HomeMy WebLinkAbout8-30-19 UDC SOIL SAMPLELaboratories, Inc.
Environmental Testing Laboratory Since 1949
Date of Report: 09/12/2019
Mark Magargee
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Client Project:Brookside Market
BCL Project:
BCL Work Order:
Enclosed are the results of analyses for samples received by the laboratory on 8/30/2019. If you have
any questions concerning this report, please feel free to contact me.
Invoice ID:
1929229
Soil
B354388
Contact Person: Felicia Johnson
Sincerely,
Client Service Rep
Stuart Buttram
Technical Director
Certifications: CA ELAP #1186; NV #CA00014; OR ELAP #4032-001; AK UST101
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 1 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Table of Contents
Sample Information
Chain of Custody and Cooler Receipt form................................................................................................................................................................ 3
Laboratory / Client Sample Cross Reference................................................................................................................................................................ 5
Sample Results
1929229-01 - NWD-2
Volatile Organic Analysis (EPA Method 8260B)................................................................................................................................................................ 7
1929229-02 - NWD-6
Volatile Organic Analysis (EPA Method 8260B)................................................................................................................................................................ 8
1929229-03 - NCD-2
Volatile Organic Analysis (EPA Method 8260B)................................................................................................................................................................ 9
1929229-04 - NCD-6
Volatile Organic Analysis (EPA Method 8260B)................................................................................................................................................................ 10
1929229-05 - SCD-2
Volatile Organic Analysis (EPA Method 8260B)................................................................................................................................................................ 11
1929229-06 - SCD-6
Volatile Organic Analysis (EPA Method 8260B)................................................................................................................................................................ 12
1929229-07 - SED-2
Volatile Organic Analysis (EPA Method 8260B)................................................................................................................................................................ 13
Total Petroleum Hydrocarbons................................................................................................................................................................ 14
1929229-08 - SED-6
Volatile Organic Analysis (EPA Method 8260B)................................................................................................................................................................ 15
Total Petroleum Hydrocarbons................................................................................................................................................................ 16
Quality Control Reports
Volatile Organic Analysis (EPA Method 8260B)
Method Blank Analysis................................................................................................................................................................ 17
Laboratory Control Sample................................................................................................................................................................ 19
Precision and Accuracy................................................................................................................................................................ 20
Total Petroleum Hydrocarbons
Method Blank Analysis................................................................................................................................................................ 21
Laboratory Control Sample................................................................................................................................................................ 22
Precision and Accuracy................................................................................................................................................................ 23
Notes
Notes and Definitions................................................................................................................................................................ 24
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 2 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Chain of Custody and Cooler Receipt Form for 1929229 Page 1 of 2
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 3 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Chain of Custody and Cooler Receipt Form for 1929229 Page 2 of 2
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 4 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
Laboratory / Client Sample Cross Reference
Laboratory Client Sample Information
1929229-01
Sampling Point:
Sampling Location:
Project Number:
COC Number:---
---
---
NWD-2
Receive Date:
Sampling Date:
Sample Depth:
Lab Matrix:
---
08/30/2019 08:50
08/30/2019 07:40
Solids
Mark MagargeeSampled By:Sample Type:Soil
1929229-02
Sampling Point:
Sampling Location:
Project Number:
COC Number:---
---
---
NWD-6
Receive Date:
Sampling Date:
Sample Depth:
Lab Matrix:
---
08/30/2019 08:50
08/30/2019 07:45
Solids
Mark MagargeeSampled By:Sample Type:Soil
1929229-03
Sampling Point:
Sampling Location:
Project Number:
COC Number:---
---
---
NCD-2
Receive Date:
Sampling Date:
Sample Depth:
Lab Matrix:
---
08/30/2019 08:50
08/30/2019 07:55
Solids
Mark MagargeeSampled By:Sample Type:Soil
1929229-04
Sampling Point:
Sampling Location:
Project Number:
COC Number:---
---
---
NCD-6
Receive Date:
Sampling Date:
Sample Depth:
Lab Matrix:
---
08/30/2019 08:50
08/30/2019 08:00
Solids
Mark MagargeeSampled By:Sample Type:Soil
1929229-05
Sampling Point:
Sampling Location:
Project Number:
COC Number:---
---
---
SCD-2
Receive Date:
Sampling Date:
Sample Depth:
Lab Matrix:
---
08/30/2019 08:50
08/30/2019 08:10
Solids
Mark MagargeeSampled By:Sample Type:Soil
1929229-06
Sampling Point:
Sampling Location:
Project Number:
COC Number:---
---
---
SCD-6
Receive Date:
Sampling Date:
Sample Depth:
Lab Matrix:
---
08/30/2019 08:50
08/30/2019 08:15
Solids
Mark MagargeeSampled By:Sample Type:Soil
1929229-07
Sampling Point:
Sampling Location:
Project Number:
COC Number:---
---
---
SED-2
Receive Date:
Sampling Date:
Sample Depth:
Lab Matrix:
---
08/30/2019 08:50
08/30/2019 08:25
Solids
Mark MagargeeSampled By:Sample Type:Soil
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 5 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
Laboratory / Client Sample Cross Reference
Laboratory Client Sample Information
1929229-08
Sampling Point:
Sampling Location:
Project Number:
COC Number:---
---
---
SED-6
Receive Date:
Sampling Date:
Sample Depth:
Lab Matrix:
---
08/30/2019 08:50
08/30/2019 08:30
Solids
Mark MagargeeSampled By:Sample Type:Soil
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 6 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
BCL Sample ID:1929229-01 Client Sample Name:
Constituent Result Units Method Bias Quals
MB Lab
Volatile Organic Analysis (EPA Method 8260B)
Run #
NWD-2, 8/30/2019 7:40:00AM, Mark Magargee
MDLPQL
Benzene mg/kg 0.0018ND0.0050 EPA-8260B 1ND
1,2-Dibromoethane mg/kg 0.0019ND0.0050 EPA-8260B 1ND
1,2-Dichloroethane mg/kg 0.0017ND0.0050 EPA-8260B 1ND
Ethylbenzene mg/kg 0.0022ND0.0050 EPA-8260B 1ND
Methyl t-butyl ether mg/kg 0.0017ND0.0050 EPA-8260B 1ND
Naphthalene mg/kg 0.0023ND0.0050 EPA-8260B 1ND
Toluene mg/kg 0.0020ND0.0050 EPA-8260B 1ND
Total Xylenes mg/kg 0.0034ND0.010 EPA-8260B 1ND
t-Amyl Methyl ether mg/kg 0.00017ND0.0050 EPA-8260B 1ND
t-Butyl alcohol mg/kg 0.0040ND0.050 EPA-8260B 1ND
Diisopropyl ether mg/kg 0.00043ND0.0050 EPA-8260B 1ND
Ethanol mg/kg 0.13ND1.0 EPA-8260B 1ND
Ethyl t-butyl ether mg/kg 0.00014ND0.0050 EPA-8260B 1ND
Total Purgeable Petroleum
Hydrocarbons
mg/kg 0.13ND0.20 Luft-GC/MS 1ND
1,2-Dichloroethane-d4 (Surrogate)%70 - 121 (LCL - UCL)106 EPA-8260B 1
Toluene-d8 (Surrogate)%81 - 117 (LCL - UCL)98.3 EPA-8260B 1
4-Bromofluorobenzene (Surrogate)%74 - 121 (LCL - UCL)99.1 EPA-8260B 1
QC
Batch IDDilutionInstrumentAnalystDate/Time
Run
Prep DateMethodRun #
08/31/19 09:00 08/31/19 14:42 BYM MS-V3 1 B055714EPA-8260B 1
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 7 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
BCL Sample ID:1929229-02 Client Sample Name:
Constituent Result Units Method Bias Quals
MB Lab
Volatile Organic Analysis (EPA Method 8260B)
Run #
NWD-6, 8/30/2019 7:45:00AM, Mark Magargee
MDLPQL
Benzene mg/kg 0.0018ND0.0050 EPA-8260B 1ND
1,2-Dibromoethane mg/kg 0.0019ND0.0050 EPA-8260B 1ND
1,2-Dichloroethane mg/kg 0.0017ND0.0050 EPA-8260B 1ND
Ethylbenzene mg/kg 0.0022ND0.0050 EPA-8260B 1ND
Methyl t-butyl ether mg/kg 0.0017ND0.0050 EPA-8260B 1ND
Naphthalene mg/kg 0.0023ND0.0050 EPA-8260B 1ND
Toluene mg/kg 0.0020ND0.0050 EPA-8260B 1ND
Total Xylenes mg/kg 0.0034ND0.010 EPA-8260B 1ND
t-Amyl Methyl ether mg/kg 0.00017ND0.0050 EPA-8260B 1ND
t-Butyl alcohol mg/kg 0.0040ND0.050 EPA-8260B 1ND
Diisopropyl ether mg/kg 0.00043ND0.0050 EPA-8260B 1ND
Ethanol mg/kg 0.13ND1.0 EPA-8260B 1ND
Ethyl t-butyl ether mg/kg 0.00014ND0.0050 EPA-8260B 1ND
Total Purgeable Petroleum
Hydrocarbons
mg/kg 0.13ND0.20 Luft-GC/MS 1ND
1,2-Dichloroethane-d4 (Surrogate)%70 - 121 (LCL - UCL)108 EPA-8260B 1
Toluene-d8 (Surrogate)%81 - 117 (LCL - UCL)103 EPA-8260B 1
4-Bromofluorobenzene (Surrogate)%74 - 121 (LCL - UCL)98.5 EPA-8260B 1
QC
Batch IDDilutionInstrumentAnalystDate/Time
Run
Prep DateMethodRun #
08/31/19 09:00 08/31/19 15:07 BYM MS-V3 1 B055714EPA-8260B 1
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 8 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
BCL Sample ID:1929229-03 Client Sample Name:
Constituent Result Units Method Bias Quals
MB Lab
Volatile Organic Analysis (EPA Method 8260B)
Run #
NCD-2, 8/30/2019 7:55:00AM, Mark Magargee
MDLPQL
Benzene mg/kg 0.0018ND0.0050 EPA-8260B 1ND
1,2-Dibromoethane mg/kg 0.0019ND0.0050 EPA-8260B 1ND
1,2-Dichloroethane mg/kg 0.0017ND0.0050 EPA-8260B 1ND
Ethylbenzene mg/kg 0.0022ND0.0050 EPA-8260B 1ND
Methyl t-butyl ether mg/kg 0.0017ND0.0050 EPA-8260B 1ND
Naphthalene mg/kg 0.0023ND0.0050 EPA-8260B 1ND
Toluene mg/kg 0.0020ND0.0050 EPA-8260B 1ND
Total Xylenes mg/kg 0.0034ND0.010 EPA-8260B 1ND
t-Amyl Methyl ether mg/kg 0.00017ND0.0050 EPA-8260B 1ND
t-Butyl alcohol mg/kg 0.0040ND0.050 EPA-8260B 1ND
Diisopropyl ether mg/kg 0.00043ND0.0050 EPA-8260B 1ND
Ethanol mg/kg 0.13ND1.0 EPA-8260B 1ND
Ethyl t-butyl ether mg/kg 0.00014ND0.0050 EPA-8260B 1ND
Total Purgeable Petroleum
Hydrocarbons
mg/kg 0.13ND0.20 Luft-GC/MS 1ND
1,2-Dichloroethane-d4 (Surrogate)%70 - 121 (LCL - UCL)105 EPA-8260B 1
Toluene-d8 (Surrogate)%81 - 117 (LCL - UCL)101 EPA-8260B 1
4-Bromofluorobenzene (Surrogate)%74 - 121 (LCL - UCL)102 EPA-8260B 1
QC
Batch IDDilutionInstrumentAnalystDate/Time
Run
Prep DateMethodRun #
08/31/19 09:00 08/31/19 15:32 BYM MS-V3 1 B056001EPA-8260B 1
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 9 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
BCL Sample ID:1929229-04 Client Sample Name:
Constituent Result Units Method Bias Quals
MB Lab
Volatile Organic Analysis (EPA Method 8260B)
Run #
NCD-6, 8/30/2019 8:00:00AM, Mark Magargee
MDLPQL
Benzene mg/kg 0.0018ND0.0050 EPA-8260B 1ND
1,2-Dibromoethane mg/kg 0.0019ND0.0050 EPA-8260B 1ND
1,2-Dichloroethane mg/kg 0.0017ND0.0050 EPA-8260B 1ND
Ethylbenzene mg/kg 0.0022ND0.0050 EPA-8260B 1ND
Methyl t-butyl ether mg/kg 0.0017ND0.0050 EPA-8260B 1ND
Naphthalene mg/kg 0.0023ND0.0050 EPA-8260B 1ND
Toluene mg/kg 0.0020ND0.0050 EPA-8260B 1ND
Total Xylenes mg/kg 0.0034ND0.010 EPA-8260B 1ND
t-Amyl Methyl ether mg/kg 0.00017ND0.0050 EPA-8260B 1ND
t-Butyl alcohol mg/kg 0.0040ND0.050 EPA-8260B 1ND
Diisopropyl ether mg/kg 0.00043ND0.0050 EPA-8260B 1ND
Ethanol mg/kg 0.13ND1.0 EPA-8260B 1ND
Ethyl t-butyl ether mg/kg 0.00014ND0.0050 EPA-8260B 1ND
Total Purgeable Petroleum
Hydrocarbons
mg/kg 0.13ND0.20 Luft-GC/MS 1ND
1,2-Dichloroethane-d4 (Surrogate)%70 - 121 (LCL - UCL)108 EPA-8260B 1
Toluene-d8 (Surrogate)%81 - 117 (LCL - UCL)101 EPA-8260B 1
4-Bromofluorobenzene (Surrogate)%74 - 121 (LCL - UCL)100 EPA-8260B 1
QC
Batch IDDilutionInstrumentAnalystDate/Time
Run
Prep DateMethodRun #
08/31/19 09:00 08/31/19 15:58 BYM MS-V3 1 B056001EPA-8260B 1
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 10 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
BCL Sample ID:1929229-05 Client Sample Name:
Constituent Result Units Method Bias Quals
MB Lab
Volatile Organic Analysis (EPA Method 8260B)
Run #
SCD-2, 8/30/2019 8:10:00AM, Mark Magargee
MDLPQL
Benzene mg/kg 0.0018ND0.0050 EPA-8260B 1ND
1,2-Dibromoethane mg/kg 0.0019ND0.0050 EPA-8260B 1ND
1,2-Dichloroethane mg/kg 0.0017ND0.0050 EPA-8260B 1ND
Ethylbenzene mg/kg 0.0022ND0.0050 EPA-8260B 1ND
Methyl t-butyl ether mg/kg 0.0017ND0.0050 EPA-8260B 1ND
Naphthalene mg/kg 0.0023ND0.0050 EPA-8260B 1ND
Toluene mg/kg 0.0020ND0.0050 EPA-8260B 1ND
Total Xylenes mg/kg 0.0034ND0.010 EPA-8260B 1ND
t-Amyl Methyl ether mg/kg 0.00017ND0.0050 EPA-8260B 1ND
t-Butyl alcohol mg/kg 0.0040ND0.050 EPA-8260B 1ND
Diisopropyl ether mg/kg 0.00043ND0.0050 EPA-8260B 1ND
Ethanol mg/kg 0.13ND1.0 EPA-8260B 1ND
Ethyl t-butyl ether mg/kg 0.00014ND0.0050 EPA-8260B 1ND
Total Purgeable Petroleum
Hydrocarbons
mg/kg 0.13ND0.20 Luft-GC/MS 1ND
1,2-Dichloroethane-d4 (Surrogate)%70 - 121 (LCL - UCL)114 EPA-8260B 1
Toluene-d8 (Surrogate)%81 - 117 (LCL - UCL)103 EPA-8260B 1
4-Bromofluorobenzene (Surrogate)%74 - 121 (LCL - UCL)95.5 EPA-8260B 1
QC
Batch IDDilutionInstrumentAnalystDate/Time
Run
Prep DateMethodRun #
08/31/19 09:00 08/31/19 16:23 BYM MS-V3 1 B056001EPA-8260B 1
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 11 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
BCL Sample ID:1929229-06 Client Sample Name:
Constituent Result Units Method Bias Quals
MB Lab
Volatile Organic Analysis (EPA Method 8260B)
Run #
SCD-6, 8/30/2019 8:15:00AM, Mark Magargee
MDLPQL
Benzene mg/kg 0.0018ND0.0050 EPA-8260B 1ND
1,2-Dibromoethane mg/kg 0.0019ND0.0050 EPA-8260B 1ND
1,2-Dichloroethane mg/kg 0.0017ND0.0050 EPA-8260B 1ND
Ethylbenzene mg/kg 0.00220.0095 0.0050 EPA-8260B 1ND
Methyl t-butyl ether mg/kg 0.0017ND0.0050 EPA-8260B 1ND
Naphthalene mg/kg J0.00230.0036 0.0050 EPA-8260B 1ND
Toluene mg/kg 0.00200.041 0.0050 EPA-8260B 1ND
Total Xylenes mg/kg 0.00340.074 0.010 EPA-8260B 1ND
t-Amyl Methyl ether mg/kg 0.00017ND0.0050 EPA-8260B 1ND
t-Butyl alcohol mg/kg 0.0040ND0.050 EPA-8260B 1ND
Diisopropyl ether mg/kg 0.00043ND0.0050 EPA-8260B 1ND
Ethanol mg/kg 0.13ND1.0 EPA-8260B 1ND
Ethyl t-butyl ether mg/kg 0.00014ND0.0050 EPA-8260B 1ND
Total Purgeable Petroleum
Hydrocarbons
mg/kg 0.130.65 0.20 Luft-GC/MS 1ND
1,2-Dichloroethane-d4 (Surrogate)%70 - 121 (LCL - UCL)110 EPA-8260B 1
Toluene-d8 (Surrogate)%81 - 117 (LCL - UCL)99.0 EPA-8260B 1
4-Bromofluorobenzene (Surrogate)%74 - 121 (LCL - UCL)99.8 EPA-8260B 1
QC
Batch IDDilutionInstrumentAnalystDate/Time
Run
Prep DateMethodRun #
08/31/19 09:00 08/31/19 16:49 BYM MS-V3 1 B056001EPA-8260B 1
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 12 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
BCL Sample ID:1929229-07 Client Sample Name:
Constituent Result Units Method Bias Quals
MB Lab
Volatile Organic Analysis (EPA Method 8260B)
Run #
SED-2, 8/30/2019 8:25:00AM, Mark Magargee
MDLPQL
Benzene mg/kg J0.00180.0029 0.0050 EPA-8260B 1ND
1,2-Dibromoethane mg/kg 0.0019ND0.0050 EPA-8260B 1ND
1,2-Dichloroethane mg/kg 0.0017ND0.0050 EPA-8260B 1ND
Ethylbenzene mg/kg 0.00220.0050 0.0050 EPA-8260B 1ND
Methyl t-butyl ether mg/kg 0.0017ND0.0050 EPA-8260B 1ND
Naphthalene mg/kg 0.0023ND0.0050 EPA-8260B 1ND
Toluene mg/kg 0.00200.012 0.0050 EPA-8260B 1ND
Total Xylenes mg/kg 0.00340.017 0.010 EPA-8260B 1ND
t-Amyl Methyl ether mg/kg 0.00017ND0.0050 EPA-8260B 1ND
t-Butyl alcohol mg/kg 0.0040ND0.050 EPA-8260B 1ND
Diisopropyl ether mg/kg 0.00043ND0.0050 EPA-8260B 1ND
Ethanol mg/kg 0.13ND1.0 EPA-8260B 1ND
Ethyl t-butyl ether mg/kg 0.00014ND0.0050 EPA-8260B 1ND
Total Purgeable Petroleum
Hydrocarbons
mg/kg 0.130.20 0.20 Luft-GC/MS 1ND
1,2-Dichloroethane-d4 (Surrogate)%70 - 121 (LCL - UCL)108 EPA-8260B 1
Toluene-d8 (Surrogate)%81 - 117 (LCL - UCL)103 EPA-8260B 1
4-Bromofluorobenzene (Surrogate)%74 - 121 (LCL - UCL)105 EPA-8260B 1
QC
Batch IDDilutionInstrumentAnalystDate/Time
Run
Prep DateMethodRun #
08/31/19 09:00 08/31/19 17:14 BYM MS-V3 1 B056001EPA-8260B 1
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 13 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
BCL Sample ID:1929229-07 Client Sample Name:
Constituent Result Units Method Bias Quals
MB Lab
Total Petroleum Hydrocarbons
Run #
SED-2, 8/30/2019 8:25:00AM, Mark Magargee
MDLPQL
Diesel Range Organics (C12 - C24)mg/kg A521.311010 EPA-8015B/TPH
d 1ND
Tetracosane (Surrogate)%40 - 130 (LCL - UCL)92.4 EPA-8015B/TPH
d 1
QC
Batch IDDilutionInstrumentAnalystDate/Time
Run
Prep DateMethodRun #
09/04/19 15:00 09/09/19 20:10 JGM GC-5 1.017 B056476EPA-8015B/TPHd 1
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 14 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
BCL Sample ID:1929229-08 Client Sample Name:
Constituent Result Units Method Bias Quals
MB Lab
Volatile Organic Analysis (EPA Method 8260B)
Run #
SED-6, 8/30/2019 8:30:00AM, Mark Magargee
MDLPQL
Benzene mg/kg 0.0018ND0.0050 EPA-8260B 1ND
1,2-Dibromoethane mg/kg 0.0019ND0.0050 EPA-8260B 1ND
1,2-Dichloroethane mg/kg 0.0017ND0.0050 EPA-8260B 1ND
Ethylbenzene mg/kg 0.0022ND0.0050 EPA-8260B 1ND
Methyl t-butyl ether mg/kg 0.0017ND0.0050 EPA-8260B 1ND
Naphthalene mg/kg 0.0023ND0.0050 EPA-8260B 1ND
Toluene mg/kg 0.0020ND0.0050 EPA-8260B 1ND
Total Xylenes mg/kg 0.0034ND0.010 EPA-8260B 1ND
t-Amyl Methyl ether mg/kg 0.00017ND0.0050 EPA-8260B 1ND
t-Butyl alcohol mg/kg 0.0040ND0.050 EPA-8260B 1ND
Diisopropyl ether mg/kg 0.00043ND0.0050 EPA-8260B 1ND
Ethanol mg/kg 0.13ND1.0 EPA-8260B 1ND
Ethyl t-butyl ether mg/kg 0.00014ND0.0050 EPA-8260B 1ND
Total Purgeable Petroleum
Hydrocarbons
mg/kg 0.13ND0.20 Luft-GC/MS 1ND
1,2-Dichloroethane-d4 (Surrogate)%70 - 121 (LCL - UCL)109 EPA-8260B 1
Toluene-d8 (Surrogate)%81 - 117 (LCL - UCL)100 EPA-8260B 1
4-Bromofluorobenzene (Surrogate)%74 - 121 (LCL - UCL)100 EPA-8260B 1
QC
Batch IDDilutionInstrumentAnalystDate/Time
Run
Prep DateMethodRun #
08/31/19 09:00 08/31/19 17:39 BYM MS-V3 1 B056001EPA-8260B 1
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 15 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
BCL Sample ID:1929229-08 Client Sample Name:
Constituent Result Units Method Bias Quals
MB Lab
Total Petroleum Hydrocarbons
Run #
SED-6, 8/30/2019 8:30:00AM, Mark Magargee
MDLPQL
Diesel Range Organics (C12 - C24)mg/kg 1.3ND10 EPA-8015B/TPH
d 1ND
Tetracosane (Surrogate)%40 - 130 (LCL - UCL)102 EPA-8015B/TPH
d 1
QC
Batch IDDilutionInstrumentAnalystDate/Time
Run
Prep DateMethodRun #
09/04/19 15:00 09/09/19 20:57 JGM GC-5 0.993 B056476EPA-8015B/TPHd 1
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 16 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
Quality Control Report - Method Blank Analysis
Constituent QC Sample ID MB Result Units Lab Quals
Volatile Organic Analysis (EPA Method 8260B)
MDLPQL
QC Batch ID: B055714
Benzene B055714-BLK1 0.0050NDmg/kg 0.0018
1,2-Dibromoethane B055714-BLK1 0.0050NDmg/kg 0.0019
1,2-Dichloroethane B055714-BLK1 0.0050NDmg/kg 0.0017
Ethylbenzene B055714-BLK1 0.0050NDmg/kg 0.0022
Methyl t-butyl ether B055714-BLK1 0.0050NDmg/kg 0.0017
Naphthalene B055714-BLK1 0.0050NDmg/kg 0.0023
Toluene B055714-BLK1 0.0050NDmg/kg 0.0020
Total Xylenes B055714-BLK1 0.010NDmg/kg 0.0034
t-Amyl Methyl ether B055714-BLK1 0.0050NDmg/kg 0.00017
t-Butyl alcohol B055714-BLK1 0.050NDmg/kg 0.0040
Diisopropyl ether B055714-BLK1 0.0050NDmg/kg 0.00043
Ethanol B055714-BLK1 1.0NDmg/kg 0.13
Ethyl t-butyl ether B055714-BLK1 0.0050NDmg/kg 0.00014
Total Purgeable Petroleum Hydrocarbons B055714-BLK1 0.20NDmg/kg 0.13
1,2-Dichloroethane-d4 (Surrogate)B055714-BLK1 105 %70 - 121 (LCL - UCL)
Toluene-d8 (Surrogate)B055714-BLK1 98.9 %81 - 117 (LCL - UCL)
4-Bromofluorobenzene (Surrogate)B055714-BLK1 98.6 %74 - 121 (LCL - UCL)
QC Batch ID: B056001
Benzene B056001-BLK1 0.0050NDmg/kg 0.0018
1,2-Dibromoethane B056001-BLK1 0.0050NDmg/kg 0.0019
1,2-Dichloroethane B056001-BLK1 0.0050NDmg/kg 0.0017
Ethylbenzene B056001-BLK1 0.0050NDmg/kg 0.0022
Methyl t-butyl ether B056001-BLK1 0.0050NDmg/kg 0.0017
Naphthalene B056001-BLK1 0.0050NDmg/kg 0.0023
Toluene B056001-BLK1 0.0050NDmg/kg 0.0020
Total Xylenes B056001-BLK1 0.010NDmg/kg 0.0034
t-Amyl Methyl ether B056001-BLK1 0.0050NDmg/kg 0.00017
t-Butyl alcohol B056001-BLK1 0.050NDmg/kg 0.0040
Diisopropyl ether B056001-BLK1 0.0050NDmg/kg 0.00043
Ethanol B056001-BLK1 1.0NDmg/kg 0.13
Ethyl t-butyl ether B056001-BLK1 0.0050NDmg/kg 0.00014
Total Purgeable Petroleum Hydrocarbons B056001-BLK1 0.20NDmg/kg 0.13
1,2-Dichloroethane-d4 (Surrogate)B056001-BLK1 98.7 %70 - 121 (LCL - UCL)
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 17 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
Quality Control Report - Method Blank Analysis
Constituent QC Sample ID MB Result Units Lab Quals
Volatile Organic Analysis (EPA Method 8260B)
MDLPQL
QC Batch ID: B056001
Toluene-d8 (Surrogate)B056001-BLK1 99.3 %81 - 117 (LCL - UCL)
4-Bromofluorobenzene (Surrogate)B056001-BLK1 97.7 %74 - 121 (LCL - UCL)
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 18 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
Quality Control Report - Laboratory Control Sample
Constituent
Control Limits
PercentPercentSpike
QC Sample ID Type Result Level Units Recovery RPD Recovery RPD Quals
Volatile Organic Analysis (EPA Method 8260B)
Lab
QC Batch ID: B055714
Benzene B055714-BS1 LCS 0.13220 0.12500 106 70 - 130mg/kg
Toluene B055714-BS1 LCS 0.12344 0.12500 98.8 70 - 130mg/kg
1,2-Dichloroethane-d4 (Surrogate)B055714-BS1 LCS 0.048580 0.050000 97.2 70 - 121mg/kg
Toluene-d8 (Surrogate)B055714-BS1 LCS 0.049300 0.050000 98.6 81 - 117mg/kg
4-Bromofluorobenzene (Surrogate)B055714-BS1 LCS 0.050860 0.050000 102 74 - 121mg/kg
QC Batch ID: B056001
Benzene B056001-BS1 LCS 0.13499 0.12500 108 70 - 130mg/kg
Toluene B056001-BS1 LCS 0.12666 0.12500 101 70 - 130mg/kg
1,2-Dichloroethane-d4 (Surrogate)B056001-BS1 LCS 0.051800 0.050000 104 70 - 121mg/kg
Toluene-d8 (Surrogate)B056001-BS1 LCS 0.050730 0.050000 101 81 - 117mg/kg
4-Bromofluorobenzene (Surrogate)B056001-BS1 LCS 0.051460 0.050000 103 74 - 121mg/kg
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 19 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
Quality Control Report - Precision & Accuracy
Constituent Sample IDType Result Result Added Units RPD Recovery RPD Recovery Quals
Source Spike Percent Percent
Control Limits
Volatile Organic Analysis (EPA Method 8260B)
Source Lab
QC Batch ID: B055714 Used client sample: N
MSBenzene 0.13006 70 - 130ND0.12500 1041927434-47 mg/kg
MSD 0.14200 8.8 20 70 - 130ND0.12500 1141927434-47 mg/kg
MSToluene 0.12418 70 - 130ND0.12500 99.31927434-47 mg/kg
MSD 0.12867 3.6 20 70 - 130ND0.12500 1031927434-47 mg/kg
MS1,2-Dichloroethane-d4 (Surrogate)0.049850 70 - 121ND0.050000 99.71927434-47 mg/kg
MSD 0.051850 3.9 70 - 121ND0.050000 1041927434-47 mg/kg
MSToluene-d8 (Surrogate)0.048280 81 - 117ND0.050000 96.61927434-47 mg/kg
MSD 0.049190 1.9 81 - 117ND0.050000 98.41927434-47 mg/kg
MS4-Bromofluorobenzene (Surrogate)0.051380 74 - 121ND0.050000 1031927434-47 mg/kg
MSD 0.049410 3.9 74 - 121ND0.050000 98.81927434-47 mg/kg
QC Batch ID: B056001 Used client sample: N
MSBenzene 0.12203 70 - 130ND0.12500 97.61927434-50 mg/kg
MSD 0.13622 11.0 20 70 - 130ND0.12500 1091927434-50 mg/kg
MSToluene 0.11758 70 - 130ND0.12500 94.11927434-50 mg/kg
MSD 0.12417 5.5 20 70 - 130ND0.12500 99.31927434-50 mg/kg
MS1,2-Dichloroethane-d4 (Surrogate)0.049520 70 - 121ND0.050000 99.01927434-50 mg/kg
MSD 0.050690 2.3 70 - 121ND0.050000 1011927434-50 mg/kg
MSToluene-d8 (Surrogate)0.050520 81 - 117ND0.050000 1011927434-50 mg/kg
MSD 0.049650 1.7 81 - 117ND0.050000 99.31927434-50 mg/kg
MS4-Bromofluorobenzene (Surrogate)0.050470 74 - 121ND0.050000 1011927434-50 mg/kg
MSD 0.051960 2.9 74 - 121ND0.050000 1041927434-50 mg/kg
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 20 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
Quality Control Report - Method Blank Analysis
Constituent QC Sample ID MB Result Units Lab Quals
Total Petroleum Hydrocarbons
MDLPQL
QC Batch ID: B056476
Diesel Range Organics (C12 - C24)B056476-BLK1 10NDmg/kg 1.3
Tetracosane (Surrogate)B056476-BLK1 111 %40 - 130 (LCL - UCL)
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 21 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
Quality Control Report - Laboratory Control Sample
Constituent
Control Limits
PercentPercentSpike
QC Sample ID Type Result Level Units Recovery RPD Recovery RPD Quals
Total Petroleum Hydrocarbons
Lab
QC Batch ID: B056476
Diesel Range Organics (C12 - C24)B056476-BS1 LCS 95.726 83.893 114 58 - 131mg/kg
Tetracosane (Surrogate)B056476-BS1 LCS 3.6354 3.3557 108 40 - 130mg/kg
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 22 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
Quality Control Report - Precision & Accuracy
Constituent Sample IDType Result Result Added Units RPD Recovery RPD Recovery Quals
Source Spike Percent Percent
Control Limits
Total Petroleum Hydrocarbons
Source Lab
QC Batch ID: B056476 Used client sample: Y - Description: SED-2, 08/30/2019 08:25
MSDiesel Range Organics (C12 - C24)199.52 54 - 119110.13 84.175 106 A011929229-07 mg/kg
MSD 196.11 1.7 30 54 - 119110.13 84.746 101 A011929229-07 mg/kg
MSTetracosane (Surrogate)3.2495 40 - 130ND3.3670 96.5 A011929229-07 mg/kg
MSD 3.5027 7.5 40 - 130ND3.3898 103 A011929229-07 mg/kg
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 23 of 24Report ID: 1000937692
Laboratories, Inc.
Environmental Testing Laboratory Since 1949
Mark R. Magargee PG, CHg
6730 Canaletto Avenue
Bakersfield, CA 93306
Project:
Project Number:
Project Manager:
Soil
Brookside Market
Mark Magargee
Reported:09/12/2019 13:33
Notes And Definitions
J Estimated Value (CLP Flag)
MDL Method Detection Limit
ND Analyte Not Detected
PQL Practical Quantitation Limit
A01 Detection and quantitation limits are raised due to sample dilution.
A52 Chromatogram not typical of diesel.
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation.
4100 Atlas Court Bakersfield, CA 93308 (661) 327-4911 FAX (661) 327-1918 www.bclabs.com Page 24 of 24Report ID: 1000937692