�o�2 —.-----'--------------------'------------------ .—���—_mn««o --------- 0-7-/-l-"7-/,l-3, '--'—'—'---'' 4-Bromofluorobenzene (SUR) _ 74 60-140 o�uu p�m, mo= Not o�en�uor< MoL MoL=Mmmouon�nuunumu noL=Repomnoom�ouonumu DF= Dilution / A Lab Request 326052 Page 17 of 17 ASSOCIATED LABORATORIES QC SUMMARY FOR LAB REQUEST #326052 Is QCB cfilp`..�:��QC113828 h 8015.8 Method rpar 0 A GC g �q p'py _P77I.-P/Z i� jng " 'm,�ht'� - .., .Matrix;' gig" ma Bia ry . ... . n um Blank RD� Analyte Result Units MDL Notes _T QC1138287MBI TPH Gasoline ND mg/Kg 0.018 3 ---------- — ----------------------------- ------------- ----------- ...... ND = Not Detected or < MDL MDL = Method Detection Limit RDL = Reporting Detection Limit DF = Dilution Factor ASSOCIATED LABORATORIES Analytical Results Report Lab Request 326052 Page 1 of 3 ASSOCIATED LABORATORIES QC SUMMARY FOR LAB REQUEST #326052 Analyst� rpansh Method A, 8021 B !QCB 10*,.�,,,�!OCJ 138288 Matrix ,S blid Analyzed 07116/2413, Instrument , {group) ND = Not Detected or < MOIL MOIL = Method Detection Limit ROL = Reporting Detection Limit OF = Dilution Factor ASSOCIATED LABORATORIES Analytical Results Report Lab Request 326052 Page 2 of 3 Matrix Duplicate Blank "mary Blank Spike Amount Spike Result i Recoveries Analyte Result units .--..MDL ROL Notes IVIS IVISD IVIS IVISD QC1138288MB1 I RPD I %I Benzene NO mg/Kg 0.0006 0.005 - ---------------------- Ethylbenzene .......• ................... ................................ NO mg/Kg 0.0005 0.005 ---- ---------------------------------------------------- Source: 326052-001 ---------------------------------- IVITBE NO mg/Kg 0.0009 0.035 0.12 0.12 ------------ mg/Kg . . --- --------------------- Toluene -------- --------------------------------------- NO mg/Kg 0.0004 0.005 --------------------- -- ----------- * ------------------- Ethylbenzene Xyle . nes (Tot . af) ---------------------- ND mg / Kg -6.0-61 -2 -- 0.015 ----- ....... — --------------------------------- -------- 0.1 20 0103 . ii<� mg --------------- 10'0 86- -------- ------ Toluene NO m L ....... icamma C lk m Su mg/Kg 'A. 88 11.7 Spike Amount Spike Result Recoveries NO Limits 0.364 0.317 -------------------- Analyte LCS LCSD ( LCS LCSD Units LCS LCSDI RPD ON Rec RPDJ Notes 70-130 30 QC1 138288LCSI, QC1 138288LCSD1 Benzene 0.12 0.12 0.120 0.116 mg/Kg 100 97 3 70-130 30 - --------------- ------- Ethylbenzene ---- --------------------- ---------------- ------------------------- 0.12 0.12 0.127 0.124 mg/Kg 106 103 ---------- ------ ------------------------------------- 2 70-130 30 Toluene -------------------- 0.12 0.12 0.123 0.119 mg/Kg 103 99 .... ......................... 3 70-130 30 Xylenes (Total) -------------------------------- ---------- ----------- ------- . ... 0.36 0.36 0.386 0.376 mg/Kg 107 104 ---------------------------------------------- -3. 70-130. - 30 ------- ND = Not Detected or < MOIL MOIL = Method Detection Limit ROL = Reporting Detection Limit OF = Dilution Factor ASSOCIATED LABORATORIES Analytical Results Report Lab Request 326052 Page 2 of 3 Matrix Duplicate Sample Spike Amount Spike Result i Recoveries Limits I Analyte iAmountl IVIS IVISD IVIS IVISD Units I RPD I %I Notes QC1138288MS1, QC1138288MSDI Source: 326052-001 Benzene NO 0.12 0.12 0.119 0.108 mg/Kg . . --- 99 --- 90 9.7 70-130 30 -70--130 -30 ----------- * ------------------- Ethylbenzene NO ---- 0 . .1 - 2 012 -------- 0.1 20 0103 . ii<� mg --------------- 10'0 86- 15.2- ------ Toluene NO 0.12 0.12 0.118 0.105 mg/Kg 98 88 11.7 70-130 30 ..... ..... --- -------------------------------------- Xylenes (Total) NO * ------------------ 0.36 0.36 0.364 0.317 -------------------- ----------- mg/Kg 101 88 * ------------ 13.8 ---------------------- 70-130 30 ND = Not Detected or < MOIL MOIL = Method Detection Limit ROL = Reporting Detection Limit OF = Dilution Factor ASSOCIATED LABORATORIES Analytical Results Report Lab Request 326052 Page 2 of 3 Notes and Definitions B Analyte was present in an associated method blank. Associated sample data was reported with qualifier. C Laboratory Contamination. D The sample duplicate RPD was not within control limits, the sample data was reported without further clarification. DF Dilution Factor DW Sample result is calculated on a dry weigh basis J Reported value is estimated L The laboratory control sample (LCS) or laboratory control sample duplicate (LCSD) was out of control limits. Associated sample data was reported with qualifier. M The matrix spike (MS) or matrix spike duplicate (MSD) was not within control limits due to matrix interference. The associated LCS and /or LCSD was within control limits and the sample data was reported without further clarification. MDL Method Detection Limit NC The analyte concentration in the sample exceeded the spike level by a factor of four or greater, spike recovery and limits do not apply. ND Analyte was not detected or was less than the detection limit. P Sample was received without proper preservation according to EPA guidelines. RDL Reporting Detection Limit S The surrogate recovery was out of control limits due to matrix interference. The associated method blank surrogate recovery was within control limits and the sample data was reported without further clarification. T Sample was extracted /analyzed past the holding time. T2 Sample was analyzed ASAP but received and analyzed past the 15 minute holding time. ND = Not Detected or < MDL MDL = Method Detection Limit RDL = Reporting Detection Limit DF = Dilution Factor �r ASSOCIATED LABORATORIES Analytical Results Report -r Lab Request 326052 Page 3 of 3 FAX 714-S38-1209 Section X Client: Ael-C- Proj ect: Date Received: Name: es No Sample(s) received in cooler: V-e No (Skip Section 2) Shipping Thfonnation: 11, ) Section 2 Was the cooler packed with: v'' Ice Ice Packs Bubble Wrap Styrofoam Paper None Other Sample temperature:' �- (Acceptance range is 0 to 6 Deg. C. or arrival on ice.) Section 3 YES NO N/A Was a COC received? ✓ Is it properly cam feted? s, sam .lin date and time, si ature, test j/ Were custody seals pre sent? If Yes -- were gLey intact? Were all sam les sealed in lastic ba s? t/ Did all samples arrive intact? If no, indicate below. Did all bottle labels a gree with COC? , dates and times) Were correct containers used for the tests required? Was a sufficient amount of sample sent for tests indicated? Was there heads ace in VOA vials? Were the containers labeled with correct reservatives? Was total residual chlorine measured ish Bioassay samples onl ? -r: ji zne answer is no, please inrorm rash Bioassay .Dept. immediately. e Section 4 Explanations/Comments Section 5 Was Project Manager notified of discrepancies: Y / iN N/A Completed By: Date: aL6A3 Created on 7/6/2012 13:29 :00 a7 /p7 m CD (A) .. rn � o rp ID QI Z Number of Containers 3 T C, p '� O v rn m � � W n n O � r I Z O rr oo n m m �° 1 t° 0 V) -i r C co, 0 Q XX C n v C) z I tD K -.. ca m '"• �.. -... _.. ^�.: "i. w„_ O O m Q Q-. "�. o, =O CD CL t? a o o C r- n Q. ? O Q O 0t a. . . cD H��-5 `c r-- Cr Laboratory Sample a� c � Number +�� �, ,,, �,� `•..n, '' ., ,, Sample Matrix: Soll(S) Sludge(SL), Aqueous(A) 50 r14 N< CD X u .. rn � o rp ID QI Z Number of Containers 3 T C, p '� O v rn m � � W n n O � r I Z O rr oo n m m �° 1 t° 0 V) -i r C co, 0 Q XX C .Q C) z I tD K >a ca m wZ n cn m .i Number of Containers d N � W N ca `y.. M Number of Containers � W ca `y.. tD K O m Q Q-. o, =O CD CL Q. ? O Q O 0t 1' a 0 0 33 0 B CD M =I IS-%L I (D (D CL CL tr or -4 3 (D a --1 0 0 c M 0 B -0 S " X ID ;L su 0 (D (D CD X < t J 11� c Ox CL t7F >w Pj L C cr cr 0 In cc,—rl Z3 su tG T 1 co - 0. 0 cr -n M c: 0 0 0 0 0 0 G MO A D �� (D co(0 M w Z 7ET S�D M CD --IZ CD (D 0,) X Z; >1 4e c M 0 CO 3 M 0 su 0 (D m Ox t7F >w Pj A cr 0 A 0 cr M M Z-4 (D tG T 1 co - r> 0 cr -n M c: 0 0 0 0 0 0 G MO A D �� (D co(0 M w Z 0 CA Vi M C a 7 7 144 CO 3 M _0 TIT Ci 9 0 o c, (D co CD —Z 0 0 OD (D CA C a 7 7 =CL 0 JIN a 33 33 w cn 0) (D SD jF CD B cr a r- fn 0) =r 10 a 144 'm 0 0 , Number of Containers 9 0 o c, CIO 0 0 OD C a 7 7 =CL 0 a 33 33 w cn 0) (D SD jF CD B cr a r- fn 0) =r 10 a CL CL @D 0 ca c D< Oca (n < = 0 CD CL MRS_ 0 Z Z 0 15 Laboratory Sample Number Sample Matrix: Soil(S) Sludge(SL), Aqueous(A) > z ID (D w (D CL MA I AOft c cn �I M 0 0 Number of Containers CIO (M CD OD • CO CD :r cn 0) (D SD jF CD B cr CL CL @D 0 c D< Oca (n < = 0 CD CL MRS_ 0 Z Z 0 15 0 0 :3 MA I AOft c cn �I M 0 0