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M/D TOTCO, INC. 6910 MEANY AVENUE BAKERSFIELD, CALIFORNIA 93308 SOILS CONFIRMATION-SAMPLING INVESTIGATION FORMER CLASS V INJECTION WELL 3011 ANTONINO AVENUE BAKERSFIELD, CALIFORNIA 93308 Completed: APRIL 7, 1993 Pedormed by: Dayne L. Frary, Geologist Jeff Campbell Environmental Consulting 8559 Farmers Lane -Bakersfield, California 93307 (805) 845-8797 JEFF. CAMPBELL ENVIRONMENTAL CONSUL TING MID TOTCO, INC. 6910 MEANY AVENUE BAKERSFIELD, CALIFORNIA 93308 SOILS CONFIRMATION-SAMPLING INVESTIGATION FORMER CLASS V INJECTION WELL 3011 ANTONINO AVENUE BAKERSFIELD, CALIFORNIA 93308 Completed: APRIL 7, 1993 Pedormed by~ Dayne L. Frary, Geologist Jeff Campbell Environmental Consulting 8559 Farmers Lane Bakersfield, California 93307 (805) 845-8797 8559 FARMERS LN. BAKERSFIELD, CALIFORNIA 93307 TELEPHONE 845-8797 - TABLE OF CONTENTS 1.0 Introduction 1 2.0 'Background 1 3.0 Condensed Protocols 2 3.1 Borehole Drilling 2 3.2 Soil Sampling 2 3.3 Borehole Abandonment 3 4.0 Field Investigation 3 4.1 Soil Boring 3 4.2 Soil Description 3 5.0 Laboratory Analyses and Results 3 5.1 Chain-of-Custody and Transport 3 5.2 Laboratory Analyses 4 5.3 Analytical Results 4 6.0 Conclusions 5 7.0 Recommendation 5 8.0 Limitations 6 9.0 Certification 7 EXHIBITS Figures Figure 1 Location Map Figure 2 Site Map and Cross-Section of Former Class V Injection Well Tables Table 1 Boring Log Table 2 Summary of Analytical Results APPENDICES Appendix A Phase II Soils Investigation Workplan Appendix B Unified Soil Classification System Appendix C Chain-of-Custody Documentation Appendix D Zalco Laboratories, Inc. Reports of Soil Analyses SOILS CONFIRMATION-SAMPLING INVESTIGATION FORMER M/D TOTCO, INC. CLASS V INJECTION WELL 3011 Antonino Avenue Bakersfield, California 93308 1.0 INTRODUCTION This report describes the completion of subsurface soil sampling activities and laboratory analyses as required by the Kern County Environmental Health Services Department (County) at the former Class V injection well operated by M/D TOTCO, Inc. The former well was located just West of the rear of the M/D TOTCO, Inc. office and shop building at 3011 Antonino Avenue in Bakersfield (see Figure 1). Mr. Jeff Campbell, Environmental Consultant, served as project manager and site safety officer. Soil samples were collected under the supervision of and described by Mr. Dayne L. Frary, a California Registered Geologist. Ms. Flora Darling, Hazardous Materials Specialist, served as the County's on-site representative. 2.0 BACKGROUND Mr. Campbell's report, MID TOTCO. Inc. Dry_ Well Characterization and Site Remediation, provides details of the former well, clarifier, and piping system location and construction, site history, geology, hydrogeology, and all activities performed in the initial portion of the project. The initial report was dated February 4, 1993. The results of the primary soil sampling and laboratory analyses are also included in the initial report. The surface elevation of the site is approximately 400 feet above mean sea level. The depth to the uppermost water table underlying the site is believed to be betWeen 35 and 50 feet below surface grade (flosg). The water table was not reached or intercepted during borehole drilling operations. The property had been leased to M/D TOTCO, Inc. for some 14 years. The company utilized the well for waste-water collection and elimination by drainage through a gravel pack (see Figure 2). The waste water was generated as rinsate by the cleaning of oil well drilling tools with a high-pressure washer and by use of a wash basin inside the shop. Rinsate was piped by gravity to a clarifier, thence to the concrete, gravel-lined well. The total depth of the well at the base of the gravel Pack was approximately 17Jbsg. The well was altered for abandonment during Mr. Campbell's field investigation in January, I993. The piping, concrete liner, gravel pack, and known contaminated soil were removed M~-~O~L~, la~. 04-93 1 IUUH __ SITE LOCATION ' - NOT TO SCALE / .// / ~ ~ JEFF CAMPBELL __.~_~ ENVIRONMENTAL CONSULTING ,,I .... ~_~ MD/TOTCO, INC. 3011 ANTONINO A~NUE BA~RSFIELD, C~IFO~IA 93308 I SITE MAP AND CROSS-SECTION OF ORIGINAL CLASS V INJECTION WELL 3011 ANTONINO AVENUE OFFICE / SHOP STRUCTURE BOREHOLE WASH BASIN LOCATION CLARIFIER (CEMENTED) AERIAL VIEW ORIGINAL CROSS-SECTIONAL VIEW CLASS V INJECTION WELL ABANDONED JANUARY 1993 DRAWINGS NOT TO SCALE FIGURE'2 using a backhoe to a depth of 22 fosg. All were transported to VenVirotek, a licensed disposal facility in Arvin, California. The clarifier was abandoned by filling it with concrete to surface grade. The former well excavation was backfilled with clean, off-site, borrow sand. The County subsequently reqUired that additional sampling be undertaken to demonstrate, that uncontaminated native soil existed a minimum of five (5) feet below the last reported depth of excavated (removed) contaminated soil. A workplan was prepared by Mr. Frary on February 19, 1993 detailing the subsurface soil sample collection procedures and required laboratory analyses to be performed on each sample. Mr. Campbell prepared the site health and safety plan which was submitted with ,the workplan to the County. The workplan is included as Appendix A. 3.0 CONDENSED PROTOCOLS 3.1 Borehole Drilling Melton Drilling Company (Melton Drilling), under'the supervision of Mr. Frary, was utilized to drill the confirmation soil boring at the M/D TOTCO, Inc. site. Melton Drilling operated a truck-mounted, B57 drilling rig utilizing a 6-inch diameter, continuous-flight, hollow-stem auger to advance the boring. All boring equipment was steam-cleaned prior to arrival on-site. The boring was placed directly over the original Class V injection well location as shown on the Site Map (see Figure 2). Descriptions of the penetrated sediments were recorded on the boring log (see Table 1). All observed changes were noted by the geologist, and the soil types were described using the Unified Soil Classification System (see Appendix B). 3.2 Soil Sampling A 2.5-inch diameter by 18-inch length "undisturbed sample" was collected (or attempted) at 22, 27, and 32 fosg using a split-spoon sampler lined with three, 6-inch long, brass sample rings. The sampler was driven ahead of the auger bit by a 140-lb., down-hole hammer. The soil contained in the upper and middle sample rings was described, and the descriptions were recorded on the Boring Log (see Table 1). The bottom sample, when recovered, is normally selected for the laboratory analyses. The ends are sealed with Teflon or aluminum foil, capped, and wrapped with duct tape. The sample is then placed in an ice chest chilled with cracked ice (or Blue Ice) to 4 degrees Centigrade to maintain chemical integrity for transport to the laboratory. The purpose of the Soil Sampling Protocol is to ensure the accuracy of the results of 04-93 2 laboratory analyses. This is accomplished in part by the use of steam-cleaned drilling' equipment. In addition, the split-spoon samplers and brass sample rings are washed in a solution of trisodium phosphate (TSP), rinsed in tap water, and then final-rinsed in distilled water prior to drilling and sample retrieval. The sample identifications (IDs) are recorded on a chain-of-custody document. The chain-of-custody remains with the samples through transport and delivery to a California Department of Health Services (DoHS)-certified laboratory for analysis. At the laboratory the sample count, IDs, and requested analyses are verified, the documentation is signed, and a copy is retUrned to the responsible consultant. 3.3 Borehole Abandonment After the boring is drilled and sampled, it is properly abandoned to the surface using hydrated bentonite clay chips and topped with clean, off-site borrow soil. The surface is level-patched with asphalt or level-sealed with concrete, depending on composition. 4.0 FIELD INVESTIGATION 4.1 Soil Boring On March I I, 1993, Melton Drilling, under the supervision of Mr. Frary, drilled one (1), six-inch diameter soil boring through the center of the tbrmer Class V injection well for the purpose of confirmation soil sampling. The boring was drilled to a total depth of 33 jbsg. Samples were recovered at 22, 27, and 32 fosg. Following sample collection, the boring was abandoned from 33 to 22 fl~sg with hydrated bentonite chips, and from 22 Jbsg to surface grade with the clean, borrow, backfill sand. The surface Was repaired with asphalt cold-patch, restoring it to near original condition. 4.2 Soil Description The soils encountered during the investigation consisted of fluvial (river-deposited) sands which were generally fine- to medium-grained, quartzitic, very friable, and somewhat cobbly between 28 and 33 Jbsg. No hydrocarbon stains or odors were observed or noted in the three (3) split-spoon samples or in the cuttings. Detailed descriptions of these sands are provided on the Boring Log (see Table 1). 5.0 LABORATORY ANALYSES AND RESULTS 5.1 Chain-of-Custody and Transport A chain-of-custody document was prepared listing the three (3) soil samples and the JEFF CAMPBELL ENVIRONMENTAL CONSULTING BORING LOC. DAYNE L. FRARY. GEOLOGIST CLIENT: MD-TOTCO, INC. DRILLING COMPANY: Melton SITE ADDRESS: 3011 Antonino Ave., Bakersfield CA 93308 DRILLING METHOD: Hollow-Stem Auger DRILLING DATE: March 11, 1993 SAMPLING METHOD: Split-Spoon LOGGED BY: D.L. Frary BORING DIAMETER: 6 Inches DEPTH TO WATER: Water Not Encountered TOTAL DEPTH: 33 Feet DEPTH BLOWS SAMPLE LITHOLOGIC DESCRIPTION LITH. USCS RECOV. (Feett per 6 in. I.D. GENERAL INFORMATION SYMBOL SYMBOL RATIO 0 Asphalt parking surface Sand: clean, borrow backfill from 0.25 feet to 21.75 feet below surface grade (fbsg) 5 10 15 20 2~ 12-15-19 002-008-22 Sand: It bm, f-reed gr, qtztc, rare cs grains & '.~ .'.'.'.'.'-'~ '.' SP-SW 3/3 very friable :.%..'.:r ~ .'.. 27' 13-30-45 002-008-27 Sand: med brn, med gr, qtztc, no stain or :;."ii::'?';.'i.'~'.;' SP 3/3 · 128 fbsg; difficult drilling · '--. ,,?2 63-63-NP 002-008-32 Sand: med brn, v fine-reed gr, qtztc, cs-gr '. '..'. ~ ....SP-SW 1/3 33 hornfels debris, no stain cr odor, moist, very ~...................:. friable; granite cobble jammed in middle brass ring prevented complete recovery NP: Not Penetrated I Sarnpl/ng Depths in #al/cs TABLE 1 MD-TOTCO, Inc. April 1993 required analyses to be performed by Zalco Laboratories, Inc. (Zalco) prior to transport. The samples were chilled to 4 degrees ~Centigrade in an ice chest filled with cracked ice and were immediately transported and delivered to Zalco on March 11, 1993. The chain-of-custody was signed at the laboratory upon sample receipt, and a copy was returned to Mr. Campbell. It is included as Appendix C. 5.2 Laboratory Analyses All 3 soil samples were analyzed at Zalco Laboratories in Bakersfield, California for the following constituents: 1) Total Petroleum Hydrocarbons as Gasoline by Dolls LUFT Method (EPA 8015-mod. equivalent) 2) Total Petroleum Hydrocarbons as Diesel by Dolls LUFT Method (EPA 8015-mod. equivalent) 3) Aromatic Volatile Organics (Benzene, Toluene, Xylenes, and Ethylbenzene) by EPA Method 8020 4) Volatile Organics by EPA Method 8240 5) Semivolafile Organics by EPA Method 8270 6) CAM Metals: Barium, Cadmium, Copper, and Lead by EPA Method 6010. 5.3 Analytical Results Zalco completed the laboratory analyses and reported the results on March 23 and 30, 1993. For all hydrocarbon/organic analyses listed in section 5.2 of this report, the results for the three (3) samples were nondetectable (ND) for each constituent. Only naturally-occurring background levels of the CAM metals barium and copper were reported in the 3 samples. Barium was reported at 34 mg/kg in the sample collected at 22 flosg, at 39 mg/kg in the sample collected at 27 fosg, and at 31 mg/kg in the sample collected at 32 fosg. The Soluble Threshold Limit Concentration (STLC) for barium is 100 mg/l. Copper was reported at 14 mg/kg in the sample collected at 22Jbsg, at 13 mg/kg in the sample collected at 27fosg, and at 21 mg/kg in the.sample collected at 32 fosg. The STLC for copper is 25 mg/l. Only the sample collected at '329'bsg exhibited a background level of cadmium at 0.7 mg/kg, which is below the STLC of 1.0 mg/l.. It was not detected in the overlying 22- and 27-Jbsg samples. Lead was not detected in any of the samples. The Summary of Laboratory Results is included as Table 2. The laboratory reports are MD-TOTCO, Inc. 0~-~3 ~ JEFF CAMPBELL ENVIRONMENTAL CONSULTING SUMMARY OF ANALYTICAL RESULTS I DAYNE L. FRARY, GEOLOGIST D=22 fbsg D=27 fbsg D=32 fbsg Minimum Maximum EPAor DollS Lab Method Sample I.D. Sample I.D. Sample I.D. Reporting Concentration and Analyzed Constituents 002-008-22 002-008-27 002-008-32 Level limit mg/kg mg/kg mg/kg mg/kg mg/kg Dolls LUFT - TPH-Diesel ND ND ND 10 100 DollS LUFT - TPH-Gasoline ND ND ND 10 100 8020 - Aromatic Volatile Organics Benzene ND ND ND 0.005 1 Toluene ND ND ND 0.005 50 ×ylenes ND ND ND 0.005 50 Ethyl benzene N D N D N D 0.005 50 8240 - Volatile Organics All listed constituents ** ND ND ND ** ..... 8270 - Semivolatile Organics All listed constituents ** ND ND ND ** ..... 6010 - CAM Metals Barium 34 39 31 5 100 * Cadmium ND ND 0.7 0.5' 1 * Copper 14 13 21 2.5 25 * Lead ND ND ND 2.5 5 * Soil samples were collected and submitted to Zalco Laboratories, inc. on March 11, 1993. Results were reported by Zalco Laboratories, Inc. on March 23 & 30, 1993. D= xx fbsg: Sample collection depth in feet below surface grade IND: Not detected at the indicated minimum reporting level · · Soluble Threshold Limit Concentration (mg/I) · * · Refer to Zalco laboratory reports (see Appendix D) TABLE 2 M/D TOTCO, Inc. April 1993 included as Appendix D. 6.0 CONCLUSIONS Based on field observations and laboratory analytical data, it is concluded as follows: 1. As depicted on the Boring Log (Table 1), the native soil underlying the former M/D TOTCO, Inc. site and Class V injection well at a depth of at least 33 Jbsg consists of river-deposited sands which are fine- to coarse-grained, pebbly and cobbly in part, and generally free of finer clastic fractions of silt and clay. 2. No stains or odors indicating the presence of hydrocarbon or other organic contamination were noted during field screening of drill cuttings, and samples collected from depths of 22, 27, and 32 Jbsg. 3. Laboratory. results of the three soil samples .(summarized in Table 2) indicated that gasoline, diesel, aromatic volatile organics, volatile organics, and semivolatile organics were nondetectable. 4. The analyses for 4 required CAM metals indicated background levels for barium and copper in the three samples. A background level for cadmium of 0.7 mg/kg was indicated only in the sample collected at 32 Jbsg; it was nondetectable in the samples collected at 22 and 27 Jbsg. Lead was nondetectable in all three samples. 5. Ground water is believed to exist between 35 and 50Jbsg. The water table was not reached or intercepted during drilling operations. 6. The underlying sands below the bottom of the former Class V injection well (total depth of the former well = 17 Jbsg) remained uncontaminated as demonstrated by laboratory analyses of samples collected at 22, 27, and 32fosg. All overlying contaminated material was removed when the well was abandoned and remediation effected during Mr. Campbell's initial investigation, 7.0 RECOMMENDATION Based upon the information submitted in this report and the above conclusions, final closure is recommended for the former M/D TOTCO, Inc. Class V injection well site. MD-TOTCO. Inc. 04-93 5 8.0 LIMITATIONS The results contained in this report are based upon the information acquired during the initial and confirmation-sampling investigations. The conclusions are based solely on and limited 'to the following: 1. Current ground water, geologic, and hydrogeologic conditions; variations in the soil and ground water, or other factors not readily apparent may exist beyond the area explored and remediated during this investigation. Changes in ground water conditions may occur in the future due to variations in rainfall, regional water use, or other factors not apparent at the time this investigation was performed. 2. Chemical compounds targeted for laboratory analysis and results documented by Zalco Laboratories, Inc. of Bakersfield, California. 3. The consultants' professional procedures, on-site observations, and knowledge of Federal, State, and Kern County regulations. The services performed by Jeff Campbell Environmental Consulting and Dayne L. Frary, Geologist have been conducted in a manner consistent with the level of care and skill ordinarily exercised by members of the environmental services profession currently practicing under similar conditions in Kern County. No other warranty, expressed or implied, is given. MI)-'r(YrCO, Is:. 04-9} 6 __ 9.0 CERTIFICATION This document has been prepared and reviewed by the following undersigned, California- licensed, professional consultants. Dayne L. Frary Registe[ed Geologist No. 4456 Registered Environmental Assessor No. 02980 Registered Environmental Assessor No. 03773 MD-TOTCO, Inc. 04-93 7 APPENDIX A PHASE II WORKPLAN PHASE II SOILS INVESTIGATION WORKPLAN MD-TOTCO, INC. FORMER CLASS V INJECFION WELL 1.0 INTRODUCTION This workplan descnbes the project background, and drilling, sampling, and analytical activities to be' performed at the former location of the Class V injection well located at 3011 Antonino Avenue, within a portion of the northwest Bakersfield ci~ limit. The plan addresses requirements submitted to MD-TOTCO, Inc by Ms. Flora Darling, Hazardous Materials Specialist with lhe Kern Coumy Environmental Heahh SerVices Department (County). Additional work is required by ~he County to identify the vemcal extent of contamination by obtaining "clean" soil samples from at least five fee! below the last recorded contaminated sampling point in order to allow for closure of the former well. The previous phase of the investigation was performed and reported by Mr. Jeff Campbell, Environmental Consultant, and was dated February d-. 1993. 2.0 BACKGROUND Mr. Campbell's report, M-D TOTCO. Inc. D~ Well Characterization and Site ~ provides details of the former well and piping system location and construction, and all activities performed pnor to the preparation of this workplan. The property has been leased to M-D TOTCO. Inc for some I't- years. The company utilized the on-site "dry well" for waste-water collection and elimination by drainage through gravel_ The waste water was generated as rinsate by die cleaning of oil well drilling tools with a high-pressure washer and by use' of a wash basin inside the neighboring shop. Rinsate was piped by gravily to a clarifier, thence to the concrete/gravel-lined well. The total dep& of ~he well at &e base of the external gravel liner was approximately 17 feet below surface grade (fbsg). At present, the well has been altered for abandonment; the concrete liner, external gravel pack, and known contaminated soil have been removed to a depth of 22 fbsg and transported to VenVirotek, a licensed disposal facility in Arvin, California. The 1 piping has also been removed, and the clarifier is to be filled with concrete which will render it useless. The excavation was backfilled with clean, off-site borrow soil 3.0 ACFIVI~ AND PROCEDURES 3.1 Soil Boring One (1), 6-inch diameter bonng will be advanced through the center of the former well location for collection of additional samples at 22. 27, and 32 fbsg. Melton Drilling Company will provide the truck-mounted rig with a continuous-flight. hollow-stem auger which will be utilized to dnll the boring. All boring equipmen! xvill be steam-cleaned prior to arrival at the site in order to minimize the possibilily of contaminating the samples. In addition, split-spoon samplers and sample rings will be washed in a solution of trisodium phosphate (TSP). rinsed in tap water, and then final-rinsed in distilled water After the bonng has been sampled at ~2 fbsg (T.D.), it will be backfilled to 22 feet ~vith bentonite pellets and then with the clean borrow soil presently in the excavation to the surface. Any additional soil found to be contaminated will be transported under manifest to the VenVirotek disposal faCility on the scheduled work day. 3.2 Soil Sampling 2.5-inch diameter by 18-inch length "undisturbed" samples will be collected at 22, 27, and 32 fbsg using a split-spoon sampler lined with three (3), 6-inch, brass sample rings. The sampler will be driven ahead of the auger bit at the appropriate depth by a l't-O-pound, down-hole hammer It will not be necessary to collect samples in the clean import soil belween surface grade and 22 fbsg. The soils recovered in the upper and middle nngs will be descnbed by the California Registered Geologist, who will record the descriptions on the boring log according to the Unified Soil Classification System (USC, S). The same samples will be screened for initial indications of hydrocarbon contamination using a' photoionization detector (PID). The PID 'readings will also'be recorded on the 2 boring log. The lower sample will be sealed with Teflon gaskets, capped, final- sealed with duct tape, labeled, and placed in an ice chest chilled with Blue Ice to ar° Centigrade to preserve its chemical integrity'. The sample identifications and their requested laboratory analyses will be recorded on a chain-of-custody document. The chain of-custody will remain with the samples dlrough delivery to Zalco Laboratories, Inc.. a State-certified laboratory: a copy of the completed chain-of-custody will be returned to the geologist at the time of delivery. Upon completion of die analyses, the reported results will be signed and certified by the chief chemist and mailed to the geologist. 3.3 laboratory Analyses A total of three (3) soil samples will be delivered to Zalco Laboratones, Inc. in Bakersfield on die scheduled work day. The following analyses will be specified for each sample: Volatile Organics by EPA Method 82't-0 Semivolatile Organics by EPA Method 8270 TPH as gasoline by EPA Modified Method 801 S TPH as diesel by EPA Modified Method 80155 Aromatic Volatile Organics by EPA Method 8020 CAM metals: Banum, Cadmmm, Copper, and Lead ~.0 REPORT PREPARATION Upon receipt of die laboratory analyses, the geologist will prepare a detailed report of the drilling and sampling program, including all laboratory results for the samples. Additional illustrations such as revised site maps and cross-sections will be included as needed. Conclusions and recommendatiOns will be considered and reported pending die outcome of the laboratory analyses. APPENDIX B UNIFIED SOIL CLASSIFICATION SYSTEM Unified Soil CI~ssification System Major D/v/s/ohS !G~.. s.~l Soil Descr/pt/on Well Grm~ GRAVEl_ ~ GRAVEL ~ ,.~} .' G~t Must t~ an equal COARSE GRAINED 'man ~4.~=~) With F'mes SOIL (Mo~ 'i'nan ~0~ Well Grn~d SAND. Grm~lly SAND.. Clean Must lm~ an eqml dism~ution o/F'm~ ~ Ia~r SAND SAND Me.urn. ~ ~ s,~rD. ~'~,~.) ~ Lair Thaa *,~ S'~,~) With Fine~ ~ SILT. Saint% Ino~am~ C:I~Y. Salty, o~ ~il~ CT..AY. SILT & CLAY CL L~ m ~,.~aum GRAINED (L~uid t_i,~ii Le~ Than $0%)' ~ to Medium SOIL (Mom Tlma 50~ lnm'~an~ SILT, Mi~.oua SILT & ~Y ~ ~ ~ ~d T_{~it Mom ~ 50%) Z~ ~Y ~ m~ ~. It[GHLY ORGANIC SOIL I~AT ~ o~r m~ ~ m~. l~rticle Size Limits SILT &: CLAY SAND tru~GRAvEL! C~ COBBLES I BOULDERS APPENDIX C CHAIN-OF-CUSTODY DOCUMENTATION & To: · "L___,_ ~ ' CHAIN OF CUSTODY DOCUMENT job Number: 002- O©~ · ^llention: ~ample Type: (check one) Drinking Water Surface Water _ Wastewater Oil .~ Soil Sludge Other (specify) ~ample Description(s): ;ample Number Date Collected Collector's Name Type of Analysis ';ample(s) Relinquished to Lab byM ..~ ;ample(s) Recej.ved in Lab by: ~' ~ b~<..LL~.C.I~'L/Lc~.J I ' ) Sample Relinquished by: ) SampJe Received by: ;ample Condition When Received By Lab: ~'~ Lab Signalure: APPENDIX D ZALCO LABORATORIES, INC. REPORTS OF ANALYTICAL RESULTS (~ k~--) ZALCO LABORATORIES, lNG. Analytical ~ Consulting Seevices Jeff Campbell Environmental Laboratory No: 35073-1 8559 Farmers Lane Date Received: 3-11-93 Bakersfield, CA 93307 Date Reported: 3-23-93 Attention: Jeff Campbell Sample: Soil Sample Description: 002-008-22 Sampled by D. Frary on 3-11-93 mq/kq Volatile Aromatic Hydrocarbons Benzene < 0.005 Toluene < 0.005 Ethyl Benzene < 0.005 Xylenes < 0.005 Method: EPA 8020 Date Analyzed: 3-17-93 Minimum Reporting Level = 0.005 mg/kg mq/kg Total Petroleum Hydrocarbons as Gasoline < 10 as Diesel < 10 Method: DOHS Luft Manual Date Analyzed as Gasoline: 3-17-93 Date Analyzed as Diesel: 3-16-93 Minimum Reporting Level as Gasoline : 10 mg/kg Minimum Reporting Level as Diesel : 10 mg/kg Jim Etherton Lab Operations Manager JE/ccw 4309 Armour Avenue Bakersfield, California 93308 F8051 295-0539 FAX F805i 395-3069 VOiA'L~E 'i)i~C$ ANALYS/~ DATA SI~ET ._. 75-34-3 '- 1,.1-Dichloroe~e ...... - ~.- . ~/. < 108-88-3 Toluene ~- · ......... :...~ 5~.---~ 156-60-5 . ~ tr~s-l,2-Dichloroe~ene . :~ < 108-90-7 Chloro~nzene ..... ~ ..... . .= '.-5 < 67-66-3 ._. Chlorofo~ ..... · .... 5 < 630-20-6 1,1,1,2-Te~achloroe~e 5-. < 107-06-2 1,2-Dichloroe~e .... 5 < 100-41-4 E~y~nzene ....... 5 < 78-93-3 2-Bu~one ........ 100 < 100-42-5 St~ene ......... 5 < 71-55-6 1,1,1-Trichloroe~e 5 < 1330-20-7 Xylene (To~l) ...... 5 < 563-58-6 1,1-Dichloropropene 5 < 108-86-1 Bromo~nzene ....... 5 < 56~23-5 C~n Tetrachloride 5 < 95-49-8 2-Chlorotoluene ..... 5 < 124-48-1 Bromodichlorome~e . 5 < 106-43-4 4-Chlorotoluene ..... 5 < 78-87-5 1,2-Dichloroprop~e 5 < 541-73-1 1,3-Dichloro~nzene 5 < 10061-02-6 t~s-l,3-Dichloropro~ne 5 < 106-46-7 1,4-Dichloro~nzene 5 < 79-01-6 Trichloroe~e ..... 5 < 95-50-1 1,2-Dichlorobenzene 5 < The Lab ID for data on this page is QH6X751. Partial reproductions of this report are not valid. Above data applies to submitted sample only. < - Compound analyzed for but not detected. The reported value is the minimum attainable detection limit for the sample. Billing Code: 9187 Analyst: ~Jw~/ Data Release. Authorization: QC report can be made available for an additional fee. Information concer~ing non-target analytes can be made available for an additional fee for a ·period of 90 days after receipt of this report. ~ OiSAIICS ANALYSIS DATA SHEET -£aboratory Naue: Z~LCO ~BS Concentration: LOV Date Extracted: 03/29/93 Lab Sample ID: 3527~-I Sample Hatrix: $0I~ Date Analyzed: 03/29/93 Client Sample ID: 00~-008-~ Percent Hotsture: Dilution Factor: ~.0 EPA ]fETHOD 8270 SAS Number u~/k~ CAS Number u~/k~ 62-75-9 N-Nitrosodimetbylamine . . 330 < 86-73-7 Fluorene ......... 330 < 108-95-2 Phenol ......... 330 < 100-10-6 *4-Nitroaniline ...... 1600 < ~111-44-4 bis(2-Chloroetbyl)Etber . 330 < 534-52-1 4,6-Dinitro-2-Metbylphenol 1600 ~5-57-8 2-Chloropbenol ...... 330 < 86-30-6 N-Nttrosodiphenylamine (1) 330 < 541-73-1 1,3-Dicblorobenzene . . 330 < 103-33-3 Azobenzene ......... 330 < 106-46-7 1,4-Dichlorobenzene . . . 330 < 101-55-3 4-Bromopbenyl-phenyletber 330 < 100-51-6 Benzyl Alcohol ...... 330 < 118-74-1 Bexacblorobenzene .... 330 95-50-1 1,2-Dichlorobenzene . . 330 < 87-86-5 Pentachlorophenol . . 1600 < 95-48-7 2-Metb~lpbenol ...... 330 < 85-01-8 Pbenantbrene ....... 330 < 108-60-1 Bta(2-cbloroisopropyl)etber 330 < 120-12-7 Anthracene ........ 330 < 106-44-5 4-Methylpbenol ...... 330 < 84-74-2 Di-n-Butylpbthalate . ... 330 < 621-64-7 N-Nitroso-Di-n-Propylamine 330 < 206-44-0 Fluorantbene ........ 330 < 57-72-I ~exacbloroetbane ..... 330 < 129-00-0 Pyrene ......... 330 < ~8-95-3 Nitrobenzene ....... 330 < 85-68-7 Butylbenzylpbtbalate . . . 330 < 78-59-1 Isopborone ....... 330 < 91-94-1 3,3'-Dichlorobenzidine . . 660 < ~8-75-5 2-Nitrophenol ...... 330 < 56-55-3 Benzo(a)Anthracene .... 330 < 105-67-9 2,4-Dimetbylpbenol .... 330 < 117-81-7 bis(2-Etbylbexyl)Pbtbalate 330 < 65-85-0 Benzoic Acid ....... 1600 < 218-01-9 Chrysene ........ 330 < 111-91-1 bis(2-Chloroetboxy)Metbane 330 < 117-84-0 Di-n-Octyl Pbthalate . . . 330 < 120-83-2 2,4-Dtchlorophenol .... 330 < 205-99-2 Benzo(b)Fluoranthene . . 330 <. 120-82-1 1,2,4-Trichlorobenzene . 330 < 207-08-9 Benzo(k)Fluoranthene . . . 330 < 91-20-3 Naphthalene ....... 330 < 50-32-8 Benzo(a)Pyrene ...... 330 < 106-47-8 4-Chloroaniline ..... 330 < 193-39-5 Indeno(1,2,3-cd)Pyrene . 330 < ~7-68-3 Hexachlorobutadiene . . . 330 < 53-70-3 Dibenz(a,b)Antbracene . 330 < 59-50-7 4-Chloro-3-Methylpbenol 330 < 191-24-2 Benzo(g,b,i)Perylene . 330 91-57-6 2-Metbylnaphtbalene . . . 330 < 319-84-6 alpha-BBC ........ 330 < 77-47-4 Bexacblorocyclopentadiene 330 < 319-85-7 beta-BBC ........ 330 < 95-95-4 2,4,5-Tricblorophenol . 1600 < 319-86-8 delta-BBC ........ 330 < 91-58-7 2-Chloronapbthalene . . . 330 < 58-89-9 Lindane ......... 330 < 88-74-4 2-Nitroanillne ...... 1600 < 76-44-8 Heptachlor ........ 330 < 131-11-3 Dimethyl Phthalate .... 330 < 309-00-2 Aldrin .......... 330 < 208-96-8 Acenaphthylene ..... 330 < 1024-57-3 Heptachlor epoxide .... 330 < 99-09-2 3-Nitroaniline ...... 1600 < 959-98-8 Endosulfan I ....... 330 < ~3-32-9 Acenaphthene ...... 330 < 60-57-1 Dieldrin ......... 330 51-28-5 2,4-Dinitrophenol .... 1600 < 72-55-9 4,4'-DDE ......... 330 < 100-02-7 4-Nitrophenol ...... 1600 < 72-20-8 Endrin .......... 330 < 132-64-9 Dibenzofuran ....... 330 < 33213-65-9 Endosulfan II ...... 330 < 121-14-2 2,4-Dtnitrotoluene .... 330 < 72-54-8 4,4'-DDD ...... ; . · 330 606-20-2 2,6-Dinitrotoluene . . 330 < 1031-07-8 Endosulfan sulfate .... 330 < 7005-72-3 4-Cblorophenyl-phenyletber 330 < 50-29-3 4,4'-DDT ......... 330 The Lab ID for data on this page is NHgX2751. < - Compound analyzed for but not detected. The reported value ts the minimum attainable detection limit for the sample.. Page*l ORGANICS ANALYSIS DATA SHEE! ~aboratory Name: ZALCO ~A~S Concentration: LQV Date Extracted: 03/29/93 Lab Sample ID: 35275-1 Sample Hatrix: S~L .Date Analyzed: 03/29/93 ~lient. Sample ID: 002-008-22 Percent Moisture: Dilution Factor: 1.0 EPA HETHOD 8270 !AS Number ug/k~ CAS Number ug/kg .84-66-2 Diethylphthalate ..... 330 < 53494-70-5 Endrin aldehyde .* . . . 330 < The Lab ID for data on this page is NM9X2751. Partial reproductions of this report are not valid. Above data applies to submitted sample only. Billing Code: 9184 Analyst: .~ Data Release Authorization: QC Report can be made available for an additional fee. Information concerning non-target analytes can be made available for an additional fee for a period of 90 days after receipt of this report. Page 2 ZALCO LABORATORIES, INC. Analytical Consulting Seevioes Jeff Campbell Environmental Laboratory No: 35275-1 8559 Farmers Lane Date Received: 3-27-93 Bakersfield, CA 93307 Date Reported: 3-30-93 Attention: Jeff Campbell Sample: Brown Solid (type i) Sample Description: 002-008-22, Old Lab #35703-1 Sampled by D. Frary on 3-11-93 CAM - Title 22 Chapter 30, Article 11 No Free Liquid Total Extractable TTLC/STLC Concentration Concentration MRL Method/ (TC) mg/kg WET, (EC) mg/1 TC/EC' Reference Barium, Ba 10000/100 34 5.0/0.1 6010/1 Cadmium,.Cd 100/1.0 < 0.5 0.5/0.01 6010/1 Copper, Cu 2500/25 14 2.5/0.05 6010/1 Lead, Pb 1000/5.0 < 2.5 2.5/0.05 6010/1 TTLC Total Threshold Limit Concentration, mg/kg STLC Soluble Threshold Limit Concentration, mg/1 in extract WET Waste Extraction Test: pH 5.0 Solution, 0.2 M Citrate Buffer Deionized water for Chromium (VI) Orqanic Constituents Method/Reference Volatile Organics See Attached Report 8240/1 Semivolatile Organics See Attached Report 8270/1 MRL~ Minimum Reporting Level Method References: 1. EPA SW-846, 1986 3rd Edition JE/ccw 4309 Armour Avenue Bakersfield, I~.alifonnia 93:~019 FRn~l ~R~-6-)~ FAX r8051 395-3069 ZALC;O LABORATORIES, INI . Analytical Consulting Seevioes Jeff Campbell Environmental Laboratory No: 35275-2 8559 Farmers Lane Date Received: 3-27-93 Bakersfield, CA 93307 Date Reported: 3-30-93 Attention: Jeff Campbell Sample: Brown Solid (type i) Sample Description: 002-008-27, Old [ab #35703-2 Sampled by D. Frary on 3-11-93 CAM - Title 22 Chapter 30, Article 1 No Free Liquid Total Extractable TTLC/STLC Concentration Concentration. MRL Method/ (TC) mg/kg WET, (EC) mg/1 TC/EC Reference Barium, Ba 10000/100 39 5.0/0.1 6010/1 Cadmium, Cd 100/1.0 < 0.5 0.5/0.01 6010/1 Copper, Cu 2500/25 13 2.5/0.05 6010/1 Lead, Pb 1000/5.0 < 2.5 2.5/0.05 6010/1 TTLC Total Threshold Limit Concentration, mg/kg STLC Soluble Threshold Limit Concentration, mg/1 in extract WET Waste Extraction Test: pH 5.0 Solution, 0.2 M Citrate Buffer Deionized water for Chromium (VI)' Orqanic Constituents mq/kq MRL Method/Reference Petroleum Hydrocarbons 10 DOHS Luft Method As Gasoline < 10 As Diesel < 10 Date Analyzed: 3-30-93 Volatile Aromatic Hydrocarbons 0.005 8020/1 Date Analyzed: 3-30-93 Benzene < 0.005 Toluene < 0.005 Ethyl Benzene < 0.005 Xylenes < 0.005 MRL : Minimum Reporting Level Method References: 1. EPA SW-846, 1986 3rd Edition ~ JE/ccw 4309 Armour Avenue Bakersfield, Califonnim ~)3301~ ~..AT'rr~ ORGANICS ANALYSIS DATAF ,T Laboratory Name: ZALCO LABS Concentration: LOW Date Extracted: 03/16/93 Lab Sample ID: 35073-2 Sample Matrix: SOIL Date Analyzed: 03/16/93 Client Sample ID: 002-008-27 Percent Moisture: Dilution Factor: 1.0 NETHOD 8240 CAS N,~mher ug/kg CAS Number ug/kg 74-87-3 Chloromethane ...... 5 < 74-95,3 Dibromomethane ...... 5 75-71-8 Dichlorodifluoromethane 5 < 124-48-1 Dibromochloromethane . 5 < 74-83-9 Bromomethane ....... 5 < 79-00-5 1,1,2-Trichloroethane 5 < 75-01-4 Vinyl Chloride ...... 5 < 71-43-2 Benzene ......... 5 < 75-00-3 Chloroethane ....... 5 < 10061-01-5 cis-l,3-Dichloropropene 5 < 75-69-4 Trichlorofluoromethane 5 < 75-25-2 Bromoform ........ 5 75-09-2 Methylene Chloride .... 5 < 108-10-1 4-Methyl-2-Pentanone . 100 < 67-64-1 Acetone ......... 100 < 591-78-6 2-Mexanone ........ 100 < 75-15-0 Carbon Disulfide ..... 5 < 127-18-4 Tetrachloroethene .... 5 75-35-4 1,1-Dlchloroethene .... ' 5 < 79-34-5 1,1,2,2-Tetrachl°roethane 5 75-34-3 1,1-Dichloroethane .... 5 < 108-88-3 Toluene ......... 5 156-60-5 trans-l,2-Dichloroethene . 5 < 108-90-7 Chlorobenzene ...... 5 < 67-66-3 Chloroform ........ 5 < 630-20-6 1,1,1,2-Tetrachloroethane 5 107-06-2 1,2hDichloroethane .... 5 < 100-41-4 Ethylbenzene ....... 5 < 78-93-3 2-Butanone ..... 100 < 100-42-5 Styrene ......... 5 71-55-6 1,1,1-Trichloroethane 5 < 1330-20-7 Xylene (Total) 563-58-6 1,1-Dichloropropene 5 < 108-86-1 Bromobenzene ....... 5 56-23-5 Carbon Tetrachloride 5 < 95-49-8 2-Chlorotoluene ..... 5 < 124-48-1 Bromodichloromethane 5 < i06=43-4 4-Chlorotoluene ..... 5 78-87-5 1,2-Dichloropropane . 5 < 541-73-1 1,3-Dichlorobenzene 10061-02-6 trans-l,3-Dichloropropene 5 < 106-46-7 1,4-Dichlorobenzene . 5 < 79-01-6 Trichloroethene ..... 5 < 95-50-1 1,2-Dichlorobenzene 5 The Lab ID for data on this page is PX10X732. Partial reproductions of this report are not valid. Above data applies to submitted sample only. < - Compound analyzed for but not detected. The reported value is the minimum attainable detection limit for the sample. Billing Code: 9187 Analyst: ~-/ Data Release Authorization: .y~..~/~ QC report can be made available for an additional fee. Information concer~ing non-target analytes can be ~ade available for an additional fee for a period of 90 days after receipt of this report. OE6AIlCS AlII. ISIS DATA SHEET Laboratory Name: ZALCO LABS Concentration: LOV Date Extracted: 03/16/93 Lab Sample ID: 35073-~ Sample Hatrix: SOIL Date Analyzed: 03/23/93 Client Sample ID: 002-008-27 Percent Noisture: Dilution Factor: 1.0 HPAHETHOD 8270 CAS Number UG/EG CAS Humb~r UG/KG 62-75-9 N-Nitrosodimethylamine . . 330 < 86-73-7 Fluorene ...... ; . . 330 < .108-95-2 Phenol .......... 330 < 100-10-6 4-Nitroaniline ...... 1600 111-44-4 bia(2-Cbloroetbyl)Etber . 330 < 534-52-1 4,6-Dinitro-2-Hetb¥1phenol 1600 < 95-57-8 2-Chlorophenol.. ..... 330 < 86-30-6 N-Nitrosodiphenylamine (1) 330 < 541-73-1 1,3-Dichlorobenzene . . . 330 < 103-33-3 Azobenzene ........ 330 106-46-7 1,4-Dicblorobenzene . . . 330 < 101-55-3 4-Bromopbenyl-pbenyletber 330 100-51-6 Benzyl Alcohol ...... 330 < 118-74-1 Hexachlorobenzene .... 330 < 95-50-1 1,2-Dicblorobenzene . . 330 < 87-86-5 Pentachloropbenol . . . 1600 < 95-48-7 2-Methylpbenol ...... 330 < 85-01-8 Phenanthrene ....... 330 < 108-60-1 Bis(2-cbloroisopropyl)etber 330 < 120-12-7 Anthracene . ....... 330 < 106-44-5 4-Hethylpbenol ...... 330 < 84-74-2 Di-n-Butylpbtbalate . . . 330 < 621-64-7 N-Nitroso-Di-n-Propylamine 330 < 206-44-0 Fluorantbene ....... 330 < 67-72-1 Hexachloroethane . . 330 < 129-00-0 Pyrene .......... 330 < 98-95-3 Nitrobenzene ....... 330 < 85-68-7 Butylbenzylphthalate . . 330 < 78-59-1 Isophorone ........ 330 < 91-94-1 3,3'-Dicblorobenzidine . . 660 < 88-75-5 2-Nitropbenol ...... 330 < 56-55-3 Benzo(a)Anthracene .... 330 < 105-67-9 2,4-Dimetbylphenol . . . 330 < 117-81-7 bis(2-Ethylbexyl)Phtbalate 330 < 65-85-0 Benzoic Acid .... 1600 < 218-01-9 Chrysene' . ..... ~ . . 330 < 111-91-1 bis(2-Chloroethoxy)Metbane 330 < 117-84-0 Di-n-Octyl 'Pbthalate . . . 330 < 120-83-2 2,4-Dicblorophenol .... 330 < 205-99-2 8enzo(b)Fluoranthene . 330 120-82-1 1,2,4-Tricblorobenzene 330 < 207-08-9 Benzo(k)Fluoranthene . . 330' < 91-20-3 Naphthalene ....... 330 < 50-32-8 Benzo(a)Pyrene ...... 330 < 106-47-8 4-Chloroaniline ..... 330 < 193-39-5 Indeno(1,2,3-cd)Pyrene . . 330 < 87-68-3 Hexacblorobutadiene . . . 330 < 53-70-3 Dtbenz(a,h)lntbracene . . 330 59-50-7 4-Chloro-3-Methylphenol 330 < 191-24-2 Benzo(g,h,i)Perylene . 330 < 91-57-6 2-Metbylnaphtbalene . 330 < 319-84-6 alpba-BHC ........ 330. < 77-47-4 Hexachlorocyclopentaliene 330 < 319-85-7 beta-B~C ......... 330 < 95-95-4 2,4,5-Tricbloropbenol . . 1600 < 319-86-8 delta-B~C ........ 330 < 91-58-7 2-Cbloronaphthalene . . 330 < 58-89-9 Lindane ........ 330 < 88-74-4 2-Nitroaniline ...... 1600 < 76-44-8 Heptachlor ........ 330 < 131-11-3 Dimethyl Phthalate . . . 330 < 309-00-2 Aldrin .......... 330 208-96-8 Acenaphthylene ...... 330 < 1024-57-3 Heptachlor epoxide .... 330 < 99-09-2 3-1itroaniltne ...... 1600 < 959-98-8 Endosulfan I ....... 330 83-32-9 Acenapbthene . . . , . . . 330 < 60-57-1 Dieldrin ......... 330 51-28-5 2,4-Dtnttrophenol .... 1600 < 72-55-9 4,4'-DDE ......... 330 < 100-02-7 4-Hitropbenol .... 1600 < 72-20-8 Endrin ....... 330 < 132-64-9 Dtbenzofuran ....... 330 < 33213-65-9 Endoaulfan II ..... .. 330 121-14-2 2,4-Dinitrotoluene . . . 330 < 72-54,8 4,4'-DDD ......... 330 606-20-2 2,6-Dinitrotoluene .... 330 < 1031-07-8 Endosulfan sulfate .... 330 < 7005-72-3 4-Chloropben¥1-phenyletber 330 < 50-29-3 4,4'-DDT ......... 330 < The Lab ID for data on this page ts NKSX0732. ( - Compound analyzed for but not detected. The reported value is the minimum attainable detection limit for the sample. Page Analycioal OonsulCing Services .. Jeff Campbell Environmental Laboratory No: 35275-3 8559 Farmers Lane Date Received: 3-27-93 Bakersfield, CA 93307 Date Reported:. 3-30-93 Attention: Jeff Campbell Sample: Soil Sample Description: 002-008-32, Old Lab #35703-3 Sampled by D. Frary on 3-11-93 Orqanic Constituents mq/kq MRL Method/Reference Petroleum Hydrocarbons, 10 DOHS Luft Method As Gasoline < 10 As Diesel < 10 Date Analyzed: 3-29-93 Volatile Organics See Attached Report 8240/1 Semivolatile Organics See Attached Report 8270/1 MRL = Minimum Reporting Level Method References: 1. EPA SW-846, 1986 3rd Edition JE/ccw 4:309 Armour Avenue Bakersfield' I_-;alifornia 9:3308 f8051 395-0539 FAX (8051 395-3069 ~l~k~__] ZALCO LABORATORIES, INC. AnalyCioal ~ Consulting Seevices Jeff Campbell Environmental Laboratory No: 35073-2 8559 Farmers Lane Date Received: 3-11-93 Bakersfield, CA 93307 Date Reported: 3-23-93 Attention: Jeff Campbell Sample: Soil Sample Description: 002-008-27 Sampled by D. Frary on 3-11-93 Enclosed please find the results of the analyses of the above described sample by E.P.A. Method 8240 for Volatile Organics, 8270 for Semivolatile Organics. If there are any questions, please feel free to call. Lab Operations Manager JE/ccw ~ 4309 Armour Avenue Bekersfielci. California Et3308 · r8051 395-0539 FAX (8051 395-3069 VOIATW~ ORC.,~'~CS ANAI.~ DATA ~ Laboratory Name: ZALCO LABS Concentration: ~W Da~e Extracted: 03/29/93 L~ S~ple ID: 35275-3 S~ple Matrix: SOIL Date ~alyzed: 03/29/93 Client S~le ~: 002-008-32 Percent Moisture: Dilution Factor: 1.0 ~D 8240 C~~e= ug/kg C~N~e= ug/kg 74-87-3 Ch~o:ome~e~. ..... 5 < 74-95-3 D~b=omome~e ...... 5 < 75-7~-8 D~ch~o=od~uo:ome~e 5 < ~24-48-~ D~b=omoch~o:ome~e . . . 5 < 74-83-9 B:omome~e ....... 5 < 79-00-5 ~,~,2-~:~ch~o=oe~e 5 < 75-0~-4 V~ny~ Ch~o=~de 5 < 7~-43-2 Benzene ......... 5 <' 75-00-3 Ch~o=oe~e ....... 5 < ~006~-0~-5 c~s-~,3-D~ch~o=op=opene 5 < 75~69-4 ~=~ch~o=o~uo=ome~e 5 < 75-25-2 B=omo~o~ ........ 5 < 75-09-2 He~y~ene Ch~o=~e .... 5 < ~08-~0-~ 4-He~y~-2-~en:~one . . . ~00 < &7-&4-~ Rce~one .......... ~00 < 59~-78-~ 2-Hex~one ........ ~00 < 75-~5-0 Ca=bon D~su~E~de ..... 5 < ~27-~8-4 ~e:=ach~o=oe~ene .... 5 < 75-35-4 ~,~-D~ch~o=oe~ene .... 5 < 79-34-5 ~,~,2,2-~e:=ach~o=oe~e 5 < 75-34-3 ~,~-D~ch~o=oe~e .... 5 < ~08-88-3 ~o~uene ......... 5 < ~5&-60-5 ::~s-~,2-D~ch~o=oe~ene . 5 < ~08-90-7 Ch~o=obenzene .. ..... . 5 < ~7-~&-3 Ch~o=o~o~ ........ 5 < ~30-20-~ ~,~,~,2-~e::ach~o=oe~e 5 < ~07-0~-2 ~,2-D~ch~o:oe~e .... 5 < ~00-4~-4 S~y~benzene ....... 5 < 78-93-3 2-8u~one ........ ~00 < ~00-42-5 ~:y:ene ......... 5 < 7~-55-~ ~,~,~-~=~ch~o=oe~e 5 < ~330-20-7 Xy~ene (~o~) ...... 5 < 563-58-~ :,~-D~ch~o:op=opene 5 < ~08-8~-~ B=omobenzene ....... 5- < 5~-23-5 C~bon ~e:=ach~o=~de .. 5 < 95-49-8 2-Ch~o:o:o~uene ...... 5 < ~24-48-~ ~=omod~ch~o=ome~e . 5 < ~06-43-4 4-Ch~o=o:o~uene ..... 5 < 78-87-5 ~,2-D~ch~o:op:op~e 5 < 54~-73-~ ~,3-D~ch~o=obenzene . . 5 < 79-0~-~ T:~ch~o=oe~ene ..... 5 < 95-50-~ ~,2-D~ch~o:obenzene . . 5 < The Lab ID for data on this page is QH7X753. Partial reproductions of this report are not valid. Above data applies to submitted sample only. < - Compound analyzed for but not detected. The reported value is the minimum attainable detection limit for the sample. Billing Code: 9187 Analyst: ~v~/ Data Releas~ Authorization: QC report can be made available for an additional fee. Information concerning non-target analytes can be made available for an additional fee for a period of 90 days after receipt of this report. ; O~GAwzcs AMALYSIS DATA SHEE! ~aboratory Name: ZALCO LABS Concentrat/on: LOg Date Extracted: 03/29/93 '.ab Sample ID: 35~75-3 Sample Matrix: SOIL Date Analyzed: 03/29/93 :lient Saaple ID: 00~Z008-32 Percent Moisture: Dilution Factor: 1.0 KPAHETHOD 8270 ~AS Number u~/k~ CAS Number u~/k~ 62-75-9 g-Nitroaodimethylauine . 330 < 86-73-7 Fluorene .......... 330 < '08-95-2 Phenol ......... 330 < 100-10-6 4-Nitroaniline ...... 1600 < .11-44-4 bis(2-¢hloroethyl)Ether . 330 < 534-52-1 4,6-Oinitro-2-Methylphenol 1600 < 95-57-8 2-Chlorophenol ...... 330 < 86-30-6 N-Nitrosodiphenylamine (1) 330 < ~41-73-1 1,3-Oichlorobenzene . . . 330 < 103-33-3 Azobenzene ........ 330 < .06-46-7 1,4-Oichlorobenzene . . 330 < 101-55-3 4-Bromophenyl-phenylether 330 < · 00-5i-6 Benzyl Alcohol ...... 330 < 118-74-1 Hexachlorobenzene . . . 330 95-50-1 1,2-Dicblorobenzene . . . 330 < 87-86-5 Pentacbloropbenol .... 1600 ~5-48-7 2-Methylphenol ...... 330 < 85-01-8 Phenanthrene ....... 330 .08-60-1 Bia(2-cbloroisopropyl)etber 330 < 120-12-7 Anthracene ........ 330 < 106-44-5 4-Methylphenol ...... 330 < 84-74-2 Dt-n-Butylphthalate . . . 330 < ~21-64-7 N-Nitroao-Di-n-Prop¥1amine 330 < 206-44-0 Fluorantbene ....... 330 < i7-72-1 Rexachloroethane ..... 330 < 129-00-0 Pyrene ......... 330 < 98-95-3 Nitrobenzene ....... 330 < 85-68-7 8utylbenzylphtbalate . . . 330 < 78-59-1 Isophorone ........ 330 < 91-94-1 3,3'-Dichlorobenztdine . . 660 < t8-75-5 2-Nitrophenol ...... 330 < 56-55-3 Benzo(a)Anthracene . . . 330 < i05-67-9 2,4-Dlmethylphenol .... 330 < 117-81-7 bis(2-Ethylhexyl)Phthalate 33.0 65-85-0 Benzoic Acid ....... 1600 < 218-01-9 Cbryaene ..... ' 330 < !11-91-1 bis(2-Cbloroetboxy)Methane 330 < 117-84-0 Dt-n-Octyl Pbthalate . . . 330 .20-83-2 2,4-Oichloropbenol .... 330 < 205-99-2 Benzo(b)Fluorantbene . . . 330 120-82-1 1,2,4-Trtchlorobenzene . . 330 < 207-08-9 Benzo(k)Fluorantbene . . . 330 ~1-20-3 Naphthalene ....... 330 < 50-32-8 Benzo(a)Pyrene ...... 330 :.06-47-8 4-Chloroaniline ..... 330 < 193-39-5 Indeno(1,2,3-cd)Pyrene . . 330 < 87-68-3 Hexachlorobutadiene . . 330 < 53-70-3 Dibenz(a,h)Anthracene . . 330 < 59-50-7 4-Chloro-3-Methylphenol 330 < 191-24-2 Benzo(g,h,i)Perylene . . 330 < ~1-57-6 2-Metbylnapbtbalene . . 330 < 319-84-6 alpba-BHC ........ 330 <' /7-47-4 ~emacblorocyclopentadiene 330 < 319-85-7 .beta-BRC ......... 330 < 95-95-4 2,4,5-Trichloropbenol . 1600 < 319-86-8 delta-BHC ........ 330 < Jl-58-7 2-Cbloronapbthalene . . . 330 < 58-89-9 Lindane ......... 330 18-74-4 2-Nitroaniline ...... 1600 < 76-44-8 'Heptachlor ........ 330 < 131-11-3 Dimeth71 Phthalate .... 330 < 309-00-2 Aldrin .......... 330 < 208-96-8 Acenaphthylene ...... 330 < 1024-57-3 Heptachlor epoxide .... 330 a9-09-2 3-Nitroaniline ...... 1600 < 959-98-8 Endosulfan I ...... 330 a3,32-9 Acenaphthene ........ 330 < 60-57-1 Dieldrin ......... 330 < 51-28-5 2,4-Oinitropbenol .... 1600 < 72-55-9 4,4'-DDE ......... 330 < £00-02-7 4-litroPbenol ...... 1600 < 72~20-8 Endrin .......... 330 < ~32-64-9 Oibenzofuran ....... 330 < 33213-65-9 Endosulfan II ...... 330 121-14-2 2,~-Ointtrotoluene .... 330 < 72-54-8 4,4'-DOD ......... 330 < 506-20-2 2,6-~initrotoluene .... 330 < 1031-07-8 Endosulfan sulfate .... 330 < ~005-72-3 4-Chlorophenyl-phenylether 330 < 50-29-3 4,4'-DDT ......... 330 < The Lab ID for data on tb/s page /s ~Mgz2753. ( - Compound analyzed for but not detected. ?he re~orted * value is the minimum attainable detect/on limit for the sample. Page 'Laboratory Name: ZAL¢O LABS Concentration: LOW Date Extracted: 03/29/93 · Lab Sauple'ID: 35275-3 Sample Hatrtx: SOIL Date"Analrzed: 03/29/93 Client Sample ID: 002-008-32 Percent Hoisture: Dilution Factor: 1.0 EPA HETHOD 8270 CA~ Number u~/kg CAS Number u~/k~ 84-66-2 Diethylpbtbalate ..... 330 < 53494-70-5 Endrin aldehyde ..... 330 < The Lab ID for data on this page is NMgX27§3. Partial reproductions of this report are not valid. Above data applies to submitted sample only. Billing Code: 9184 Analyst: Data Release Authorization: QC Report can be made available for an additional fee. Information concerning non-target analytes can be made available for an additional fee for a period of 90 days after receipt of this report. Page 2 ZAL_CO. LABORATORIES, INC. Analytioal & Consulting Servioes Jeff Campbell Environmental Laboratory No: 35073-3 8559 Farmers Lane Date Received: 3-11-93 Bakersfield, CA 93307 Date Reported: 3-23-93 Attention' Jeff Campbell Sample: Soil Sample Description: 002-008-32 Sampled by D. Frary on 3-11-93 CAM - Title 22 Chapter 30, Article 11 No Free Liquid Total Extractable TTLC/STLC Concentration Concentration MRL Method/ (TC) mg/kg WET, (EC) mg/1 TC/EC Reference Barium, Ba 10000/100 31 5.0/0.1 6010/1 Cadmium, Cd 100/1.0 0.70 0.5/0.01 6010/1 Copper, Cu 2500/25 21 2.5/0.05 6010/1 Lead, Pb 1000/5.0 < 2.5 2.5/0.05 6010/1 TTLC Total Threshold Limit Concentration, mg/kg STLC Soluble Threshold Limit Concentration, mg/1 in extract WET Waste Extraction Test: pH 5.0 Solution, 0.2 M Citrate Buffer Deionized water for Chromium (VI) MRL Minimum Reporting Level Method References: 1. EPA SW-846, 1986 3rd Edition s Manager JE/ccw ~, 4309 Armour Avenue Bekerefielcl. Californie ~)3308 cRl-l.~l ..~.c:t6-(-]939 FAX r8051 395-3069 e VOI~T~'tR ORGANICS ANALYSIS DATA SfmmT ~Laboratory Name: ZALCO LABS Concentration: LOW Date Extracted: Lab Sample ID: METHOD-BLANK Sample Matrix: SOIL Date Analyzed: 03/16/93 Client Sample.ID: METHOD-BLANK Percent Moisture: Dilution Factor: 1.0 METHOD 8240 CAS Number ug/kg CAS Number ug/kg 74-87-3 Chloromethane ...... 5 < 74-95-3 Dibromomethane ..... 5 75-71-8 Dichlorodifluoromethane 5 < 124-48-1 Dibromochlorometha~e . 5 < 74-83-9 Bromomethane ....... 5 < 79-00-5 1,1, 2-Trichloroethane 5 < 75-01-4 Vinyl Chloride ..... 5 < 71~43-2 Benzene ......... 5 < 75-00-3 Chloroethane ....... 5 < 10061-01-5 cis-l,3-Dichloropropene 5 75-69-4 Trichlorofluoromethane . 5 < 75-25-2 Bromoform ........ 5 75-09-2 Methylene Chloride .... 5 < 108-10-1 4-Methyl-2-Pentanone . . . 100 < 67-64-1 Acetone ......... 100 < 591-78-6 2-Mexanone ........ 100 < 75-15-0 Carbon Disulfide ..... 5 < 127-18-4 Tetrachloroethene .... 5 < 75-35-4 1,1-Dichloroethene .... .5 < 79-34-5 1,1,2,2-Tetrachloroethane 5 < 75-34-3 1,1-Dichloroethane .... 5 < 108-88-3 Toluene ......... 5 < 156-60-5 trans-l,2-Dichloroethene . 5 < 108-90-7 Chlorobenzene ...... 5 < 67-66-3 Chloroform ........ 5 < 630-20-6 1,1,1,2-Tetrachloroethane 5 < 107-06-2. 1,2-Dichloroethane .... 5 < 100-41-4 Ethylbenzene ....... 5 < 78-93-3 2-Butanone ........ 100 < 100-42-5 StYrene ......... 5 < .71-55-6 1,1,1-Trichloroethane 5 < 1330-20-7 Xylene (Total) ...... 5 < 563-58-6 1,1-Dichloropropene 5 < 108-86-1 Bromobenzene ....... 5 56-23-5 Carbon Tetrachloride . 5 < 95-49-8 2-Chlorotoluene ..... 5 < 124-48-1 Bromodichloromethane 5 < 106-43-4 4-Chlorotoluene ..... 5 78-87-5 1,2-Dichloropropane 5 < 541-73-1 1,3-Dichlorobenzene 5 10061-02-6 trans-l,3-Dichloropropene 5 < 106-46-7 1,4-Dichlorobenzene . 5 < 79-01-6 Trichloroethene ..... 5 < 95-50-1 1,2-Dichlorobenzene 5 < The Lab ID for data on this page is PX2MBLK. Partial reproductions of this report are not valid. Above data applies to submitted sample only. < - Compound analyzed for but not detected. The reported value is the minimum attainable detection limit for the sample. Billing Code: 9187 Analyst: Data Release~Authorization: QC report can be made available for an additional fee. Information concerning non-target analytes can be made available for an additional fee for a period of 90 days after receipt of this report. VOI2tl~R ORGANICS ANALYSISDATASHEET Laboratory Name: ZALCO LABS Concentration: LOW Date Extracted: 03/29/93 Lab Sample ID: METHOD-BLANK Sample Matrix~ SOIL Date Analyzed: 03/29/93 Client Sample ID: METHOD-BLANK Percent Moisture: Dilution Factor: 1.0 ~D 8240 CAS Number ug/kg CAS Number ug/kg 74-87-3 Chlorometha~e ...... 5 < 74-95-3 DibromomeLhane ...... 5 < 75-71-8 Dichlorodifluoromethane 5 < 124-48-1 Dibromochloromethane . . 5 < 74-83-9 Bromome~hane ..... -.. 5 < 79-00-5 1,1,2-Trichloroethane . . 5 < -75-01-4 Vinyl Chloride ...... 5 < 71-43-2 Benzene ......... 5 < 75-00-3 Chloroethane ....... 5 < 10061-01-5~cis-l,3-Dichloropropene 5 < 75-69-4 Trichlorofluoromethane . 5 < 75-25-2 Bromoform ........ 5 < 75-09-2 Methylene Chloride .... 5 < 108-10-1 4-Hethyl-2-Pent~none 100 < 67-64-1 Acetone ......... 100 < 591-78-6 2-Hexanone ....... .. 100 < 75-15-0 Carbon Disulfide ..... 5 < 127-18-4 Tetrachloroethene .... 5 < 75-35-4 1,1-Dichloroethene .... 5 < 79-34-5 1,1,2,2-Tetrachloroethane 5 75-34-3 1,1-Dichloroethane .... 5 < 108-88-3 Toluene ......... 5 < 156-60-5 trans-l,2-Dichloroethene . 5 < 108-90-7 Chlorobenzene. ...... 5 · 67-66-3 Chloroform ........ 5 < 630-20-6 1,1,1,2-Tetrachloroethane 5 < 107-06-2 1,2-Dichloroethane .... 5 < 100-41-4 Ethylbenzene ....... 5 < 78-93-3 2-Butanone ........ 100 < 100-42-5 Styrene ......... 5 · 71-55-6 1,1,1-Trichloroethane 5 · 1330-20-7 Xylene (Total) ...... 5 · 563-58-6 1,1-Dichloropropene 5 · 108-86-1 Bromobenzene ....... 5 · 56-23-5 Carbon Tetrachloride 5 · .95-49-8 2-Chlorotoluene ..... 5 · 124-48-1 Bromodichloromethane 5 · 106-43-4 4-Chlorotoluene . .... 5 · 78-87-5 1,2-Dichloropropane 5 · 541-73-1 1,3-Dichlorobenzene . 5 · 10061-02-6 trans-l,3-Dichloropropene 5 · 106-46-7 1,4-Dichlorobenzene 5 · 79-01-6 Trichloroethene ..... 5 · 95-50-1 1,2-Dichlorobenzene . 5 · The Lab ID for data on this page is QHSMBLK. Partial reproductions of this report are not valid. Above data applies to submitted sample only. · - Compound analyzed for but notdetected. The reported value is the minimum attainable detection.limit for the sample. Billing Code: 9187 Analyst: ~v~ Data ReleasetAuthorization: QC report can be made available for an additional fee. Information concerning non-target analytes can be made available for an additional fee for a period of 90 days after receipt of this report. OHGAilCS AIALISIS DATA SHEET Laboratory Naue: ZALCO LABS Concentration: LOW' Date Extracted~ 03/16/93 'Lab Sample ID: HETHOD BLA~g Sample Hatrix: SOIL Date Analyzed: 03/23/93 ,~lient Sample ID: HEYHODBLANK Percent Hoisture: Dilution Factor: EPA lfKTHOD 82?0 FAS Number UG/KG FAS Number U~/KG 62-75-9 N-Nitrosodimethylamine . . 330 < 86-73-7 Fluorene ......... 330 < __108-95-2 Phenol .......... 330 < 100-10-6 4-Nitroaniline ...... 1600 < 111-44-4 bis(2-Chloroethyl)£ther 330 < 534-52-1 4,6-Dinitro-2-Hethylphenol 1600 < 95-57-8 2-Chlorophenol ...... 330 < 86-30-6 N-Hitrosodiphenylamine (1) 330 < 541-73-1 1,3-Dicblorobenzene . . . 330 ( 103-33-3 Azobenzene ........ 330 < 106-46-7 l',4-Dicblorobenzene . . 330 < 101-55-3 4-Bromopbenyl-phenylether 330 100-51-6 Benzyl Alcohol ...... 330 < 118-74-1 Hexacblorobenzene .... 330 < 95-50-1 1,2-Dichlorobenzene . . 330 < 87-86-5 Pentachlorophenol . . . 1600 < 95-48-7 2-Methylphenol ...... 330 < 85-01-8 Phenanthrene ....... 330 < 108-60-1 Bis(2-cbloroisopropyl)etber 330 < 120-12-7 Anthracene ...... 330 < i06-44-5 4-Methylphenol ...... 330 < 84-74-2 Di-n-Butylphthalate 330 < 621-64-7 N-Nitroso-Di-n-Propylamine 330 < 206-44-0 Fluoranthene ....... 330 < 57-72-1 Hexachloroethane ..... 330 < 129-00-0 Pyrene ......... 330 < 98-95-3 Nitrobenzene ........ 330 < 85-68-7 Butylbenzylpbtbalate . . . 330 < 78-59-1 Isopborone ........ 330 < 91-94-1 3,3'-Dichlorobenzidine . 660 < 88-75-5 2-Nitropbenol ...... 330 < 56-55-3 Benzo(a)Antbracene .... 330 < 105-67-9 2,4-Dimethylpbenol .... 330 < 117-81-7 bis(2-Ethylbexyl)Pbtbalate 330 65-85-0 Benzoic Acid ....... 1600 < 218-01-9 Chrysene ......... 330 < 111-91-1 bts(2-Chloroethoxy)~ethane 330 < 117-84-0 Dt-n-Octyl Phthalate . 330 < 120-83-2 2,4-Dtchlorophenol .... 330 < 205-99-2 Benzo(b)Fluorantbene . 330 < 120-82-1 1,2,4-Trichlorobenzene 330 < 207-08-9 Benzo(k)Fluoranthene . 330 91-20-3 Naphthalene ....... 330 < 50-32-8 Benzo(a)Pyrene ...... 330 < 106-47-8 4-Cbloroaniline .... 330 < 193-39-5 Indeno(1,2,3-cd)Pyrene . . 330 87-68-3 Hexachlorobutadiene . 330 < 53-70-3 Dtbenz(a,h)Antbracene . 330 < 59-50-7 4-Chloro-3-Methylphenol . 330 < 191-24-2 Benzo($,h,i)Perylene . . 330 91-57-6 2-Metbylnapbtbalene . 330 < 319-84-6 alpba-BHC ........ 330 < 77-47-4 Hexachlorocyclopentadtene 330 (' 319-85-7 beta-BHC ......... 330 < 95-95-4 2,4,5-Tricblorophenol . . 1600 < 319-86-8 delta-BHC ........ 330 < 91-58-7 2-Cbloronaphthalene . . 330 < 58-89-9 Lindane ......... 330 88-74-4 2-Nttroaniline ...... 1600 < 76-44-8 Heptacblor ........ 330 < 131-11-3 Dimethyl Phthalate . . . 330 < 309-00-2 Aldrin ........... 330 < 208-96-8 Acenaphthylene ...... 330 < 1024-57-3 Heptachlor epoxide .... 330 < 99-09-2 3-Hitroaniline ...... 1600 < 959-98-8 Endosulfan I ...... 330 < 83-32-9 Acenaphthene ....... 330 < 60-57-1 Dieldrin ......... 330 < 51-28-5 2,4-Dtnitrophenol .... 1600 < 72-55-9 4,4'-DDE ......... 330 < 100-02-7 4-Nitrophenol ...... 1600 < 72-20-8 Endrin .......... 330 < 132-6~-9 Dibenzofuran ....... 330 < 33213-65-9 Endosulfan II ...... 330 121-14-2 2,4-Dtnttrotoluene .... 330 < 72-54-8 4,4'-DDD ......... 330 < 606-20-2 2,6-Dinitrotoluene .... 330 < 1031-07-8 Endosulfan sulfate . . . 330 < 700§-72-3 4-Chlorophenyl-phenylether 330 < 50-29-3 4,4'-DDT ......... 330 < The Lab ID for data on this page is NK?MBLK. ( - Compound analyzed for but not detected. The reported value is the minimum attainable detection limit for the sample. Pase 1 Oi6AIlCS AIALYSIS DATA SHEET -Laboratory Name: ZALCO LA~S Conc~n~ra~ion: BOW ~Lab Sanple ID: HETHOD BLANK Sample ffatrix: SOIL Date Analyzed: 03/23/93 ~lient Sample ID: NETHOD BLANK Percent Hoisture: Dilution Factor: 1.0 KPAHETHOD 8270 CAS Number UG/KG CAS Number UG/KG 84-66-2 Dietbylpbtbalate .... 330 < 53494-70-5 Endrin aldehyde ..... 330 < The Lab ID for data on this page is NK7NBLK. Partial reproductions of this report are not valid. Above data applies to submitted sample only. Billing Code: 9184 Analyst: ~ Data Release Authorization: ~ QC Report can be made available for an additional fee. Information concerning non-~target analytes can be made available for an additional fee for a period of 90 days after receipt of this report. Page 2 OIGIIlCS ~ILYSIS DATA SHEET Laboratory Name: ZALCO LABS Concentration: LOg Date Extracted: 03/29/93 ~tab Sauple ID: HETHOD BLA~ Sasple Hatrix: SOIL Date Analyzed: 03/29/93 :lient Sample ID: HETHOD BLANK Percent Hoisture: Dilution Factor: 1,0 EPA lf~THOD 82?0 CAS Number . u~/k~ CAy Number 62-75-9 N-Hitrosodimethylamine . . 330 ( 86-73-7 Fluorene ......... 330 < 108-95-2 Phenol .......... 330 < 100-10-6 4-Hitroaniline ...... 1600 111-44-4 bis(2-Chloroethyl)£ther 330 < 534-52-1 4,6-Dinitro-2-Hethylphenol 1600 95-57-8 2-Chlorophenol ...... 330 < 86-30-6 N-Nltrosodiphenylamine (1) 330 541-73-1 1,3-Dichlorobenzene . 330 <. .103-33-3 Azobenzene ........ 330 106-46-7 1,4-Dichlorobenzene . ... 330 < 101-55-3 4-Bronophenyl-phenylether 330 100-51-6 Benzyl Alcohol ...... 330 < 118-74-1 Hexachlorobenzene .... 330 95-50-1 1,2-Dichlorobenzene . . 330 < 8?-86-5 Pentachlorophenol .... 1600 95-48-? 2-Eethylphenol .... 330 < 85-01-8 Phenanthrene ....... '330 108-60-1 Bis(2-chloroisopropyl)ether 330 < 120-12-7 Anthracene ........ 330 106-44-5 4-Methylphenol ...... 330 ( 84-74-2 Di-n-Butylphthalate . 330 621-6'4-? N-Nitroso-Di-n-Propylamine ~30 < 206-44-0 Fluoranthene ....... ~30 67-72-1 Hexachloroethane ..... 330 < 129-00-0 Pyrene .......... 330 < 98-95-3 Nitrobenzene ....... 330 < 85-68-7 Butylbenzylpbtbalate . . 330 78-59-1 Isophorone ........ 330 < 91-94-1 3,3'-Dicblorobenzidine . 660 < 88-75-5 2-Nitropbenol ...... 330 < 56-55-3 Benzo(a)Anthracene .... 330 < 105-67-9 2,4-Dimetb~lphenol . . . 330 < 117-81-7 bis(2-Etbylbexyl)Phthalate 330 < 65-85-0 Benzoic Acid ....... 1600 < 218-01-9 Cbrysene . . ....... 330 < 111-91-1 bis(2-Chloroetboxy)~etbane 330 < 117-84-0 Di-n-Octyl Phtbalate . . . 330 120-83-2 2,4-Dichloropbenol .... 330 < 205-99-2 Benzo(b)Fluoranthene . 330 120-82-1 1,2,4-Tricblorobenzene . 330 < 207-08-9 Benzo(k)Fluoranthene . . . 330 < 91-20-3 Naphthalene ...... 330 < 50-32-8 Benzo(a)Pyrene ...... 330 106-47-8 4-Cbloroaniline ..... 330 < 193-39-5 Indeno(1,2,3-cd)Pyrene . . 330 < 87-68-3 Hexacblorobutadiene . . 330 < 53-70-3 Dibenz(a,b)Antbracene . . 330 < 59-50-7 4-Cbloro-3-Metbylphenol 330 < 191-24-2 Benzo(g,h,i)Per~lene . . 330 < 91-57-6 2-Metbylnaphtbalene . . 330 < 319-84-6 alpba-BHC ....... 330 < 77-47-4 Hexachlorocyclopentadiene ~30 < 319-85-7 beta-BHC ......... 330 < 9~-95-4 2,4,5-Trichlorophenol . . 1600 < 319-86-8 delta-BHC ........ 330 < 91-58-7 2-Chloronaphthalene . 330 < 58-89-9 Lindane ......... 330 < 88-74-4 2-N~troaniline ~ ..... 1600 < 76-44-8 Heptacblor ........ 330 < 131-11-3 Dimethyl Phthalate . . . 330 < 309-00-2 Aldrin .' ......... 330 < 208-96-8 Acenaphtbylene ...... 330 < 1024-57-3 Heptachlor epoxide .... 330 < 99-09-2 3-Nitroaniline ...... 1600 < 959-98-8 Endosulfan I ..... . . 330 < 83-32-9 Acenaphthene ....... 330 < 60-57-1 Dieldrin ......... 330 < 51-28-5 2,4-Dtnitrophenol .... 1600 < 72-55-9 4,4'-DDE ......... 330 < 100-02-7 4-Nitropbenol ...... 1600 < 72-20-8 Endrin ......... 330 132-64-9 Dibenzofuran ....... 330 < 33213-65-9 Endosulfan II ...... 330 < 121-14-2 2,4-Dinitrotoluene .... 330 < 72-54-8 4,4'-DDD ........ 330 606-20-2 2,6-Dinitrotoluene .... 330 < 1031-07-8 Endosulfan sulfate .... 330 7005-72-3 4-Cblorophenyl-pbenyletber 330 < 50-29-3 4,4'-DDT ......... 330 < The Lab ID for data on this page ~s NH?HBLE. < - Compound analyzed for but not detected. The reported value is the minimum attainable detection limit for the sample. Page I -- ORGANICS A~LYSIS DATA SHEET ~Laboratory Name: 2ALCO LABS Concentration: LOg Date Extracted: 03/29/93 Lab Sample ID: HETHOD BLANK Sample Hatrix: SOIL Date Analyzed: 03/29/93' Client Sample ID: METHOD BLANK Percent Moisture: Dilution Factor: 1.0 EPA IfETHOD 82?0 CAS Number ~ u~/k~ CAS Number u~/k~ 84-66-2 Diethylphtbalate ..... 330 < 53494-70-5 Endrin aldehyde ..... 330 < The Lab ID for data on this page is NM?HBLK. Partial reproductions of this report are not valid. Above data applies to submitted sample only. Billing Code: 9184 Anal?st: ~-~%, Data Release Authorization: ~.~ QC Report can be made available for an additional fee. Information concerning non-target analytes can be made available for an additional fee for a period of 90 days after receipt of this report. Page 2 JEFF CAMPBELL ENVIRONMENTAL CONSUL TING SOIL INVESTIGATION WORK PLAN M/D TOTCO, INC. FORMER CLASS V INJECTION 'WELL 3011 ANTONINO AVENUE BAKERSFIELD, CALIFORNIA Submitted To: Steve McCalley, R.E.H.S., Di ~c~tur Kern County Environmental Health Services Department Date · Submitted: March 2, 1993 Completed By: Dayne L. Frary, R.G., R.E.A. Submitted By: Jeff Campbell Environmental Consulting 8559 Farmers Lane Bakersfield, California 93307 8559 FARMERS LN. BAKERSFIELD, CALIFORNIA 93307 )TELEPHONE (85) 845-8797. Table of Contcnls i.() inlr(x-Juclion i 2.0 Background I 3.0 Activities and Procedures 2 3. 1 Soil Boring; 2 3.2 Soil Sampling 2 3.3 l,a bora ~ory Aha lysis 3 ~.0 Report Preparation 3 5.0 Workplan (~erliticalion 4- Appendix I lcahh and Sately Plan SOII~ INVIJSTIGATION WORKPLAN MI)-'i'OTCO. IN(Z i~ORMER CLASS V INJ~71'ION WF.I.I. i.0 INTROI)UCIION This workplan describes lhe project background, and drilling, sampling, and analytical aclivilies lo tx' pertormed al Ihe t0rmer Iocarion of lhe (~lass V injeclion well located at 3OI! Antonino Avenue. within a portion of tile northwest Bakerstield oily limit. The plan addresses requiremenls submiued 1o MI)-TOT(7(), Inc. by bls. Flora l)arling, itazardous Malenals Specialist with the Kern Counly l!nvironmenlal l leahh Se~'ices l)epanmenl (Count),). Addilionai work is required by the Cbuno' to identify the Vertical extent of contamination by obtaining "clean" soil samples from at least five feet below the last recorded contaminated sampling poinl in order lo allow ~or closure of ~lle ~ormer well. The previous phase o~' lhe investigation was performed and reported by Mr. Jeff Campbell. Environmental Consuhanl, and was daled February ~1-, 1993. 2.0 BACK(;ROIJNI) Mr. (:ampbc'll's reporl, M 1) TOTCO. Inc. 1)~ Well Characlerizalion and Sile ]:~?.nl~l~'Ll/f~, provides delails of thc former well and pipin~ system location and conslruclion, and all aclivilies pert0rmed prior 1o Ibc preparation of Ibis workplan. The property has been leased u) M-l) TOTCO, Inc t°r some 14 years. The company utilized the on-site "dry well" for waste-water collection and elimination by drainage lhrough gravel. The waste water was generaled as rinsale by d-~e cleaning of oil well dnlling tools Widl a high pressure washer and by use of a wash basin inside the neighboring shop. Rinsate was piped by gravily to a clanfier, thence Io the concrele/gravel lined well. The total depdl of the well a~ lhe base of the external gravel liner was approximately. 17 feet below surface grade (fbsg). At present, tile well has been altered for abandonment: tile concrete liner, external gravel pack. and known conlaminalcd soil have been reniovcd Ia a dcplh of 22 fbsg and transporlcd Io VcnVirolck. a licensed disposal facilily in Arvin, California. ]'he 1 piping has also been removed, and the clarifier is Io be tilled wilh concrete which will render it useless. The excavation was backfilled with clean, off-site borrow soil. 3.0 ACTIVi'I'IbZS AND PROCEI)IJRES 3.1 Soil Boring One (i'), 6-inch diameter bonng will be advanced through the center of the t0rmer well location for colleclion of additional samples at 22, 27, and 32 f'bsg. Mellon Drilling Company will provide the truck-mounted ng with a continuous-flight, hollow-slem auger which will be utilized to drill the bonng. All I~)nng equipment will be steam-cleaned pnor to arrival at the site in order to minimize the possibilily of contaminaling Ihe samples. In addition, splil-slxx)n samplers and sample nngs will be washed in a solulion of Imodium phosphale (TSP), rinsed in lap wmer, and then final-nnsed in distilled water. After fl~c bonng has bccn sampled at 32 fbsg (T.D.), it will be backfilled to 22 feet wilh bentonite pellets and lhen wid'~ the clean borrow soil presendy in lhe excavation It) the surface. Any additional soil found lo be contaminated will be tr,~nsporwd under manifesl lo lhe VenVirotek disposal JaciJily on the scheduled work. day. 3.2 Soil Sampling 2.5-inch'diameter by 18-inch length "undisturbed" samples will be collecled al 22, 27, and 32 fbsg using a split spoon sampler lined with three (3). 6 inch. brass sample rings. The sampler will be driven ahead of the auger bil al Iht appmpnale deptla by a 140pound. down hole hammer. It will not be necessary ~o collec~ samples in d-~e clean impon soil between surface grade and 22 fbsg. The soils recovered in the upper and middle nngs will be descnbed by the California Registered Gcx)logisl. who will record Ihe descnptions on the bonng log according to the Unified Soil Classificanon System (USUS). The same samples Will be screened t0r initial indicalions of hydrocarbon contamination using a photoionizmion detector (PID). The PID readings will also be recorded on the boring log. The lower sample will be sealed with Teflon gaskets, capped, final- sealed with duct tape, labeled, and placed in an ice chest chilled with Blue Ice ar° Centigrade to preserve its chemical integrity. The sample identifications and their requested laboratory analy~es will be recorded on a chain-of-cuslody documenl. The chain-of-custody will' remain wilh the samples through delivery ~o Zalco Laboratones, Inc., a State-certified 'laboratory: a copy of the compleled chain-of-custody will be relumed Io lhe geologisl al Ihe time of delivery. Upon completion of thc analyses, thc reported results will be signed and certified by lhe chief chemist and mailed lo lhe geologist. 3.3 Laboralory Analyses A lolai of three (3) soil samples will be delivered to Zalco La bora tones, Inc. in Bakersfield on die scheduled work day. The following analyses will be specified for ~ each sample: Volatile Organics by EPA Method 82't-0 Semivolalile Organics by EPA Melhod 8270 TPH as gasoline by EPA Modified Method 8015 TPH as diesel by EPA Modified Method 8015 Aromalic Volatile Organics by EPA Method 8020 CAM me~als: Barium, Cadmium, Copper, and Lead ar.0 REPORT PREPARATION 1Jpon receipl of the laboralory analyses, lhe geologisl will prepare a delailed report of the drilling and sampling program, including all laboratory results for the samples. Additional illustrations such as revised site maps and cross-sections will be included as needed. Conclusions and recommendations will be considered and reported pending the outcome of the laboratory analyses. WORK. PI.AN CERTIIqCATION This workplan t0r addilional sampling al lhe MD-TOTCO. Inc. t0rmer ('.lass V injection well was prepared by a California Regislered Geologisl and t!nvironmental Assessor expenenced in Ihe managemenl of soils and ground-waler investigations and approved by fl~e Kern Coumy Environmenlal Heahh Services l)epartmenl. Submilted by: Dayne L Frary Regislered Geologisi State of .California No. 4456 Registered Environmemal Assessor State of California No. ).980 APPENDIX Health and Safety Plan GENERIC HEALTH AND SAFETY PLAN Introduction: Jeff Campbell Environmental Consulting (JCEC) has developed this health and safety plan for use by all JCEC associates. This health and safety plan establishes the policies and procedures which protect workers and the public from potential hazards posed by work at a typical site. J.C.E.C. considers safety the highest priority during work at a site containing potentially hazardous materials and has establish a policy of minimizing exposure which must be upheld on all projects. All project activities will be conducted in a manner that minimizes the probability of injury, accident or incident occurrence. The plan does not focus on the specific work activity planned for a specific site. It must remain flexible because of the nature of~ that require deviations from the original plan. This flexibility allows modification by the J.C.E.C. site supervisors. This plan takes into account the preliminary information currently available from discussions .with the project management team. This plan is written in accordance with SB 198 CAL / OSHA Safety Orders. Site History and Scope of Work: J.C.E.C. performs site investigations, site characterizations, site remediation and similar environmental related surveys. These sites Commonly involve borehole sampling procedures. Borehole sampling often invOlves.a borehole drilling rig, which employs the use of a hollow stem auger and a split spoon sampler. Key Personnel and Management: J.C.E.C. maintains a policy of providing its personnel, subcontractors, and authorized visitors with information and procedures in order to protect them and the adjacent community from and adverse effects that might result from the work at the job site involving potentially hazardous substances. All JCEC personnel will read and agree to comply with the health and safety procedures set forth in this manual. Visitors Will not be admitted to the site unless they have also read and agreed to these procedUres. Site Operations Supervisor: J.C.E.C. designates a Site Operations Supervisor (SOS) who implements and enforces project safety programs and procedures. The SOS will ensure that the daily safety meetings are held and will interface as required with other sire representatives. The SOS takes the following action(s) when appropriate: Orders the immediate shut down of site activities in the case of a medical emergency or unsafe practice. Ensures protective clothing and equipment are properly used, maintained and stored ~ Restricts visitors from areas of potential .eXposure to harmful substances. A safety log will be kept for all J.C.E.C. activities. This log will include daily safety meeting topics,' training given, air monitoring information, first aid administered, visits of all outside personnel and any incidents of a health and safety nature. The SOS has responsibility for implementing and enforcing the safety program and procedures. He will oversee any personnel monitoring and will decide when action levels have been reached which require more stringent protection. The SOS establishes and enforces the protective equipment to be used for various site activities and will maintain contact with the J.C.E.C. Safety Administrator. Field Project Manager: The Field Project Manager (FPM) has responsibility for all field activities and enforces safe work practices by all crew members. He watches for any ill effects on any of the crew members, especially those symptoms caused by heat stress of chemical exposure. The FPM oversees the safety of. anyone who enters the site and maintains communication with J.C.E.C. Site Operations Supervisor. Equipment Operators: Equipment operators will be responsible for the maintenance, inspection and safe operation of all equipment. Personnel Safety Responsibilities: Although the employer is responsible for providing a safe and healthful work place, each employee is responsible for his / her supervisor. All personnel will follow the policies set forth in the J.C.E.C. Health and Safety Manual. Completed and submitted by: Jeff Campbell, Registered Environmental Assessor State of California No. 3773 fRACT OPTIONS FOR LW:AKING Site Specific Time Accounting Sheet Permit #- Site Specific Status'Changes: Employee # Employee Signature Site Name or Address~cT'%~ Funding (Local, State, of Federal~c Cat~ egory Activity Hours Date ucoe Code Description ( 10the ) Data Entered By: Date: CONTRACT OPTIONS FOR LEAKING TANKS Site Specific Time Accounting Sheet Permit # Site Specific Status Changes: Employee # Employee Signature Site Name or Address Funding (Local, State, of Federal) Cat. egory Activity Hours Date ucoe Code Description ( 10the ) Notes: ~ ~~,~ Data Entered BY: Date: Env. Health 580 4113 137 (Rev. §/89) KERN COUNTY ENVIRONMENTAL SERVICES DEPARTMENT INVESTIGATION RECORD ' BUSINESS OWNER DBA ADDRESS OF VIOLATION ~// APN CT SPECIALIST/INSPECTOR CHRONOLOGICAL RECORD OF INVESTIGATION DATE TIME NARRATIVE %~o ~ ~ 2700 "M" Street, Suite 3000 Bakersfield, California 93301 I~e: Former T~ite~ V Inj~n Well located at 3011 Antonino Avenue Bakersfield, California. Dear Mr. McCalley: In response to your letter dated April 9, 1993 confirming the closure of the former Class V injection well site located at 3011 Antonino avenue, which was formerly occupied by M/D TOTC©. Jeff Campbell Environmental Consulting acting on behalf of M/D TOTCO wishes - . to convey the following 1. MID TOTCO no longer leases/occupies-the site located at 3011 Antonino Avenue. Therefore, M~ TOTCO has no control of current conditions or future operations conducted on this site. 2. The former Class V injection well was abandoned and removed, so future usage of the injection well by occupants of this site is not possible. 3. As a former lessee of the subject property, MID TOTCO has completed the appropriate procedures enabling your department to confirm that the former Class V injection well site is free of pollutants and poses no threat to water quality. 4. John Antonino of Valley Steel Construction is the owner of the subject property and should be responsible for operations conducted at this site. M/D TOTCO has had no involvement with this site as. of March 31, 1993. ~ 8559 FARMERS LN. BAKERSFIELD, CALIFORNIA 93307 ~TELEPHONE ~805~ 845-8797 ~,~ JEFF CAMPBELL ENVIRONMENTAL CONSUL TING Jeff Campbell Environmental Consulting wishes to maintain that M/D TOTCO has no~ interest or responsibility involving the site located at 3011 Antonino Avenue as of March 31, 1993. If you have any questions or require additional information please contact Jeff Campbell or Dayne Frary at 845-8797. Respectfully, · Je~ c~n~ell, R.E.A. : ~ 8559 FARMERS LN. BAKERSFIELD, CALIFORNIA 93307 ' ~TELEPHONE (805).__ 845-8797 ENVIRONM ?AL HEALTH SERVICe-DEPARTMENT STEVE McCALLEY, R.E.H.S. i~~~'. 2700 'M" Street, Suite 300 DIRECTOR W Baker.field, CA 93301 (806) 801-3S36 (805) 841-342~ FAX April 9, 1993 M/D Totco, Lac. 6910 Moony Avenue Bakersfield, CA 93308 Ancntion Gary Pittman SUBJECT: CLASS V SHALLOW INJECTION WELL LOCATED AT 3011 ANTONINO AVENUE, BAKERSFIELD, CALIFORNIA Dear Mr. Pinman: This letter confirms thc completion of site investigation a*. the above location. With the provision that the information to this agency was accurate and representative of existing conditions, it is the position of this office that no further action is required at this time. Please be advised that this letter does not relieve you of any liability under the Code of Federal Regulations or Water Code for past, present, or future operations at the site. Further, it does not relieve you of the responsibility to clean up existing, additional, or previously unidentified conditions at the site which cause or threaten to cause pollution or nuisance or otherwise pose a threat to water quality or public health. Additionally, be advised that changes in the present or proposed use of the site may require further site characterization and mitigation activity. It is your responsibility to notify this agency of any chtxnges in report content, future contamination findings, or site usage. If you have any questions regarding this matter, please contact Flora Darling at (805) 861-3636, Extension 549. Sincerely, Steve McCalle~2~Dt~rector By: ~/Joe Carlos, R.E.H.S. Interim Program Supervisor Hazardous Materials Management Program FD:jrw cc: U.S. Environmental Protection Agency' (EPA) Attn: Martin Zeleznie Regional Water Quality Control Board, Fresno Attn: Dale Essary (hm~lsrlins~o'~o-h.mS$) (~ ~i~[: JEFF CA MPBEL L EN VII IONMENTA L CONSUL TIN( FFebruary 4, 1993 t Lydia Von Sydow Registered Environmental Assessor Environmental Health Services Department, County of Kern 2700 "M" Street Suite 300 Bakersfield, California 93301 Re: C~3mpJ~t[on of the charact_erJzat[on ~em~ject on property leased by M-D T_O_T_CO_Jocated at 3011 Antonino Avel~ Celifornia~ Dear Ms. Von Sydow' The characterization and site remediation project has been completed. As requested a copy of this report accompanies this letter. The subject dry well located at 3011 Antonino Avenue Bakersfield, California is abandoned and its use eliminated. After review of the project report, correspondence should be directed to Gary Pittman M-D T©TCO representative and John Antonino the property owner. Additionally, please direct copies 'of any correspondence to Jeff Campbell Environmental Consulting so we can complete our file regarding this Project. Gary Pittman John Antonino M-D TOTCO Valley Steel Construction 6910 Meany Avenue 3304 Pierce Road Bakersfield, California 93308 Bakersfield, California 93308 If you have questions or require additional information, please contact Jeff Campbell at (805) 845-8797. 'Jeff C'aYnpbell, Registered Environmental Assessor. , C 8559FARMERSLN'BAKERSFIELD'CAL/FORNIA93307 ~TELEPHONE (805J 845-8797 ·. a§elsod ~¥10i ssaJpp~ s,~sseJppv pue 'oleo '~oq~ o~ Ou~oqs id~aoaB uJnla~ ~. ~ pa~anUaQ azeO ~ ~oq~ ol · :'-~1 ~a ~a~ :~.~.T.V ~'~ ~ ~ ~ . ~ G~ ' I~e~ leuo~eu~a~ul ~oj asn ~ou o~ ~ ~:_.m ~ =m ~ ~ ~' ~ ~-'~~ pep~AOJd eSeJeAoOi!e~ ooueJnsuIpeUl~eOoN m ~ '~ o ~ ~ -S 'L9~ hE8 0Eh d o · ~ ~ . Thank you for using Re~um Receipt Se~iCe. UJ_~ SHALLOW INJizL;IIoN WELL _.HJac. KLiST 02/'93 PAGE 1 YACiLiTY NAME: TOTCO DATE OF iNSPECTION: 12/28/92 TIME: iNSPECTOR{S): LYDIA V. VON SYDOW _AL~LJ.L'i'±UN_-kL PART± ~.IPANTS: i. GENERAL iNFOR~iATiON A. iNTRODUCE YOURSELF AND ALL OTHERS (SHOW CR. EDENTiALS} B. EXPLAIN WHY YOU ARE THERE, C. {LEGAL INFO} OWNERS NA}iE: JOHN :%NYONiNO ADDH~SS: CITY: BAKERSFIELD STATE: (_:A ZiP: PHONE NU}'IBER: D. OFERATOR'S NAME: 'POTCO ADDRESS: 69i0 HEANY AVE. CITY: BAKERSFIELD STATE: C.4 .4PN: PHONE NUHBER: (SWAP BUSINESS CARDS, ALSO ASK FOR BUSINESS. E. PARENT COMPANY: ADDkESS: CiTT: STATE: ZiP: ARE THEY A SUBSiDiARY OF A CORPORATioN: YES f'. CONTACT PERSON: PHONE NUbiBER: -i. iN'!'ERViEW THE CPERATOR/~'~ATURE ,)F BL~SiNESS .8. ARE THEY A >iEMBER. OF :~:~ ASSOCiATiON: ~:. ARE THEY AWARE OF ANY WATER SUPPLY LOCATiON/OWNERSHiP: C~ALiF. ~ATEB CO, 0, SITE HISTORY YEARS OF OCCUPATION: i5 PREVIOUS OWNERS: UNKNOWN PREVIOUS OPERATORS: UNKNOWN P A E. PRODUCTS OR SERVZCPiS OFFERED: OiLFEELD EG;f_:ZPbiENT F, BRIEF DESC. R ~ PTIO['J OF ANY PROCESS, OPER. Ai' iON HAiNTENANCE THAT PRODU(ES WASTE: EQU.[P}fEiqT REPAIR G. WHAT CHEHiCALS .ARE STORED ON :SITE' NON/ H. DO THEY HAVE }~ATERiAL SAFETY DATA SHEETS: YES [. DESCRIBE THE WASTE J)-iSPOSAL PB:.ACTiq:E~,: RE( J. SOLVENT HAULER: lqA VERIP'iCATiON RECEIPTS' MU~' U~!'~!~: K, t~:ASTE OiL HAULER: NA VERiFiCATiON R. ECEiPT%: HO:,f ',i:~'TESi' L. WASTE ANTIFREEZE HAULER: NA RECEIPTS: ~.Ot,.' OFTEN: }~. WASTE SLUDGE HAULER' 2ECEiPT$: HOk: OP'TEiq: _'J: OTHER WASTES: R[[CKiPiS: M(R~: ~' ASK FOR ~ iTE ~',~ ~9, - -- ~.'-~{l: ................... _ , '.l:_z .} k;P P l~!'rY AN[} Aa-.dt_;iL'i'b ......... PL:{NS FOR THE DISPOSAL :5Y:6TE}i: ~ii. [NSPE('T THE FAC!LZ'TY (;EN~RAL SITE CONDiTiONS H(~L}SEi{EEPING: FAiR EASE t)ff ENTR, Y: COOPERAVigN: GOOD SURROUNDING LAND USE: ~ A. GENERAL APPEARANCE OF THE WELL(S}: ;{ASHR:'Ri'K ~_OiqN'ECTED 'PO ~' DRYe'ELL. B. SUSCEPTiBiLiTY TO SPILLS: YES C. CLASS V WELL{S): ONE STATUS: ACTIVE YEARS OF OPERATION; i5+ D, OiL/WATER SE~'ARATOR, OR GREASE TRAP USED: ORYWELL PAGE ' 3 E. ARE THE WELLS PUMPED cOUT: HOW OFTEN: F. DO THE WELLS EVER GET ffL[JJ~,ED G. CONSTRUCTION DETAILS (MEASURE) TOTAL DEPTH: DIAMETER: ~_.A~Z~_, : H. ARE THE iNJECTiON WELLS REGULATED BY A STATE Ok LOCAL PROGRAM: R. WC~C.B i. PERMIT: NO J. HOW ARE SPILLS OR AC. CiDENTS HANDLED: k, WHERE DOES THE FLOOR/LOT DRAINAGE WATER GO: STREE'F h. CAR WASH: ~O HOW IS THE EFFLUENT DISPOSED.: (:.LEANERS USED: M. HOW MANY AUTOS ARE SERVICED DAILY: NONE DOCUMENTS TO REQUEST MAP OF FACiLiTY AS-BUiLT DiAGRAbiS, PLUMBING PLANS DRILLERS LOGS MO[qiTO~ING WELL DATA [LOW DIAGRAbJ OF PNt~L.E ...... WAS~[ GEt. qERA'FiON, AND DISPOSAL 5~ANIFESTS FOR WAb'r~ DISPOSAL MATERIAL SAFETY DATA SHEETS UNDERGROUND iNJECTiON CONTROL PROGRAM INSPECTION REPORT AGENCY: KERN COUNTY ENViRON'...,iENTAL HEALTH SERVICES DEPARTHE_"{T INSPECTOR: LYDIA V. VON SYDOW FACILITY INFORMATION FACiLiTY NAME: TOTCO PARENT COMPANY: ADDRESS: 6910 MEANY AVE ~±l~: BAKERSFIELD STATE: CA ZiP: ~o~lAuT NAHE: POSITION: DESCRiPTiON OF WASTE STREAH: RiNSATE DESCRiPTiON OF INJECTION WELL: WA:SHRACK CONNECTED ~O DRYWELL DESCRiPTiON OF ACTIVITY THAT HAY ENDANe_~: L~.~ui~u wA'! ~LLATED TO INJECTION WELLS OR TANKS e.g. PONDS, SPILLS): iNSPECTiON iNFORMATiON iNSPECTiON DATE: iZ/28/'92 NUHBER OF WELLS: ONE WELL TYPE AUTO SERVICE: iNDUSTRiAL WASTE: hb A(;RicULTL.:RA~ 'WA~TE STORH WATER: OTHER: STATUS OF WELLS ACTIVE: ABANDONED: YES UNDER ~)ONSTRUC:TiON: OTiqER iNJECTATE SAMPLED: YES VIOLATION FOUND: YES FOLLOW-UP NEEDED: YES COMbiENTS: KERN COUNTY HAZARDOUS WASTE iNCIDENT REPORT KERN CO. ENV. HEALTH SERVICES TERRY L. GRAY (805) ~61-3636 DOT iD ~U~BER: CHEM, ~AME/~AJOR CO~PONgNT: iMPORi'JJJT A[~iiTi(:~J.L HAZARD:___TOXIC ___FLA~.~LE ___F'UBB ___SOLh5 ___~EACTiVg , OOg~O~[?g _=iix ___CIO, DOT iD HUMBER: HEALTH AND D{ViRONNENTAL CONTA~{INATION: 0i___~.[~ .................. ,~__~:~i~L- _227 222- r~..r,:.~,:~ ~ ................................... ,)V___=~iLDL[FE .................. {J~8___:~C;(DED ~Rh' _ ................. HEALTH EI~K ~SE~H~E~T Z~D$~]: .................... O~___[~R~E~,T .................. i~J___~,US~L.~)iD .................. Di~OR~AT!O~ PHO~{ED-[N? i'___ ~___ ~F Y~3~, [~A'?E ..... i i___FO<'DS'?L{FF~ .................. '?~E~ B~': ........ i3___7~LL~)}~3 .................. COMPUTER Y~P[{T (CHECK) .... CLE~K'~ ~.ql,l~=~.[~'-~'~[': ........ i4___~t{~A~S .................. DATE OF ~OTiF[CATiO~ {<'F. HZALTH ,_.~'- ~u~'"=:= = ,~,., ...... 30~ .... ~___:L'?HER: .................. [~ATE OF ~OTIFiCATiO~ O~ ~ED[A ...................... ENVIRONMENTAL HEALTH SERVICES DEPARTMENT STEVE McCALLEY, R.E.H.S. ~ 2700 "M" Street, Suite 300 DIRECTOR ~! Bakersfield, CA 93301 (805) 861-3636' (805) 861-3429 FAX M/D TOTCO, Inc. March 10, 1993 6910 Meany Avenue Bakersfield, CA 93308 Attention: Gary Pittman SUBJECT: CLASS V SHALLOW INJECTION WELL LOCATED AT 3011 ANTONINO AVENUE, BAKERSFIELD, CA Dear Mr. Pittman: This letter is an official notice to inform you that the property noted above'has been determined by Kern County Environmental Health Services Department (KCEHSD) to be the site of a Class V shallow injection well. The well has been identified as a wash rack connected to a drywell. This notice is being sent to YOU because you have been identified as the operator of the injection well located at the property listed above. Pursuant to Code of Federal Regulations 40 (40 CFR), Section 144.12 (a), "no owner or operator shall.., operate [an injection well].., in a manner that allows the movement of fluid containing any contaminant into underground sources of drinking water, if the presence of that contaminant may cause a violation of any primary drinking water regulation.., or may otherwise adversely affect the health of persons." This Department is aware that closure of the well and site characterization has been initiated prior to this notice. All site work must comply with the KERN COUNTY AND EPA REGION 9 GUIDELINES FOR CLOSURE OF SHAIJ.OW DISPOSAL WELLS. The booklet cites the minimum required for site work plan activities, contractor requirements, example illustrations of well designs, and sampling methods and procedures. Be advised that KCEHSD may have additional requirements not listed in the EPA closure guideline booklet. In accordance with Kern County Ordinance Code G-5541, Section 8.04.100 the Department is authorized to charge for inspections, review of repons, and. laboratory service costs incUrred in the process of obtaining compliance with any violations noted. Be advised that you will be billed at the rate of $24.80 per hour for oversight during the abatement of violations connected to the Class V well. M/D TOTCO, Inc. Subject: Class V Shallow Injection Well March 10, 1993 Page 2 If you have any questions regarding this Order, you may contact' me at (805) 861-3636, extension 582. Sincerely, Steve McCalley, Director By: · Lydia V. von Sydow, R.E.A. Hazardous Materials Inspector Environmental Health Services Department LVS:cas cc: U.S. Environmental Protection Agency (EPA) ATTN: Martin Zeleznik Regional Water Quality Control Board - Fresno AT'fiN: Dale Essary John B. Antonino Jeff Campbell Environmental Consulting ATI'N: Jeff Campbell ~lydia~totco.uic ENVIRONMENTAL HEALTH SERVICES DEPARTMENT STEVE McCALLEY, R.E.H.S. ~ 2700 "M" Street, Suite 300 DIRECTOR V/~ Bakersfield, CA 93301 (805) 861-3636 (805) 861-3429 FAX M.D. Totco, Inc. March 4, 1993 6910 Meany Street Bakersfield, CA 93308 ATTN: Gary Pittman/Larry Esparza SUBJECT: Former Totco Site Class V Injection Well 3011 Antonino Street, Bakersfield, CA Gentlemen: This office has reviewed the workplan submitted by Jeff Campbell, Environmental Consulting for the above-referenced site. The workplan, which addresses areas of concern enumerated in this Department's letter dated February 16, 1993, is acceptable for the completion of investigation for the former Class V injection well. Please notify this office 48 hours prior to beginning work in order that a Hazardous Materials Specialist may be present. Work must commence before April 5, 1993. All reports must be copied to this office for review and approval before a closure letter may be issued. If you have any questions, you may contact me at (805) 861-3636, Extension 549. Sincerely, Steve McCalley, Director By: Flora Darling, R.E.H.S., R.E.A. Hazardous Mater/als Specialist III Hazardous Materials Program FD:cas cc: Jeff Campbell, Environmental Consulting Dayne L. Frary, R.G. ~fl0ra~otco.ltr JEFF CAMPBELL ENVIRONMENTAL CONSUL TING March 2, 1993 Steve McCalley, R.E.H.S. Director Environmental Health Services Department 2700 "M" Street, Suite 3000 Bakersfield, California 93301 Re: Former TOTCO Site Class V Injection Well located at 3011 Antonino Avenue Bakersfield, California. Dear Mr. McCalley: In accordance with your letter dated February 16, 1993 requiring additional soil sampling of the former Class V injection well site, Jeff Campbell Environmental Consulting acting on behalf of M/D TOTCO submits and requests approval for the attached work description and health/safety plan. We regret the procedures and report completed prior to your letter was not in compliance with Class V injection well closure requirements.' In order to review our protocol in determining compliance requirements for a site, we request a copy of K.C.E.H.S.D.'s letter notifying M/D TOTCO that the 3011 Antonino Avenue site was deemed a Class V injection well site. Jeff Campbell Environmental Consulting wishes to maintain a professional relationship with the K.C.E.H.S.D., and will work diligently to comply with all regulations and/or requirements enlisted by your department. If you have any questions or require additional information please contact Jeff Campbell or Dayne Frary at 845-8797. R~espectf~ly, ( 8559 FARMERS LN. BAKERSFIELD, CALIFORNIA 93307 )TELEPHONEi f(805~ 845-8797 ENVIRONMENTAL HEALTH SERVICES DEPARTMENT STEVE McCALLEY, R.E.H.S. ~ 2700 "M" Street, Suite 300 DIRECTOR ~! Bakersfield, CA 93301 (805) 861-3636 (805) 861-3429 FAX February 16, 1993 M.D. Totco, Inc. 6910 Meany Street Bakersfield, CA 93308 Attention: Gary Pittman/Larry Esparza SUBJECT: FORMER TOTCO SITE CLASS V INJECTION WELL 3011 ANTONINO STREET, BAKERSFIELD, CA Gentlemen: This office is in receipt of a Site Characterization Report prepared by Jeff Campbell, Environmental Consulting, for the above-referenced facility. The report is not acceptable to this Department due to several factors which have not been satisfactorily addressed. 1. The laboratory analysis of selected soil samples have demonstrated, that Barium, Copper, Cadmium, and Lead exceed drinking water standards. 'Additional soil analyses are required.. 2. Soil samples for laboratory analyses of TPH diesel, TPH gasoline, and BTEX was not collected at the lowest level of the excavation. The Environmental Protection Agency (EPA) requires a minimum of five feet of clean soil beneath the lowest part of the contaminati°n plume. Confirmation samples were not collected at the total depth of the excavation (22 feet below surf'ace grade). 3. Laboratory analyses of soil for semi volatfles (solvents) was not performed. 4. A professional geologist or cml engineer registered in'the State of California did not perform the work or sign the report as required by EPA Region 9 and Kern County Environmental Health Services Department guidelines for shallow disposal wells. In order for this office to issue a closure document for the site, the following work must be performed by a registered professional geologist or civil engineer. M.D. Totco, Inc. Subject: Former Totco Site - Class V Injection Well February 16, 1993 Page 2 Soil borings to a depth below 22 feet with attendant soil sampling at five-foot intervals until five consecutive feet of soft is free of contaminants. Laboratory analyses of collected soil samples shall be analyzed for TCPH, TPH diesel and gasoline, BTEX, Solvents, and CAM Metals barium, cadmium, copper, and lead~ A workplan describing how the work will be performed'and a health and 'safety plan must be submitted to this office for approval before the work commences. The workplan must reach this office before March 15, 1993. If you have any questions, please contact me at (805) 861-3636. Sincerely, Steve McCalley, Director By~io"mrDarlfi'ffg, R.E.H.., R.E.A. Hazardous Materials Specialist III Hazardous Materials Program FD:cas ~flora\totco.ltr UIC PAPERWORK CHECKLIST 1. SHALLOW INJECTION WELL CHECKLIST and ~ ~e [ ] disk UNDERGROUND INJECTION CONTROL PROGRAM~Ie,~[ ] file O~ re~e;~ o~ [ ] RWQCB 2. COMPLAINT FORM [ ~" file 3. TRACKING NUMBER [ ~'~'fite 4. PROPERTY RECORD and APN MAP [ ]. file 5. WORK ORDER LOG SHEET (1 per RP) [~J~ accounting ['~/ file 6. PROP 65 REPORT (if needed) [ ~__Janet 7. LOG ONTO COMPUTER [ ~ 8. NOTIFICATION LETTER (DRAFT) [ ] 9. NOTIFICATION LETTER (FINAL) [ ] owner [ ] file [ ] cc's ADDITIONAL PARTICIPANTS: " A. In~roduce Yourself and All O~hers (Show Credentials) B. Explainwhyyou are t.~ere, go over t. he No=ice of Inspection. Have them read and sign it C. (Need Legal Info.) Owner' s Name: Address: Phone No. D. Operator' s Name: , Address: ~ ,~// ,d/~/; ~/~U Phone No.: (SWAP BUSINESS CARDS, also ask for business license) E. Paren='Company: ... Ad,tess: Are =Aey a su~sidiary of a coz~ora=ion? Are =Aey in¢or~ora=ed in t. he State?: F. Con=ac= Person: Phone #: A. How Long in Business?: B. Are t.~ey a Member of an Asso=ia=ion?: C. Are t,~ey aware of any Wa=er Supply Well Lace:ion/Ownership D. Si=e History - Years of O¢cupa=ion, Prevxuus Owners and Uses of the Facility: E. Produc:s or Services Offered?: F. Brief Description of any Process, 09era=ion, or Maintenance ~.~a= Produces Was=e: G. Wha= Chemicals are Stored on Site?: H. Ma:erla£ Safety Data Shes=s?: UNDERGROUND ZNJECTZON CONTROL PROGRAM ZNBPECTZON REPORT &qenc¥ Znspecto~ Fac±~ ~n~orma~±on Facility Name Phone Parent Company Address City State Zip Con=ac~ Name and Position DesoripCion of waste sCre-~ Description of injection well Description of activity that may endanger ground wa=er but not related to injection wells or =an~s (e.g. ponds, spills) I~sDection Information Inspection Date N,,~er of Wells Well T~e Auto Service Indus=rial Waste Agricultural Drainage Storm Water Other Status of Wells Active Abandoned Under Construction Other Injectate Sampled(Y/N) Violation Found(Y/N) Follow-Up Needed(Y/N) RCRA Facility(Y/N) Comments LO~TI~ O~ OlSC~OB OR TH~T~gD DISC~Og [DA~ ~O TX~ OE ~O~& O~ D[BC~' ~ l N~E ~D ~D~SS O~ P~ RESPONSIBLE ~OR DISC~GE, l~ ~0~: AREA ~ I SCENE TYPE: OI~INDUS~IAL 04 RU~AGRI.] 01 STATE H~ 05~BLIC STRU~E 09 OTHER NATER NELL 13 02~CO~ERCIAL 05 NILD ~DS J 02 COU~ ~ 06 ~ PRIVATE S~UC~ 10 AIRPORT/~ILY~ 14 OESERT 03~RESIDENTIAL ~ 03 CI~ ~ 07 C~AL/~ATERNAY 11 E~ LOT 15 BRUSH~I 99 OTHER:SPECIFY · 04 PRIVATE ~ 08 DO. TIC NAT~ NEL~ 12 ~/POND 16 OILEIELD SOURCE ,OF RELEASE CIRC~ST~CES OF REL~E CAUSE O~ REL~E 01 OIL R~INERY 01 ~HILE BEING ~NUEA~D 11 DURING CO~AINER 01 EQUIP~ 02 .... ~. ~UPACT~ER 02~ILE IN STO~Gg . OR CONDUIT R~PAIR O~ 03 ~NISC. FIXED FACILX~ 03~DURING NO~ END USE 12 ILLEGAL DISPOSAL 03 .A~ O~ NA~ 04 ..MOTOR VEHICLE 04 WHILE BEING LOADED 96 THR~T~ED REL~SE 04 ACCID~ 05 TRAIN 05 HHILE IN ~SIT ONLY; NO DISC~RGE 05 ILLE~ DISPOSAL 06 AIRC~FT 06 WHILE VEHICLE PARKED 97 REL~SE OR INCIDENT 98~KNO~ 07~PIPELINE 07 DURING VEHICLE ACCID~T HITIGATEO AT TZ~ 99 / OT~R: 08~UNDERGROUND T~K ~08 DURING FIRE/EXPL. OF REPORT 98~NKNONN :09 DURING AIR C~SH 98 UNKNOWN 99 ~OTHER: ~ i0 NHILE AB~DONED 99 'OTHER: LIST THE ONE, ~0 OR THREE MOST SIGNIFI~T $UBST~CES DISC~GED OR THR~TENED TO BE DISC~GED: CH~. N~E/~OR COMPONE~: ~~ ~ CONCENT~TION ~OU~ AT RISK ~OUNT RELEASED ~OIOA~IV~ /~ASTE~G~ [3] [~] CHEH. H~E/~OR CO~ON~: ZHPORTAHT ~DITIOHAL CO~EHTS/DETAILS: (USE REVUE CO.OH R~ACTIVg CO~OSIVE ~ ~IX LIO. C~EH, N~E/~OR COHPON~T: [3] HAZED: . TOXIC __F~BLE [ .P~E .,.SOLID ..... ..... :_:__J___: ............. H~LTH ~D ENVIRONMENTAL CONT~INATION: INDICATE ACTU~ (*A') OR POT~TX~ ('P') FOR APPLX~LE IT~ OI~IR 02~CANAL/WATERMAY INTERNAL USE ONLY: 03~E/POND 05 ,, CROP9 08 LIVESTOCK INVESTX~TxON REFE~ ~S TO: 07 MILDLIPE 08~OODED ~ H~TH RISK ASSE9~ ~KXNG~ 09~DESERT ~0 BRUSHL~D INFO~ION PHON~-IN? ~ N IF YES, DATE 11 .FOODSTUFFS T~ --12~ROUND~AT~ ~ DATE REPORT RECEIVED BY ~TH D~NT 13~NELLING ~ COMPUTER INPUT (CHECK) ~ CL~*S INITI~ 14 H~ DATE OF N~IFI~TION OP H~TH OEFIC~ BOS 99 O~ER: OATS OF IHOTIFI~TION OP WORK ORDER LOG SHEE~ Date: /~/~//~ ~- Wor~ Order #: EM0*~; /~ Tracking #: WO Category: Haz____mats APN:__-~-__-~-__ WO Type: ~--~ Reimb.: Y ~' N RP Code: WORK-ORDER NAME: /j~ ~ Fd~,'~e~ -~c~ ~;~ RESPONSIBLE PARTY (RP) NAME: ~o~0 RP CONTACT: RP ADDRESS: ~ I0 ~e~ ~ RP CITY: ~¢r~i~l~ STATE: C.~ ZIP: ~d~ RP PHONE NOS.: ( ) ( ) INSPECTOR= ~~ ~, ~ ~o~ EXT. PROGRAM: ~MMP-Enf~ HHMP-Permitting DESCRIPTION: /~~ LOCATION: FACILITY NAME: ,,~'~/~ ~ f REPORTING PERSON: P~ONE NO. COMMENTS: KERN CO U NTY OFFICE MEMORAND [ TO : ACCOUNTING DATE FROM : /--( ~ ~ .~ C ~ ~'~ SUBJECT; CLOSURE OF WORK ORDERS WORK ORDER NUMBER ~'.~ ~ WORK ORDER NAME H D~ iz.,,~n~ - .~ .~.~-~'~,~, 5AST DATE WORK ORDER WAS UTILIZED /'~-~-~.L PROGRAM MANAGER KERN COUN-, ¢ ENVIRONMENTAL HEALTH SERVICES L, EPARTMENT SERvicE AND COMPLAINT FORM Date '::;.:.; //~,**'/';* '~? ............................. ,~.-...;:... Tlme;....; ................. ~ ~ervlce Reque;t ~' Complaint CT No.....~,...;~: .............................................................. , ............ ; ........................................... ,_o,.,,o. ............ ....... ....... ........................................................ ,,,, .................................................................................. Ohectlon~ ..... : ........................ ~ ............................................................................................................................................................................................. Reporting ~rson ............................................................................... Address .................................................................................. Phone .....................~ .......... ~o~rty Owner ............................................... ~ ............ Address .......................................................................... ~one ............................. ~ ' ...:..'/ ..,.. I .--~' ,/-' .. /-.: .-~.~ / ,... Reason for Request / ~..v . ~'..'r ~."~.~ .: .. ~- ~;, / . ~,.~*~-. ..* ...-. ~.- .. -...~;. : ...~;.~.::.; ............................................................................... ~ ~r ~ ~ , ~ ~',-'~. -'~ ....... :"';'*-- .... 7 .................................... :' .................. :'; ..................................................................................................................................................... ~ ~ Information .,.,~?, .....;.~ ........... ,- ~ Taken by /// ,~ ' ~ RESULTS OF . . ,/; ; ................................................................................................................................................................................................................................................ ~ Complainant notified of results .......... ~ ....................... Investigated by ................................................................................................................. Dateo...'.'.:.'-~...j~-o~.o..j...o.,';; Environmental Health 580 4113 2029 (Rev.