HomeMy WebLinkAboutUST 12/18/1997I L ItORIZ~I'~I I~~ROI~II~II~I~AI. I1~1¢
I ~ Specialists in Site Assessment, Remedial Testing, Design and Operation
I
I TANK CLOSURE REPORT
I a~
Beacon Station No. 596
3225 Pierce Road
I Bakersfield, California
for
I Mr. Kenneth R. Earnest
i Ultramar Inc.
525 West Third Street
Hanford, California 93230
I by
Horizon Environmental Inc.
I Report No. 1596.15
,
I Senior Project Manager
i REA-00868
Re~steYred'Geolo~ist
I C.E.G. No. 1935
I
December 18, 1997
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5011 Golden Foothill Parkway, Suite 7 · El Dorado Hills,CA 95762 * (916) 939-2170 · FAX (916) 939-2172
I P.O. Box 5283 * Bakersfield, CA 93388 · (805) 589-8389 · FAX (805) 589-1456
Beacon Station 596 December 18, 1997
Bakersfield. California Tank Closure Report
CONTENTS
INTRODUCTION .................................................................................................................. 1
SITE DESCRIPTION AND BACKGROUND ...................................................................... 2
FIELD WORK ........................................................................................................................ 3
RESULTS ............................................................................................................................... 6
DISTR/BUTION .................................................................................................................... 7
LIMITATIONS 7
REFERENCES ....................................................................................................................... 7
FIGURES
Figure 1: Site Vicinity Map
Figure 2: Site Plan
Figure 3: UST Excavation Soil Sampling Plan
Figure 4: Overexcavation Soil Sampling Plan
I TABLES
Table 1: Soil Sample Analytical Data
I
I APPENDICES
i Appendix A: Horizon Environmental Inc. Field Methods and Procedures
Appendix B: Monitoring Well Destruction Permits
Appendix C: Laboratory Analytical and Chain-of-Custody Reports: Soil Samples -
I Gasoline Dispenser Island & New Underground Storage Tank Cavity
Appendix D: Laboratory Analytical and Chain-of-Custody Reports: Soil Samples -
Former Underground Storage Tanks & Overexcavation
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596-15.tcr ii HORIZON ENVIRONMENTAL INC.
Specialists in Site Assessment, Remedial Testing, Design and Operation
TANK CLOSURE REPORT
at
Beacon Station No. 596
3225 Pierce Road
Bakersfield, Califomia
for
Ultramar Inc.
INTRODUCTION
At the request of Ultramar Inc. (Ultramar), Horizon Environmental Inc. (Horizon) conducted
soil sampling activities following excavation and removal of underground storage tanks
(USTs) and associated product pipelines at the above-referenced site (Figure 1). In addition,
Horizon collected samples during site overexcavation activities and at the limits of the
remedial overexcavation. Additional sampling was conducted in the gasoline dispenser
island area and in the excavation for the new gasoline USTs.
The work was performed as described in Horizon's Soil Management plan. dated February 1,
1997 and previously submitted for this site. Tasks included collecting native soil samples
from the floor and sidewalls of the former UST cavities, product dispenser trenches and
piping trenches, and collecting characterization samples from excavated, stockpiled soils.
Former facilities and the location of soil samples collected are depicted on the Site Plan,
Figure 2. The results of the investigation have been compiled in this Tank Closure Report.
I
5011 Golden Foothill Parkway, Suite 7 · El Dorado Hills,CA 95762 · (916) 939-2170 · FAX (916) 939-2172
P.O. Box 5283 ° Bakersfield, CA 93388 ° (805) 589-8389 ° FAX (805) 589-1456
Beacon Station 596 December 18, 1997
Bakersfield, California Tank Closure Repoi~t
SITE DESCRIPTION AND BACKGROUND
Beacon Station No. 596 is an operating gasoline and diesel fueling station and truck stop
located on the southwest comer of the intersection of Pierce Road and Gilmore Street at
3225 Pierce Road in Bakersfield, California. The site is at an elevation of approximately
405 feet above mean sea level. Bakersfield is located in Kern County in the southern portion
of the Great Valley geomorphic province of California. The Kern River is located
approximately one mile southeast of the site. Oil and gas is produced on the property west
of Highway 99, which is adjacent to the site on the west.
Prior to the UST removal/replacements and the remedial excavation, the site consisted of a
station building, a truck scale, two 10,000-gallon capacity unleaded gasoline
USTs,
two
15,000-gallon capacity diesel USTs, seven dispenser islands, a canopy, a lubrication pit with
an aboveground oil tank. Location of the USTs,
office
and
storage,
a
truck
wash
and
dispenser islands, and other pertinent site features prior to removal or remodeling are
on the Site Plan (Figure 2). During the period of overexcavation activities, all of
indicated
the surface features/structures were removed, except for the station building, truck scale, and
truck wash.
Previous environmental work at the site was performed by Horizon and others. In 1992,
SSB Environmental Consultants, Inc. (SSB) conducted a preliminary subsurface
investigation consisting of soil borings B-1 through B-8. In February 1993, CET
Environmental Services, Inc. (CET) conducted a subsurface investigation consisting of soil
borings B-9 through B-13, installing vadose-zone wells V-1 through V-4, and conducting an
in-situ bioremediation feasibility study. In August 1993, Remediation Testing and Design
(RTD) conducted a soil gas screening and limited vacuum extraction test at the site. In
August 1993, groundwater monitoring wells MW-l, MW-2 and MW-3 were installed by
Acton-Mickelson-van Dam, Inc (AMvD) at the site November 12, 1993. In March 1995,
Horizon installed groundwater monitoring wells MW-4 and MW-5 (Horizon, May 11,
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1596-15.tcr 2 HORIZON ENVIRONMENTAL INC.
I
Beacon Station 596 December 18, 1997
Bakersfield. California Tank Closure Rep0~ t
1995). In August 1996, Horizon installed groundwater recovery well RW-1, air sparge well
AS-I, and vapor extraction well V-5, and conducted a groundwater pumping test and a
combined air sparging and soil vapor extraction test. Subsurface soils beneath the site
consist primarily of fine-grained sand. Groundwater was present beneath the site at a depth
of approximately 20 feet in July 1997.
FIELD WORK
Prior to beginning the field work, a site-specific health & safety plan was prepared. All
Horizon activities were completed in compliance with the State of California Water
Resources Control Board's Leaking Underground Fuel Tanks (LUFT) Manual, and Kern
County Environmental Health Services Department (KCEHSD) guidelines. All Horizon
field work followed the Horizon Environmental Inc. Field Methods and Procedures
(Appendix A). Horizon obtained a permit for well destruction in anticipation of destroying a
vapor well(s) during UST removal/replacement (Appendix B). All UST removal and
excavation work was performed by JNS Construction (JNS) of Clovis, Califomia.
Soil Sampling For Gasoline Dispensers and Excavation Cavity_ For Replacement UST:;
On February 25, 1997, Horizon personnel collected soil samples fi.om depths of 2 feet and 6
feet beneath surface grade (bsg) at the unleaded gasoline dispenser islands and associated
product lines in the area east of the station building as shown on the UST Excavation Soil
Sampling Plan (Figure 3). Mr. Steve Underwood of the City of Bakersfield Fire Department
was onsite to observe the soil sampling activities. The purpose of this sampling work was to
assess the subsurface soils for hydrocarbon impact.
On February 26, the cavity for the replacement gasoline USTs was excavated. The
excavated soils were separated into "clean" and "impacted" stockpiles based on field
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1596-15.tcr 3 HORIZON ENVIRONMENTAL INC.
I
Beacon Station 596 December 18, 1997
Bakersfield. California Tank Clo~ure Repo~ [
I screening with a portable organic vapor meter (OVM). Characterization soil samples were
collected from both stockpiles for compositing by the laboratory.
!
All the soil samples were prepared and chilled for transport under chain-of-custody (COC)
I protocol on the sampling date-of-collection and sent to West Analytical Laboratory (WEST),
i a State-certified laboratory in Davis, California (Certificate No. 1346). Composited soil
samples from beneath the dispenser islands and from the soils excavated from the new UST
i cavity were analyzed for total petroleum hydrocarbons as gasoline (TPHg), the gasoline'
constituents benzene, toluene, ethylbenzene and xylenes (BTEX) and methyl tertiary-butyl
I ether (MTBE) by modified Environmental Protection Agency (EPA) Method 8015/8020.
The laboratory results are summarized in Table 1. Copies of the laboratory and COC reports
I are included in Appendix C. Approximately 425 cubic yards (c.y.) of soil with hydrocarbon
concentrations below laboratory reporting limits were stockpiled for later use as backfill.
I
Removal of USTs and Sampling Activities
Ion Figure 3, USTs T-1 and T-2, each with a 15,000-gallon capacity, and USTs
As
depicted
T-3 and T-4, each with a 10,000-gallon capacity, all of single-walled, steel construction,
I were located in the west-central portion of the site, between the station building and the
truck wash. USTs T-1 and T-2 were reportedly used to store diesel fuel and USTs T-3 and
I T-4 were reportedly used to store unleaded gasoline for retail sale. On July 17, 1997, Mr.
Steve Underwood of the City of Bakersfield Fire Department was onsite with Horizon
I personnel to observe UST removal and transport, and excavation soil sampling activities.
I Upon removal by JNS, all of the USTs appeared to be in good condition with no noticeable
i holes. USTs T-1 and T-2 had minimal rusting, UST T-3 had moderate to heavy rusting and
some pitting, and UST T-4 had moderate rusting and no pitting. The USTs were manifested
I and transported offsite by Erickson Trucking for disposal. Soil samples were collected by
Horizon personnel from native soil at depths of approximately 2 feet and 6 feet below the
I ends of all four USTs, from the middle of the diesel USTs T-1 and from
T-2,
beneath
the
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1596-15.tcr 4 HORIZON ENVIRONMENTAL INC.
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I Beacon Station 596 December 18, 1997
Bakersfield. California ' Tank Closure Report
I product lines at approximately 20 linear feet intervals, and from beneath the three diesel fuel
dispensers directly west of the station building. Horizon personnel collected
I characterization samples from the stockpiled soils for laboratory compositing and analyses.
I All the soil samples were prepared and chilled for transport under COC protocol on the
sampling date-of-collection and sent to Kiff Analytical (Kiff)), a State-certified laboratory in
I Davis, California (Certificate No. 2236). The requested analyses included: TPHg, BTEX
and MTBE by modified EPA Methods 8015/8020. Selected samples were additionally
I analyzed for total petroleum hydrocarbons as diesel (TPHd) and total petroleum
i hydrocarbons as motor oil (TPHmo). The laboratory results are summarized in Table 1.
Copies of the laboratory and COC reports are included in Appendix D.
I
Overexeavation and Sampling Activities
I Overexcavation activities and backfilling were conducted between July 17 and August 15,
1997 as shown on the Overexcavation Soil Sampling Plan (Figure 4). Excavation activities
I were guided by field screening of the soils'with an OVM and overnight results of
analytical
sampling. The overexcavation was extended down to the water table, which was measured
I by Horizon personnel, to be at 18 feet
approximately
bsg
in
July
1
997.
Overexcavated soil was stockpiled onsite. Soil samples were collected from each stockpile
and analyzed to evaluate hydrocarbon content. Four discrete soil samples were collected for
every 100 c.y. of excavated soil using procedures described in Appendix A. Each group of
four discrete samples was composited by the laboratory into one sample which represented
100 cy, as required by the disposal facility. After receiving analytical results, the stockpiled
soils were transported by Dillard Trucking (Dillard) of Byron, California, to McKittrick
Waste Disposal (McKittrick) facility in McKittrick, California for disposal.
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1596-15.tcr 5 HORIZON ENVIRONMENTAL INC.
I
I Beacon Station 596 December 18, 1997
Bakersfield. California Tank Closure Report
I RESULTS
I The final limits of the overexcavation are shown on Figure 4. The excavation was
approximately 75 feet wide (east to west) by 140 feet long (north to south) and averaged
I approximately 22 feet deep. The calculated excavation volume was approximately 8,500
c.y. McKittrick records indicate 10,805 tons of soil was transported from the site to their
I facility.
I During the course of the overexcavation, air sparge wells, vapor extraction wells, recovery
i well RW-1, and groundwater monitoring well MW-3 were destroyed. Also removed were
the diesel fuel dispensers and islands, the lubrication pit, and the canopy. The cavity for the
I replacement diesel UST was excavated east of and parallel to the former diesel UST (see
Figure 4).
I
Overexcavation activities in the northwest comer of the unleaded dispenser islands was
I limited due to the proximity of the station building. Residual TPHg was indicated in the soil
sample collected at 17 feet bsg (S-GPLI-17'). Soil samples collected at the limits of the
I UST/diesel dispenser overexcavation were all below laboratory reporting limits, except for
an area along the west wall (TPHd and MTBE indicated by sample DTP-15-W-MP), and an
I area along the east wall (TPHg, TPHd, MTBE, and a trace of BTEX indicated in sample
GTP-15-E-MP). The overexcavation in these two areas were limited by the property
I boundary to the west, and the truck scales and station building to the east.
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1596-15.tcr 6 HORIZON ENVIRONMENTAL INC.
I
I Beacon Station 596 December 18, 1997
Bakersfield. California Tank Closure Report
I DISTRIBUTION
I We recommend a copy of this report be forwarded to:
I Mr. Steve Underwood Mr. John Noonan
Bakersfield City Fire Department CWQCB-CVR
Hazardous Materials Division 3614 East Ashlan Avenue
I 1715 Chester Avenue Fresno, California 93726
Bakersfield, California 93301
,1
LIMITATIONS
I
This report was prepared in accordance with the methods and procedures in the attached
I field methods and generally accepted standards of environmental geological practice in
i California at the time of the investigation. The investigation was conducted solely for the
purpose of evaluating environmental conditions of the soil and groundwater with respect to
I gasoline and diesel related hydrocarbons at the site. No soil engineering or geotechnical
references are implied or should be inferred. Evaluation of the geological conditions at the
I site for the purpose of this investigation is made from a limited number of observation
points. Subsurface conditions may vary away from the available data points. This report is
I the property of Horizon Environmental Inc. and Ultramar Inc. for their use and distribution.
I
REFERENCES
I
SSB Environmental Consultants, Inc., 1992, Prelirnina~_ Subsurface Investigation of the
I Soil Quality at Beacon Truck Stop Number 596, 3225 Pierce Road, Bakersfield,
California (File No. SSB 91-1054-02).
I Acton-Mickelson-van Dam, Inc., November 12, 1993, Soil and Grot~ndwater Invest~ation,
Beacon Station No. 596.
I Acton-Mickelson-van Dam, Inc., November 21, 1994, Subsurface Investigation Work Plan,
Beacon Station No. 596.
I
1596-15.tcr 7 HORIZON ENVIRONMENTAL INC.
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I Beacon Station 596 December 18, 1997
Bakersfield. California ' Tank Closure Report
I CET Environmental Services, Inc., 1993, Site Assessment Report For Ultramar's Beacon
Station No. 596, 3225 Pierce Road, Bakersfield, California (Project No. 2042).
I Remediation Testing and Design, September 28, 1993, Soil Gas Screening and Vacuum
Extraction Feasibili~_ Testing at Beacon Truck Stop #596, 3225 Pierce Road,
i Bakersfield, California
Horizon Inc., May 11, 1995, Report of Additional Subsurface Investigation at Beacon
I Station No. 596, 3225 Pierce Road, Bakersfield, California
E1 Dorado Environmental, Inc., May 30, 1997. Second Quarter 1997 Ground Water
I Monitoring Report, Beacon Station No. 596, 3225 Pierce Road, Bakersfield,
California.
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1596-15.tcr 8 HORIZON ENVIRONMENTAL INC.
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I Figures
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I X
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i NORTH
Source: U.S.G.S. 7-1/2 Minute Topographic Map
Oildale, California ~
Photorevised 1968
I 0 2,000 4,000
Scale In Feet
I I ~. HORIZON ENVIRONMENTAL INC,~ ''I'II'I-
SITE VICINITY MAP FlCURE
I I Project Numben 1.596.01 I ~.. B~. D. Nston BEACON STATION NO. 596
I Prepared ~. 0. &=r~er I Rte: 4/S5 3225 PIERCE ROAD 1
I Reviewed ~ I ReviIed Dete: BAKERSFIELD, CALIFORNIA
I
Of Sewer Maintenance
Hole Cover ~,, ._
Former
I Generator Shed Diesel
Former ! And Trash Bin Truck
Lube -~ J Dispenser Scale IIW-1
I
Storage ~ :..~ ......
~ ~ ~ ~ ~ ~ I ~ Unleaded I
~ ~ .... ~ ~ ~ I ~Dispenser I
~ ~ F--.~ .... ~ '" I
Building I
~ New Tank I
'
Lube ~ .L II ~ Cavity
Office
MW-4
Telephone/Electricol
Line
~ ~ B~.~ ' ~' Water ~ne ', I
~ ~ -- ~ /wa former ''
I Diesel U~s
~ ~ Truck Umit Of ~.~ I
~ Wash Overexcavation
< ~ . uw~ i
0 I MW-8~ Groundwater Uonitoring Well i NORTH
i
~ V-8~ Destroyed Vapor Extraction Well i
~-1~ Destroyed Recove~ Well
V~ Destroyed Vapor Extraction Well
0 50 1 O0
~-2~ Destroyed Groundwater Monitoring Well
Sours: ngum a~m~ From Omwlng Prodded Approximate Scale In Feet
~ 81TE P~N
~ B~OON ~A~ON NO. 596 2
~ QILAfORE
Generator t l~
Shed I ['~~_~ V ~
,,,,,, ,- , '
Dispenser [ I
' Gosoline ~roduct
Unleaded I
If ....... ; Dispenser I
II ,e ,7 8,~ I Station 2~ Islonds ~s
~ ~ .... ~ ...... ~ Building : : I
Diesel ~ ~ ~t ...................... ~
~ Product~ ........ ~ ::
I
.
.' Lines 1~ ~( ....... %% -- I ~: i Il ~ I
I .--~ ~'~' ....... ~.~ ~ '
I
~ ~ i0
' I 1~ :::::::::::::::::::::::: ~ ..................................
I 7 10~ ....................... ~ ~ I
' J~6 ~ 9) m ~ Gasoline USTs k mw-~ New Gasoline
~ ~ ~ i~ ~ ~1 ~ ~ UST Cavity I
I ~ . L._..~.....~ t .... Unleaded
~ ~ :, ~ ~-~ Product J
. · / Limits Ot
~ ~ 11 UST Excavation Lines
I
USTs New Gasoline UST I
Cavity Soil
[ lruck- ~ Approximote ~rope~7
7 i I
EXP~NATION;
~-~ Groundwater Monitoring Well
18 · Soil Sample
I: S-GPL1-2 6: T1-2-M 12: ~-2-E 17:P~-2
S-GPL1-6 T1-6-M ~-6-E P~-6
S-GPLI-17 7: T1-2-N 13: ~-2-~ P~-15
2:S-GP~-2 T1-6-N ~-6-W 18:PLC-2
3:S-GP~-2 T1-6-S T4-6-E PLC-15
S-GP~-6 9: T2-2-M 15: T4-2-W 19: SP-O226-A thru D
4:S-GPL4-2 T2-6-M T4-6-W 20: SP-O226-E thru X
S-GPL4-6 10: ~-2-N 16:P~-2
S-GPL4-11 ~-6-N ~-6
s= s-o.~-~ ~1= ~-~-s ~-~s 0 50 100
S-GP~-6 ~-6-S
Source: Rgure M~ifi~ From Drawing Pro~ded
~ u~.r. Approximate Scale In Feet
x~c. UST EXCAVATION SOIL
~O~IZO~
-- SAMPLING PLAN
Proj~t Numben 1596.15 ~awn ~ D. Neton B~CON STATION NO. 596 3
Prepar~ ~: G. ~er ~te: 12/e7 3225 PIERCE ROAD
R~e~ ~: R~s~ ~te: BAKERSFIELD, CALIFORNIA
Oenerato~
Trash
~1~ i / ~1 II Dispenser
J I I Islands
I ' I ........ *
I I I '' , , 0
~ ~ I ~ ~ DTP-15-SE ~ Replacement
~ ~ ; j ~ .~-~ Diesel U~
~ ~ ~-~OL-8-S Dmits Of Remedial
~ ~ Overexaavation
lruck ~ ......
NORTH
M~-$~ Groundwoter ~onitoring Well
DTP-15-SE, Soil Sample
0 50 1 O0
s,ur~: H~m ~l~ From ~m~l.~ p~,~ Approximate Soale In Feet
~ Ul~m,t.
~ ~n ~**~.~ ~ 8~C0~ SI~O~ ~0.
Prepar~ ~ O. ~r J ~: 12/97 3225 PIERCE ROAD
R~ewed ~ J R~ ~: BAKERSRE~, CALIFORNIA
Tables
Beacon Station No. 596 December 18, 1997
3225 Pierce Road. Bakersfield. California Tank Closure Report
Table 1
TPH d Ethyl
Sample No. Sampled TPH g [TPH mo] NITBE Benzene Toluene benzene Xylenes
(ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm)
Gasoline·Product~ ~ ~Lines ~: . ~.~ · · ~'~.'.. ... ' ~ .~'~ .. ~
S-GPLI-2' 02/25/97 12,000 NA 560 220 1,700 460 2,200
S-GPLI-6' 02/25/97 14,000 NA 300 290 2,000 550 2,500
S-GPLI-17' 02/26/97 5,200 NA 400 41 710 190 880
S-GPL2-2' 02/25/97 310 NA <0.50 <0.050 0.96 0.57 3.6
S-GPL2-6' 02/25/97 <1.0 NA 0.070 <0.0050 0.016 0.014 0.11
S-GPL3-2' 02/25/97 <1.0 NA <0.050 <0.0050 0.0064 <0.0050 0.015
S-GPL3-6' 02/25/97 <1.0 NA <0.050 <0.0050 <0.0050 <0.0050 0.011
S-GPL4-2' 02/25/97 2,600 NA <5.0 1.3 110 62 450
S-GPL4-6' 02/25/97 1,600 NA 41 14 74 29 150
S-GPL4-11' 02/26/97 11 NA 12 <0.050 0.56 0.069 0.80
S-GPL5-2' 02/25/97 41 NA 5.5 <0.050 1.5 0.82 7.9
S-GPL5-6' 02/25/97 2.7 NA 4.9 <0.0050 0.056 0.013 0.18
· Removal~ of GaSOline USTC: T-3 and T-4 ..'!~:~?.~"..!~./iii:~ '':~' ? i ~. ~ ~" ~ · i ....
T3-2-E 07/17/97 <1.0 NA <0.050 <0.0050 <0.0050 <0.0050 <0.0050
T3-6-E 07/17/97 56 NA <5.0 <0.50 <0.50 <0.50 <0.50
T3-2-W 07/17/97 <1.0 NA 0.28 <0.0050 <0.0050 <0.0050 <0.0050
T3-6-W 07/17/97 280 NA <10 <1.0 <1.0 <1.0 1.4
T4-2-E 07/17/97 <1.0 NA <0.20 <0.020 <0.020 <0.020 <0.020
T4-6-E 07/17/97 330 NA <20 <2.0 <2.0 <2.0 <2.0
T4-2-W 07/17/97 520 NA <20 <2.0 <2.0 2.6 10
T4-6-W 07/17/97 67 NA <5.0 <0.50 <0.50 <0.50 1.4
GTP-SW15'-N 07/18/97 430 NA <10 <1.0 <1.0 7.6 22
GTP-SWI5'-S 07/18/97 <1.0 NA 0.33 <0.0050 <0.0050 <0.0050 <0.0050
GTP-SWl5'-W 07/18/97 4.5 NA 1.6 <0.050 <0.050 <0.050 <0.050
GTP-SW15'-E 07/18/97 560 NA <20 <2.0 <2.0 2.1 9.8
GTP-SW15'-E 07/22/97 <1.0 NA <0.050 <0.0050 <0.0050 <0.0050 <0.0050
GTP-15'-E-MP 07/25/97 5.6 19 0.92 <0.020 0.13 0.10 0.82
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1596-15.tcr I HORIZON ENVIRONMENTAL INC.
I
I Beacon Station No. 596 December 18, 1997
3225 Pierce Road. Bakersfield. CalifornTfi Tank Closure Report
I Table 1
I TPH d Ethyl
Sample No. Sampled TPH g [TPH mo] MTBE Benzene Toluene benzene Xylenes
(ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm)
RemOval of Diesel USTs: T-l:and T.2 ::'~. ':": ' "
T1-2-M 07/17/97 270 3,400 < 10 < 1.0 < 1.0 < 1.0 <1.0
TI-6-M 07/17/97 670 5,300 <20 <2.0 <2.0 <2.0 2.1
T1-2-N 07/17/97 480 5,400 <10 <I.0 <1.0 1.7 1.5
T1-6-N 07/17/9q 630 9,900 <10 <1.0 <1.0 1.9 3.5
T1-2-S 07/17/97 420 7,000 <20 <2.0 <2.0 <2.0 <2.0
TI-6-S 07/17/97 290 4,200 <20 <2.0 <2.0 <2.0 <2.0
T2-2-M 07/17/97 380 4,500 <10 <1.0 <1.0 1.6 <1.0
T2-6-M 07/17/97 120 6,400 <10 <1.0 <1.0 <1.0 <1.0
T2-2-N 07/17/97 100 2,000 < 10 < 1.0 < 1.0 < 1.0 < 1.0
T2-6-N 07/17/97 250 7,600 <20 <2.0 <2.0 <2.0 <2.0
T2-6-S 07/17/97 210 5,300 <20 <2.0 <2.0 <2.0 <2.0
T2-2-S 07/17/97 240 7,600 <20 <2.0 <2.0 <2.0 <2.0
DTP-SWI5'-W 07/19/97 4.6 640 <0.50 <0.050 <0.050 <0.050 <0.050
DTP-I 5'-W-MP 07/25/97 <1.0 34 0.47 <0.0050 <0.0050 <0.0050 0.0051
DTP-SW-15 07/31/97 <1.0 <1.0[<10] <0.050 <0.0050 <0.0050 <0.0050 <0.0050
DTP-15-SE 07/31/97 <1.0 <1.0[<10] <0.050 <0.0050 <0.0050 <0.0050 <0.0050
CL-8-S 08/01/97 <1.0 <1.0 <0.050 <0.0050 <0.0050 <0.0050 <0.0050
~DieselPr°d:UCtLines ~i,,".::,i~:i:~:~::i i i'-'.'... .. ' ,
PLA-2' 07/22/97 540 19,000 <20 <5.0 <5.0 <5.0 13
PLA-6' 07/22/97 280 11,000 <20 <2.0 <2.0 <2.0 6.8
PLA-15' 07/22/97 520 6,200 <20 <2.0 <2.0 <2.0 6.2
PLB-2' 07/22/97 600 16,000 <20 <5.0 <5.0 <5.0 20
PLB-6' 07/22/97 810 34,000 <20 <2.0 7.2 8.2 44
PLB-I 5' 07/22/97 810 7,800 <20 <2.0 <2.0 3.3 9.9
PLB2-2' 07/22/97 1.3 28 <0.50 <0.050 <0.050 <0.050 0.084
PLB2-6' 07/22/97 830 5,700 < 10 < 1.0 1.0 10 68
PLC-2' 07/22/97 2,400 38,000 <20 <2.0 2.3 14 10
PLC-6' 07/22/97 1,600 21,000 <20 <2.0 <2.0 6.1 17
PLC-15' 07/22/97 770 5,300 <20 <2.0 <2.0 <2.0 3.6
1596-15.tcr II HORIZON ENVIRONMENTAL INC.
I
Beacon Station No. 596 ~ December 18, 1997
3225 Pierce Road. Bakersfield. Caliform'~'~ Tank Closure Report
Table 1
TPH d Ethyl
Sample No. Sampled TPH g [TPH mol MTBE Benzene Toluene benzene Xylenes
(ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm)
LP1-6 07/22/97 <1.0 1.8 [<10] <0.050 0.0050 0.0050 0.0050 0.0050
DI- 15'-NE 07/24/97 <0.50 <1.0 0.31 <0.0050 <0.0050 <0.0050 <0.0050
D.I.-15'-NE 07/28/97 <0.50 <1.0 <0.050 <0.0050 <0.0050 <0.0050 <0.0050
D.I.-15'-NW 07/28/97 <0.50 <1.0 <0.050 <0.0050 <0.0050 <0.0050 <0.0050
DI-15'-NMP 07/29/97 <1.0 <1.0 <0.050 <0.0050 <0.0050 <0.0050 <0.0050
S-0905-PL2 09/05/97 <1.0 NA <0.0050 <0.0050 <0.0050 <0.0050 <0.0050
S-0905-PL6 09/05/97 <1.0 NA <0.0050 <0.0050 <0.0050 <0.0050 <0.0050
S-0905-PL6 09/05/97 <1.0 NA <0.0050 <0.0050 <0.0050 <0.0050 <0.0050
SP-0226-A,B,C,D 02/26/97 2,700 NA 220 13 360 120 660
SP-0226-E,F,G,H 02/26/97 4.9 NA 0.80 0.0068 0.21 0.15 1.0
SP-0226-I,J,K,L 02/26/97 <1.0 NA <0.050 <0.0050 <0.0050 <0.0050 0.010
SP-0226-M,N,O,P 02/26/97 <1.0 NA 0.33 <0.0050 0.043 0.012 0.079
SP-0226-Q,R,S,T 02/26/97 13 NA 1.9 <0.050 0.40 0.17 1.3
SP-0226-U,V,W,X 02/26/97 < 1.0 NA 0.12 <0.0050 0.016 0.0081 0.077
SP1 A,B,C,D 07/17/97 210 5,200 <20 <2.0 <2.0 <2.0 3.5
SP1 E,F,G,H 07/17/97 180 6,000 <20 <2.0 <2.0 <2.0 <2.0
SP1 I,J,K,L 07/17/97 500 5,900 <20 <2.0 <2.0 <2.0 19
SP1 M,N,O,P 07/17/97 670 8,000 <20 <2.0 <2.0 <2.0 3.5
SP2 A,B,C,D 07/17/97 680 NA <20 <2.0 <2.0 <2.0 24
SP2 E,F,G,H 07/17/97 320 NA <20 <2.0 <2.0 <2.0 3.6
SP2-I,J,K,L 07/17/97 120 NA <10 <1.0 <1.0 <1.0 <1.0
SP1-A,B,C,D 07/19/97 200 6,200 <20 <2.0 <2.0 <2.0 <2.0
GSP-A,B,C,D 07/22/97 1,400 NA <20 <2.0 2.11 16 81
GSP-A,B,C,D 07/23/97 1,100 NA <20 <2.0 7.3 17 140
GSP-E,F,G,H 07/23/97 640 NA <20 <2.0 <2.0 5.9 39
GSP-I,J,K,L 07/23/97 1,100 NA <20 <2.0 9.5 22 150
GSP-A,B,C,D 08/04/97 <1.0 22 <0.050 <0.0050 <0.0050 <0.0050 <0.0050
GSP-E,F,G,H 08/04/97 <1.0 35 <0.050 <0.0050 <0.0050 <0.0050 <0.0050
1596-15.tcr III HORIZON ENVIRONMENTAL INC.
I
I Beacon Station No. 596 December 18, 1997
3225 Pierce Road, Bakersfield, California Tank Closure Repo~ I
I Table 1
I TPH d
Sample No. Sampled TPH g [TPH mo] MTBE Benzene Toluene Ethyl Xylenes
benzene
(ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm)
GSP-I,J,K,L 08/04/97 <1.0 84 <0.050 <0.0050 <0.0050 <0.0050 <0.0050
GSP-M,N,O,P 08/04/97 <1.0 190 <0.050 <0.0050 <0.0050 <0.0050 <0.0050
GSP-Q,R,S,T 08/04/97 <1.0 <0.0050 <0.050 <0.0050 <0.0050 <0.0050 <0.0050
S/°ckpiledS°il: ~ Overex~avation of Diesel USTsi.~'.i:!'= "? :::': .::~ :'::.~.:': :.'i.::~ .' :'.'
DSP-A,B,C,D 07/22/97 450 2,100 <20 <2.0 <2.0 <2.0 <2.0
DSP-E,F,G,H 07/22/97 390 2,700 <20 <2.0 <2.0 <2.0 <2.0
DSP-I,J,K,L 07/22/97 220 1,600 <20 <2.0 <2.0 <2.0 <2.0
DSP-M,N,O,P 07/22/97 16 1,300[<500] <5.0 <0.50 <0.50 <0.50 <0.50
DSP-A,B,C,D 07/23/97 130 3,300 <20 <2.0 <2.0 <2.0 <2.0
DSP-E,F,G,H 07/23/97 100 3,100 <20 <2.0 <2.0 <2.0 <2.0
DSP-I,J,K,L 07/23/97 47 980 <20 <2.0 <2.0 <2.0 <2.0
DSP-M,N,O,P 07/23/97 64 1,400 <20 <2.0 <2.0 <2.0 <2.0
DSP-Q,R,S,T 07/23/97 67 1,800 <20 <2.0 <2.0 <2.0 <2.0
DSP-A,B,C,D 07/24/97 1,400 3,200 <20 <2.0 14 30 220
DSP-E,F,G,H 07/24/97 380 1,600 <10 <1.0 3.4 5.2 32
DSP-I,J,K,L 07/24/97 700 1,700 < 10 < 1.0 6.0 14 92
DSP-M,N,O,P 07/24/97 880 4,500 <10 <1.0 9.7 18 120
DSP-Q,R,S,T 07/24/97 630 2,800 < 10 < 1.0 4.3 12 82
DSP-U,V,W,X 07/24/97 910 4,100 < 10 < 1.0 8.4 18 120
CSP-A,B,C,D 07/25/97 <1.0 93 <0.050 <0.0050 <0.0050 <0.0050 <0.0050
CSP-E,F,G,H 07/25/97 <1.0 170 <0.050 <0.0050 <0.0050 <0.0050 <0.0050
CSP-I,J,K,L 07/25/97 <1.0 77 <0.050 <0.0050 <0.0050 <0.0050 <0.0050
CSP-M,N,O,P 07/25/97 10 980 <0.20 <0.020 <0.020 0.024 0.051
CSP-Q,R,S,T 07/25/97 <1.0 200 <0.050 <0.0050 <0.0050 <0.0050 <0.0050
DTP-A,B,C,D 07/28/97 390 7,000 <20 <2.0 2.3 5.1 32
DTP-E,F,G,H 07/28/97 68 3,100 <0.50 <0.050 0.11 0.14 1.4
DTP-I,J,K,L 07/28/97 13 510 <0.20 <0.020 0.027 0.080 0.17
DTP-M,N,O,P 07/28/97 260 4,100 <2.0 <0.20 1.7 3.5 22
DTP-Q,R,S,T 07/28/97 350 14,000 <2.0 0.21 2.5 5.0 25
DTP-U,V,W,X 07/28/97 140 6,600 <2.0 <0.20 0.69 1.0 4.7
I1596-15.tcr IV HORIZON ENVIRONMENTAL INC.
Beacon Station No. 596 December 18, 1997
3225 Pierce Road. Bakersfield. California Tank Closure Report
Table 1
TPH d Ethyl
Sample No. Sampled TPH g [TPH mol MTBE Benzene Toluene benzene '
Xylenes
(ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm)
DSP-A,B,C,D 07/29/97 81 1,100 <5.0 <0.050 0.20 0.063 1.9
DSP-E,F,G,H 07/29/97 24 790 <2.0 <0.050 <0.050 <0.050 0.52
DSP-I,J,K,L 07/29/97 30 2,900 <2.0 <0.050 <0.050 <0.050 0.72
CSP-A,B,C,D 07/30/97 <0.50 26 <0.050 <0.0050 <0.0050 <0.0050 <0.0050
DSP-A,B,C,D 07/30/97 120 890 [410] <2.0 <0.020 0.36 1.4 9.7
I)SP-E,F,G,H 07/30/97 150 1,1001770] <2.0 <0.020 0.53 1.8 12
DSP-I,J,K,L 07/30/97 390 1,8001810] <20 <0.20 1.9 4.6 33
DSP-A,B,C,D 07/31/97 56 1,700[160] <5.0 <0.050 0.068 0.17 1.4
DSP-E,F,G,H 07/31/97 24 530[<100] <2.0 <0.020 <0.020 0.083 0.13
DSP-I,J,K,L 07/31/97 29 520[<100] <2.0 <0.020 <0.020 0.094 0.042
DSP-A,B,C,D-S 08/01/97 20 240[< 100] <2.0 <0.020 0.22 0.12 0.12
DSP-E,F,G,H-S 08/01/97 53 7701100] <2.0 <0.020 <0.020 0.41 2.6
DSP-I,J,K,L-S 08/01/97 88 7901130] <2.0 <0.020 <0.020 0.90 6.1
DSP-M,N,O,P-S 08/01/97 52 300[<100] <2.0 <0.020 <0.020 0.45 2.8
DSP-Q,R,S,T-S 08/01/97 130 5401120] <2.0 <0.020 0.42 1.6 11
DSP-A,B,C,D-N 08/01/97 54 3,200 <2.0 <2.0 0.30 0.52 4.5
DSP-E,F,G,H-N 08/01/97 35 2,700 <2.0 <2.0 0.27 0.38 2.5
DSP-I,J,K,L-N 08/01/97 28 1,600 <2.0 <2.0 0.24 0.18 1.9
TPHg = total petroleum hydrocarbons as gasoline ppm = parts per million
TPHd = total petroleum hydrocarbons as diesel MTBE = methyl tertiary butyl-ether
TPHmo = total petroleum hydrocarbons as motor oil NA = not analyzed
1596-15.tcr V HORIZON ENVIRONMENTAL INC.
Appendix A
Horizon Environmental Inc.
FIELD METHODS AND PROCEDURES
The following section describes field procedures that will be utilized by Horizon Environmental Inc. (Horizon)
personnel in performance of the tasks involved with this project.
1.0 HEALTH AND SAFETY PLAN
Field work performed by Horizon and subcontractors at the site will be conducted according to guidelines
established in a Site Health and Safety Plan (SHSP). The SHSP is a document that describes the hazards that
may be encountered in the field and specifies protective equipment, work procedures, and emergency
information. A copy of the SHSP will be at the site and available for reference by appropriate parties during
work at the site.
2.0 LOCATING UNDERGROUND UTILITIES
Prior to commencement of work on site, the location of underground utilities will be researched with the
assistance of Underground Service Alert (USA). USA will contact the owners of the various utilities in the
vicinity of the site to have the utility owners mark the locations of their underground utilities. Work associated
with the boring and monitoring well installation will be preceded by manual hand augering to a minimum
depth of 5 feet below grade to avoid contact with underground utilities.
3.0 SOIL EXCAVATION
Permits will be acquired prior to the commencement of work at the site. If a mobile laboratory is not available
to analyze excavated soil, the soil will be evaluated using a field calibrated (using isobutylene) Thermo-
Environmental Instruments Model 580 Organic Vapor Meter (OVM) or equivalent instrument. This
evaluation will be done upon arrival of the soil at the ground surface in the excavator bucket by removing the
top portion of soil from the bucket, and then placing the intake probe of the OVM against the surface of the
soil in the bucket. Field instruments such as the OVM are useful for measuring relative concentrations of
vapor content, but cannot be used to measure levels of hydrocarbons with the accuracy of laboratory analysis.
Samples will be taken from the soil in the bucket by driving laboratory-cleaned brass sleeves into the soil. The
samples will be sealed in the sleeves using Teflon sheets, plastic caps, and plastic zip-lock bags; labeled; and
promptly placed in iced storage. If mobile laboratory or field subjective analyses suggest the presence of
hydrocarbons in the soil, additional excavation and soil sampling will be performed, using similar methods. If
groundwater is encountered in the excavation, groundwater grab samples will be collected from the excavation
using a clean Teflon® bailer. The groundwater samples will be collected as described below under
"Groundwater Grab Samples". The excavation will be backfilled or fenced prior to departure from the site.
4.0 GROUNDWATER GRAB SAMPLES
Groundwater grab samples will be obtained from the excavation using a clean teflon bailer. The samples will
be transferred to appropriate clean glass containers in such a manner as to minimize loss of volatile
constituents, and so that there is no headspace in the sample container and air bubbles are not present in the
samples when they are inverted. If air bubbles are found, resampling will occur. The samples will be
refrigerated and transported promptly to the laboratory.
I
I
I
I
I
I
I
I
I Appendix B
!
!
!
!
!
!
!
!
!
!
!
!
!
07/17/97 THU 14:46 FAX 805 862 8701 K C ENVIRONMENTAL HLTH
· ~ cou~
ENVIRON~AL IiF..4L~ SERVICES DEPAKI/VIENT Appllc~.ion Da~: ~-/~--~7
2700 'M" STREET, SUI'I~ 300 No. of Wells/Borings: __
BAKERSFIELD, CA 93301 Fro No.:
Well No(s).: _
This applicagon is to: [] Construct I-! Modify ~ D~y
T~S~
A~ ~. ~ ~ ~ 3
I. Well sim app~! is m~d b~f~ ~g ~y w~ ml~ ~ wgl ~oa. It ~ ~la~i
~e sm~e at whi~ ~ ~tion ~ ~uk~ ~le~ i~gon Is ~ved 0r ~le~t
3. A ~ ~ ~ ~ ~ent office ~ mquff~d oa ~e m~3~ ~ ~y ~t w~ ~ ~ oomm~ ~ 24 ho~ ~fo~
' ~e' p~meat 0~y-~ ~pl~ .........
~.'~ AI[w61~ c~ted ofPVC'l~ted ~ a c~~ si~ w~m ~~ my ~ m~
~ov~.~tion.is~$~occ~ .,. ,.. , . . . .. :
6. ~y m~s~on.or n~compli~ce wi~ ~d P~it Coa~ti~ or.~c~ will result
W~ 0~" , ' ., . ' '
7. A ~py of ~ De~t of W~ K~ D~l~'s Repo~ ~ weft ~ ~i~s of ~, :~r qu~i~ ~ys~,
builm of wei~ m~ ~ ~bmi~d ~ ~ Ea~o~en~ H~ ~ic~ ~~t wi~ 14 ~ a~ compl~on of~e
'' Wo~ , '
G~E~L CONDffIONS OF THIS PERMIT FOR DESTRUCTION:
!. A well ~on ~li~fi~ m~ ~ ~ wi~ ~s ~p~ if a well. ~ ~ ~ ~ h ~ ~ conj~ction
wi~ a te~ ~Io ~iL
2. ~~ pr~d~ m~t b f°llow~ ~ p= ~-~0. ', · ·
3. Phcem~ of ~e ~ m~'~ wimesscd by a ~n~fiv~ of ~ ~~ T~-fo~-ho~ ~ced noti~ is
~u~ for ~ appo~c
SPEC~L COND~ONS:
~PLICATiON BECOMES A PERMIT WHEN ~PROVED
THIS
07/17/97 THU 14:47 FAX 805 862 8701 K C ENVIRONMENTAL HLTH ,~.uu.,
~ CON~U~ON ~0 ·
III I[ I III I II I l I I I L I I II I
...... ~... ..... ~..,.,. .... .. ....... ,~:...:... ......................................... ... '.~f
S~ ..... & OAUOE
~ OF B~~ ~UO & D~ .
A~ & D~ . ,.
~ P~~. ~OD "" ';' '
I II I IIII ~ I III I I I
FA~~~ ~ s ~~of~ ~~ ~ m~ ~ ~m of~ ~
I I I IIII I I I I I II I
,, , , , ,,, ~~:a;~.~:,.-
DemH O~U~ P~~ ~ '~ ............
!
THIS APPUCATION BECOMES A PERMIT WHEN APPROVED
I
Appendix C
I February 26, 1997
Sample Log 16478
I Gary Barker
Horizon Environmental Inc.
,· ~ 5011 Golden Foothill Pkwy., Suite 7
E1 Dorado Hills, CA 95762
I Subject: Analytical Results for 10 Soil Samples
Identified as: Beacon 596 (Proj.o# 1596.15)
Received: 02/25/97
I
Dear Mr. Barker:
!
Analysis of the sample(s) referenced above has been completed.
iThis report is written to confirm results communicated on
February 26, 1997 and describes procedures used to analyze the
samples.
I Sample(s) were analyzed using the following method(s):
i "BTEX" (EPA Method 8020/Purge-and-Trap)
"TPH as Gasoline" (Modified EPA Method 8015/Purge-and-Trap)
Please refer to the following table(s) for summarized analytical
I results and contact us at 916-753-9500 if have
you
questions
regarding
procedures or results. The chain-of-custody document is enclosed.
I Approved by:
I
Sample Log 16478
MTBE (Methyl-t-butyl ether) By EPA Method 8020/602
From : Beacon 596 (Projo # 1596.15)
Sampled : 02/25/97
Received : 02/25/97
Matrix : Soil
Measured
(MRL) .g/kg Value .g/k~
S-GPL1-2' (50) -560
s-GpL1-6' (50) 300
S-GPL2-2' (.50) <.50
S-GPL2-6' (.050) .070
S-GPL3-2' (.050) <.050
S-GPL3-6' (.050) <.050
S-GPL4-2' (5°0) <5.0
S-GPL4-6' (5°0) 41
S-GPL5-2' (.50) 5.5
S-GPL5-6' (.50) 4.9
Approved BY:
Joel Kiff {
Senior Chemist
I Sample Log 16478
' 16478--01
i Sample: S-GPL1-2'
From : Beacon 596 (Proj. # 1596.15)
Sampled : 02/25/97
I Dilution : 1:1000 QC Batch : 2157E
Matrix : Soil
I Measured
Parameter (MRL) .g/k~ Value
'1 Benzene . (5°0) 220
Toluene ( 5 o 0 ) 1700
Ethylbenzene ( 5.0 ) 460
I Total Xylenes (5.0) 2200
TPH as Gasoline (1000) 12000
i Surrogate Recovery *** Diluted Out
~ ' o ~ ~ ~ ~ .~ ~ ~ime in seconds
I
~te ~Uz~ ~-26-~
Col~ : 0.~ X ~ ~ek Rtx-l~1 ~ni~
I
Sample Log 16478
16478-02
Sample: S-GPL1-6'
From : Beacon 596 (Proj. # 1596.15)
Sampled : 02/25/97
Dilution : 1:1000 QC Batch : 2157E
Matrix : Soil
Measured
Parameter (MRL) ~k~ Value .~k~
(5.0) 290
Benzene
Toluene (5.0) 2000
Ethylbenzene (5.0) 550
Total Xylenes (5.0) 2500
TPH as Gasoline (1000) 14000
Surrogate Recovery *** Diluted Out
time in seconds:
J~l
I Sample Log 16478
16478--03
I Sample: S-GPL2-2'
From : Beacon 596 (Proj. # 1596.15)
Sampled : 02/25/97
I Dilution : 1:10 QC Batch 2157D
:
Matrix : Soil
I Measured
Parameter (MRL) .g/kg Value .g/k~
I (.050) <.050
Benzene
Toluene (.050) .96
Ethylbenzene (.050) .57
ITotal Xylenes (.050) 3.6
TPH as Gasoline (10) 310 *
iSurrogate Recovery 89 %
· Product is not typical gasoline.
I Sample Log 16478
16478--04
i Sample: S-GPL2-6'
From : Beacon 596 (Projo # 1596.15)
Sampled : 02/25/97
I Dilution : 1:1 QC Batch : 6182N
Matrix : Soil
I Measured
Parameter (MRL) ~/k~ Value
I (.0050) <.0050
Benzen~
Toluene (.0050) .016
Ethylbenzene (.0050) .014
ITotal Xylenes (.0050) .11
TPH as Gasoline (1.0) <1.0
iSurrogate Recovery 102 %
I
~ m m ~ m~m time in second~
~ ~1 I
~te ~ed: ~-26-~ J~l Ki{{
Col~ ~ 0.~ ID X ~ ~tek ~tx-lFOl $~i~
I Sample Log 16478
16¢78--05
From . Beacon 596 (Proj. # 1596.15)
Sampled : 02/25/97
I Dilution : 1:1 QC Batch : 6182M
Matrix : Soil
I Measured
Parameter (MRL).~/kg Valuers/kg
I Benzene ° (.0050) <.0050
Toluene (.0050) .0064
Ethylbenzene (.0050) <.0050
I Total Xylenes (.0050) .015
TPH as Gasoline (1o0) <1.0
i Surrogate Recovery 104 %
~ ° o . ~ ~. ti.e in seconds
o~
O ~ ~
~ ~1 I
Date fl~l~ ~-26-~ J~l ~ /
Column : ~53~ ID X ~ ResteE ~x-l~l $~ior C~mist
I
I Sample Log 16478
~47~-0~
i Sample: S-GPL3-6'
From : Beacon 596 (Proj. # 1596.15)
Sampled : 02/25/97
I Dilution : 1:1 QC Batch
:
6182M
Matrix : Soil
I Measured
Parameter (MRL) .g/k~ Value .g/k~
I (.0050) <.0050
Benzene
Toluene (.0050) <.0050
Ethylbenzene (.0050) <.0050
I Total Xylenes (.0050) .011
TPH as Gasoline (1o0) <1.0
i Surrogate Recovery 107 %
I
o= ' ~ ~o ~ ~ ~~ time in seconds~
O~
0
~te ~al~e~ ~-~-~ Joel
~ol~ : 0.~ ID X ~ ~tek ~x-1~1 Seni~
I
I Sample Log 16478
i Sample: S-GPL4-2'
From : Beacon 596 (Proj. # 1596.15)
Sampled : 02/25/97
I Dilution : 1:100 QC Batch : 2157D
Matrix : Soil
I Measured
Parameter (MRL) =q/kg Value .q/kg
IBenzene (.5~)
1.3
Toluene (.50) 110
Ethylbenzene (.50) 62
ITotal Xylenes (.50) 450
TPH as Gasoline (100) 2600
iSurrogate Recovery *** Diluted Out
I
I
· ~ ~ ~ ~ ~ ~ o~-o~ time in seconds
I
Date ~al~z~ ~-26-~
Sample Log 16478
Sample. S-GPL4-6'
From : Beacon 596 (Proj. # 1596.15)
Sampled : 02/25/97
Dilution : 1:100 QC Batch : 2157D
Matrix : Soil
Measured
Parameter (MRL) .g/k~ Value ~xkg
(.50) 14
Benzene
Toluene (.50) 74
Ethylbenzene (.50) 29
Total Xylenes (.50) 150
TPH as Gasoline (100) 1600
Surrogate Recovery *** Diluted Out
time in seconds
I Sample Log 16478
1~478--O9
Sample: S-GPL5-2'
I From : Beacon 596 (Proj. # 1596.15)
Sampled : 02/25/97
I Dilution : 1:10 QC Batch : 6182N
Matrix : Soil
I Measured
Parameter (MRL) .gzk~ Value .~zk~
IBenzene (.050) <.050
Toluene (.050) 1.5
Ethylbenzene (.050) .82
i T
otal Xylenes (.050) 7.9
TPH as Gasoline (10) 41
Surrogate Recovery 90 %
!
I
o ~ ~ ~m time in seconds
O\
0
~al~z~ ~-~-~ J~l ~
il
I Sample Log 16478
16478--10
Sample: S-GPL5-6'
I From : Beacon 596 (Projo # 1596.15)
Sampled : 02/25/97
I Dilution : 1:1 Qc Batch : 6182N
Matrix : Soil
I Measured
Parameter (MRL) m~/~g Value m~/~g
IBenzene (.0050) <.0050
Toluene (.0050) .056
Ethylbenzene (.0050) .013
ITotal Xylenes (.0050) .18
TPH as Gasoline (1.0) 2.7
ISurrogate Recovery 109 %
'
0
Date ~ 02-26-~ Joel Kiff
~l~ I ~ ID X ~ ResteE Rtx-1701 Se~ C~mist
m m m m m m m mm m mm m mm m m mm mm m m m
Ultramar Inc. BEACON
CHAIN OF CUSTODY REPORT
BeaconS, ation No.~~, Sample~(Print Name)_~~ 6~¥)wJ ANALYSE8
Proj~ L~a~n ~ ~liation /
m~ o
' ~1~ NoJld~~n Dat~ T~ Lab No.
~oli~ b~: (S~aturo/~ffiliation) / ' ~ato lime Dato lime
... ~eli~uish~ by: (8~e/A~iliation) Date Time ~lure/~]iation) Daie Time
Dale
Time
Date Time R~eiv /Affiliation)
Re~.To¢~;'~--'~'~ eilmto/ ' UCRAMA" INC.
~~~~ / ~5 West Third Street
· Hanford, CA 9~0
WHITE: Return to Client with Re~ YELLOW: Laboralo~ Copy PINK: Originator Copy ~-~
mm mm m m mm m m mm m m m m {m m m m m m m
Ullramar Inc. BEACON
CHAIN OF CUSTODY REPORT
Beacon Station No. Sampler (Print Name) Date I Form No. ~
Project No. Sampler (S~;Fjature) ~ ~-"-e-'~-+z~:~'~/ ~'- .,~' ~7
r' J~~ x ~ ~
~ O
Sample NoJIdentifi~tbn Date Time Lab No. m ~ - z REMARKS
~elinq~y: (S~lu~e/Attili~lion). D~le Time ~~~gn~l~e~ffili~lio~ D~le Time
.~ ~quish~ by: (Sig~e/Affiliation) Date Time R~eiv~ bF~m/Affih~tion) ' Date Time
... ..........
Bill t~ ~ O~RAMARqNC.
Re~d To: ~~ ~~ / 5~Wesl Third Slreet
~ ~/~ .~ -- Hanford, CA~O // .
Atlention: ~-~~ ~g~¢7~
WHITE: Return to Client with Repod YELLOW: Laboralow Copy PINK: Originator Copy - -~ ~,,~,¢
February 27, 1997
Sample Log 16483
Gary Barker
Horizon Environmental Inc.
5011 Golden Foothill Pkwy., Suite 7
E1 Dorado Hills, CA 95762
Subject: Analytical Results for 8 Soil Samples
Identified as: Beacon 596 (Proj. # 1596.15)
Received: 02/26/97
Dear Mr. Barker:
Analysis of the sample(s) referenced above has been completed.
This report is written to confirm results communicated on
procedures used to analyze the
February
27,
1997
and
describes
samples.
Sample(s) were analyzed using the following method(s):
"BTEX" (EPA Method 8020/Purge-and-Trap)
"TPH as Gasoline" (Modified EPA Method $015/Purge-and-Trap)
Please refer to the following table(s) for summarized analytical
results and contact us at 916-753-9500 if you have questions
regarding
procedures or results. The chain-of-custody document is enclosed.
Approved by:
Stewart Podolsky
Senior Chemist
Sample Log 16483
E (Methyl-t-butyl ether) By EPA Method 8020/602
From : Beacon 596 (Proj. # 1596.15)
Sampled : 02/26/97
Received : 02/26/97
Matrix : Soil
Measured
(MRL) .g/kg Value ,g/kg
SP-0226-A,B,C,D (5.0) 220
SP-0226-E,F,G,H (.050) .80
SP-0226-I,J,K,L (.050) <.050
SP-0226-M,N,O,P (.050) .33
(.50) 1.9
SP-0226-Q,R, S,T
SP-0226-U,V,W,X (.050) .12
S-GPLi-17' (5.0) 400
S-GPL4-11' (.50) 12
Approved BY:
Joel Kiff
Senior Chemist
I Sample Log 16483
16483--01
Sample: SP-O226-A,B,C,D
I From : Beacon 596 (Proj. # 1596.15)
Sampled : 02/26/97
I Dilution : 1:100 QC Batch : 6182R
Matrix : Soil
I Measured
Parameter (MRL) .~/k~ Value .~/k~
IBenzene (.50) 13
Toluene (.50) 360
Ethylbenzene (.50) 120
ITotal Xylenes (.50) 660
TPH as Gasoline (100) 2700
iSurrogate Recovery *** Diluted Out
I
~ O~ ~ ~ ~'~' ~ ~ime in seconds
I '
~e ~z~ 02-~-~
~1~ : ~ ID X ~ ~ ~x-1701
I
I Sample Log 16483
16483--02
Sample: SP-O226-E,F,G,H
I From : Beacon 596 (Proj. # 1596.15)
Sampled : 02/26/97
I Dilution : 1:1 QC Batch : 2157G
Matrix : Soil
I Measured
Parameter (MRL) mg/kg Value ~/kg
Benzene (.0050) .0068
Toluene (.0050) .21
Ethylbenzene (.0050) .15
Total Xylenes (.0050) 1.0
TPH as Gasoline (1.0) 4.9
Surrogate Recovery 100 %
!
,o ;o ~ ;o ~-~r ~- time in seconds
~ ~ ~1 I
~te ~aluz~ 02-27-~ J~l ~{{
Col~ : 0.~ X ~ ~e~ Rtx-l~l ~ ~mist
I
Sample Log 16483
16483-03
Sample: SP-O226-I,J,K,L
From : Beacon 596 (Projo # 1596.15)
Sampled : 02/26/97
Dilution : 1:1 QC Batch : 6182R
Matrix : Soil
I Measured
Parameter (MRL) .g/kg Value .g/k~
Benzene (.0050) <.0050
Toluene (.0050) <.0050
Ethylbenzene (.0050) <.0050
Total Xylenes (.0050) .010
TPH as Gasoline (1.0) <1.0
Surrogate Recovery 102 %
I
· ," ~ ~0 ~ ~ ~o o ~ime in seconds
I '
~ ~ ~' %, ~ ~.__
~te ~al~ ~-26-~ 3~1 Kf{{ /
~l~n : ~ ID X ~ ~t~ Rtx-1701 Seni~ ~emist ~
I Sample Log 16483
16483-04
Sample: SP-O226-M,N,O,P
I From : Beacon 596 (Proj. # 1596.15)
Sampled : 02/26/97
I Dilution : 1:1 QC Batch : 2157G
Matrix : Soil
I Measured
Parameter (MRL) ~k~ Value ~/kg
IBenzene (.0050) <.0050
Toluene (.0050) .043
Ethylbenzene (.0050) .012
ITotal Xylenes (.0050) .079
TPH as Gasoline (1.0) <1.0
iSurrogate Recovery 97 %
I
~ ~ ~ ~ m ~ ~ time in seconds
og
~1~ : ~ X 60m Restek Rtx-l~l Se~i~
I
I Sample Log 16483
164~3--05
i Sample: SP-0226-Q,R,S,T
From : Beacon 596 (Projo # 1596.15)
Sampled : 02/26/97
I Dilution : 1:10 QC Batch : 6182R
Matrix : Soil
I Measured
Parameter (MRL) ~g/kg Value ~g/k~
Benzene (.650)
<.050
Toluene (.050) .40
Ethylbenzene (.050) .17
Total Xylenes (.050) 1.3
TPH as Gasoline (10) 13
Surrogate Recovery 90 %
ISample Log 16483
16483--06
Sample: SP-O226-U,V,W,X
I From : Beacon 596 (Projo # 1596.15)
Sampled : 02/26/97
I D
ilution : 1:1 QC Batch : 2157G
Matrix : Soil
I Measured
Parameter (MRL) .~/kg Value .~/kg
IBenzene (.0050)' <.0050
Toluene (.0050) .016
Ethylbenzene (.0050) .0081
ITotal Xylenes (.0050) .077
TPH as Gasoline (1.0) <1.0
iSurrogate Recovery 97 %
I
0
I
I Sample Log 16483
16483--07
i Sample: S-GPLi-17'
From : Beacon 596 (Proj. # 1596.15)
Sampled : 02/26/97
I Dilution : 1:100 QC Batch : 6182S
Matrix : Soil
I Measured
Parameter (MRL) .~g Value .g/k~
IBenzene (.50) 41
Toluene (.50) 710
Ethylbenzene (.50) 190
ITotal Xylenes (.50) 880
TPH as Gasoline (100) 5200
iSurrogate Recovery *** Diluted Out
I
~ime
in
seconds
! ·
I
Date ~1~
~o1~ : ~ ID X ~ ~e~ek ~x-1701 S~i~ ~is~
I
I Sample Log 16483
~6483--08
,!
From : Beacon 596 (Proj. # 1596.15)
Sampled : 02/26/97
I Dilution : 1:10 QC Batch : 6182S
Matrix : Soil
i Measured
Parameter (MRL) .~/kg Value .~/kg
Benzene (.050) <.050
i· Toluene (.050) .56
Ethylbenzene (.050) .069
I T
otal Xylenes (.050) .80
TPH as Gasoline (10) 11
Surrogate Recovery 91 %
,!
!
I
~ ~ mc0 ~.~ ~ime in seconds
0 ~ ~ ~
~1~ : ~ ID X ~ ~st~ Rtx-1701 S~i~ Chest
Ull~'amar Inc. BEACON
CHAIN OF CUSTODY REPORT
Beacon Station No. 'Print Name) Form No.
ANALYSES of
Project Location
[ ~ample NoJIdentification/' Date Time Lab No. REMARKS
I ' / -
I
7
I
/.-/-7'
Relinquish~$'~. (Signalure/Aftiliation) Date Time Received by: (Signature/Affiliation) Date. I Ti'ne
~'l'quished by: (Signatur~ation, D_ate Time Received by: (Signature/Affiliation) Date IT, ~.e._..
I
Relinquished by: (Signature/Affiliation) /~ Time Received~.~../~by: {Si§nature/Aff~..t~)t~/.j~,.~.~ ~c/~ ~'~'~ ~//~/~[~]50Date I li 'ne
Bill ~0~.' ULTRAMAR INC.
Report To: /'~-,/f~-'~' ~/i~-/=r'~/~., 525 West Third Street
,~,~ ,7~,u E,-, ,,',,~.~:: ,~ ,~.,.~..~' . ,anforU. CA 93230.
' ' Attention: ,/~"~.4.~,..,,~'7"~'
WHITE: Return to Client with Report YELLOW: Laboratory Copy PINK: Originator Copy ~.~ 8oo~ ,,,,,o
I(IFF Report Number' 10292
Date · 08/03/97
IANALYTICAL
LLC
Gary Barker
Horizon Environmental Inc.
5011 Golden Foothill Pkwy., Suite 7
El Dorado Hills, CA 95762
Subject' Analysis of 9 Soil Samples
Project Name · Beacon 596
Project Number' 1596.15
Dear Mr. Barker,
Chemical analysis of the samples referenced above has been completed. Summaries of the data are contained
on the following pages. Sample(s) were received under documented chain-of-custody. US EPA protocols for
sample storage and preservation were followed.
Kiff Analytical is certified by the State of California (# 2236). If you have any questions regarding pro. cedures
or results, please call me at 916-297-4800.
Sincerely,
720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
I IAIVALYT/CAL Date' 08/03/97
/-LC'
Project Name' Beacon 596
Project Number: 1596.15
Sample' DSP-I,J,K,I.-8 Matrix' Soil
Sample Date :08/01/97
Method
Measured Reporting Analysis Date
Parameter ' Value Limit Units Metl'iod Analyzed
Benzene < G.0~)0 0.020 mg/Kg - EPA 8020 08/02/97
Toluene < (~,020 0.020 mg/Kg EPA 8020 08/02/97
Ethylbenzene 0,90 0.020 mg/Kg EPA 8020 08/02/97
Total Xylenes $,1 0.020 mg/Kg EPA 8020 08/02/97
Methyl-t-butyl ether < 2,0 2.0 mg/Kg EPA 8020 08/02/97
TPH as Gasoline 88 2.0 M EPA
mg/Kg
801
5
08/02/97
TPH as Diesel 790 1.0 mg/Kg M EPA 8015 08/03/97
TPH as Motor Oil 130 10 mg/Kg M EPA 8015 08/03/97
aaa-Trifluorotoluene (8020 Surrogate) 98.9 % Recovery EPA 8020 08/02/97
aaa-Trifluorotoluene (Gasoline Surrogate) 89.7 % Recovery M EPA 8015 08/02/97
1-chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 08/03/97
I Sample' DSP-M,N,O,P-S Matrix' Soil
Sample Date :08/01/97
I Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
i Benzene < 0,020 0.020 mg/Kg EPA 8020 08/02/97
Toluene < 4),020 0,020 mg/Kg EPA 8020 08/02/97
Ethylbenzene 0,45 0,020 mg/Kg EPA 8020 08/02/97
i Total Xylenes 2,G 0.020 rog/Kg EPA 8020 08/02/97
Methyl-t-butyl ether < 2,0 .2.0 rog/Kg EPA 8020 08/02/97
TPH as Gasoline 52 2.0 mg/Kg M EPA 8015 08/02/97
I TPH as Diesel 300 1.0 mg/Kg M EPA 8015 08/03/97
TPH as Motor'Oil < 100 10 rog/Kg M EPA 8015 08/03/97
I aaa-Trifluorotoluene (8020 Surrogate) 100 % Recovery EPA 8020 08/02/97
aaa-Trifluorotoluene (Gasoline Surrogate) 87.4 % Recovery M EPA 8015 08/02/97
i 1-chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 08/03/97
I Approved By: Joel Kiff
I 720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
KIFF
Report Number' 10292
I IANALYTICAL Date' 08/03/97
LLC
'1
i Project Name' Beacon 596
Project Number' 1596.1 5
I
Sample: DSP-Q,R,S,T-S Matrix: Soil
I Date :08/01/97
Sample
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
I Benzene < 0.020 0.020 rog/Kg EPA 8020 08/02/97
Toluene 0.42 0.020 mg/Kg EPA 8020 08/02/97
I Ethylbenzene 1.6 0.020 mg/Kg EPA 8020 08/02/97
· Total Xylenes 11 0.020 mg/Kg EPA 8020 08/02/97
Methyl-t-butyl ether < 2.0 2.0 mg/Kg EPA 8020 08/02/97
I TPH as Gasoline 130 2.0 rog/Kg M EPA 8015
08/02/97
TPH as Diesel 540 1.0 mg/Kg M EPA 8015 08/03/97
I TPH as Motor Oil 120 10 mg/Kg M EPA 8015 08/03/97
aaa-Trifluorotoluene (8020 Surrogate) 97.6 % Recovery EPA 8020 08/02/97
i aaa-Trifluorotoluene (Gasoline Surrogate) 93.6 % Recovery M EPA 8015 08/02/97
1-chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 08/03/97
I Sample' DSP-A,B,C,D-N Matrix' Soil
Sample Date :08/01/97
I Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
Benzene < 0.020 0.020 mg/Kg EPA 8020 08/02/97
I 0.30 0.020 mg/Kg EPA 8020 08/02/97
Toluene
Ethylbenzene 0.52 0.020 mg/Kg EPA 8020 08/02/97
Total Xylenes 4.5 0.020 mg/Kg EPA 8020 08/02/97
I 2.0 mg/Kg EPA 8020 08/02/97
Methyl-t-butyl
ether
2.0
TPH as Gasoline 54 2.0 mg/Kg M EPA 8015 08/02/97
I TPH as Diesel 3200 1.0 mg/Kg M EPA 8015 08/03/97
aaa-Trifluorotoluene (8020 Surrogate) 100 % Recovery EPA 8020 08/02/97
I (Gasoline Surrogate) 87.2 % Recovery M EPA 8015 08/02/97
aaa-mrifluorotoluene
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 08/03/97
!
I Approved By: Joel Kiff
i 720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
Date · 08~03~97
Project Name' Beacon 596
Project Number' 1596.15
Sample- DSP-E,F,G,H-N Matrix' Soil
Sample Date :08/01/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 0.020 0.020 mg/Kg EPA 8020 08/02/97
Toluene 0.27 0.020 rog/Kg EPA 8020 08/02/97
Ethylbenzene 0.38 0.020 mg/Kg EPA 8020 08/02/97
Total Xylenes 2.5 0.020 rog/Kg EPA 8020 08/02/97
Methyl-t-butyl ether < 2.0 2.0 mg/Kg EPA 8020 08/02/97
TPH as Gasoline 35 2.0 M EPA 8015 08/02/97
mg/Kg
TPH as Diesel 2700 1.0 rog/Kg M EPA 8015 08/03/97
aaa-Trifluorotoluene (8020 Surrogate) 101 % Recovery EPA 8020 08/02/97
aaa-Trifluorotoluene (Gasoline Surrogate) 86.7 % Recovery M EPA 8015 08/02/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 08/03/97
Sample' DSP-I,J,K,L-N Matrix' Soil
Sample Date :08/01/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
Benzene < 0,020 0.020 rog/Kg EPA 8020 08/02/97
Toluene 0,24 0.020 rog/Kg EPA 8020 08/02/97
Ethylbenzene 0.18 0,020 mg/Kg EPA 8020 08/02/97
Total Xylenes 1,9 0.020 mg/Kg EPA 8020 08/02/97
Methyl-t-butyl ether < 2,0 2.0 mg/Kg EPA 8020 08/02/97
TPH as Gasoline 28 2.0 mg/Kg M EPA 8015 08/02/97
TPH as Diesel 1600 1.0 rog/Kg M EPA 8015 08/03/97
aaa-Trifluorotoluene (8020 Surrogate) 103 % Recovery EPA 8020 08/02/97
aaa-Trifluorotoluene (Gasoline Surrogate) 84.1 % Recovery M EPA 8015 08/02/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 08/03/97
Approved By: Joel Kiff z ~,
720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
I KiFF Report Number · 10292
I 'ANALYT'CALLLc Date' 08/03/97
I P
roject Name · Beacon 596
Project Number: 1596.15
I
Sample: CL-8-S Matrix: Soil
I Sample Date :08/01/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units MetHod Analyzed
I Benzene < 0.0050 0.0050 mg/Kg EPA 8020 08/02/97
Toluene < 0.0050 0.0050 mg/Kg EPA 8020 08/02/97
i Ethylbenzene < 0.0050 0.0050 mg/Kg EPA 8020 08/02/97
Total Xylenes < 0.0050 0.0050 mg/Kg EPA 8020 08/02/97
Methyl-t-butyl ether < 0.050 0.050 mg/Kg EPA 8020 08/02/97
I TPH as Gasoline < 1.0 1.0 mg/Kg M EPA 8015 08/02/97
TPH as Diesel < 1.0 1.0 rog/Kg M EPA 8015 08/03/97
I TPH as Motor Oil < 10 10 mg/Kg M EPA 8015 08/03/97
aaa-Trifluorotoluene (8020 Surrogate) 103 % Recovery EPA 8020 08/02/97
i aaa-Trifluorotoluene (Gasoline Surrogate) 81.8 % Recovery M EPA 8015 08/02/97
1-chlorooctadecane (Diesel Surrogate) 105 % Recovery M EPA 8015 08/03/97
I
I Approved By: Jo~l'Ki~f-
i 720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
(diesel)
UIl 'amir Im . BEACON
CHAIN OF CUSTODY FIEPORT
Project Location -,"' ~iation / ~ '-'
Sample No./Identification Date Time Lab No. ~ ~ i.-. ~d REMARKS
Relinquis.l~l by: ($ignalure/Aflilialion) Dale Time Received by: (S~nalure/Aflilialion) Date Time
~/(nquished by: (S~inatur/q~iliation) Date Time Received by: (S~nature/Afliliation) Date Time
Relinquished by: ($~nature/Affiliation) Date~._._ __Time Receiv~ed by: (Skjnature~tAffiliation)/ Date Time
Bill to: ULTRAMAR INC. j '
Re.l~!To:~ ~ 525 West Third Street
'- Attention:
WHITE: Return to Client withReport YELLOW: Laboratory Copy PINK: Originator Copy ~.~,~,
I(IFF Report Number' 10286
Date · 07/30/97
I IANALYTICAL
LLC
!
Gary Barker
Horizon Environmental Inc.
5011 Golden Foothill Pkwy., Suite 7
El Dorado Hills, CA 95762
Subject: Analysis of 4 Soil Samples
Project Name · Beacon 596
Project Number: 1596.15
Dear Mr. Barker,
Chemical analysis of the samples referenced above has been completed. Summaries of the data are contained
on the following pages. Sample(s) were received under documented chain-of-custody. US EPA protocols for
sample storage and preservation were followed.
Kiff Analytical is certified by the State of California (# 2236). If you have any questions regarding procedures
or results, please call me at 916-297-4800.
Sincerely,
JoeI,Kiff
I
i 720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
I Date · 07/30/97
Project Name' Beacon 596
Project Number' 1596.15
Sample' DSP-A,B,C,D Matrix' Soil
Sample Date :07/29/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
Benzene < 0.050 0.050 mg/Kg . EPA 8020 07/29/97
Toluene 0.20 0.050 mg/Kg EPA 8020 07/29/97
Ethylbenzene 0.063 0.050 mg/Kg EPA 8020 07/29/97
Total Xylenes 1.9 0.050 mg/Kg EPA 8020 07/29/97
Methyl-t-butyl ether < 5.0 5.0 mg/Kg EPA 8020 07/29/97
TPH as Gasoline 81 5.0 mg/Kg M EPA 8015 07/29/97
TPH as Diesel 1100 50 mg/Kg M EPA 8015 07/29/97
aaa-Trifluorotoluene (8020 Surrogate) 99.5 % Recovery EPA 8020 07/29/97
aaa-Trifluorotoluene (Gasoline Surrogate) 84.5 % Recovery M EPA 8015 07/29/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/29/97
I Sample · DSP-E,F,G,H Matrix: Soil
Sample Date :07~29~97
Method
I Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 0.050 0.050 rog/Kg EPA 8020 07/29/97
I Toluene < 0,050 0.050 mg/Kg EPA 8020 07/29/97
Ethylbenzene < 0.050 0.050 mg/Kg EPA 8020 07/29/97
Total Xylenes 0.52 0.050 mg/Kg EPA 8020 07/29/97
i Methyl-t-butyl ether < 2.0 2.0 rog/Kg EPA 8020 07/29/97
TPH as Gasoline 24 2.0 mg/Kg M EPA 8015 07/29/97
I TPH as Diesel 790 100 mg/Kg M EPA 8015 07/29/97
aaa-Trifluorotoluene (8020 Surrogate) 102 % Recovery · EPA 8020 07/29/97
I aaa-Trifluorotoluene (Gasoline Surrogate) 82.9 % Recovery M EPA 8015 07/29/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/29/97
Approved By: JoilKiff ~ I
I 720 Olive Drive, Suite D Davis, CA 95616 916-297-4800`) ~
'" I
KIFF
Report Number- 10286
IANALYTICALL£c Date' 07~30~97
Project Name' Beacon 596.
Project Number' 1 596.1 5
Sample: DSP-I,J,K,L Matrix: Soil
Sample Date :07/29/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units MetHod Analyzed
Benzene < 0.050 0.050 mg/Kg - EPA 8020 07/29/97
Toluene < 0.050 0.050 mg/Kg EPA 8020 07/29/97
Ethylbenzene < 0.050 0.050 mg/Kg EPA 8020 07/29/97
Total Xylenes 0.72 0.050 mg/Kg EPA 8020 07/29/97
Methyl-t-butyl ether < 2.0 2.0 mg/Kg EPA 8020 07/29/97
TPH as Gasoline 30 2.0 rog/Kg M EPA 8015 07/29/97
TPH as Diesel 2900 100 mg/Kg M EPA 8015 07/29/97
aaa-Trifluorotoluene (8020 Surrogate) 102 % Recovery EPA 8020 07/29/97
aaa-Trifluorotoluene (Gasoline Surrogate) 83.7 % Recovery M EPA 8015 07/29/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/29/97
Sample' D.I.-15'.N-M.P. Matrix' Soil
Sample Date :07/29/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl~od Analyzed
Benzene < 0,0050 0,0050 mg/Kg EPA 8020 07/29/97
Toluene < 0,0050 0,0050 mg/Kg EPA 8020 07/29/97
Ethylbenzene < 0,0050 0.0050 mg/Kg EPA 8020 07/29/97
Total Xylenes < 0,0050 0,0050 mg/Kg EPA 8020 07/29/97
Methyl-t-butyl ether < 0,050 0,050 mg/Kg EPA 8020 07/29/97
TPH as Gasoline < 1,0 1.0 mg/Kg M EPA 8015 07/29/97
TPH as Diesel < t.0 1.0 mg/Kg' M EPA 8015 07/30/97
aaa-Trifluorotoluene (8020 Surrogate) 102 % Recovery ' EPA 8020 07/29/97
aaa-Trifluorotoluene (Gasoline Surrogate) 82.4 % Recovery M EPA 8015 07/29/97
1-Chlorooctadecane (Diesel Surrogate) 62.3 % Recovery M EPA 8015 07/30/97
I
I 720 Olive Drive, Suite D Davis, CA 95616 916-297-4800'~ _
I
KIFF ' Report Number · 10291
Date ·08/01/97
I IANALYTICAL
LLC
I
I Gary Barker
Horizon Environmental Inc.
5011 Golden Foothill Pkwy., Suite 7
I El Dorado Hills, CA 95762
Subject · Analysi.s of 5 Soil Sample~
I P
roject Name · Beacon 596
Project Number: 1596.15
I
i Dear Mr. Barker,
Chemical analysis of the samples referenced above has been completed. Summaries of the data are contained
I on the following pages. Sample(s) were received under documented chain-of-custody. US EPA protocols for
sample storage and preservation were followed.
I
Kiff Analytical is certified by the State of California (# 2236). If you have any questions regarding procedures
I or results, please call me at 916-297-4800.
Sincerely,
!
I
i 720 Olive Drive, Suite D Davis, CA 95616 916-297-4800 --
I(IFF Report Number · 10291
I IANALYTICAL Date-08/01/97
LLC
I Project Name' Beacon 596
Project Number' 1596,15
Sample' DSP-A,B,C,D Matrix' Soil
I Sample Date :07/31/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
I Benzene < 0.050 0.050 mg/Kg EPA 8020 08/01/97
Toluene 0.066 0.050 mg/Kg EPA 8020 08/01/97
i Ethylbenzene 0.17 0.050 rog/Kg EPA 8020 08/01/97'
Total Xylenes 1.4 0.050 mg/Kg EPA 8020 08/01/97
Methyl-t-butyl ether < 5.0 5.0 mg/Kg EPA 8020 08/01/97
I TPH as Gasoline 56 5.0 M EPA
mg/Kg
801
5
08/01/97
TPH as Diesel 1700 10 mg/Kg M EPA 8015 08/01/97
I TPH as Motor Oil 160 100 mg/Kg M EPA 8015 08/01/97
aaa-Trifluorotoluene (8020 Surrogate) 102 % Recovery EPA 8020 08/01/97
i aaa-Trifluorotoluene (Gasoline Surrogate) 84.1 % Recovery M EPA 8015 08/01/97
1-chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 08/01/97
I Sample' DSP-E,F,G,H Matrix' Soil
', I Sample Date :07/31/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
I Benzene < 0,020 0.020 mg/Kg EPA 8020 08/01/97
Toluene < 0.020 0.020 mg/Kg EPA 8020 08/01/97
Ethylbenzene 0.083 0.020 mg/Kg EPA 8020 08/01/97
i Total Xylenes 0.13 0.020 mg/Kg EPA 8020 08/01/97
Methyl-t-butyl ether < 2.0 2.0 mg/Kg EPA 8020 08/01/97
TPH as Gasoline 24 2.0 rog/Kg M EPA 8015 08/01/97
I TPH as Diesel 530 10 mg/Kg ' M EPA 8015 08/01/97
TPH as Motor Oil < 100 100 mg/Kg M EPA 8015 08/01/97
I aaa-Trifluorotoluene (8020 Surrogate) 102 % Recovery EPA 8020 08/01/97
aaa-Trifluorotoluene (Gasoline Surrogate) 84.8 % Recovery M EPA 8015 08/01/97
I 1-chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 08/01/97
I Approved By: .
I 720 Olive Drive, Suite D Davis, CA 95616 916-297-48~ _---.
II(IFF
I IANALYTICAL Date' 08/01/97
/..£¢
IProject Name' Beacon 596
Project Number: 1596.1 5
!
Sample: DSP-I,J,K,L. Matrix: Soil
I Sample Date :07/31/97
Method
Measured Reporting Analysis Date
i Parameter Value Limit Units Metl'iod Analyzed
Benzene < 0,020 0,020 mg/Kg - EPA 8020 08/01/97
Toluene < 0,020 0.020 mg/Kg EPA 8020 08/01/97
I Ethylbenzene 0,094 0,020 mg/Kg EPA 8020 08/01/97
Total Xylenes 0,042 0,020 mg/Kg EPA 8020 08/01/97
Methyl-t-butyl ether < 2,0 2.0 mg/Kg EPA 8020 08/01/97
I TPH as Gasoline 29 2.0 mg/Kg M EPA 8015 08/01/97
TPH as Diesel 520 10 mg/Kg M EPA 8015 08/01/97
I TPH as Motor Oil < 100 100 M
mg/Kg
EPA
801
5
08/01/97
aaa-Trifluorotoluene (8020 Surrogate) 103 % Recovery EPA 8020 08/01/97
I aaa-Trifluorotoluene (Gasoline Surrogate) 83.8 % Recovery M EPA 8015 08/01/97
1-chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 08/01/97
I Sample' DTP-SW-15' Matrix' Soil
Sample Date :07/31/97
I
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
I Benzene < 0,0050 0,0050 mg/Kg EPA 8020 08/01/97
Toluene < 0,0050 0,0050 mg/Kg EPA 8020 08/01/97
Ethylbenzene < 0,0050 0.0050 mg/Kg EPA 8020 08/01/97
I Total Xylenes < 0,0050 0.0050 rog/Kg EPA 8020 08/01/97
Methyl-t-butyl ether < G,050 0.050 mg/Kg EPA 8020 08/01/97
I TPH as Gasoline < 1.0 1.0 mg/Kg M EPA 8015 08/01/97
TPH as Diesel < 1.0 1.0 mg/Kg . M EPA 8015 08/01/97
TPH as Motor Oil < 10 10 mg/Kg M EPA 8015 08~01/97
I aaa-Trifluorotoluene (8020 Surrogate) 102 % Recovery EPA 8020 08/01/97
aaa-Trifluorotoluene (Gasoline Surrogate) 81.4 % Recovery M EPA 8015 08/01/97
I 1-chlorooctadecane (Diesel Surrogate) 80.7 % Recovery M EPA 8015 08/01/97
I 720 Olive Drive, Suite D Davis, CA 95616 916-2974800/
I KIFF
Report Number: 10291
IANALYTICAL Date' 08/01/97
LLC
Project Name' Beacon 596
Project Number: 1596,15
Sample: DTP-15'-SE Matrix: Soil
Sample Date :07/31/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl~od Analyzed
Benzene < 0,0050 0.0050 mg/Kg .EPA 8020 08/01/97
Toluene < 0,0050 0.0050 mg/Kg EPA 8020 08/01/97
Ethylbenzene < 0,0050 0.0050 mg/Kg EPA 8020 08/01/97
Total Xylenes < 0,0050 0.0050 mg/Kg EPA 8020 08/01/97
Methyl-t-butyl ether < 0,050 0,050 mg/Kg EPA 8020 08/01/97
TPH as Gasoline < 1.0 1.0 mg/Kg M EPA 8015 08/01/97
TPH as Diesel < 1.0 1.0 mg/Kg M EPA 8015 08/01/97
TPH as Motor Oil < 10 10 mg/Kg M EPA 8015 08/01/97
aaa-Trifluorotoluene (8020 Surrogate) 103 % Recovery EPA 8020 08/01/97
aaa-Trifluorotoluene (Gasoline Surrogate) 81.6 % Recovery M EPA 8015 08/01/97
1-chlorooctadecane (Diesel Surrogate) 77.4 % Recovery M EPA 8015 08/01/97
I
I
I
I 720 Olive Drive, Suite D Davis, CA 95616 916-297-4~0 -~.
U~mmmr In(:, BEACON
C,Am O~ Cus~ouY ~EPO~ /~ ~ ~ /
Project/,..,¢.~.-N°'/~J Sampler ~/~gnature)~ ~ ~ .~~'" ..... ~J =~ 0~ ~ ' ~/
Sa~le NoJIde~ifi~t~n Date Time Lab No. = ~ ~ z REMARKS
i
Re~is~y: (S~nature/Affiliation) Date Time R~eiv~ by: (S~natur~Affiliation) Date Time
.Reli~uish~ by: (Signature/Affiliation) Date Time ~R~eiv~ by:(~ ~ature/Affiliation) ' Date Time
.Re~ To:~ ~i~ to: UlT',MAR INC.
' ' ~7~ ~~ ~ 525 West Third Street
~_? Hanford, CA 932~0 ~ /~ ~
~ . Attention: ~~~ ~ ~
WHITE: Return to Client with Re~ YELLOW: Laboralo~ Copy PINK: Odginalor Copy ,~.,~, ,~
I Date · 07/31/97
Gary Barker
Horizon Environmental Inc.
5011 Golden Foothill Pkwy., Suite 7
El Dorado Hills, CA 95762
Subject · Analysis of 4 Soil Samples.
Project Name * Beacon 596
Project Number' 1596.15
Dear Mr. Barker,
Chemical analysis of the samples referenced above has been completed. Summaries of the data are contained
on the following pages. Sample(s) were received under documented chain-of-custody. US EPA protocols for
sample storage and preservation were followed.
Kiff Analytical is certified by the State of California (# 2236). If you have any questions regarding procedures
or results, please call me at 916-297-4800.
Sincerely,
%,
!
!
!
I 720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
KIFF
Report Number' 10289
I IANALYTICAL Date' 07/31/97
£LC
I Project Name' Beacon 596
Project Number: 1596.15
I
Sample: DSP-A,B,C,D Matrix: Soil
I Sample Date :07/30/97
Method
Measured Reporting' Analysis Date
I Parameter Value Limit Units Metl'iod Analyzed
Benzene < 0,020 0.020 rog/Kg - EPA 8020 07/31/97
Toluene 0,36 0.020 mg/Kg EPA 8020 07/31/97
i Ethylbenzene '~,4 0.020 mg/Kg EPA 8020 07/31/97
Total Xylenes 9,7 0.020 mg/Kg EPA 8020 07/31/97
Methyl-t-butyl ether < 2,0 2.0 mg/Kg EPA 8020 07/31/97
I TPH as Gasoline '~ 20 2.0 mg/Kg M EPA 8015 07/31/97
TPH as Diesel 890 100 mg/Kg M EPA 8015 07/31/97
I TPH as Motor Oil 410 100 mg/Kg M EPA 8015 07/31/97
aaa-Trifluorotoluene (8020 Surrogate) 99.1 % Recovery EPA 8020 07/31/97
I aaa-Trifluorotoluene (Gasoline Surrogate) 91.3 % Recovery M EPA 8015 07/31/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/31/97
I Sample' DSP-E,F,G,H Matrix' Soil
Sample Date :07/30/97
I Method
Measured Reporting Analysis Date
Parameter Value Limit Units Meti'iod Analyzed
i Benzene < 0,020 0,020 mg/Kg EPA 8020 07/31/97
Toluene 0,53 0,020 mg/Kg EPA 8020 07/31/97
Ethylbenzene 1,8 0,020 mg/Kg EPA 8020 07/31/97
I Total Xylenes 12 0.020 mg/Kg EPA 8020 07/31/97
Methyl-t-butyl ether < 2.0 2.0 rog/Kg EPA 8020 07/31/97
I TPH as Gasoline 150 2.0 mg/Kg M EPA 8015 07/31/97
TPH as Diesel 1100 100 mg/Kg 'M EPA 8015 07/31/97
TPH as Motor Oil 770 100 .mg/Kg M EPA 8015 07/31/97
I aaa-Trifluorotoluene (8020 Surrogate) 99.3 % Recovery EPA 8020 07/31/97
aaa-Trifluorotoluene (Gasoline Surrogate) 94.5 % Recovery M EPA 8015 07/31/97
I 1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/31/97
il Approved i
I 720 Olive Drive, Suite D Davis, CA 95616 916-297-4tj800
Date · 07/31/97
Project Name' Beacon 596
Project Number' 1596.15
Sample: DSP-I,J,K,L Matrix: Soil
Sample Date :07/30/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
Benzene < 0.20 0.20 mg/Kg . EPA 8020 07/31/97
Toluene 1.9 0.20 mg/Kg EPA 8020 07/31/97
Ethylbenzene 4.6 0.20 mg/Kg EPA 8020 07/31/97
Total Xylenes 33 0.20 mg/Kg EPA 8020 07/31/97
Methyl-t-butyl ether < 20 20 rog/Kg EPA 8020 07/31/97
TPH as Gasoline 390 20 mg/Kg M EPA 8015 07/31/97
TPH as Diesel 1800 100 mg/Kg M EPA 8015 07/31/97
TPH as Motor Oil 810 100 mg/Kg M EPA 8015 07/31/97
aaa-Trifluorotoluene (8020 Surrogate) 102 % Recovery EPA 8020 07/31/97
aaa-Trifluorotoluene (Gasoline Surrogate) 85.4 % Recovery M EPA 8015 07/31/97
1-Chiorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/31/97
Sample' CSP-A,B,C,D Matrix' Soil
Sample Date :07~30~97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 0,0050 0.0050 mg/Kg EPA 8020 07/31/97
< 0.0050 0.0050 mg/Kg EPA 8020 07/31/97
Toluene
Ethylbenzene < 0.0050 0.0050 rog/Kg EPA 8020 07/31/97
Total Xylenes < 0.0050 0.0050 mg/Kg EPA 8020 07/31/97
Methyl-t-butyl ether < 0.050 0.050 mg/Kg EPA 8020 07/31/97
TPH as Gasoline < 0.50 0.50 mg/Kg M EPA 8015 07/31/97
TPH as Diesel 26 1.0 mg/Kg 'M EPA 8015 07/31/97
aaa-Trifluorotoluene (8020 Surrogate) 102 % Recovery EPA 8020 07/31/97
aaa-Trifluorotoluene (Gasoline Surrogate) 81.8 % Recovery M EPA 8015 07/31/97
1-Chlorooctadecane (Diesel Surrogate) 76.8 % Recovery M EPA 8015 07/31/97
.~'
720 Olive Drive, Suite D Davis, CA 95616 916-297-~00
m mm m m mm m mmmmm m m m mm m m m mm mm mm mm
UBIrimlr Inc. BETON
CHAIN OF CUOTODY REPORT
Beacon Station No. Sampler...
Sa~e NoYmde~ifi~tbn Date Time 1 .h No. = -,- z REMARKS
~-~.~ ~. ~ ~~z - c,'~ .~- ¢~~.~
..~~.~./~.,. ...... ~_ / ~,, (.: ~/~
R~li~i~d b~: (8~~tIili~li~) D~I~ Ti~ ~B~ivd b~: (8?~l~mlAffiliaIion) Dal~ Ti~e
525 West Third Street
~~e ~ Hanford, CA
. Attention:
WHITE: Relum lo Ol~enI w)Ih Re~ YELLOW: Labomlo~ Oopy PINK: Odg)naloF
I{IFF Report Number · 10283
Date ·07/29/97
I ANALYTICAL
LLC
I Gary Barker
Horizon Environmental Inc.
5011 Golden Foothill Pkwy., Suite 7
I El Dorado Hills, CA 95762
Subject :'Analysis of 8 Soil Samples
I P
roject Name' Beacon 596
Project Number · 1596.15
I
Dear Mr. Barker,
I
Chemical analysis of the samples referenced above has been completed. Summaries of the data are contained
Ion the following pages. Sample(s) were received under documented chain-of-custody. US EPA protocols for
sample storage and preservation were followed.
I
Kiff Analytical is certified by the State of California (# 2236). If you have any questions regarding procedures
i or results, please call me at 916-297-4800.
Sincerely,
I 3o~1 Kiff
I
I
720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
' I(IFF
Report Number' 10283
I Project Name' Beacon 596
Project Number: 1596.15
I
Sample' DTP-A,B,C,D Matrix' Soil
I Sample Date :07~28/97
Method
Measured Reporting Analysis Date
I Parameter Value Limit o Units Method Analyzed
Benzene < 2.0 2.0 mg/Kg · EPA 8020 07/28/97
Toluene 2°3 2.0 mg/Kg EPA 8020 07/28/97
i Ethylbenzene 5ol 2.0 mg/Kg EPA 8020 07/28/97
Total Xylenes 32 2.0 mg/Kg EPA 8020 07/28/97
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/28/97
I TPH as Gasoline 390 200 mg/Kg M EPA 8015 07/28/97
TPH as Diesel 7000 100 rog/Kg M EPA 8015 07/28/97
I aaa-Trifluorotoluene (8020 Surrogate) 101 % Recovery EPA 8020 07/28/97
aaa-Trifluorotoluene (Gasoline Surrogate) 86.2 % Recovery M EPA 8015 07/28/97
i 1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/28/97
Sample' DTP-E,F,G,H Matrix' Soil
Sample Date :07/28/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metliod Analyzed
Benzene < 0,050 0.050 mg/Kg EPA 8020 07/29/97
Toluene 0,11 0.050 mg/Kg EPA 8020 07/29/97
Ethylbenzene 0,14 0.050 mg/Kg EPA 8020 07/29/97
Total Xylenes 1o4 0.050 mg/Kg EPA 8020 07/29/97
Methyl-t.butyl ether < 0,50 0,50 mg/Kg EPA 8020 07/29/97
TPH as Gasoline 68 5.0 mg/Kg M EPA 8015 07/29/97
TPH as Diesel 3100 100 mg/Kg M EPA 8015 07/29/97
aaa-Trifluorotoluene (8020 Surrogate) 104 % Recovery EPA 8020 07/29/97
aaa-Trifluorotoluene (Gasoline Surrogate) 85.9 % Recovery M EPA 8015 07/29/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery' M EPA 8015 07/29/97
720 Olive Drive, Suite D Davis, CA 95616 ' 916-297-z~/00
KIFF
Report Number' 10283
I IAIVALYTICA Date' 07~29/97
I Project Name' Beacon 596
Project Number' 1596,15
I
Sample' DTP-I,J,K,L Matrix' Soil
I Sample Date :07/28/97
Method
Measured Rep.orting Analysis Date
~· Parameter Value Limit . Units Method Analyzed
Benzene < 0.020 0.020 mg/Kg · EPA 8020 07/29/97
Toluene 0.027 0.020 mg/Kg EPA 8020 07/29/97
! · Ethylbenzene 0,080 0.020 mg/Kg EPA 8020 07/29/97
Total Xylenes 0,17 0.020 mg/Kg EPA 8020 07/29/97
Methyl-t-butyl ether < 0,20 0.20 mg/Kg EPA 8020 07/29/97
I TPH as Gasoline 13 2.0 mg/Kg M EPA 8015 07/29/97
TPH as Diesel 510 10 mg/Kg M EPA 8015 07/28/97
I aaa-Trifluorotoluene (8020 Surrogate) 105 % Recovery EPA 8020 07/29/97
aaa-Trifluorotoluene (Gasoline Surrogate) 86.0 % Recovery M EPA 8015 07/29/97
i 1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/28/97
I Sample · DTP-M,N,O,P Matrix: Soil
Sample Date :07/28/97
Method
I Measured Reporting _Ap_ alysis Date
Parameter Value Limit Units MetHod Analyzed
Benzene < 0.20 0.20 mg/Kg EPA 8020 07/28/97
i Toluene 1o7 0.20 mg/Kg EPA 8020 07/28/97
Ethylbenzene 3°5 0.20 mg/Kg EPA 8020 07/28/97
Total Xylenes 22 0.20 mg/Kg EPA 8020 07/28/97
I Methyl-t-butyl ether < 2.0 2.0 mg/Kg EPA 8020 07/28/97
TPH as Gasoline 260 20 rog/Kg M EPA 8015 07/28/97
I TPH as Diesel 4100 100 mg/Kg M EPA
80
1
5
07/28/97
aaa-Trifluorotoluene (8020 Surrogate) 103 % Recovery EPA 8020 07/28/97
i aaa-Trifluorotoluene (Gasoline Surrogate) 84.6 % Recovery M EPA 8015 07/28/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/28/97
!
I 720 Olive Drive, Suite D Davis, CA 95616' 916-2974800 ~/
I(IFF
Report Number' 10283
I IANALYTICALLLc Date' 07/29/97
Project Name' Beacon 596
Project Number' 1596.15
Sample: DTP-Q,R,S,T Matrix: Soil
Sample Date :07/28/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl~od Analyzed
Benzene 0,21 0.20 rog/Kg - EPA 8020 07/29/97
Toluene 2,5 0.20 mg/Kg EPA 8020 07/29/97
Ethylbenzene 5,0 0.20 mg/Kg EPA 8020 07/29/97
Total Xylenes 25 0.20 mg/Kg EPA 8020 07/29/97
Methyl.t-butyl ether < 2.0 2.0 mg/Kg EPA 8020 07/29/97
20 mg/Kg M EPA 8015 07/29/97
TPH
as
Gasoline
350
TPH as Diesel '~4000 100 mg/Kg M EPA 8015 07/28/97
aaa-Trifluorotoluene (8020 Surrogate) 101 % Recovery EPA 8020 07/29/97
aaa-Trifluorotoluene (Gasoline Surrogate) 87.6 % Recovery M EPA 8015 07/29/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/28/97
Sample' DTP-U,V,W,X Matrix' Soil
Sample Date :07/28~97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
Benzene < 0.20 0.20 mg/Kg EPA 8020 07/28/97
Toluene 0.69 0.20 mg/Kg EPA 8020 07/28/97
Ethylbenzene 1.0 0.20 mg/Kg EPA 8020 07/28/97
Total Xylenes 4.7 0.20 mg/Kg EPA 8020 07/28/97
Methyl-t-butyl ether < 2.0 2.0 mg/Kg EPA 8020 07/28/97
TPH as Gasoline 140 20 mg/Kg M EPA 8015 07/28/97
TPH as Diesel 6600 100 mg/Kg M EPA 801
5
07/29/97
aaa-Trifluorotoluene (8020 Surrogate) 104 % Recovery EPA 8020 07/28/97
aaa-Trifluorotoluene (Gasoline Surrogate) 84.2 % Recovery M EPA 8015 07/28/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/29/97
Approved By:
720 Olive Drive, SuiteD Davis, CA 95616'916-297-4~1~0
~_~,'
I(IFF
Report Number ' 10283
I IAIVALYTICAL Date' 07/29/97
L£C
I Project Name' Beacon 596
Project Number' 1596.15
I
Sample: D.I.-15'-NE Matrix: Soil
I Sample Date :07/28/97
Method
Measured Reporting Analysis Date
i Parameter Value Limit Units Method Analyzed
Benzene < 0,0050 0,0050 mg/Kg . EPA 8020 07/28/97
Toluene < 0,0050 0.0050 mg/Kg EPA 8020 07/28/97
i Ethylbenzene < 0,0050 0.0050 mg/Kg EPA 8020 07/28/97
Total Xylenes < 0,0050 0,0050 mg/Kg EPA 8020 07/28/97
Methyl-t-butyl ether < 0,050 0,050 mg/Kg EPA 8020 07/28/97
I 0.50 mg/Kg M EPA 8015 07/28/97
TPH
as
Gasoline
0.50
TPH as Diesel < 1.0 1.0 mg/Kg M EPA 8015 07/29/97
I aaa-Trifluorotoluene (8020 Surrogate) 104 % Recovery EPA 8020 07/28/97
aaa-Trifluorotoluene (Gasoline Surrogate) 82.4 % Recovery M EPA 8015 07/28/97
i 1-Chlorooctadecane (Diesel.Surrogate) 93.5 % Recovery M EPA 8015 07/29/97
I Sample' D,I,-15'-NW Matrix' Soil
Sample Date :07/28/97
Method
I Measured Reporting Analysis Date
Parameter Value Limit Units MetHod Analyzed
Benzene < 0,0050 0,0050 rog/Kg EPA 8020 07/28/97
i Toluene < 0,0050 0,0050 mg/Kg EPA 8020 07/28/97
Ethylbenzene < 0,0050 0,0050 mg/Kg EPA 8020 07/28/97
Total Xylenes < 0,0050 0.0050 rog/Kg EPA 8020 07/28/97
i Methyl-t,butyl ether < 0,050 0,050 mg/Kg EPA 8020 07/28/97
TPH as Gasoline < 0,50 0.50 mg/Kg M EPA 8015 07/28/97
I TPH as Diesel < 1,0 1,0 mg/Kg M EPA 8015 07/29/97
aaa-Trifluorotoluene (8020 Surrogate) 105 % Recovery EPA 8020 07/28/97
i aaa-Trifluorotoluene (Gasoline Surrogate) 82,5 % Recovery M EPA 8015 07/28/97
1-Chlorooctadecane (Diesel Surrogate) 91,7 % Recovery M EPA 8015 07/29/97
I
I '
Approved By: Jo
I 720 Olive Drive, Suite D Davis, CA 95616' 916-297-480(~_.J -'-"
UIt~amar Inc. /
CHAIN OF CUSTODY REPORT 0~ ~ ~ BEACON
~T~-~ ~ ~. ~ ~ -- o
Reli~~r__~~ / / Date Time R~oiv~by:(S~natur~A,iliation) .~.~, . / ~ Bale Time
~uish~ by: (S~ ~A~iaii~) /Dale Time R~eiv~ by: (S~natur~A~ilialion) '
~h~ by: (S~nalur~Affiliat~n~ ' D~t~ Time R v~ by: (S~nature/A~iliation) Date Time
Hanford, CA 9323~
WHITE: Return to Client with Re~d YELLOW: Laboralo~ Copy PINK: Originalor Copy
Date · 07/28/97
I Gary Barker
Horizon Environmental Inc.
5011 Golden Foothill Pkwy., Suite 7
I El Dorado Hills, CA 95762
Subject · Analysis of 7 Soil Samples
I Name' Beacon 596
Project
Project Number' 1596.15
i Dear Mr. Barker,
Chemical analysis of the samples referenced above has been completed. Summaries of the data are contained
I on the following pages. Sample(s) were received under documented chain-of-custody. US EPA protocols for
sample storage and preservation were followed.
Kiff Analytical is certified by the State of California (# 2236). If you have any questions regarding procedures
I or results, please call me at 916-297-4800.
Sincerely,
J~el Kiff
I I
!
720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
I(IFF
I IAIVAI..¥TICAL Date' 07/28/97
LLC
I P
roject Name' Beacon 596
Project Number: 1596.15
!
Sample: CSP-A,B,C,D Matrix: Soil
I Sample Date :07/25/97
Method
Measured Reporting Analysis Date
i Parameter Value Limit Units MetHod Analyzed
Benzene < 0,0050 0,0050 mg/Kg · EPA 8020 07/27/97
Toluene < 0,0050 0.0050 mg/Kg EPA 8020 07/27/97
i Ethylbenzene < 0,0050 0.0050 mg/Kg EPA 8020 07/27/97
Total Xylenes < 0,0050 0,0050 mg/Kg EPA 8020 07/27/97
Methyl-t-butyl ether < 0,050 . 0.050 mg/Kg EPA 8020 07/27/97
I as < 1,0 1,0 rog/Kg M EPA 8015 07/27/97
TPH
Gasoline
TPH as Diesel 93 10 mg/Kg M EPA 8015 07/27/97
I aaa-Trifluorotoluene (8020 Surrogate) 99.7 % Recovery EPA 8020 07/27/97
aaa-Trifluorotoluene (Gasoline Surrogate) 78.9 % Recovery M EPA 8015 07/27/97
I 1-Chlorooctadecane (Diesel Surrogate) 71.2 % Recovery M EPA 8015 07/27/97
I Sample * CSP-E,F,G,H Matrix: Soil
Sample Date :07/25/97
Method
I Measured Reporting Analysis Date
Parameter Value Limit Units Metl~od Analyzed
Benzene < 0,0050 0,0050 mg/Kg EPA 8020 07/27/97
i Toluene < 0,0050 0.0050 rog/Kg EPA 8020 07/27/97
Ethylbenzene < 0,0050 0,0050 mg/Kg EPA 8020 07/27/97
Total Xylenes < 0,0050 0,0050 mg/Kg EPA 8020 07/27/97
i Methyl-t-butyl ether < 0,050 0,050 mg/Kg EPA 8020 07/27/97
TPH as Gasoline < 1,0 1.0 mg/Kg M EpA 8015 07/27/97
I TPH as Diesel 170 10 mg/Kg M EPA 8015 07/27/97
aaa-Trifluorotoluene (8020 Surrogate) !03 % Recovery · EPA 8020 07/27/97
I aaa-Trifluorotoluene (Gasoline Surrogate) 81.8 % Recovery M EPA 8015 07/27/97
1-Chlorooctadecane (Diesel Surrogate) 113 % Recovery M EPA 8015 07/27/97
I 720 Olive Drive, Suite D D avis, CA 956~1:°::~-2B9Y~-4~0I
" KIFF
Report Number' 10282
I IANALYTICAL Date' 07/28/97
LLC
I Project Name' Beacon 596
Project Number: 1596.15
I
Sample: CSP-I,J,K,L Matrix: Soil
I Sample Date :07/25/97
Method
Measured Reporting _A~. alysis Date
i Parameter Value Limit Units Method 'Analyzed
Benzene < 0,0050 0.0050 mg/Kg · EPA 8020 07/27/97
Toluene < 0,0050 0.0050 rog/Kg EPA 8020 07/27/97
i Ethylbenzene < 0,0050 0,0050 mg/Kg EPA 8020 07/27/97
Total Xylenes < 0,0050 0.0050 mg/Kg EPA 8020 07/27/97
Methyl-t-butyl ether < 0,050 0,050 mg/Kg EPA 8020 07/27/97
I TPH as Gasoline < 1.0 1.0 mg/Kg M EPA 8015 07/27/97
TPH as Diesel 77 10 mg/Kg M EPA 8015 07/27/97
I aaa-Trifluorotoluene (8020 Surrogate) 102 % Recovery EPA 8020 07/27/97
aaa-Trifluorotoluene (Gasoline Surrogate) 81.1 % Recovery M EPA 8015 07/27/97
i 1-Chlorooctadecane (Diesel Surrogate) 97.0 % Recovery M EPA 8015 07/27/97
Sample' CSP-M,N,O,P Matrix' Soil
Sample Date :07/25/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units MetHod Analyzed
Benzene < 0,020 ' 0,020 mg/Kg EPA 8020 07/27/97
Toluene < 0,020 0,020 rog/Kg EPA 8020 07/27/97
Ethylbenzene 0,024 0.020 mg/Kg EPA 8020 07/27/97
Total Xylenes 0,051 0,020 mg/Kg EPA 8020 07/27/97
Methyl-t-butyl ether < 0,20 0,20 mg/Kg EPA 8020 07/27/97
TPH as Gasoline 10 5.0 mg/Kg M EPA 8015 07/27/97
TPH as Diesel 980 100 mg/Kg M EPA 8015 07/28/97
aaa-Trifluorotoluene (8020 Surrogate) '98.4 % Recovery EPA 8020 07/27/97
aaa-Trifluorotoluene (Gasoline Surrogate) 85.9 % Recovery M EPA 8015 07/27/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/28/97
Approved By: JIII~K,~
720 Olive Drive, Suite D Davis, CA 95616 916-29748t00
I(IFF
Report Number · 10282
I IANALYTICAL Date' 07/28/97
LLC
I Project Name: Beacon 596
Project Number: 1596.1 5
I
Sample: CSP-Q,R,S,T Matrix: Soil
I Sample Date :07/25/97
Method
Measured R_eporting Analysis Date
i. Parameter Value Limit Units Metl'iod Analyzed
Benzene < 0.0050 0.0050 mg/Kg EPA 8020 07/27/97
Toluene < 0.0050 0.0050 mg/Kg EPA 8020 07/27/97
i Ethylbenzene < 0.0050 0.0050 mg/Kg EPA 8020 07/27/97
Total Xylenes < 0.0050 0.0050 mg/Kg EPA 8020 07/27/97
Methyl-t-butyl ether < 0.050 0.050 mg/Kg EPA 8020 07/27/97
I TPH as Gasoline < 1.0 1.0 mg/Kg M EPA 8015 07/27/97
TPH as Diesel 200 10 rog/Kg M EPA 8015 07/28/97
I aaa-Trifluorotoluene (8020 Surrogate) 101 % Recovery EPA 8020 07/27/97
aaa-Trifluorotoluene (Gasoline Surrogate) 81.6 % Recovery M EPA 8015 07/27/97
I 1-Chlorooctadecane (Diesel Surrogate) 130 % Recovery M EPA 8015 07/28/97
Sample · DTP-15'-W-M.P. Matrix: Soil
Sample Date :07/25/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl~od Analyzed
Benzene < 0.0050 0.0050 mg/Kg EPA 8020 07/27/97
Toluene < 0.0050 0.0050 mg/Kg EPA 8020 07/27/97
Ethylbenzene < 0.0050 0.0050 mg/Kg EPA 8020 07/27/97
Total Xylenes 0o0051 0.0050 mg/Kg EPA 8020 07/27/97
Methyl-t-butyl ether 0.47 0.020 mg/Kg EPA 8020 07/27/97
TPH as Gasoline < 1.0 1.0 mg/Kg M EPA 8015 07/27/97
TPH as Diesel 34 1.0 mg/Kg M EPA 8015 07/28/97
aaa-Trifluorotoluene (8020 Surrogate) 104 % Recovery EPA 8020 07/27/97
aaa-Trifluorotoluene (Gasoline Surrogate) 82.4 % Recovery M EPA 8015 07/27/97
1-Chlorooctadecane (Diesel Surrogate) 94.3 % Recovery M EPA 8015 07/28/97
Approved By: Jl~i Kiff
720 Olive Drive, SuiteD Davis, CA95616 916-297-4~)
" KIFF
Report Number' 10282
I IANALYTICAL Date' 07~28~97
I Project Name' Beacon 596
Project Number' 1596.15
!
Sample: OTP-15'-E-M.P. Matrix: Soil
I Sample Date :07125107
Method
Measured Rep.erring Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
I Benzene < 0,020 0.020 mg/Kg . EPA 8020 07/27/97
Toluene 0.13 0.020 mg/Kg EPA 8020 07/27/97
i Ethylbenzene 0.10 0.020 mg/Kg EPA 8020 07/27/97
Total Xylenes 0.82 0.020 mg/Kg EPA 8020 07/27/97
Methyl-t-butyl ether 0.92 0.20 mg/Kg EPA 8020 07/27/97
I mg/Kg M EPA 8015 07/27/97
TPH
as
Gasoline
5.6
2.0
TPH as Diesel 19 1.0 rog/Kg M EPA 8015 07/28/97
I aaa-Trifluorotoluene (8020 Surrogate) 101 % Recovery EPA 8020 07/27/97
aaa-Trifluorotoluene (Gasoline Surrogate) 85.5 % Recovery M EPA 8015 07/27/97
I 1-Chlorooctadecane (Diesel Surrogate) 97.0 % Recovery M EPA 8015 07/28/97
I
I Approved By: ..~, Kiff 11 ._~
I 720 Olive Drive, Suite D Davis, CA 95616 916-297'4~0
mmmmmmmmmmmmmmmmmmm
Ultrimar Inc. / ~ c~ ~P~,- BEACON
CHAIN OF CUSTODY REPORT
Beacon Station No. Sampler (Print Name) Date/
Pro,~ No. 8a~na~ ~
Proj~ L~,~. - ~,~n ...... / ~
Sam~e No/Ide~ifimt~n Date Time Lah No. = ~ ~= ~ REMARKS
~ ~/~~-~. ~. - ~ / / / /
~uish~ by: (S~dAfiiliation) ~ate Time ~eib~ by: (S~natur~Afliliatio~ Date Time
;~~ ~~=~//~ F~ 7/,,-~ - . ............
Reli~uish~ by: (S~nalu{e/Affiliation) Date Ti~e Date Time
~eiv~ by: (S~natur~Affilialion)
Ro~n
To:~ ~~ lil~to: ULTRAMAR INC.
~~ ~ 525 West Third Street
~ Hanford, CA 932~
~ITE: Return to Client with Re~d YELLOW: Laborato~ Copy PINK: Originator Copy
I
I
I
I
I Appendix D
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Date · 08~06~97
CAI_
I LLC
!
I Gary Barker
Horizon Environmental Inc.
5011 Golden Foothill Pkwy., Suite 7
. El Dorado Hills, CA 95762
,I
Subject · Analysis of 5 Soil Samples
I Project Name · Beacon 596
Project Number' 1596.15
Dear Mr. Barker,
Chemical analysis of the samples referenced above has been completed. Summaries of the data are contained
on the following pages. Sample(s) were received under documented chain-of-custody. US EPA protocols for
sample storage and preservation were followed.
Kiff Analytical is certified by the State of California (# 2236). If you have any questions regarding procedures
or results, please call me at 916-297-4800.
Sincerely,
720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
~ANALYT~CALLLc Date' 08/06/97
Project Name' Beacon 596
Project Number' 1596.15
Sample: CSP-A,B,C,D Matrix: Soil
Sample Date :08/04/97
Method
· Measured Reporting Analysis Date
Parameter Value Limit Units Metl-iod Analyzed
Benzene < 0.0050 0.0050 mg/Kg EPA 8020 08/05/97
Toluene < 0.0050 0.0050 mg/Kg EPA 8020 08/05/97
Ethylbenzene < 0.0050 0.0050 mg/Kg EPA 8020 08/05/97
Total Xylenes < 0.0050 0.0050 mg/Kg EPA 8020 08/05/97
Methyl-t-butyl ether < 0.050 0.050 mg/Kg EPA 8020 08/05/97
TPH as Gasoline < 1.0 1.0 rog/Kg M EPA 8015 08/05/97
TPH as Diesel 22 1.0 mg/Kg M EPA 8015 08/05/97
aaa-Trifluorotoluene (8020 Surrogate) 95.2 % Recovery EPA 8020 08/05/97
aaa-Trifluorotoluene (Gasoline Surrogate) 74.4 % Recovery M EPA 8015 08/05/97
1-chlorooctadecane (Diesel Surrogate) 87.5 % Recovery M EPA 8015 08/05/97
Sample: CSP-E,F,G,H Matrix: Soil
Sample Date :08/04/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
Benzene < 0.0050 0.0050 mg/Kg EPA 8020 08/05/97
Toluene < 0.0050 0.0050 mg/Kg EPA 8020 08/05/97
Ethylbenzene < 0.0050 0.0050 rog/Kg EPA 8020 08/05/97
Total Xylenes < 0.0050 0.0050 mg/Kg EPA 8020 08~05/97
Methyl-t-butyl ether < 0.050 0.050 mg/Kg EPA 8020 08/05/97
TPH as Gasoline < 1.0 1.0 mg/Kg M EPA 8015 08/05/97
TPH as Diesel 35 1.0 mg/Kg M EPA 8015 08/05/97
aaa-Trifluorotoluene (8020 Surrogate) 96.5 % Recovery EPA 8020 08/05/97
aaa-Trifluorotoluene (Gasoline Surrogate) 74.2 % Recovery M EPA 8015 08/05/97
1-chlorooctadecane (Diesel Surrogate) 91.7 % Recovery M EPA 8015 08/05/97
I
I Approved By: /.Jl"e, Kiff-- .----
720 Olive Drive, Suite D Davis, CA 95616 916-297-~,8~0
I ~'/
KIFF
Report Number' 10317
I ''AJVAIY"rlCA~L~c Date' 08/06/97
Project Name · Beacon 596
Project Number' 1596.15
Sample: CSP-I,J,K,L Matrix: Soil
Sample Date :08/04/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units MetHod Analyzed
< 0.0050 0.0050 mg/Kg EPA 8020 08/05/97
Benzene
Toluene < 0.0050 0.0050 rog/Kg EPA 8020 08/05/97
Ethylbenzene < 0.0050 0.0050 mg/Kg EPA 8020 08/05/97
Total Xylenes < 0.0050 0.0050 mg/Kg EPA 8020 08/05/97
Methyl-t-butyl ether < 0.050 0.050 mg/Kg EPA 8020 08/05/97
TPH as Gasoline < 1.0 1.0 mg/Kg M EPA
801
5
08/05/97
TPH as Diesel 84 1.0 mg/Kg M EPA 8015 08/06/97
aaa-Trifluorotoluene (8020 Surrogate) 96.9 % Recovery EPA 8020 08/05/97
aaa-Trifluorotoluene (Gasoline Surrogate) 74.9 % Recovery M EPA 8015 08/05/97
1-chlorooctadecane (Diesel Surrogate) 96.1 % Recovery M EPA 8015 08/06/97
Sample' CSP-M,N,O,P Matrix' Soil
Sample Date :08/04/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl-iod Analyzed
Benzene < 0.0050 0.0050 mg/Kg EPA 8020 08/05/97
Toluene < 0.0050 0.0050 mg/Kg EPA 8020 08/05/97
mg/Kg EPA 8020 08/05/97
Ethylbenzene
0.OO50
0.0050
Total Xylenes < 0.0050 0.0050 mg/Kg EPA 8020 08/05/97'
Methyl.t-butyl ether < 0.050 0.050 mg/Kg EPA 8020 08/05/97
TPH as Gasoline < 1.0 1.0 mg/Kg M EPA 8015 08/05/97
TPH as Diesel 190 1.0 mg/Kg M EPA 8015 08/06/97
aaa-Trifluorotoluene (8020 Surrogate) 96.6 % Recovery EPA 8020 08/05/97
aaa-Trifluorotoluene (Gasoline Surrogate) 74.0 % Recovery M EPA 8015 08/05/97
% Recovery M EPA 8015 08/06/97
1
(Diesel
Surrogate)
1
01
I
I Approved By:
I 720 Olive Drive. Suite D Davis, CA 95616916-297-4~(,00
I KiFF Report Number' 10317
I I~ANALY'7'~C,~.~ Date' 08/06/97
Project Name' Beacon 596
I Project Number' 1596.15
I
Sample' CSP-Q,R,S,T Matrix' Soil
I Sample Date :08/04/97
Method
Measured . Reporting _Analysis Date
Parameter Value Limit Units Method Analyzed
I Benzene < 0.0050 0.0050 mg/Kg EPA 8020 08/06/97
Toluene < 0.0050 0.0050 mg/Kg EPA 8020 08/06/97
Ethylbenzene < 0.0050 0.0050 rog/Kg EPA 8020 08/06/97
I Total Xylenes < 0.0050 0.0050 rog/Kg EPA 8020 08/06/97
Methyl-t-butyl ether < 0.050 0.050 m§/Kg EPA 8020 08/06/97
I TPH as Gasoline < 1.0 1.0 mg/Kg M EPA 8015 08/06/97
TPH as Diesel 93 1.0 mg/Kg M EPA 8015 08/06/97
~ I aaa-Trifluorotoluene (8020 Surrogate) 97.3 % Recovery EPA 8020 08/06/97
I aaa-Trifluorotoluene (Gasoline Surrogate) 75.6 % Recovery M EPA 8015 08/06/97
1-chlorooctadecane (Diesel Surrogate) 98.8 % Recovery M EPA 8015 08/06/97
I
,I
720 Olive Drive, Suite D Davis, CA 95616 916-297~8.00
I
U~amar Ino. / /~ ~ / 7' BEACON
CHAIN OF CUSTODY REPORT
Beacon Station No. Sampler (Print Name)"' I Form No. /
Project Localion f ~-JlJll~tion _~' ~ _=. .-~ E
- II
Sample No./Identitication Date Time Lab No. m -- z REMARKS
C_..S~ ... Ell.., ,,e., .~., T" ,~ ....- 05" ~ '" '"' ~ Y ,-',~,,~,,~.r, ~
Relinquis~ by: (Signature/Affiliation) Date Time Rec._~eived by: (Sigr~alure/Affilialion! .... Date Time
~.~nquishod blt: {$ignat.~Affiliation) 'Date limo Received by: {SignaturetAffiliation) Date lime
Relinquish~l by: {SignaturotAffiliation) Date lime I:~ived blt: {Si0naturetAffiliation) Date lime
' ' Bi~l'i~: UklRAMJi R INC.
Report To: ~,~,,~_~..,.~::~,,~~ /} 525 West Third Street
/~..~ ~ I} Hanford, CA 9323~0~,
~ ^ttention: ~,~,~-~ ~
WH~IE: Return to Client wilh Report ¥[t. kOW: Laboratory Coplt PI~K: Originator Copy ~.,~,, ,~
I IFF Report Number' 10430
I IANALYTICAL Date' 09/14/97
LLC
Gary Barker
Horizon Environmental Inc.
5011 Golden Foothill Pkwy., Suite 7
El Dorado Hills, CA 95762
Subject' Analysis of 2 Soil Samples
Project Name * Beacon 596
Project Number - 1596.15
Dear Mr. Barker,
Chemical analysis of the samples referenced above has been completed. Summaries of the data are contained
on the following pages. Sample(s) were received under documented chain-of-custody. US EPA protocols for
sample storage and preservation were followed.
Kiff Analytical is certified by the State of California (# 2236). If you have any questions regarding procedures
or results, please call me at 916-297-4800.
Sincerely,
'J4~el Kiff ' '
-/
I
i 720 Olive Drive, Suite D Davis, CA 95616 916-297-4800 --
Project Name · Beacon 596
Project Number' 1596.1 5
Sample' S-0905-PL2 Matrix' Soil
Sample Date :0@/05/97
Method
Parameter Measured R_eportin9 Analysis Date
Value Limit Units Method Analyzed
< 0.0050 0.0050 mg/Kg EPA 8020 09/10/97
Benzene
Toluene < 0.0050 0.0050 mg/Kg EPA 8020 09/10/97
Ethylbenzene < 0.0050 0.0050 mg/Kg EPA 8020 09/10/97
Total Xylenes < 0.0050 0.0050 mg/Kg EPA 8020 09/10/97
Methyl-t-butyl ether < 0.050 0.050 mg/Kg EPA 8020 09/10/97
TPH as Gasoline < 1.0 1.0 mg/Kg M EPA 8015
09/10/97
aaa-Trifluorotoluene (8020 Surrogate) 97.3 % Recovery EPA 8020 09/10/97
aaa-Trifluorotoluene (Gasoline Surrogate) 88.0 % Recovery M EPA 8015 09/10/97
I Sample' S-0905-PL6 Matrix- Soil
Sample Date :09/05/97
Method
I Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 0.0050 0.0050 mg/Kg EPA 8020 09/10/97
i Toluene < 0.0050 0.0050 rog/Kg EPA 8020 09/10/97
Ethylbenzene < 0.0050 0.0050 rog/Kg EPA 8020 09/10/97
Total Xylenes < 0.0050 0.0050 mg/Kg EPA 8020 09/10/97
i Methyl-t-butyl ether < 0.050 0.050 mg/Kg EPA 8020 09/10/97
TPH as Gasoline ¢ 1.0 1.0 rog/Kg M EPA 8015 09/10/97
I aaa-Trifluorotoluene (8020 Surrogate) 96.6 % Recovery EPA 8020 09/10/97
aaa-Trifluorotoluene (Gasoline Surrogate) 87.8 % Recovery M EPA 8015 09/10/97
!
I
I
I Approved By: Jo~J Kiff
i 720 Olive Drive, Suite D Davis, CA 95616 916-297-48 -
Ullrammr Ino.
BEACON
CHAIN OF CUSTODY REPORT //
~7~~-'~,~, ~~ ~s~ ~0 I?':,"°'/
'
~ 0
~l~lt ~oll~e~titi~l~ Ollt Time Lab No. m ~ ~ z ~EMA~K8
, Roll__alien) Date Time R.oiv~ by: {S~nalur,A.ilialion) /~/ Dale Time
Relinquish~ by: (Signalur~Affilialion) ~le Time~ R~eiv~ by:~nalure/Aflilialion)
Reli~uish~ by: (Signalure/Alfilialioq) / Dale Time R~v~ by: (S~nalure/Aflilialion) Date Time
Repo.'o: ~7 g ~'k*; ~~ ~ ~il' Io:/ ULTRA'AR INC.
/ 525 West Third Street .
~ ~f Attention:
~ ~rn 9nl ~. .OW: Laboralo~ Copy PINK: Originalor Copy
Date · 08~03~97
!
Gary Barker
Horizon Environmental Inc.
5011 Golden Foothill Pkwy., Suite 7
El Dorado Hills, CA 95762
Subject: Analysis of 9 Soil Samples
Project Name · Beacon 596
Project Number' 1596.15
Dear Mr. Barker,
Chemical analysis of the samples referenced above has been completed. Summaries of the data are contained
on following pages. Sample(s) were chain-of-custody. LIS I::PA protocols for
the
received
under
documented
sample storage and preservation were followed.
Kiff Analytical is certified by the State of California (# 2236). If you have any questions regarding procedures
or results, please call me at 916-297-4800.
Sincerely,
Joel Kiff
720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
KIFF Report Number · 10292
I IANALYTICALLLc Date' 08/03/97
I P
roject Name' Beacon 596
Project Number: 1596.15
!
Sample: DSP-A,B,C,D-S Matrix: Soil
I Sample Date :08/01/97 Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl-iod Analyzed
I Benzene < 0.020 0.020 mg/Kg EPA 8020 08/02/97
Toluene 0.22 0.020 mg/Kg EPA 8020 08/02/97
i Ethylbsnzene 0.12 0.020 mg/Kg EPA 8020 08/02/97
Total Xylenes 0.62 0.020 rog/Kg EPA 8020 08/02/97
Methyl-t-butyl ether < 2.0 2.0 rog/Kg EPA 8020 08/02/97
I TPH as Gasoline 20 2.0 mg/Kg M EPA 8015 08/02/97
TPH as Diesel 240 1.0 rog/Kg M EPA 8015 08/03/97
I TPH as Motor Oil < 100 10 mg/Kg M EPA 8015 08/03/97
aaa-Trifluorotoluene (8020 Surrogate) 103 % Recovery EPA 8020 08/02/97
i aaa-Trifluorotoluene (Gasoline Surrogate) 83.8 % Recovery M EPA 8015 08/02/97
1-chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 08/03/97
I Sample' DSP-E,F,G,H-S Matrix' Soil
Sample Date :08/01/97
I Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
Benzene < 0.020 0.020 mg/Kg EPA 8020 08/02/97
I < 0.020 0.020 EPA 8020 08/02/97
Toluene
mg/Kg
Ethylbenzene 0.41 0.020 rog/Kg EPA 8020 08/02/97
Total Xylenes 2.6 0.020 mg/Kg EPA 8020 08/02/97
I < 2.0 2.0 mg/Kg EPA 8020 08/02/97
Methyl-t-butyl
ether
TPH as Gasoline 53 2.0 mg/Kg M EPA 8015 08/02/97
I TPH as Diesel 770 1.0 mg/Kg M EPA 8015 08/03/97
TPH as Motor Oil < 100 10 rog/Kg M EPA 8015 08/03/97
I aaa-Trifluorotoluene (8020 Surrogate) 101 Recovery
%
EPA
8020
08/02/97
aaa-Trifluorotoluene (Gasoline Surrogate) 86.5 % Recovery M EPA 8015 08/02/97
1-chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 08/03/97
!
I Joel Kiff I
Approved
By:
720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
i KiFF Report Number · 10272
Date · 07/25/97
Gary Barker
Horizon Environmental Inc.
5011 Golden Foothill Pkwy., Suite 7
El Dorado Hills, CA 95762
Subject · Analysis of 7 Soil Samples
Project Name · Beacon 596
Project Number' 1596.15
Dear Mr. Barker,
Chemical analysis of the samples referenced above has been completed. Summaries of the data are contained
on the following pages. Sample(s) were received under documented chain-of-custody. US EPA protocols for
sample storage and preservation were followed.
Kiff Analytical is certified by the State of California (# 2236). If you have any questions regarding procedures
or results, please call me at 916-297-4800.
Sincerely,
Kiff~
I
720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
KIFF
I Project Name' Beacon 596
Project Number' 1596.15
I
Sample. DSP-A,B,C,D Matrix' Soil
I Sample Date :07/24/97
Method
Measured R_eporting _An_ alysis Date
Parameter Value Limit Units Metl'iod - Analyzed
I Benzene < 2,0 2,0 mg/Kg - EPA 8020 07/25/97
Toluene 14 2,0 mg/Kg EPA 8020 07/25/97
i Ethylbenzene 30 2,0 mg/Kg EPA 8020 07/25/97
Total Xylenes 220 2,0 mg/Kg EPA 8020 07/25/97
Methyl-t,butyl ether < 20 20 mg/Kg EPA 8020 07/25/97
I TPH as Gasoline 1400 20 mg/Kg M EPA 8015 07/25/97
TPH as Diesel 3200 1.0 mg/Kg M EPA 8015 07/24/97
I aaa-Trifluorotoluene (8020 Surrogate) 101 % Recovery EPA 8020 07/25/97
aaa-Trifluorotoluene (Gasoline Surrogate) 88.7 % Recovery M EPA 8015 07/25/97
i 1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/24/97
I Sample' DSP-E,F,G,H Matrix' Soil
Sample Date :07/24/97
Method
I Measured Rep.orting Analysis Date
Parameter Value Limit Units Mettioo Analyzed
Benzene < '1.0 1.0 rog/Kg EPA 8020 07/24/97
i Toluene 3.4 1.0 mg/Kg EPA 8020 07/24/97
Ethylbenzene 5.2 1.0 rog/Kg EPA 8020 07/24/97
Total Xylenes 32 1.0 mg/Kg EPA 8020 07/24/97
i Methyl-t-butyl ether < 10 10 mg/Kg EPA 8020 07/24/97
TPH as Gasoline 380 10 mg/Kg M EPA 8015 07/24/97
I TPH as Diesel 1600 1,0 mg/Kg M EPA 8015 07/24/97
aaa-Trifluorotoluene (8020 Surrogate) 104 % Recovery . EPA 8020 07/24/97
i aaa-Trifluorotoluene (Gasoline Surrogate) 85,1 % Recovery M EPA 8015 07/24/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/24/97
I
!
I 720 Olive Drive, Suite D Davis, CA 95616 916-297-481~
KIFF
Report Number. 10272
IANALYTICA Date' 07/25/97
Project Name' Beacon 596
Project Number' 1596.15
Sample' DSP-I,J,K,L Matrix' Soil
Sample Date :07/24/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
Benzene < 1,0 1,0 mg/Kg - EPA 8020 07/24/97
Toluene 6,0 1,0 mg/Kg EPA 8020 07/24/97
Ethylbenzene 44 1.0 mg/Kg EPA 8020 07/24/97
Total Xylenes 92 1.0 rog/Kg EPA 8020 07/24/97
Methyl-t-butyl ether < 10 1'0 mg/Kg EPA 8020 07/24/97
TPH as Gasoline 700 10 rog/Kg M EPA 8015 07/24/97
TPH as Diesel 1700 1.0 mg/Kg M EPA 8015 07/24/97
aaa-Trifluorotoluene (8020 Surrogate) 97.8 % Recovery EPA 8020 07/24/97
aaa-Trifluorotoluene (Gasoline Surrogate) 85.5 % Recovery M EPA 8015 07/24/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/24/97
Sample' DSP-M,N,O,P Matrix' Soil
Sample Date :07/24/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 1.0 1.0 rog/Kg EPA 8020 07/24/97
Toluene 9.7 1.0 mg/Kg EPA 8020 07/24/97
Ethylbenz®ne 18 1.0 mg/Kg EPA 8020 07/24/97
Total Xyle~les 120 1.0 mg/Kg EPA 8020 07/24/97
Methyl-t-butyl ether < 10 10 mg/Kg EPA 8020 07/24/97
TPH as Gesoline 880 10 mg/Kg M EPA 8015 07/24/97
TPH as Diesel 4500 1.0 mg/Kg M EPA 8015 07/25/97
aaa-Trifluorotoluene (8020 Surrogate) 97.8 % Recovery EPA 8020 07/24/97
aaa-Trifluorotoluene (Gasoline Surrogate) 88.4 % Recovery M EPA 8015 07/24/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/25/97
72.0 Olive Drive, Suite D Davis, CA 95616 916-297-48~0~
I(IFF
Report Number' 10272
I 'AJlVAIYT'ICALLLc Date' 07/25/97
I Project Name' Beacon 596
Project Number' 1596.1 5
I
Sample: DSP-Q,R,S,T Matrix: Soil
I Sample Date :07/24/97
Method
Measured Reporting Analysis Date
I Parameter Value Limit Units Method Analyzed
Benzene < 1.0 1.0 mg/Kg EPA 8020 07/24/97
Toluene 4.3 1.0 mg/Kg EPA 8020 07/24/97
i Ethylbenzene 12 1.0 mg/Kg EPA 8020 07/24/97
Total Xylenes 82 1.0 mg/K§ EPA 8020 07/24/97
Methyl-t-butyl ether < 10 10 mg/Kg EPA 8020 07/24/97
I mg/Kg M EPA 8015 07/24/97
TPH
as
Gasoline
63O
10
TPH as Diesel 2800 1.0 mg/Kg M EPA 8015 07/25/97
I aaa-Trifluorotoluene (8020 Surrogate) 100 % Recovery EPA 8020 07/24/97
aaa-Trifluorotoluene (Gasoline Surrogate) 85.6 % Recovery M EPA 8015 07/24/97
i 1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/25/97
I Sample- DSP-U,V,W,X Matrix' Soil
Sample Date :07/24/97
Method
i Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 1.0 1.0 mg/Kg EPA 8020 07/25/97
Toluene 8.4 1.0 mg/Kg EPA 8020 07/25/97
I 1.0 mg/Kg EPA 8020 07/25/97
Ethylbenzene
1
8
Total Xylenes 120 1.0 mg/Kg EPA 8020 07/25/97
Methyl-t-butyl ether < 10 10 mg/Kg EPA 8020 07/25/97
I TPH as Gasoline 910 10 mg/Kg M EPA 8015 07/25/97
i TPH as Diesel 4100 1.0 mg/Kg M EPA 8015 07/25/97
aaa-Trifluorotoluene (8020 Surrogate) 103 % Recovery EPA 8020 07/25/97
aaa-Trifluorotoluene (Gasoline Surrogate) 88.4 % RecoverY M EPA 8015 07/25/97
I Surrogate) Diluted Out % Recovery M EPA 8015 07/25/97
1
(Diesel
I
I Appr°ved BY:Kiff
i 720 Olive Drive, Suite D Davis, CA 95616 916-297-48~O
Report Number ' 10272
I tANALYTICAL Date' 07/25/97
LLC
I Project Name' Beacon 596
Project Number' 1596.15
I
Sample' DI-15'-NE Matrix' Soil
I Sample Date :07/24/97
Method
- Measured Reporting .Analysis Date
Parameter Value Limit Units Method Analyzed.
I Benzene < 0.0050 0.0050 mg/Kg EPA 8020 07/25/97
Toluene < 0.0050 0.0050 mg/Kg EPA 8020 07/25/97
Ethylbenzene < 0.0050 0.0050 rog/Kg EPA 8020 07/25/97
I Total Xylenes < 0.0050 0.0050 mg/Kg EPA 8020 07/25/97
Methyl-t-butyl ether 0.31 0.050 mg/Kg EPA 8020 07/25/97
I TPH as Gasoline < 0.50 0.50 mg/Kg M EPA 8015 07/25/97
TPH as Diesel < 1.0 1.0 rog/Kg M EPA 8015 07/25/97
I aaa-Trifluorotoluene (8020 Surrogate) 104 % Recovery EPA 8020 07/25/97
aaa-Trifluorotoluene (Gasoline Surrogate) 83.2 % Recovery M EPA 8015 07/25/97
i 1-Chlorooctadecane (Diesel Surrogate) 97.0 % Recovery M EPA 8015 07/25/97
I
I Approved By:
I 720 Olive Drive, Suite D Davis, CA 95616 916-297-48~/Q
UIImmir Irm. BEAOON
CHAIN OF CUSTODY REPORT
Beacon Station No. Sampler (Pdnt Name) D e
Project No. Sampler (S_ignature)
Sample No./Identification Date Time Lab No. 33~ - z REMARKS
.. Rel~~~a... tion} ~~ ~~at~ lime ~iv~ b~: {Si~natur~gffilialion) ~ato lime
~uis~'~ by: (~n~Affiliation) 'D~(e/ Time R~eiv~ by: (S~natur~Affiliation) ............... Date Time
R~uish~.by: (S~natur~Affiliation) Date Ti.~e ~eiv~ by: (S~nature/Affiliation) Date Time
. . ~__ LT R INC.
~ae~ To: ~.~. ~ 525 West Third Street
[ ] ~anford, CA 9323~
WHITE: Return to Client with Re~d YELLOW: Laborato~ Copy PINK: Ori~inalor Copy
I(IFF Report Number · 10269
Date · 07/24/97
I IANALYTICAL
LLC
I Gary Barker
Horizon Environmental Inc.
5011 Golden Foothill Pkwy., Suite 7
I El Dorado Hills, CA 95762
Subject · Analysis of 8 Composite Soil Sa~mples
I P
roject Name · Beacon 596
Project Number · 1596.15
I
Dear Mr. Barker,
I
Chemical analysis of the samples referenced above has been completed. Summaries of the data are contained
Ion the following pages. Sample(s) were received under documented chain-of-custody. US EPA protocols for
sample storage and preservation were followed.
I
Kiff Analytical is certified by the State of California (# 2236). If you have any questions regarding procedures
I or results, please call me at 916-297-4800.
Sincerely,
I
I
720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
I 7. v3
' KIFF
JANALYTICAL Report Number- 10269
LLC Date · 07/24/97 '
Subject · 8 Composite Soil Samples
Project Name · Beacon 596
Project Number · 1596.15
Case Narrative
Values for TPH as Gasoline for samples with high levels of Diesel are primarily due to Diesel-range
hydrocarbons that are detected by the TPH as Gasoline test procedure.
(.4'1
720 Olive Drive, Suite D Davis, CA 95616 916-297-48~J
'I(IFF Report Number · 10269
Project Name · Beacon 596
Project Number: 1596.15
Sample: DSP-A,B,C,D Matrix: Soil
Sample Date :07/23/97
Method
Measured Reporting .A_~alysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 2.0 2.0 rog/Kg EPA 8020 07/23/97
Toluene < 2.0 2.0 mg/Kg EPA 8020 07/23/97
Ethylbenzene < 2.0 2.0 mg/Kg EPA 8020 07/23/97
Xylenes < 2.0 2.0 rog/Kg EPA 8020 07/23/97
Total
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/23/97
TPH as Gasoline 130 20 mg/Kg M EPA 8015 07/23/97
TPH as Diesel 3300 100 mg/Kg M EPA 8015 07/24/97
aaa-Trifluorotoluene (8020 Surrogate) 104 % Recovery EPA 8020 07/23/97
aaa-Trifluorotoluene (Gasoline Surrogate) 85.1 % Recovery M EPA 8015 07/23/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/24/97
Sample' DSP-E,F,G,H Matrix'Soil
Sample Date :07/23/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl-iod Analyzed
Benzene < 2.0 2.0 mg/Kg EPA 8020 07/23/97
Toluene < 2.0 2.0 mg/Kg EPA 8020 07/23/97
mg/Kg EPA 8020 07/23/97
Ethylbenzene
2.0
2.0
Total Xylenes · 2.0 2.0 rog/Kg EPA 8020 07/23/97
Methyl-t-butyl ether < 20 20 rog/Kg EPA 8020 07/23/97
TPH as Gasoline 100 20 mg/Kg M EPA 8015 07/23/97
TPH as Diesel 3100 100 mg/Kg M EPA 8015 07/24/97
aaa-Trifluorotoluene (8020 Surrogate) 104 % Recovery EPA 8020 07/23/97
aaa-Trifluorotoluene (Gasoline Surrogate) 84.5 % Recovery M EPA 8015 07/23/97
(Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/24/97
1
I
i 720 Olive Drive, Suite D Davis, CA 95616 916-297-48~0
'KIFF Report Number - 10269
Project Name' Beacon 596
Project Number' 1596.15
Sample: DSP-I,J,K,L Matrix: Soil
Sample Date :07/23/97
Method
Measured Reporting .Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 2.0 2.0 rog/Kg EPA 8020 07/23/97
Toluene < 2.0 2.0 rog/Kg EPA 8020 07/23/97
Ethylbenzene < 2.0 2,0 rog/Kg EPA 8020 07/23/97
Total Xylenes < 2.0 2.0 rog/Kg EPA 8020 07/23/97
Methyl-t-butyl ether < 20 20 rog/Kg EPA 8020 07/23/97
TPH as Gasoline 47 20 mg/Kg M EPA 8015 07/23/97
TPH as Diesel 980 100 mg/Kg M EPA 8015 07/23/97
aaa-Trifluorotoluene (8020 Surrogate) 105 % Recovery EPA 8020 07/23/97
aaa-Trifluorotoluene (Gasoline Surrogate) 83.3 % Recovery M EPA 8015 07/23/97
1-Chlorooctadecane (Diesel Surrogate) Diluted out % Recovery M EPA 8015 07/23/97
Sample' DSP-M,N,O,P Matrix' Soil
Sample Date :07/23/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 2.0 2.0 rog/Kg EPA 8020 07/23/97
Toluene < 2.0 2.0 mg/Kg EPA 8020 07/23/97
Ethylbenzene < 2.0 2.0 mg/Kg EPA 8020 07/23/97
Total Xylenes < 2.0 2.0 mg/Kg EPA 8020 07/23/97
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/23/97
TPH as Gasoline 64 20 mg/Kg M EPA 8015 07/23/97
TPH as Diesel 1400 100 mg/Kg M EPA 8015 07/24/97
aaa-Trifluorotoluene (8020 Surrogate) 103 % Recovery EPA 8020 07/23/97
aaa-Trifluorotoluene (Gasoline Surrogate) 83.0 % Recovery' M EPA 8015 07/23/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/24/97
I
I Approved By: Jo~i.Ki, V
i 720 Olive Drive, Suite D Davis, CA 95616 916-297-480b]
Date · 07/24/97
Project Name' Beacon 596
Project Number' 1596.1 5
Sample: DSP-Q,R,S,T Matrix: Soil
Sample Date :07/23/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 2.0 2.0 mg/Kg EPA 8020 07/23/97
Toluene < 2.0 2.0 rog/Kg EPA 8020 07/23/97
Ethylbenzene < 2.0 2.0 mg/Kg EPA 8020 07/23/97
Total Xylenes < 2.0 2.0 mg/Kg EPA 8020 07/23/97
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/23/97
TPH as Gasoline 67 20 rog/Kg M EPA 8015 07/23/97
TPH as Diesel 1800 100 mg/Kg M EPA 8015 07/24/97
aaa-Trifluorotoluene (8020 Surrogate) 105 % Recovery EPA 8020 07/23/97
aaa-Trifluorotoluene (Gasoline Surrogate) 84.0 % Recovery M EPA 8015 07/23/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/24/97
Sample' GSP-A,B,C,D Matrix' Soil
Sample Date :07/23/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 2.0 2.0 mg/Kg EPA 8020 07/23/97
Toluene 7.3 2.0 mg/Kg EPA 8020 07/23/97
Ethylbenzene 17 2.0 EPA 8020
mg/Kg
07/23/97
Total Xylenes 140 2.0 mg/Kg EPA 8020 07/23/97
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/23/97
TPH as Gasoline 1100 20 rog/Kg M EPA 8015 07/23/97
aaa-Trifluorotoluene (8020 Surrogate) 101 % Recovery EPA 8020 07/23/97
aaa-Trifluorotoluene (Gasoline Surrogate) 86.7 % Recovery M EPA 8015 07/23/97
720 Olive Drive, Suite D Davis, CA 95616 916-297-48Q~
II(IFF
, I ~J~IJlV~4/VTltCALLLC Date' 07/24/97
I Project Name' Beacon 596
Project Number' 1596.15
I
Sample: GSP-E,F,G,H Matrix: Soil
I Sample :07/23/97
Date
Method
Measured Reporting Analysis Date
i Parameter Value Limit Units Method Analyzed
Benzene < 2.0 2.0 mg/Kg ' EPA 8020 07/24/97
Toluene < 2.0 2.0 mg/Kg EPA 8020 07/24/97
i Ethylbenzene 5.9 2.0 mg/Kg EPA 8020 07/24/97
Total Xylenes 39 2.0 mg/Kg EPA 8020 07/24/97
Methyl-t-butyl ether < 20 20 rog/Kg EPA 8020 07/24/97
I mg/Kg M EPA 8015 07/24/97
TPH
as
Gasoline
640
20
aaa-Trifluorotoluene (8020 Surrogate) 104 % Recovery EPA 8020 07/24/97
I aaa-Trifluorotoluene (Gasoline Surrogate) 84.2 % Recovery M EPA 8015 07/24/97
I Sample' GSP-I,J,K,L Matrix' Soil
Sample Date :07/23/97
Method
I Measured Reporting Analysis Date
Parameter Value Limit Units Mett-iod Analyzed
Benzene < 2.0 2.0 mg/Kg EPA 8020 07/24/97
i Toluene 9.5 2.0 mg/Kg EPA 8020 07/24/97
Ethylbenzene 22 2.0 mg/Kg EPA 8020 07/24/97
Total Xylenes 150 2.0 mg/Kg EPA 8020 07/24/97
i Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/24/97
TPH as Gasoline 1 '100 20 rog/Kg M EPA 8015 07/24/97
I aaa-Trifluorotoluene (8020 Surrogate) 101 % Recovery EPA 8020 07/24/97
aaa-Trifluorotoluene (Gasoline Surrogate) 86.7 % Recovery M EPA 8015 07/24/97
!
I
I
I Approved By: Joil~iff
i 720 Olive Drive, Suite D Davis, CA 95616 916-297-480~
Ultmmmr Ira:. BEACON
CHAIN OF CUSTODY REPORT / ~ ~/~ ~
Beacon Station No. Sampler (Print Name) D, pte; I Form No. /
~ ~ ANALYSES .~/~? of /
Sample No./Identificat__b_ n Date Time Lab No. []~- - :- REIdARKS
R~li~uis~y: ~S~hatur~Aftiliation) . Date Time R~eiv~ by: (S~natur~Affiliation) , ~ Date Time
~uish~ by: (S~n~A~liation)' Date Time R~eiv~ by: (S~natur~Affiliati~) Date Time
Reli~uish~ by: (Signatur~Afliliation) Date Time R~eiv~ by: (S~nature/Affiliation) Date Time
' ' ~ 525 West Third Street
Hanford, CA 9~2~
WHITE: Return to Client with Re~d YELLOW: Laboralo~ Copy PINK: O~ginalor Copy ~-~"'
Date · 07/23/97
IANALYTICAL
LLC
I Gary Barker
Horizon Environmental Inc.
5011 Golden Foothill Pkwy., Suite 7
El Dorado Hills, CA 95762
Subject: Analysis of 1 Soil Sample
Project Name · Beacon 596
Project Number · 1596.15
Dear Mr. Barker,
}
Ghemical analysis of the samples referenced above has been completed. Summaries of the data are contained
~i-- on the following pages. Sample{s) were received under documented chain-of-custody. LIS EPA protocols for
sample storage and preservation were followed.
Kiff Analytical is certified by the State of Galifomia {# 2236). If you have any questions re§ard}ng procedures
I or results, please'call me at 916-297-4800.
Sincerely,
I
720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
I(IFF Report Number · 10265
I IIANALYTICALLLc Date' 07/23/07
i Project Name' Beacon 596
Project Number' 1596.15
!
Sample' LPI-6' Matrix' Soil
I Sample Date :07/22/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl~od Analyzed
I 0.0050 mg/Kg · EPA 8020 07/23/97
Benzene
0.O050
Toluene < 0.0050 0.0050 rog/Kg EPA 8020 07/23/97
Ethylbenzene < 0.0050 0.0050 mg/Kg EPA 8020 07/23/97
I Total Xylenes < 0.0050 0.0050
rog/Kg
EPA
8020
07/23/97
Methyl-t-butyl ether < 0.050 0.050 mg/Kg EPA 8020 07/23/97
I TPH as Gasoline < 1.0 1.0 mg/Kg M EPA 8015 07/23/97
TPH as Diesel 1.8 1.0 mg/Kg M EPA 8015 07/23/97
i TPH as Motor Oil < 10 10 mg/Kg M EPA 8015 07/23/97
aaa-Trifluorotoluene (8020 Surrogate) 104 % Recovery EPA 8020 07/23/97
aaa-Trifluorotoluene (Gasoline Surrogate) 82.0 % Recovery M EPA 8015 07/23/97
I (Diesel Surrogate) 96.1 % Recovery M EPA 8015 07/23/97
1
I
I
I
I
I 720 Olive Drive, Suite D Davis, CA 95616 916-297-4~)
m m mm mmm m m m m m m mm m m ~mmm mm mm m --, m
Ul~lmlr Ino.
CHAIN OF CUSTODY REPORT / 0 Z ~ ~ BEACON
Beacon Station..~_~; ~ No' Sampler
Project Location
-
Sample NoYldenlification ' Date Time Lab No. :a- ~, z REMARKS
/
Roli~: {Signature/Affiliation) Date Time Rocoivod by: {Signatumt^fliliation) Dato Time
~uish~ by: (S~natur~A~n) Oato Time R~oiv~ by: (S~natum/Affiliation) Dale Time
~li~ui~h~..~ b~: {S~natumtgffiliafion) Dato Time ~~ by:~{S~naturo/~ffiliation) Dado Time
525 West Third Street
WHITE: Return to Client with Re~d YELLOW: Laboralo~ Copy PINK: Originator Copy
I(IFF Rep od Number · 10264
Date · 07/23/97
I
I Gary Barker
Horizon Environmental Inc.
5011 Golden Foothill Pkwy., Suite 7
I El Dorado Hills, CA 95762
Subject' Analysis of '~ 7 Soil Samples
I Project Name · Beacon 596
Project Number · 1596.15
Dear Mr. Barker,
Chemical analysis of the samples referenced above has been completed. Summaries of the data are contained
I on the following pages. Sample(s) were received under documented chain-of-custody. US EPA protocols for
sample storage and preservation were followed.
Kiff Analytical is certified by the State of California (# 2236). If you have any questions regarding procedures
i or results, please call me at 916-297-4800.
Sincerely,
I
I
I
I
720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
I
I(IFF
-~~.4-~.c~ DateRep°rt' Number:07/23/97 10264
Subject · 17 Soil Samples
Project Name' Beacon 596
Project Number: 1596.15
Case Narrative
Values for TPH as Gasoline for samples with high levels of Diesel are primarily due to Diesel-range
hydrocarbons that are detected by the TPH as Gasoline test procedure.
Approved By:~e, i~K ff ~
720 Olive Drive, Suite D Davis, CA 95616 916-297-z~0
I(IFF Report Number · 10264
I ~ANALYTICALLLc Date' 07/23/97
I Project Name' Beacon 596
Project Number' 1 596.15
!
Sample' GSP-A,B,C,D Matrix' Soil
I Sample Date :07/22/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
I 2.0 mg/Kg EPA 8020 07/22/97
Benzene
2,0
Toluene 2.1 2.0 rog/Kg EPA 8020 07/22/97
Ethylbenzene 16 2.0 rog/Kg EPA 8020 07/22/97
I mg/Kg EPA 8020 07/22/97
Total
Xylenes
81
2.0
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/22/97
'1 TPH as Gasoline 1400 20 mg/Kg M EPA 8015 07/22/97
aaa-Trifluorotoluene (8020 Surrogate) 132 % Recovery EPA 8020 07/22/97
i aaa-Trifluorotoluene (Gasoline Surrogate) 147 % Recovery M EPA 8015 07/22/97
I Sample' GTP-SW15'-E Matrix' Soil
Sample Date :07/22/97
Method
i Measured Reporting Analysis Date
Parameter Value Limit Units Mett-iod Analyzed
' Benzene < 0,0050 0.0050 rog/Kg EPA 8020 07/22/97
I Toluene < 0.0050 0.0050 rog/Kg EPA 8020 07/22/97
Ethylbenzene < 0,0050 0.0050 rog/Kg EPA 8020 07/22/97
Total Xylenes < 0,0050 0.0050 rog/Kg EPA 8020 07/22/97
Methyl-t-butyl ether < 0.050 0.050 rog/Kg EPA 8020 07/22/97
I TPH as Gasoline < 1,0 1.0 rog/Kg M EPA 8015 07/22/97
I aaa-Trifluorotoluene (8020 Surrogate) 104 % Recovery EPA 8020 07/22/97
aaa-Trifluorotoluene (Gasoline Surrogate) 82.8 % Recovery M EPA 8015 07/22/97
I
I
720 Olive Drive, Suite D Davis, OA 9§818 918-297-~81~0
I(IFF Report Number · 10264
'1 ~ANALYT/CALLLc Date' 07/23/07
Project Name' Beacon 596
I Project Number' 1596.15
Sample: DSP-A,B,C,D Matrix: Soil
Sample Date :07/22/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 2,0 2.0 mg/Kg EPA 8020 07/23/97
Toluene < 2.0 2.0 mg/Kg EPA 8020 07/23/97
Ethylbenzene < 2,0 2.0 mg/Kg EPA 8020 07/23/97
Total Xylenes < 2.0 2.0 mg/Kg EPA 8020 07/23/97
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/23/97
TPH as Gasoline 450 20 rog/Kg M EPA 8015 07/23/97
TPH as Diesel 2100 200 mg/Kg M EPA 8015 07/23/97
aaa-Trifluorotoluene (8020 Surrogate) 130 % EPA 8020
Recovery
07/23/97
aaa-Trifluorotoluene (Gasoline Surrogate) 106 % Recovery M EPA 8015 07/23/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/23/97
Sample: DSP-E,F,G,H Matrix: Soil
Sample Date :07/22/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Mettiod Analyzed
Benzene < 2.0 2.0 mg/Kg EPA 8020 07/23/97
Toluene < 2.0 2.0 mg/Kg EPA 8020 07/23/97
Ethylbenzene < 2.0 2.0 mg/Kg EPA 8020 07/23/97
Total Xylenes < 2.0 2.0 mg/Kg EPA 8020 07/23/97
Methyl.t.butyl ether < 20 20 mg/Kg EPA 8020 07/23/97
TPH as Gasoline 390 20 rog/Kg M EPA 8015 07/23/97
TPH as Diesel 2700 200 mg/Kg M EPA 8015 07/23/97
aaa-Trifluorotoluene (8020 Surrogate) 129 % Recovery EPA 8020 07/23/97
aaa-Trifluorotoluene (Gasoline Surrogate) 106 % Recovery M EPA 8015 07~23~97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out %
Recovery
M
EPA
801
5
07/23/97
I Approved By: J/ ,I Ki~ff ~
i 720 Olive Drive, Suite D Davis, CA 95616 916-297-4~
I(IFF Report Number · 10264
I IANALYTICAL Date' 07/23/97
LLC
I Project Name · Beacon 596
Project Number' 1596.15
!
Sample: DSP-I,J,K,L Matrix: Soil
I Sample Date :07/22/97
Method
Measured Reporting- Analysis Date
Parameter Value Limit Units Method Analyzed
I-
· Benzene < 2.0 2.0 rog/Kg EPA 8020 07/23/97
Toluene < 2.0 2.0 rog/Kg EPA 8020 07/23/97
Ethylbenzene < 2,0 2.0 mg/Kg EPA 8020 07/23/97
I Total Xylenes < 2,0 2.0
mg/Kg
EPA
8020
07/23/97
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/23/97
I TPH as Gasoline 220 20 mg/Kg M EPA 8015 07/23/97
TPH as Diesel 1600 200 mg/Kg M EPA 8015 07/23/97
I (8020 Surrogate) 129 % Recovery EPA 8020 07/23/97
aaa-mrifluorotoluene
aaa-Trifluorotoluene (Gasoline Surrogate) 107 % Recovery M EPA 8015 07/23/97
i 1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/23/97
Sample: DSP-M,N,O,P Matrix: Soil
I Sample Date :07/22/97
Method
Measured Reporting Analysis Date
I Parameter Value Limit Units Method Analyzed
Benzene < 0.50 0.50 mg/Kg EPA 8020 07/23/97
Toluene c 0.$0 0.50 mg/Kg EPA 8020 07/23/97
I Ethylbenzene < 0,50 0.50 rog/Kg EPA 8020 07/23/97
Total Xylenes < 0.50 0.50 mg/Kg EPA 8020 07/23/97
Methyl-t-butyl ether < 5.0 5.0 mg/Kg EPA 8020 07/23/97
I TPH as Gasoline 16 5.0 mg/Kg M EPA 8015 07/23/97
i TPH as Diesel 1300 200 mg/Kg M EPA 8015 07/23/97
TPH as Motor Oil < 500 500 mg/Kg M EPA 8015 07/23/97
aaa-Trifluorotoluene (8020 Surrogate) 105 % Recovery' EPA 8020 07/23/97
I aaa-Trifluorotoluene (Gasoline Surrogate) 83.6 % Recovery M EPA 8015 07/23/97
1-chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/23/97
I Approved By: J~t Kiff
720 Olive Drive, Suite D Davis, CA 95616 916-297-41~0d
KIFF
Report Number' 10264
IANALYTIGAL Date' 07/23/97
LLC
Project Name: Beacon 596
Project Number: 1596.15
Sample: PLA-2' Matrix: Soil
Sample :07/22/97
Date
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed-
Benzene < 5.0 5.0 rog/Kg EPA 8020 07/23/97
Toluene < 5.0 5.0 mg/Kg EPA 8020 07/23/97
Ethylbenzene < 5.0 5.0 rog/Kg EPA 8020 07/23/97
Total Xylenes 13 5.0 mg/Kg EPA 8020 07/23/97
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/23/97
mg/Kg M EPA 8015 07/23/97
TPH
as
Gasoline
540
20
TPH as Diesel 19000 200 mg/Kg M EPA 8015 07/22/97
aaa-Trifluorotoluene (8020 Surrogate) 101 % Recovery EPA 8020 07/23/97
aaa-Trifluorotoluene (Gasoline Surrogate) 85.8 % Recovery M EPA 8015 07/23/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/22/97
I Sample' PLA-6' Matrix' Soil
Sample Date :07/22/97
Method
I Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 2.0 2.0 mg/Kg EPA 8020 07/22/97
Toluene < 2.0 2.0 mg/Kg EPA 8020 07/22/97
I Ethylbenzene < 2.0 2.0 mg/Kg EPA 8020 07/22/97
Total Xylenes 6.8 2.0 rog/Kg EPA 8020 07/22/97
Methyl-t-butyl ether < 20 20 rog/Kg EPA 8020 07/22/97
I TPH as Gasoline 280 20 mg/Kg M EPA 8015 07/22/97
i TPH as Diesel '~ 1000 100 rog/Kg M EPA 8015 07/23/97
aaa-Trifluorotoluene (8020 Surrogate) 102 % Recovery. EPA 8020 07/22/97
aaa-Trifluorotoluene (Gasoline Surrogate) 86.8 % Recovery M EPA 8015 07/22/97
I (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/23/97
1
I
I 720 Olive Drive, Suite D Davis, CA 95616 916-297-~4~800
I(IFF Report Number' 10264
i Project Name' Beacon 596
Project Number' 1596.15
I
Sample' PLA-15' Matrix' Soil
I Sample Date :07/22/97
Method
Parameter Measured Reporting _Analysis Date
Value Limit Units Method Analyzed
I 2.0 2.0 mg/Kg EPA 8020 07/22/97
Benzene
Toluene < 2,0 2,0 rog/Kg EPA 8020 07/22/97
Ethylbenzene < 2,0 2.0 rog/Kg EPA 8020 07/22/97
I 2.0 rog/Kg EPA 8020 07/22/97
Total
Xylenes
6,2
Methyl-t-butyl ether < 20 20 rog/Kg EPA 8020 07/22/97
I TPH as Gasoline 520 20 mg/Kg M EPA 8015
07/22/97
TPH as Diesel 6200 50 mg/Kg M EPA 8015 07/22/97
I Surrogate) 103 % Recovery EPA 8020 07/22/97
aaa-Trifluorotoluene
(8020
aaa-Trifluorotoluene (Gasoline Surrogate) 115 % Recovery M EPA 8015 07/22/97
I 1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/22/97
I Sample' PLB-2' Matrix' Soil
Sample Date :07/22/97
Method
i Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 5.0 5.0 mg/Kg EPA 8020 07/23/97
Toluene < 5.0 5.0 rog/Kg EPA 8020 07/23/97
I Ethylbenzene < 5.0 5.0 mg/Kg EPA
8020
07/23/97
Total Xylenes 20 5.0 mg/Kg EPA 8020 07/23/97
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/23/97
I TPH as Gasoline 600 20 mg/Kg M EPA 8015 07/23/97
i TPH as Diesel 1] 6000 200 rog/Kg M EPA 8015 07/22/97
aaa-Trifluorotoluene (8020 Surrogate) 101 % Recovery EPA 8020 07/23/97
;m aaa-Trifluorotoluene (Gasoline Surrogate) 88.1 % Recovery' M EPA 8015 07/23/97
! · 1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/22/97
720 Olive Drive, Suite D Davis, CA 95616 916-297-480(3
,I(IFF Report Number · 10264
IANALYTICAL Date' 07/23/97
I LLC
Project Name' Beacon 596
I Proiect Number' 1596.15
Sample: PLB-6' Matrix: Soil
Sample Date :07/22/97
Method ·
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 2.0 2.0 mg/Kg EPA 8020 07/22/97
Toluene 7.2 2.0 mg/Kg EPA 8020 07/22/97
Ethylbenzene 8.2 2.0 mg/Kg EPA 8020 07/22/97
Total Xylenes 44 2.0 mg/Kg EPA 8020 07/22/97
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/22/97
TPH as Gasoline 810 20 mg/Kg M EPA 8015 07/22/97
TPH as Diesel 34000 200 mg/Kg M EPA 8015 07/23/97
aaa-Trifluorotoluene (8020 Surrogate) 92.1 % Recovery EPA 8020 07/22/97
aaa-Trifluorotoluene (Gasoline Surrogate) 100 % Recovery M EPA 8015 07/22/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/23/97
Sample: PLB-15' Matrix: Soil
Sample Date :07/22/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 2.0 2.0 mg/Kg EPA 8020 07/22/97
Toluene < 2.0 2.0 mg/Kg EPA 8020 07/22/97
Ethylbenzene 3.3 2.0 mg/Kg EPA 8020 07/22/97
Total Xylenes 9.9 2.0 mg/Kg EPA 8020 07/22/97
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/22/97
TPH as Gasoline 810 20 mg/Kg M EPA 8015 07/22/97
TPH as Diesel 7800 100 mg/Kg M EPA 8015 07/22/97
aaa-Trifluorotoluene (8020 Surrogate) 116 % Recovery EPA 8020 07/22/97
aaa-Trifluorotoluene (Gasoline Surrogate) 114 % Recovery M EPA 8015 07/22/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/22/97
720 Olive Drive, Suite D Davis, CA 95616 916-297-48{)~
I
,I(IFF Report Number · 10260
Date · 07/21/97
IAIVALYTICA~
I
I Gary Barker
Horizon Environmental Inc.
5011 Golden Foothill Pkwy., Suite 7
I El Dorado Hills, CA 95762
Subject: Analysis of 5 Soil Samples
I Project Name ' Beacon 596
Project Number' 1596.15
Dear Mr. Barker,
Chemical analysis of the samples referenced above has been completed. Summaries of the data are contained
on the following pages. Sample(s) were received under documented chain-of-custody. US EPA protocols for
sample storage and preservation were followed.
Kiff Analytical is certified by the State of California (# 2236). If you have any questions regarding procedures
or results, please call me at 916-297-4800.
Sincerely,
?lel Kif~ II
/
I
I
I
720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
I(IFF R epor~ Number' 10260
'~!' ~V~4 LY'TtCALLLc Da~e' 07/21'97
Project Name · Beacon 596
Project Number' 1596.15
Sample' SP1-A,B,C,D Matrix' Soil
Sample Date :07/19/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metliod Analyzed
Benzene < 2,0 2,0 mg/Kg EPA
8020
07/2
1
/97
Toluene < 2.0 2.0 mg/Kg EPA 8020 07/21/97
Ethylbenzene < 2.0 2.0 mg/Kg EPA 8020 07/21/97
Total Xylenes < 2.0 2.0 mg/Kg EPA
8020
07/21/97
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/21/97
TPH as Gasoline 200 20 mg/Kg M EPA 8015 07/21/97
TPH as Diesel 6200 1.0 mg/Kg M EPA 8015 07/20/97
% Recovery EPA 8020 07/21/97
aaa-Trifluorotoluene
(8020
Surrogate)
1
04
aaa-Trifluorotoluene (Gasoline Surrogate) 85.7 % Recovery M EPA 8015 07/21/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/20/97
Sample' DTP-SW15'-W Matrix'Soil
Sample Date :07/19/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 0,050 0.050 mg/Kg EPA 8020 07/20/97
Toluene < 0,050 0.050 mg/Kg EPA 8020 07/20/97
Ethylbenzene < 0,050 0.050 mg/Kg EPA 8020 07/20/97
Total Xylenes < 0,050 0.050 mg/Kg EPA 8020 07/20/97
Methyl-t-butyl ether < 0,50 0.50 mg/Kg EPA 8020 07/20/97
TPH as Gasoline 4.6 1.0 mg/Kg M EPA 8015 07/20/97
TPH as Diesel 640 1.0 mg/Kg M EPA 8015 07/20/97
aaa-Trifluorotoluene (8020 Surrogate) 105 % Recovery EPA 8020 07/20/97
aaa-Trifluorotoluene (Gasoline Surrogate) 84.6 % Recovery M EPA 8015 07/20/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out %
Recovery
M
EPA
801
5
07/20/97
Approved By: o~Kiff
720 Olive Drive, Suite D Davis, CA 95616 916-297-4
KIFF Report Number · 10260
.
!
I Method
Reporting Analysis Date
Limit Units Method Analyzed
I 0.0050 mg/Kg EPA 8020 07/20/97
0.0050 mg/Kg EPA 8020 07/20/97
0.0050 rog/Kg EPA 8020 07/20/97
I 0.0050 mg/Kg EPA 8020 07/20/97
0.050 rog/Kg EPA 8020 07/20/97
I 1.0 mg/Kg M EPA 8015 07/20/97
% Recovery EPA 8020 07/20/97
i % Recovery M EPA 8015 07/20/97
!
Method
I Reporting Analysis Date
Limit Units Method Analyzed
0.050 mg/Kg EPA 8020 07/21/97
0.050 mg/Kg EPA 8020 07/21/97
I 0.050 mg/Kg EPA 8020 07/21/97
0.050 mg/Kg EPA 8020 07/21/97
0.50 mg/Kg EPA 8020 07/21/97
I 1.0 mg/Kg M EPA 8015 07/21/97
I % Recovery EPA 8020 07/21/97
% Recovery M EPA 8015 07/21/97
!
I
I Approved By: Jle~' Kiff ,}
av,s. CA 958~8 918-297-4aoa
C~,~- Date' 07/21/97
LLC
Project Name · Beacon 596
Project Number' 1 596.15
Sample: GTP-SW15'-E Matrix: Soil
Sample Date :07/18/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 2.0 2.0 mg/Kg EPA 8020 07/21/97
Toluene < 2.0 2.0 rog/Kg EPA 8020 07/21/97
Ethylbenzene 2.1 2.0 rog/Kg EPA 8020 07/21/97
Total Xylenes 9.8 2.0 mg/Kg EPA 8020 07/21/97
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/21/97
TPH as Gasoline 560 20 rog/Kg M EPA 8015 07/21/97
aaa-Trifluorotoluene (8020 Surrogate) 106 % Recovery EPA 8020 07/21/97
aaa-Trifluorotoluene (Gasoline Surrogate) 84.9 % Recovery M EPA 8015 07/21/97
1
!
Approved By: I Kiff
720 Olive Drive, Suite D Davis, CA 95616 916-297-48~, ,0
i m mm mm m m m m i m mm m m m i mm m m m
Ul~rammr Inc. BEACON
CHAIN OF CUSTODY REPORT ~'/~ c~ ~ O
ANALYSES ? of
Project No. Sampler~nature)" /
'Project Location ..~ ~f~iiiation .~ ~ ~
i Sample No./Identification Date Time Lab No. rni~t-.. z REMARKS
Relinqui>~h~d by: (Signature/Affiliation) Date Time Received by: (Signature/Affiliation) ........ ~. Date. Time.,
~re'iinquished by: (Signatu,,rz~f~ffiliation) D,~te' Time Received by: (Signature/Affiliation) Date Time
Relinquished by: (Signature/Affiliation) Date Time Received by: (Signature/Affiliation) 'Date Time
'' Bill t,,o'~ ULTR~R INC.
Report To:~,.~ ~ // 525 West Third Street
,,z~~ [// Hartford, CA 93,23~)
WHITE: Return to Client wilh Report YELLOW: Laboralory Copy PINK: Originator Copy
I(IFF
Report Number' 10259
Date ' 07/21/97
IANAL YTICAL
LLC
Gary Barker
Horizon Environmental Inc.
5011 Golden Foothill Pkwy., Suite 7
El Dorado Hills, CA 95762
Subject · Analysis o'f I Soil Sample
Project Name · Beacon 596
Project Number · 1596.15
I
Dear Mr. Barker,
!
Chemical analysis of the samples referenced above has been completed. Summaries of the data are contained
Ion the following pages. Sample(s) were received under documented chain-of-custody. US EPA protocols for
sample storage and preservation were followed.
I Kiff Analytical is certified by the State of California (# 2236). If you have any questions regarding procedures
I or results, please call me at 916-297-4800.
Sincerely,
~.-
I
I
I
I
720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
I 7 -/~
Date · 07/21/97
Project Name' Beacon 596
Project Number- 1596.15
Sample' GTP-SW15'-N Matrix'Soil
Sample Date :07/18/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 1.0 1.0 rog/Kg EPA
8020
07/20/97
Toluene < 1.0 1.0 mg/Kg EPA 8020 07/20/97
Ethylbenzene 7.6 1.0 mg/Kg EPA 8020 07/20/97
Total Xylenes 22 1.0 rog/Kg EPA 8020
07/20/97
Methyl-t-butyl ether < 10 10 mg/Kg EPA 8020 07/20/97
TPH as Gasoline 430 200 mg/Kg M EPA 8015 07/20/97
aaa-Trifluorotoluene (8020 Surrogate) 98.8 % Recovery EPA 8020 07/20/97
aaa-Trifluorotoluene (Gasoline Surrogate) 97.9 % Recovery M EPA 8015 07/20/97
Approved By: J~e, Kiff- II
720 Olive Drive, Suite D Davis, CA 95616 916-297-410)~0
UIIr, mir Ira:. BEACON
CHAIN OF CUSTODY REPORT /: ~)~'~ ~- ~
Beacon Station No. Sampler (~int Na ANALYSES 7 of
Project No. Sampler,,,.(~nature) //_ ~d/~~ 77~,--~,~,
Project Location ~'at~-n ,/ ~ .~
, Sample No./Identification Date Time Lab No. ~:~ - :' REMARKS
uish~dby:(S~gnatu on) ~b~e :'P~'~ '------
~ r.~lli Time Received by: (Signalure/Afliliation) Dale Time
Relinquished by: (Signalure/Allilialion) D~te Time R~eived by: (Signature/Affiliation) Date Time
" ei~ t~l: ULT~ AR ~NC.
Report T~/~
525 Wesl Third Street
· , Hanford, CA 932j;30.,,~ . x/-// ~-"-'
WHITE: Return lo Client with Report YELLOW: Laboratory Copy PINK: Originator Copy
KIFF Report Number · 10252
Date · 07/18/97
I
i Gary Barker
Horizon Environmental Inc.
5011 Golden Foothill Pkwy., Suite 7
i El Dorado Hills, CA 95762
Subject · Analysis of 27 Soil Samples
I Project Name ' Beacon 596
Project Number' 1596.15
I
Dear Mr. Barker,
I
Chemical analysis of the samples referenced above has been completed. Summaries of the data are contained
Ion the following pages. Sample(s) were received under documented chain-of-custody. US EPA protocols for
sample storage and preservation were followed.
I Kiff Analytical is certified by the State of California (# 2236). If you have any questions regarding procedures
or results, please call me at 916-297-4800.
I
Sincerely,
I
I
I
I
720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
KIFF
~ANALYTICAL Report Number' 10252
LLC Date · 07/18/97
Subject · 27 Soil Samples
Project Name · Beacon 596
Project Number · 1596.15
Case Narrative
Values for TPH as Gasoline for samples with high levels of Diesel are primarily due to Diesel-range
hydrocarbons that are detected by the TPH as Gasoline test procedure.
Approved B~' Joel Kiff' ~
720 Olive Drive, Suite D Davis, CA 95616 916-297j4800
KIFF Report Number · 10252
IANALYTICAL Date' 07/18/97
I LLC
! · Project Name' Beacon 596
,S Project Number' 1596.15
!
Sample' T1-2-M Matrix' Soil
I Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
! ~ Benzene < 1.0 1.0 rog/Kg . EPA 8020 07/18/97
Toluene < 1.0 1.0 mg/Kg EPA 8020 07/18/97
Ethylbenzene < 1.0 1.0 mg/Kg EPA 8020 07/18/97
I Total Xylenes < 1.0 1.0 mg/Kg EPA 8020 07/18/97
Methyl-t-butyl ether < 10 10 mg/Kg EPA 8020 07/18/97
I TPH as Gasoline 270 20 mg/Kg M EPA 8015 07/18/97
TPH as Diesel 3400 100 mg/Kg M EPA 8015 07/17/97
I aaa-Trifluorotoluene (8020 Surrogate) 99.6 % Recovery EPA 8020 07/18/97
aaa-Trifluorotoluene (Gasoline Surrogate) 109 % Recovery M EPA 8015 07/18/97
I
Sample' T1-6-M Matrix' Soil
I Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
I Benzene < 2,0 2.0 rog/Kg EPA 8020 07/17/97
Toluene < 2,0 2.0 mg/Kg EPA 8020 07/17/97
Ethylbenzene < 2.0 2.0 mgJKg EPA 8020 07/17/97
I Total Xylenes 2.1 2.0 rog/Kg EPA 8020 07/17/97
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/17/97
i TPH as Gasoline 670 20 mg/Kg M EPA 8015 07/17/97
TPH as Diesel 5300 100 mg/Kg M EPA 8015 07/18/97
I Recovery EPA 8020 07/17/97
aaa-mrifluorotoluene
(8020
Surrogate)
95.7
%
aaa-Trifluorotoluene (Gasoline Surrogate) 110 % Recovery . M EPA 8015 07/17/97
!
I
I 720 Olive Drive, Suite D Davis, CA 95616 916-297-z~0
I(IFF Report Number · 10252
~N~LYTICALLLc Date' 07/18/97
Project Name' Beacon 596
Project Number- 1596.15
Sample' T1-2-N Matrix'Soil
Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
Benzene < 1.0 1.0 mg/Kg EPA
8020
07/1
8/97
Toluene < 1.0 1.0 mg/Kg EPA 8020 07/18/97
Ethylbenzene 1 o7 1.0 mg/Kg EPA 8020 07/18/97
Total Xylenes 1.5 1.0
mg/Kg
EPA
8020
07/1
8/97
Methyl-t-butyl ether < 10 10 mg/Kg EPA 8020 07/18/97
TPH as Gasoline 480 20 mg/Kg M EPA 8015 07/18/97
TPH as Diesel 5400 100 rog/Kg M EPA 8015 07/18/97
% Recovery EPA 8020 07/18/97
aaa-mrifluorotoluene
(8020
Surrogate)
1
1
6
aaa-Trifluorotoluene (Gasoline Surrogate) 119 % Recovery M EPA 8015 07/18/97
Sample · T1-6-N Matrix: Soil
Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 1.0 1.0
mg/Kg
EPA
8020
07/1
7/97
Toluene < '1.0 1.0 rog/Kg EPA 8020 07/17/97
Ethylbenzene 1.9 1.0 mg/Kg EPA 8020 07/17/97
Total Xylenes 3.5 1.0 mg/Kg EPA
8020
07/1
7/97
Methyl-t-butyl ether < 10 10 mg/Kg EPA 8020 07/17/97
TPH as Gasoline 630 20 mg/Kg M EPA 8015 07/17/97
TPH as Diesel 9900 100 mg/Kg M EPA 8015 07/18/97
Surrogate) 04 % Recovery EPA 8020 07/17/97
aaa-Trifluorotoluen8
(8020
1
aaa-Trifluorotoluene (Gasoline Surrogate) 117 % Recovery M EPA 8015 07/17/97
I
I 720 Olive Drive, Suite D Davis, CA 95616 916-297-4~0
,I(IFF Report Number · 10252
IANALYTICAL Date' 07/18/97
I LLC
Project Name* Beacon 596
I Project Number' 1596.15
~1 I Sample' T1-2-S Matrix' Soil
I Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
i ~ Benzene < 2.0 2.0 mg/Kg . EPA 8020 07/18/97
'· Toluene < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Ethylbenzene < 2.0 2.0 mg/Kg EPA 8020 07/18/97
I Total Xylenes < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Methyl-t-butyl ether < 20 20 rog/Kg EPA 8020 07/18/97
i TPH as Gasoline 420 20 mg/Kg M EPA 8015 07/18/97
TPH as Diesel 7000 100 mg/Kg M EPA 8015 07/18/97
I aaa-Trifluorotoluene (8020 Surrogate) 105 % Recovery EPA 8020
07/1
8/97
aaa-Trifluorotoluene (Gasoline Surrogate) 109 % Recovery M EPA 8015 07/18/97
!
Sample' T1-6-S Matrix' Soil
I Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl~od Analyzed
I Benzene < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Toluene < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Ethylbenzene < 2.1:) 2.0 rog/Kg EPA 8020 07/18/97
I Total Xylenes < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/18/97
i TPH as Gasoline 290 20 mg/Kg M EPA 8015 07/18/97
TPH as Diesel 4200 100 mg/Kg M EPA 8015 07/18/97
I aaa-Trifluorotoluene (8020 Surrogate) 110 %
Recovery
EPA
8020
07/1
8/97
aaa-Trifluorotoluene (Gasoline Surrogate) 110 % Recovery M EPA 8015 07/18/97
!
I
I 720 Olive Drive, Suite D Davis, CA 95616 916-297-4~0
'KIFF Report Number · 10252
''ANALYT/CALLLc Date' 07/18/97
Project Name- Beacon 596
Project Number' 1596.15
Sample' T2-2-M Matrix' Soil
Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl-iod Analyzed
mg/Kg - EPA 8020 07/18/97
Benzene
.0
Toluene < 1.0 1.0 mg/Kg EPA 8020 07/18/97
Ethylbenzene 1.6 1.0 mg/Kg EPA 8020 07/18/97
Total Xylenes < 1.0 1.0
mg/Kg
EPA
8020
07/1
8/97
Methyl-t-butyl ether < 10 10 mg/Kg EPA 8020 07/18/97
TPH as Gasoline 380 20 mg/Kg M EPA 8015 07/18/97
TPH as Diesel 4500 100 mg/Kg M EPA 8015 07/18/97
(8020 Surrogate) 111 % Recovery EPA 8020 07/18/97
aaa-mrifluorotoluene
aaa-Trifluorotoluene (Gasoline Surrogate) 115 % Recovery M EPA 8015 07/18/97
Sample' T2-6-M Matrix' Soil
Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
1.0 mg/Kg EPA 8020 07/18/97
Benzene
Toluene < 1,0 1.0 mg/Kg EPA 8020 07/18/97
Ethylbenzene < 1,0 1,0 mg/Kg EPA 8020 07/18/97
Total Xylenes < 1,0 1.0
mg/Kg
EPA
8O2O
07/1
8/97
Methyl-t-butyl ether < 10 10 mg/Kg EPA 8020 07/18/97
TPH as Gasoline 120 20 mg/Kg M EPA 8015 07/18/97
TPH as Diesel 6400 100 mg/Kg M EPA 8015 07/18/97
(8020 Surrogate) 105 % Recovery EPA 8020 07/18/97
aaa-Trifluorotoluene
aaa-Trifluorotoluene (Gasoline Surrogate) 90.3 % Recovery . M EPA 8015 07/18/97
I
I Approved
i 720 Olive Drive, Suite D Davis, CA 95616 916-297-4~0
i Project Name · Beacon 596
Project Number' 1596.15
!
Sample' T2-2-N Matrix' Soil
I Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
I Benzene < 1.0 1.0 mg/Kg EPA 8020 07/18/97
Toluene < 1.0 1.0 mg/Kg EPA 8020 07/18/97
, Ethylbenzene < 1.0 1.0 rog/Kg EPA 8020 07/18/97
B Total Xylenes < 1.0 1.0 rog/Kg EPA 8020 07/18/97
Methyl-t-butyl ether < 10 10 rog/Kg EPA 8020 07/18/97
I TPH as Gasoline 100 20 rog/Kg M EPA 8015 07/18/97
TPH as Diesel 2000 100 rog/Kg M EPA 8015 07/18/97
i aaa-Trifluorotoluene (8020 Surrogate) 103 % EPA 8020
Recovery
07/1
8/97
aaa-Trifluorotoluene (Gasoline Surrogate) 87.4 % Recovery M EPA 8015 07/18/97
!
Sample' T2-6-N Matrix' Soil
I Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
~ Benzene < 2.0 2.0 rog/Kg EPA 8020 07/18/97
~· Toluene < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Ethylbenzene < 2.0 2.0 rog/Kg EPA 8020 07/18/97
I Total Xylenes < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/18/97
i TPH as Gasoline 250 20 mg/Kg M EPA 8015 07/18/97
TPH as Diesel 7600 100 mg/Kg M EPA 8015 07/18/97
I aaa-Trifluorotoluene (8020 Surrogate) 103 % Recovery EPA 8020 07/18/97
aaa-Trifluorotoluene (Gasoline Surrogate) 88.6 % Recovery M EPA 8015 07/18/97
!
720 Olive Drive, Suite D Davis, CA 95616 916-297-48,70
I
I(IFF Report Number ' 10252
'AIVAI-¥T/CA Date' 07/18197
Project Name · Beacon 596
Project Number' 1 596.1 5
Sample' T2-6-S Matrix' Soil
Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Toluene < 2.0 2.0 rog/Kg EPA 8020 07/18/97
Ethylbenzene < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Total Xylenes < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/18/97
TPH as Gasoline 210 20 mg/Kg M EPA 8015 07/18/97
TPH as Diesel 5300 100 mg/Kg M EPA 8015 07/18/97
aaa-Trifluorotoluene (8020 Surrogate) 104 % EPA 8020
Recovery
07/1
8/97
aaa-Trifluorotoluene (Gasoline Surrogate) 89.4 % Recovery M EPA 8015 07/18/97
Sample' T2-2-S Matrix' Soil
Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Toluene < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Ethylbenzene < 2.0 2.0 rog/Kg EPA 8020 07/18/97
Total Xylenes < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Methyl-t-butyl ether < 20 20 rog/Kg EPA 8020 07/18/97
TPH as Gasoline 240 20 mg/Kg M EPA 8015 07/18/97
TPH as Diesel 7600 100 mg/Kg M EPA 8015 07/18/97
aaa-Trifluorotoluene (8020 Surrogate) 104 % Recovery EPA 8020 07/18/97
aaa-Trifluorotoluene (Gasoline Surrogate) 92.1 % Recovery M EPA 8015 07/18/97
I Approved By: ~l'Kiff
720 Olive Drive, Suite D Davis, CA 95616 916-297-4~0~
I -
KIFF Report Number · 10252
~ANALYTtCALLLc Date' 07/18/97
Project Name' Beacon 596
Project Number' 1596,15
Sample' T3-2-E Matrix' Soil
Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
< 0.0050 0.0050 mg/Kg EPA 8020 07/18/97
Benzene
Toluene < 0.0050 0.0050 rog/Kg EPA 8020 07/18/97
Ethylbenzene < 0,0050 0.0050 rog/Kg EPA 8020 07/18/97
0.0050 0.0050 mg/Kg EPA 8020 07/18/97
Total
Xylenes
Methyl-t-butyl ether < 0,050 0.050 rog/Kg EPA 8020 07/18/97
TPH as Gasoline < 1.0 1.0 mg/Kg M EPA 8015 07/18/97
aaa-Trifluorotoluene (8020 Surrogate) 106 % Recovery EPA 8020 07/18/97
aaa-Trifluorotoluene (Gasoline Surrogate) 84.6 % Recovery M EPA 8015 07/18/97
I Sample' T3-6-E Matrix- Soil
Sample Date :07/17/97
Method
I Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 0.50 0.50 rog/Kg EPA 8020 07/18/97
i Toluene < 0,50 0.50 mg/Kg EPA 8020 07/18/97
Ethylbenzene < 0,50 0.50 rog/Kg EPA 8020 07/18/97
Total Xylenes < 0,50 0.50 rog/Kg EPA 8020 07/18/97
Methyl-t-butyl ether < 5,0 5.0 rog/Kg EPA 8020 07/18/97
I TPH as Gasoline 56 5.0 mg/Kg M EPA 8015 07/18/97
I aaa-Trifluorotoluene (8020 Surrogate) 111 % Recovery EPA 8020 07/18/97
aaa-Trifluorotoluene (Gasoline Surrogate) 108 % Recovery M EPA 8015 07/18/97
!
I Drive, Davis,
I(IFF Report Number · 10252
'AIVAIYT/CALLLc Date' 07/18/97
Project Name · Beacon 596
Project Number' 1596.15
Sample: T3-2-W Matrix: Soil
Sample Date :07/17/97
Method
Measured Reporting Analysis Date-
Parameter Value Limit Units Metl'iod Analyzed
Benzene · 0,0050 0.0050 mg/Kg ' EPA 8020 07/18/97
Toluene · 0.0050 0.0050 rog/Kg EPA 8020 07/18/97
Ethylbenzene · 0,0050 0.0050 mg/Kg EPA 8020 07/18/97
Total Xylenes · 0.0050 0.0050 mg/Kg EPA 8020 07/18/97
Methyl-t-butyl ether 0.28 0.050 rog/Kg EPA 8020 07/18/97
TPH as Gasoline · 1.0 1.0 mg/Kg M EPA 8015 07/18/97
aaa-Trifluorotoluene (8020 Surrogate) 104 % Recovery EPA 8020 07/18/97
aaa-Trifluorotoluene (Gasoline Surrogate) 84.9 % Recovery M EPA 8015 07/18/97
Sample: T3-6-W Matrix: Soil
Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene · 1.0 1.0 rog/Kg EPA 8020 07/18/97
Toluene · 1.0 1.0 rog/Kg EPA 8020 07/18/97
Ethylbenzene · 1.0 1.0 mg/K9 EPA 8020 07/18/97
Total Xylenes 1.4 1.0 mg/Kg EPA 8020 07/18/97
Methyl-t-butyl ether · 10 10 rog/Kg EPA 8020 07/18/97
TPH as Gasoline 280 20 mg/Kg M EPA 8015 07/18/97
aaa-Trifluorotoluene (8020 Surrogate) 103 % Recovery EPA 8020 07/18/97
aaa-Trifluorotoluene (Gasoline Surrogate) 121 % Recovery M EPA 8015 07/18/97
I
I Approved By: Jo~-/~iff
720 Olive Drive, Suite D Davis, CA 95616 916-297-480Dv/
I
I(IFF Report Number ' 10252
IANALYTICAL Date' 07/18/97
LLC
Project Name · Beacon 596
Project Number' 1596.15
I
Sample: T4-2-E Matrix: Soil
I Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
I Benzene < 0.020 0.020 rog/Kg EPA 8020 07/18/97
Toluene ¢ 0.020 0.020 mg/Kg EPA 8020 07/18/97
Ethylbenzene < 0.020 0.020 mg/Kg EPA 8020 07/18/97
I Total Xylenes 0.027 0.020 mg/Kg EPA 8020 07/18/97
Methyl-t-butyl ether < 0.20 0.20 mg/Kg EPA 8020 07/18/97
I TPH as Gasoline < 1.0 1.0 mg/Kg M EPA 8015 07/18/97
aaa-Trifluorotoluene (8020 Surrogate) 105 % Recovery EPA 8020 07/18/97
i aaa-Trifluorotoluene (Gasoline Surrogate) 60.0 % Recovery M EPA 8015 07/18/97
i Sample' T4-6-E Matrix' Soil
Sample Date :07/17/97
Method
i Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Toluene < 2.0 2.0 rog/Kg EPA 8020 07/18/97
I Ethylbenzene < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Total Xylenes < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/18/97
I TPH as Gasoline 330 20 rog/Kg M EPA 8015 07/18/97
i aaa-Trifluorotoluene (8020 Surrogate) 100 % Recovery EPA 8020 07/18/97
aaa-Trifluorotoluene (Gasoline Surrogate) 95.5 % Recovery M EPA 8015 07/18/97
720 Olive Drive, Suite D Davis, CA 95616 916-297-4~{)0
I
Report Number' 10252
Date - 07/18/97
Proiect ~ame · Boa¢on
I Project ~umber' 1fi~.1 §
Sample: T4-2-W Matrix: Soil
Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl-iod Analyzed
Benzene < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Toluene < 2.0 2.0 rog/Kg EPA 8020 07/18/97
Ethylbenzene 2.6 2.0 rog/Kg EPA 8020 07/18/97
Total Xylenes 10 2.0 mg/Kg EPA 8020 07/18/97
Methyl-t-butyl ether < 20 20 rog/Kg EPA 8020 07/18/97
TPH as Gasoline 520 20 mg/Kg M EPA 8015 07/18/97
aaa-Trifluorotoluene (8020 Surrogate) 109 % Recovery EPA 8020 07/18/97
aaa-Trifluorotoluene (Gasoline Surrogate) 120 % Recovery M EPA 8015 07/18/97
Sample: T4-6-W Matrix: Soil
Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl-iod Analyzed
Benzene < 0.50 0.50 mg/Kg EPA 8020 07/18/97
Toluene < 0.50 0.50 rog/Kg EPA 8020 07/18/97
Ethylbenzene < 0.50 0.50 mg/Kg EPA 8020 07/18/97
Total Xylenes 1.4 0.50 mg/Kg EPA 8020 07/18/97
Methyl-t-butyl ether < 5.0 5.0 rog/Kg EPA 8020 07/18/97
TPH as Gasoline 67 5.0 mg/Kg M EPA 8015 07/18/97
aaa-Trifluorotoluene (8020 Surrogate) 101 % Recovery EPA 8020 07/18/97
aaa-Trifluorotoluene (Gasoline Surrogate) 90.4 % Recovery M EPA 8015 07/18/97
720 Olive Drive, Suite D Davis, CA 95616 916-297-4~8~0
KIFF Report Number · 10252
IAIVA£¥TICAL Date-07/18/97
I LLC
Project Name · Beacon 596
I Project Number' 1596.15
Sample: SP1 A,B,C,D Matrix: Soil
Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit L~nits Method Analyz.ed
Benzene < 2.0 2.0 mg/Kg EPA 8020 07/18/97-
Toluene < 2.0 2.0 rog/Kg EPA 8020 07/18/97
Ethylbenzene < 2.0 2.0 rog/Kg EPA 8020 07/18/97
Total Xylenes 3.5 2.0 mg/Kg EPA 8020 07/18/97
Methyl-t-butyl ether < 20 20 rog/Kg EPA 8020 07/18/97
TPH as Gasoline 210 20 rog/Kg M EPA 8015 07/18/97
TPH as Diesel 5200 100 mg/Kg M EPA 8015 07/18/97
aaa-Trifluorotoluene (8020 Surrogate) 104 % Recovery EPA 8020 07/18/97
aaa-Trifluorotoluene (Gasoline Surrogate) 84.8 % Recovery M EPA 8015 07/18/97
Sample: SP1 E,F,G,H Matrix: Soil
Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Mett'iod Analyzed
Benzene < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Toluene < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Ethylbenzene < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Total Xylenes < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/18/97
TPH as Gasoline 180 20 mg/Kg M EPA 8015 07/18/97
TPH as Diesel 6000 100 mg/Kg M EPA 8015 07/18/97
aaa-Trifluorotoluene (8020 Surrogate) 104 % Recovery EPA 8020 07/18/97
aaa-Trifluorotoluene (Gasoline Surrogate) 86.1 % Recovery M EPA 8015 07/18/97
I Approved By: f(~' K~ff'
720 Olive Drive, Suite D Davis, CA -~
I 95616 916-297 8~00
~KIFF F~eport Number' 10252
IANALYTICAL Date' 07/18/97
I LLC
Project Name' Beacon 596
I Project Number' 1596.15
'1
I Sample' SP1 I,J,K,L Matrix- Soil
I Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
I Benzene < 2.0 2.0 rog/Kg EPA 8020 07/18/97
Toluene < 2,0 2.0 mg/Kg EPA 8020 07/18/97
Ethylbenzene < 2,0 2.0 mg/Kg EPA 8020 07/18/97
I Total Xylenes 19 2.0 mg/Kg EPA 8020 07/18/97
Methyl-t-butyl ether < 20 20 rog/Kg EPA 8020 07/18/97
I TPH as Gasoline 500 20 mg/Kg M EPA 8015 07/18/97
TPH as Diesel 5900 100 mg/Kg M EPA 8015 07/18/97
I aaa-Trifluorotoluene (8020 Surrogate) 102 % Recovery EPA 8020 07/18/97
I aaa-Trifluorotoluene (Gasoline Surrogate) 87.5 % Recovery M EPA 8015 07/18/97
I Sample' SPt M,N,O,P Matrix' Soil
Sample Date :07/17/97
I Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
i Benzene < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Toluene < 2.0 2.0 rog/Kg EPA 8020 07/18/97
Ethylbenzene < 2.0 2.0 mg/Kg EPA 8020 07/18/97
i Total Xylenes 3.6 2.0 mg/Kg EPA 8020 07/18/97
Methyl-t-butyl ether < 20 20 mg/Kg EPA 8020 07/18/97
TPH as Gasoline 670 20 mg/Kg M EPA 8015 07/18/97
I TPH as Diesel 8000 100 mg/Kg M EPA 8015 07/18/97
i aaa-Trifluorotoluene (8020 Surrogate) 104 % Recovery EPA 8020 07/18/97
aaa-Trifluorotoluene (Gasoline Surrogate) 111 % Recovery M EPA 8015 07/18/97
Approved By: iff
720 Olive Drive, Suite D Davis, CA 95616 916-297-4~,¢1~0
II(IFF Report Number · 10252
, I IAIVA/.¥TICA Date' 07/18/97
Project Name' Beacon 596
I Project Number' 1596.1,5
Sample: SP2 A,B,C,D Matrix: Soil
Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter' Value Limit Units MetPiod Analyzed
Benzene < 2.0 2.0 rog/Kg EPA 8020 07/18/97
Toluene < 2.0 2.0 rog/Kg EPA 8020 07/18/97
Ethylbenzene < 2.0 2.0 mg/Kg EPA 8020 07/18/97
Total Xylenes 24 2.0 rog/Kg EPA 8020 07/18/97
Methyl-t-butyl ether < 20 20 rog/Kg EPA 8020 07/18/97
TPH as GasOline 680 20 rog/Kg M EPA 8015 07/18/97
aaa-Trifluorotoluene (8020 Surrogate) 118. % Recovery EPA 8020 07/18/97
aaa-Trifluorotoluene (Gasoline Surrogate) 109 % Recovery M EPA 8015 07/18/97
Sample: SP2 E,F,G,H Matrix: Soil
Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Mettiod Analyzed
Benzene < 2.0 2.0 rog/Kg EPA 8020 07/18/97
Toluene < 2,0 2.0 mg/Kg EPA 8020 07/18/97
Ethylbenzene < 2.0 2.0 rog/Kg EPA 8020 07/18/97
Total Xylenes 3.6 2.0 mg/Kg EPA 8020 07/18/97
Methyl-t-butyl ether < 20 20 rog/Kg EPA 8020 07/18/97
TPH as Gasoline 320 20 mg/Kg M EPA 8015 07/18/97
aaa-Trifluorotoluene (8020 Surrogate) 118 % Recovery EPA 8020 07/18/97
aaa-Trifluorotoluene (Gasoline Surrogate) 107 % Recovery M EPA 8015 07/18/97
I Approved By:./loel Kiff I[
720 Olive Drive, Suite Davis. CA 95616 916-297'4800
D ~[,,x
I
KIFF
Report Number · 10252
IANALYTICAL Date' 07/18/97
LLC
Project Name' Beacon 596
Project Number' 1.596.15
I
Sample: SP2 I,J,K,L Matrix: Soil
I Sample Date :07/17/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
I Benzene < 1.0 1.0 mg/Kg EPA 8020 07/18/97
Toluene < 1.0 1.0 rog/Kg EPA 8020 07/18/97
Ethylbenzene < 1.0 1.0 mg/Kg EPA 8020 07/18/97
I Total Xylenes < 1.0 1.0 rog/Kg EPA 8020 07/18/97
Methyl-t-butyl ether < 10 10 mg/Kg EPA 8020 07/18/97
i TPH as Gasoline 120 20 mg/Kg M EPA 8015 07/18/97
aaa-Trifluorotoluene (8020 Surrogate) 118 % Recovery EPA 8020 07/18/97
aaa-Trifluorotoluene (Gasoline Surrogate) 108 % Recovery M EPA 8015 07/18/97
I
I Approved By:
720 Olive Drive, Suite D Davis, CA 95616 916-297-480~
Ultramar Inc. BEACON
CHAIN OF CUSTODY REPORT //~'~ '~ ~ ~
Beacon Station No. Sampler (Print Name) Date 7'~ Form No.
~'~ /_j/~ ANALYSES 7- / {~' ~ of
Prsj~ L~ation Affiliation / ~ ~ E
Sample No,Id ification Date Time Lab No. m - - z REMARKS
~e,~ . ~ature/ ,hlla on'
ish~by: ( 'g ur~ il~ ) Date Time R~eiv~ by: (Signature/Affiliation) Date Time
Re~nquish~y: (Signature/~filiatio) Date Time R~eiv~ by: (Signature/Affiliation) Date Time
Relinquish~ by: (Signature/Affiliation) D~te~ Time Received by: (Signature/Affiliation) Date Time
nepoaTo: ~ ~ Bi~t~ ULTRAMAR INC.
~ ~ ~ ~ ~ ~ ~ ] 525 West Third Street
~ Hanford. CA 93230 ~ ~
~t tlTF' Eehlrn ~o Clienl wilh ~eporl YFI I OW: I aboralorv Copy PtNK~ Oriqinalor Copv .... ~ ....... ~,o
Imm m m mm m m mm Imm Imm mi mi m
IJItramar Inc.
CHAIN OF CUSTODY REPORT //~ ~ G ~ BEACON
Beacon Stalion No. Sampler (Pdnt Name) ?~e _ ~../z..I of
Project No. '
Sample No./Identification Date' Time Lab No. m - - z REMARKS
~~~~Reli~ish~, bY: (Signature/Affili~on)~y~ ~ ~ ;~'~ Date ~~Timer. R~eiv~ by: (Signature/Affiliation) ~~Date Time.
Reli~uish~(signature/Affiliatidn) Date Time R~eiv~ by: (Signature/Affiliation) Date Time
Reli~uish~ by: (Signature/Affiliation) Date/ Time R~eiv~by: (S~nature/Affiliation) Date Time
WHITE: Return to Client with Repo~ YELLOW: Laboralow Copy PINK: OriqinRlor Copy
m ~ ~ ~ m m m mi m imm ~ m m m ~ mm ~ mm m
Ullramar Inc. /'~::~,..~ :5~'-.~- BEACON
CHAIN OF CUSTODY REPORT
Beacon Station No. Sampler (Pdnt Name)
D,,~ ? No.
ANALYSES '~ 7~' Form
- of
Project No. ',~~~~~
/,..s-? f.,,, fi'- ~
Project Location Affiliation / i.=_ _~
'-- m
Sample NoYldenflfication Date Time [~h No. m ~' d
- - z REMARKS
F~-/--,,Z- ~~,/,, "'/f ,,,,
,~ished by: (Signature/~ffiliation) Date Time Received by: (Signature/Affiliation) Date Time
Reli~:l~ish~6y.~(Signature/Xffiliation) Date Time Received by: (Signature/Affiliation) Date Time
Relinquished by: (Signature/Affiliation) Date Time Received by: (Signature/Affiliation) Date Time
Report 1o: /[ ill to: UL AFl INC.
(~ '(::~ ~"/.~O/~ ///~/"/'(/'/'- /'Hanford,525 WestcA Third 932S' ree3~,~,,¢_/,,~,~_
/~ 0 ~ Attention: ,
WHITE: Return to Client with Repori YELLOW: Laboratory Copy PINK: Originator Copy
Ullramar Inc. BEACGN
C.A,. o~ CUS~O~Y.~.o.~ / ~ ~-~
I~acon Station No. Sampler (Pdnt Name) _ Date j Form No.
Project No./ ~
· _d~ . ~
Project Location Affiliation / - e
,mn d
Sample No./Idenfiticalion Date Time Lab No. '" ~-- - :- FIEMARK$
:3?/, -;_T 7./<, ~' -- ~x ~ ~~ qc~,~,~o., ~.,~.~
Refin~'hodb¥: (Si~natum/~ffiliation) , Date Time Received by: {Si§nature/Affiliation) Da~e lime
~oli~uish~):~S~natur~Affiliation) Date Time fl~eiv~ by: (8~naturetAfliliafion) Date Time
~eli~uish~ by: (Si~nature/gffiliation) ~ato limo ~oiv~ by: {S~nature/~ffiliation) Date lime
Re~ To: B~: ULTRAM4R lNG.
G ~/~ ~ ~er 525 West Third Street
Hartford, CA 93230Z
Attention: /<
WHITe: Return to Client wilh ~o~d YEkkOW: kaboralo~ Copy ~I~K: Ori~inalor Copy
I(IFF Report Number · 10264
I ~AIVAIYT/CALLLc Date' 07/23/97
Project Name' Beacon 596
I Project Number' 1596.15
I
Sample' PLB2-2' Matrix' Soil
I Sample Date :07/22/97
Method
Measured. Reporting .Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
I Benzene < 0.050 0.050 rog/Kg EPA 8020 07/22/97
Toluene < 0,050 0.050 mg/Kg EPA 8020 07/22/97
Ethylbenzene < 0,050 0,050 mg/Kg EPA 8020 07/22/97
I Total Xylenes 0,084 0,050 mg/Kg EPA 8020 07/22/97
Methyl-t-butyl ether < 0.50 0.50 mg/Kg EPA 8020 07/22/97
i TPH as Gasoline 1.3 1.0 mg/Kg M EPA 8015 07/22/97
TPH as Diesel 28 10 mg/Kg M EPA 8015 07/23/97
I aaa-Trifluorotoluene (8020 Surrogate) 104 % Recovery EPA 8020 07/22/97
aaa-Trifluorotoluene (Gasoline Surrogate) 83.4 % Recovery M EPA 8015 07/22/97
1-Chlorooctadecane (Diesel Surrogate) 84.0 % Recovery M EPA 8015 07/23/97
I
Sample- PLB2-6' Matrix' Soil
I Sample Date :07/22/97
Method
Measured Reporting Analysis Date
I Parameter Value Limit Units MetHod Analyzed
Benzene < 1.0 1.0 mg/Kg EPA 8020 07/22/97
Toluene 1o0 1.0 rog/Kg EPA 8020 07/22/97
I Ethylbenzene 10 1.0 mg/Kg EPA 8020 07/22/97
Total Xylenes 68 1.0 rog/Kg EPA 8020 07/22/97
Methyl-t-butyl ether < 10 10 mg/Kg EPA 8020 07/22/97
I TPH as Gasoline 830 10 mg/Kg M EPA 8015 07/22/97
TPH as Diesel 5700 200 rog/Kg M EPA 8015 07/23/97
I aaa-Trifluorotoluene (8020 Surrogate) 123 % Recovery EPA 8020 07/22/97
aaa-Trifluorotoluene (Gasoline Surrogate) 139 % Recovery M EPA 8015 07/22/97
I 1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/23/97
I Approved By: J(~ Kiff
720 Olive Drive, Suite D Davis, CA 95616 916-297-4800'
KIFF P, eport Number · 10264
'ANALYTtCALLLc Date' 07/23/97
Project Name · Beacon 596
Project Number' 1596.15
Sample: PLC-2' Matrix: Soil
Sample Date :07/22/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 2,0 2.0 mg/Kg EPA 8020 07/23/97
Toluene 2,3 2.0 rog/Kg EPA 8020 07/23/97
Ethylbenzene 14 2.0 rog/Kg EPA 8020 07/23/97
Total Xylenes 10 2.0 rog/Kg EPA 8020 07/23/97
Methyl-t-butyl ether < 20 20 rog/Kg EPA 8020 07/23/97
TPH as Gasoline 2400 20 mg/Kg M EPA 8015 07/23/97
TPH as Diesel 38000 200 mg/Kg M EPA 8015 07/23/97
aaa-Trifluorotoluene (8020 Surrogate) 122 % Recovery EPA 8020 07/23/97
aaa-Trifluorotoluene (Gasoline Surrogate) 110 % Recovery M EPA 8015 07/23/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/23/97
Sample: PLC-6' Matrix: Soil
Sample Date :07/22/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Method Analyzed
Benzene < 2,0 2.0 rog/Kg EPA 8020 07/22/97
Toluene ¢ 2.0 2.0 rog/Kg EPA 8020 07/22/97
Ethylbenzene 6,1 2.0 mg/Kg EPA 8020 07/22/97
Total Xylenes 17 2.0 mg/Kg EPA 8020 07/22/97
Methyl-t-butyl ether < 20 20 rog/Kg EPA 8020 07/22/97
TPH as Gasoline 1600 20 rog/Kg M EPA 8015 07/22/97
TPH as Diesel 21000 200 mg/Kg M EPA 8015 07/23/97
aaa-Trifluorotoluene (8020 Surrogate) 122 % Recovery EPA 8020 07/22/97
aaa-Trifluorotoluene (Gasoline Surrogate) 113 % Recovery M EPA 8015 07/22/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/23/97
I Approved By: Kiff
720 Olive Drive, Suite D Davis, CA 95616 916-297-4800
I KiFF Report Number · 10264
'ANAL~i/'T/C~LLcc Date' 07/23/97
Project Name' Beacon 596
Project Number' 1,596.15
Sample' PLC-15' Matrix' Soil
Sample Date :07/22/97
Method
Measured Reporting Analysis Date
Parameter Value Limit Units Metl'iod Analyzed
< 2.0 2.0 rog/Kg EPA 8020 07/22/97
Benzene
Toluene < 2.0 2.0 mg/Kg EPA 8020 07/22/97
Ethylbenzene < 2.0 2.0 mg/Kg EPA 8020 07/22/97
2.0 rog/Kg EPA 8020 07/22/97
Total
Xylenes
3.6
Methyl-t-butyl ether < 20 20 rog/Kg EPA 8020 07/22/97
TPH as Gasoline 770 20 rog/Kg M EPA 8015 07/22/97
TPH as Diesel $300 100 mg/Kg M EPA 8015 07/23/97
(8020 Surrogate) 119 % Recovery EPA 8020 07/22/97
aaa-Trifluorotoluene
aaa-Trifluorotoluene (Gasoline Surrogate) 107 % Recovery M EPA 8015 07/22/97
1-Chlorooctadecane (Diesel Surrogate) Diluted Out % Recovery M EPA 8015 07/23/97
I
I
I
I ApprovedBy: JI~Kiff ,,
720 Olive Drive, Suite D Davis, CA 95616 916-297-48~,0/0
I
I
IAlpha Analytical Laboratories Inc. · 860 Waugh Lane, H-l, Ukiah, California 95482
CHEMICAL EXAMINATION REPORT (707) 468-0401
Kiff AnaLyticaL
I 720 OLive Drive
Suite 0 Date Printed Page
Oavis, CA 95616 7/29/97 1
Attn: Joel Kiff
I Batch N~rber Receipt Date CLient CLient P.O. Send Via
97-0724-004 07/24/97 09:45 KIFFLAB 10264 Mail
I METHO0 EXTRACTED TEST DATE RESULT UNITS PQL DILUTIC,
Batch 97-0724-004 consisted of 1 SampLe and 19 Tests
I SampLe 1 DSP-M,N,O,P Beacon 596
Project #1596.15 Composite 4:1
SampLe Type: Soil SampLed by: N/A SampLed: 7/22/97
I The PQL's for EPA8010 are 300 x higher
than usual due to matrix interferences.
I Halogenated VoLatiLe Organics EPA8010 7/29/97
Bromodichtoromethane ........... ND mg/kg 1.5
Bromoform ............ ND ms/kg 1.5
i Bromomethane ........... ND mg/kg 1.5
Carbon Tetrach[oride ........... ND ms/kg 1.5
Ch[orobenzene ........... ND mg/kg 1.5
ChLoroethane ........... NO ms/kg 1.5
I 2-ChLoroethyLviny[ ether ........... ND ms/kg 3
ChLoroform ........... NO ms/kg 1.5
Ch[oromethane ........... ND mg/kg 1.5
I Chtoroto[uene ........... ND mg/kg 1.5
Oibromoch[oromethane ........... ND ms/kg 1.5
1,~-Oichtorobenzene ........... ND ms/kg 1.5
1,3-OichLorobenzene ........... ND ms/kg 1.5
I........... NO ms/kg 1.5
1,4-Oichtorobenzene
Oichtorodiftuoromethane ........... ND ms/kg 1.~
1,1-DichLoroethane ........... NO ms/kg 1.5
I 1,2-Oich[oroethane ........... ND ms/kg 1.5
1,1-Dichtoroethytene ........... ND ms/kg 1.5
cis-l,2-OichtoroethyLene ........... NO ms/kg 1.5
I
I PQL - Practical Quantitation Limit ND - None Detected
* Indicates Detection Limit altered due to SampLe DiLution
I NOTES:
Bruce L. Gove
I Laboratory Director Date Printed: 7/29/97
Alpha Analytical Laboratories Inc. · 860 Waugh Lane, H-l, Ukiah, California 95482
(707) 468-0401
CHEMICAL EXAMIN/~TION REPORT
Kiff AnaLyticaL
720 OLive Drive
Suite O
Date Printed Page
Davis, CA 95616
Attn: Joel Riff 7/29/97 2
Batch N~ber Receipt Oate CLient CLient P.O. Send Via
97-0726-00& 07/24/97 09:45 KIFFLAB 10264 Mai[
METHO0 EXTRACTED TEST DATE RESULT UNITS PQL DILUTIC.
(SampLe 1 OSP-M,N,O,P Beacon 596 -- continued)
........... ND mg/kg 1.5
t rahs- 1,2-D ich L oroethyL erie
1,2-OichLoropropane
........... ND mg/kg 1.5
cis-l,3-OichLoropropytene · · · · · · . · . . . ND mg/kg 1.5
trans-l,3-OichtoropropyLene ........... ND mg/kg 1.5
MethyLene ChLoride
........... ND mg/kg 1.5
1,1,2,2-Tetrachtoroethane · · . · · · · · . . . ND mg/kg 1.5
Tetrachtoroethytene
........... ND mg/kg 1.5
1,1,1-Trichtoroethane
........... NO mg/kg 1.5
1,102-Trichtoroethane
........... ND mg/kg 1.5
Trichtoroethytene
........... ND mg/kg 1.5
Trichtoroftuoromethane ........... ND mg/kg 1.5
Vinyl ChLoride
........... ND mg/kg 1.S
MetaLs AnaLyses by ICP and GFAA
Antimony 6010 7/25/97 NO mg/kg 15.0
Arsenic OF 7060 7/28/97 6.4 mg/kg 5.0
Barium 6010 7/25/97 210 ms/kg 10.0
ND mg/kg 0.75
BeryLLium
6010
7/25/97
Cadmium 6010 7/25/97 ND mg/kg 1.00
Chromi~n 6010 7/25/97 12 ms/kg 5.00
CobaLt 6010 7/25/97 NO mg/kg 20.0
Copper 6010 7/25/97 29 ms/kg 10.0
Lead 6010 7/25/97 39 ms/kg 5.00
Mercury 7471 7/28/97 NO ms/kg .200
Motybdenun 6010 7/25/97 NO mg/kg 50.0
Nickel 6010 7/25/97 ND ms/kg 10.0
SeteniumGF 7740 7/28/97 ND ms/kg 1.0
I PQL - Practical Ouantitation Limit ND - None Detected
* Indicates Detection Limit altered due to Smnpte DiLution
iii NOTES:
Bruce L. Gove ~ /)L.~.~.~..~.__~-
I Laboratory Director Date Printed: 7/29/97
I
Alpha Analytical Laboratories Inc. * 860 Waugh Lane, H-I, Ukiah, California 95482
I(707) 468-0401
CHEMICAL EXAMINATION REPORT
Kiff Analytical
I r~O OLive Drive
Suite 0 Oate Printed Page
Davis, CA 95616 7/29/97 S
I Attn: Joel Kiff
Batch Nmber Receipt Date Client CLient P.O. Send Via
97-0724-00& 07/24/97 09:45 KIFFLAB 10264 Mail
I METHO0 EXTRACTED TEST DATE RESULT UNITS PQL DILUTIO~
(Sample 1 DSP-M,N,O,P Beacon 596 -- continued)
I Silver 6010 7/25/97 NO mg/kg 5.00
Tha[[i~zn 6010 7/25/97 ND mg/kg 7.00
Vanadi~zn 6010 7/25/97 32 mg/kg 24.0
I 7/25/97 260 mg/kg 10.0
Zinc
6010
IPGL - Practica[ quantitation Limit ND - None Detected
* Indicates Detection Limit altered due to Sample Dilution
INOTES:
I Laboratory Director Date Printed: 7/29/97
KIFF ANALYTICAL SUBCONTRACT FORM Subcontract Lab:Alpha Analytical
Please mail results to' Please fax to' 860 Waugh Lane, H-1
Ukiah, CA 95482
JOEL KI FF 916-297-4803
KIFF ANALYTICAL
720 OLIVE DRIVE, SUITE D
DAVIS, CA 95616 707-468-0401
PROJECT NAME · Beacon 596 Account No. · KIFFLAB
PROJECT NUMBER: 1596.15
-e-'.'.'.'.'.'.'.'.~m p I e Matrix Sampled Tests Due
__,-M,N,O,P l'~ SO 07/22~97 Volatile Halocarbons (EPA 8010) 07/28/97 ~
DSP-M,N,O,P . SO 07/22/97 CCR 17 Metals 07/28/97
Relinquished by : l~ Date/Time."~,.~.!~-'t D?[/~'"-' Received by: _"~_~II.0~..~/.~._~ C_~. ~
Relinquished by · Date/Time: Received by:
Ultmm r ho.
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with Re~ YELLOW: Laborato~ Copy P~NK: OHginator Copy u.~
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