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HomeMy WebLinkAboutUNDERGROUND TANKFIRE CHIEF ADMINISTRATIVE SERVICES 2101 "H" Street Bakersfield, CA 93301 VOICE (6611 326-3941 FAX (661) 852-2170 SUPPRESSION SERVICES 2101 "H" Street Bakersfield, CA 93301 VOICE (661) 326-3941 FAX (661) 852-2170 PREVENTION SERVICES SAm~ SeeWC'~. ENweom*em~ S~nWC~S 900 Truxtun Ave., Suite 210 Bo~,ersfield, CA 9:5,301 VOICE (661) 326-3979 FAX (6611 852-2171 FIRE INVESTIGATION 1715 Chester Ave. Bakersfield, CA 93301 VOICE (661) 326-3951 J FAX (661 ) 852-2172 TRAINING DIVISION 5642 Victor Ave. Bakersfield, CA 93308 VOICE 1661) 399-4697 FAX {~61) 399-5763 August 5, 2004 Mr. Roy Saunders JACO Oil Company P.O. Box 82515 Bakersfield, CA 93380-2515 CLOSURE OF 4 UNDERGROUND HAZARDOUS SUBSTANCE STORAGE TANK(S) LOCATED AT 4201 BELLE TERRACE AVE. PERMIT # BR-0315 Dear Mr. Saunders: This is to inform you that this department has reviewed the results for the preliminary assessment associated with the closure of the tanks located at the above stated address. Based upon laboratory data submitted, this office is satisfied with the assessment performed and requires no further action at this time. Accordingly, no unauthorized release reporting is necessary for this closure. If you have any questions regarding this matter, please contact me at (661) 326-3979. Sincerely, Howard H. Wines, III Hazardous Materials Specialist Registered Geologist No. 7239 Office of Environmental Services HHW/dlc cc: J. Whiting, RWQCB K. Malamma, RAM JACO OIL COMPANY BELLE TERRACE & STINE HOWARD'S MARKET SITE BAKERSFIELD, CA. SOIL CONFIRMATION SAMPLING REPORT PROJECT # 200150 MAY, 2004 2103 20th Street · Bakersfield, CA 93301 (661) 324-6152 ENVIRONMENTAL ENGINEERING SERVICES, INC. · FAX (661) 324-6172 !1 I I I I I I '1 I I I I I I I I I I I Belle Terrace Project 200150 May, 2004 TABLE OF CONTENTS 1.0 INTRODUCTION .................................................................................................. 1 2.0 SOIL SAMPLING .................................................................................................. 1 2.1 Pre-Field Investigation .................................................................................... 1 2.2 Confirming Soil Sampling .............................................................................. 1 2.3 Laboratory Analysis ........................................................................................ 2 3.0 FINDINGS .............................................................................................................. 2 3.1 Site Characteristics ............................... ' ........................................................... 2 3.2 Analytical Results ........................................................................................... 2 4.0 DISCUSSION OF RESULTS ................................................................................ 4 5.0 CONCLUSIONS AND RECOMMENDATIONS ................................................. 4 6.0 LIMITATIONS ....................................................................................................... 5 7.0 REFERENCES ....................................................................................................... 6 8.0 SIGNATURE PAGE .............................................................................................. 7 FIGURES Figure 1 Area Map Figure 2 Site Map Figure 3 Site Plan Map APPENDICES Appendix A Laboratory Results Appendix B Sampling Plan ii 2000 04 150 Belle Terrace Belle Terrace Project #200150 May 2004 1.0 INTRODUCTION On March 17, 2004, RAM conducted confirmation sampling at the Howard's Market located at Belle Terrace and Stine, Bakersfield, California. Prior to work at the site, a Job Site Safety Plan and a Site Sampling Plan were prepared. The sampling plan was reviewed in the field with Mr. Steve Underwood of the Bakersfield Fire Department's Environmental Unit prior to that start of sampling. The sampling was conducted as part of the removal of the existing underground tanks, piping and dispensers at the station. This report describes the field procedures, observations, and findings, including laboratory results, of the soil samples collected at the Site. The current use of the site is a convenience market and self-serve gas station. JACO Oil owned the UST's, dispensers, and piping that was removed. Gas sales will no longer be conducted at this site by Jaco Oil. Immediately south and adjacent to the site is a commercial location. The site is bordered on the east by Stine Road and on the north by Belle Terrace. The area directly west consists of private residences. The excavation area was located on the northeast side of the site. The scope of work for this investigation was developed in compliance with applicable Bakersfield City standards, and US-EPA S.W. 846, 3ra Ed. 2.0 SOIL SAMPLING 2.1 Pre-Field Investigation The specific sampling plan for this work was developed using RAM's standard procedures for soil sampling and is attached. A site visit was made prior to the sampling to review site conditions, sampling locations, and site safety. Proposed sampling sites were selected and numbered using the attached plot plan. 2.2 Confirming Soil Sampling Sampling was conducted on Wednesday March 17, 2004 using the site-specific sampling plan. Samples were collected at depths of 2-feet and 6-feet bgs at each end and in the center of each tank location (four tanks total). Samples were also collected at each of the four dispenser sites. Samples were collected at depths of 2-feet and 6-feet bgs. All samples were excavated to depth.using the backhoe at the site. Samples were collected into 2-inch by 6-inch brass sleeves by pushing them into the soil collected in the backhoe bucket at the proper depth. Samples were then sealed with Teflon and plastic caps. All samples were double-bagged and placed on ice. A PID model photo vac 2020, 10.6 eV UV lamp was used to sample the Void left when the brass sleeve was removed from the backhoe. These results were logged in field notes. 2000 04 150 Belle Terrace 1 I I I I I I I I I I I I I I I I I Belle Terrace Project #200150 May 2004 2.3 Laboratory Analysis All the samples collected were labeled, placed in an ice chest, cooled to 4°C, and transported to the laboratory under a completed chain-of-custody form. Selected samples were analyzed for the following constituents using EPA approved methods: · Total petroleum hydrocarbons as gasoline (TPH-g, carbon range C4-C12) using EPA Method 8015M; · Total petroleum hydrocarbons as diesel (TPH-d, carbon range C~2- C24) · Benzene, toluene, ethylbenzene, xylenes (BTEX) and fuel oxygenate methyl tert-butyl ether (MTBE) using EPA Method 8021. Analyses were performed by BC Laboratories, a state certified laboratory for the above analysis. The tentative results of the sampling were forwarded to the Bakersfield City Fire Department's Steve Underwood for their review. 3.0 FINDINGS 3.1 Site Characteristics During sampling the PID meter was used to test the soils for the presence of volatiles and the results recorded in the field notes. This included general testing in and around the site as well as testing the soils removed for sampling. Samples taken using the PID meter registered at 0.00; no further sampling was conducted beyond what is in section 2.2 based upon these readings. 3.2 Analytical Results The analytical results are summarized below and the laboratory reports are included as Appendix B. 2000 04 150 Belle Terrace 2 I I I I I I I '1 Belle Terrace Project #200150 May 2004 Summary of Laborator'~ Results SoilBoring Depth Benzene [Ethylbenzene I Toluene I Xylenes I MTBE I TPH-g I TPH-d No. (ft) (rog/kg) 9-6 (Tank 3) 6.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 9-2 (Tank 3) 2.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 6-6 (Tank 2) 6.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 6-2 (Tank 2) 2.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 3-6 (Tank 1) 6.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 3-2 (Tank 1) 2.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 1-6 (Tank 1) 6.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 1-2 (Tank 1) 2.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 2-6 (Tank 1) 6.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 2-2 (Tank 1) 2.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 5-6 (Tank 2) 6.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 5-2 (Tank 2) 2.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 4-6 (Tank 2) 6.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 4-2 (Tank 2) 2.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 8-6 (Tank 3) 6.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 8-2 (Tank 3) 2.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 7-6 (Tank 3) 6.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 7-2 (Tank 3) 2.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 12-6 (Tank 4) 6.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 12-2 (Tank 4) 2.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL . <PQL 11-6 (Tank 4) 6.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 11-2 (Tank 4) 2.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 10-6 (Tank 4) 6.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL 10-2 (Tank 4) 2.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL D2-6 Disp 2 6.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL D2-2 Disp 2 2.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL D5-6 Disp 5 6.0 ft <PQL <PQL <PQL <PQL <PQL <PQL <PQL D5-2 Disp 5 2.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL 19 D3-6 Disp 3 6.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL D3-2 Disp 3 2.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL D4-6 Disp 4 6.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL D4-2 Disp 4 2.0 ft. <PQL <PQL <PQL <PQL <PQL <PQL <PQL Notes: 1. All results shown are below standards set by the state for contamination to water (Water Quality Goals for the Central Valley Region [California Environmental Protection Agency, Regional Water Quality Control Board, Central Valley Region, August 2003]) 2. All results are reported in rog/kg I I I I I I I I I I zI 2000 04 150 Belle Terrace I ! I I I I I I I I I I I I I I I I I Belle Terrace Project #200150 May 2004 4.0 DISCUSSION OF RESULTS The level recorded for all constituents is below the standards described in the Water Quality Goals for the Central Valley Region (California Environmental Protection Agency, Regional Water Quality Control Board, Central Valley Region, August 2003). Groundwater at this location is estimated to be greater than 150 feet below ground surface (bgs). These levels are determined by the analytical method used, the degree of interference in the lab test, and is based on the QA/QC used by the lab for certification. The Regulatory Threshold (R.T.) is an amount, which varies by chemical that is typically used to determine if further investigation is need or provide an initial cleanup level. None of the concentrations found exceeded the standards described by the California EPA, or Bakersfield Fire Department, Environmental Unit. Further investigation or active remediation for these specific constituents at this site is not warranted. 5.0 CONCLUSIONS AND RECOMMENDATIONS Based on the findings, RAM concludes that levels of BTEX, MTBE, gasoline, and diesel constituents are not present above the stated regulatory levels in the soil or at levels where they would pose a potential threat to groundwater beneath the location. In addition, · The contaminate source U.T. and past improper management practices (possible overfilling) have been eliminated, · There is an impervious layer of asphalt/concrete over the area, · There is no source of water that would provide hydraulic gradient to drive remaining hydrocarbons lower, and · Natural Bio-remediation/attenuation will reduce Petroleum Hydrocarbons to non- detect in the sub-surface time. The soils sampled at this site, should be used for either backfill at this site or be allowed to be removed for beneficial use at another location, or disposed of as inert soils. RAM does not recommend any further action at this site. This report is submitted to the client for their use and submittal to the Bakersfield Fire Department's Environmental Unit for their review and approval. 2000 04 150 Belle Terrace 4 I I I I I I I I I I I I I I I I I I '1 Belle Terrace Project #200150 May 2004 6.0 LIMITATIONS RAM Environmental Engineering Services, Inc. has prepared this Report, for the exclusive use of Mr. Roy Saunders of JACO Oil as it pertains to the property located at Belle Terrace & Stine Road in Bakersfield, California. Our professional services have been performed using the degree of care and skill ordinarily exercised under similar circumstances by other professionals practicing in this field. No other warranty, expressed or implied, is made as to the professional advice in the Report. Any use of or reliance on this Report by a third party shall be at such party's sole risk. RAM assumes no responsibility for site conditions or activities that were outside the scope of the inquiry requested by Mr. Roy Saunders. It is recognized that regulatory requirements may change, including the revision of accepted action levels, which could necessitate a review of the discussion, findings, recommendations Or opinions of the Report. 2000 04 150 Belle Terrace 5 I I I I I I I I I I I I I I I I I I I Belle Terrace Project #200150 May 2004 7.0 REFERENCES Department of Water Resources (DWR), 1975, California's Ground Water, DWR Bulletin No. 118 Kern County Water Agency, Water Supply Report, 1999, May 2003. RAM Environmental Engineering Services, Inc., Soil Sampling Workplan, September 2003. Kern County Environmental Health Services Department. U.T. 35. US-EPA S.W. 846 3rd. Ed. 2000 04 150 Belle Terrace Belle Terrace Project #200150 This Soil Characterization Report for Mr. Roy Saunders, dated May 24, 2004 was prepared by RAM Environmental Engineering Services, Inc. under the responsible charge of the following professionals: . · Kevin Malamma, REA Project Manager I I I I I I I I I 2000 04 150 Belle Terrace 7 I I I I I I I I I I I I I I I FIGURES ':l I I I I I I I I I I I I I I I I I ~ XMii~ 4.6 ' '1---=' "~ T-~ ' :- ~"--, .... ... -:_ I ': /,!~ "*. >,.~i-r'a ..... " ~ ............ ~, i ~' 1', ' -:-:','..-' '; '~ L .'~r ~ -'~-i~ , I I t '" F U~ ;-F-K.~" ~ Mt /t~111 O~ use subje~ to license. ~ ~ mi ~ 20~ DeLo~e. ~a~4.5.~ 0 ~ ~ ~ ~ ~.delo~e.com ~ (~.9~ E) ~ ~om ~2-0 JACO O~ FIGU~ 1 ~ ENV~ONMENTAL MAY 2004 A~A M~ ENG~EE~G SERVICES, INC. SOIL CONF~ATION HOWA~'S M~T 2103 20TM ST~ET SA~L~G REPORT BELLE TE~CE & ST~ BA~RSFIELD, CA.93301 I 2000 04 150 FIGURE_I_AREAMAP ~ XMapl~4.5 /[ L ~: .,, ..... ~ ' '~":" ~. ~, ~:~'~ /~ I~~,~,~ ~ . ~ .... ~' .", ........ ~ ...... ~,..~  .~'' .... ;. ~' :.~3 .' };:~,,.~ '~.2,. ' · · ~ ~/~1 .... ~~~J~ ~: ,-.,',-': .... . . ~ :1-~1~-' :: '; ~:-'~ :1~31~ d~ ~1~~?/' ~ ~ ~ ~ ~1[,: .......... l,.~ ~ ~?.~:~:~.. r~-- ~- · ~ L,~~~. ,~, ' '. · ' "'~ ~ ~, ~~~-~;7~,'*'~ : ~; . ~ ';; ';~ ;" ~ ~ Dam use subjed to license. ~ ~ fl B2O~De~e.~a~4.5. 0 ~80 360 ~0 720 900 ~.delome.com MN (13.9~ E) Dm ~om 1~0 JACO O~ FIGU~ 2 ~M E~ONMENTAL MAY 2004 SITE M~ ENG~E~NG SERVICES, ~C. SO~ CONF~ATION HOWe'S M~T 2103 29TM ST~ET SA~L~G ~PORT BELLE TE~CE & ST~ BA~FIELD, CA. 93301 2000 150 FIGURE _2_SITE MAP i~ELLE TEI~.IEAC E /i I / / III iI I I III II/ F~ ~ N ,'%-~ ~ ,' -- ~ 7~~ - -- _',1 /~ "'~ '~ ~ ~ '~ Pile , ' 4 ~,ooo GAL. STOOGE TAN~ / k- ---- / '~ Il/ 5 ~__~__~__~___ [ ,'.,'" _ ,,,,, ~ ,, / ~ x EUEL ~MFI~N~ I ~ II ~ II II ~ I II II II A.C. PAVING I II II II / / / TANK 1 TI-2, TANK 2 T4-2 T2-2 T2-6 TANK 3 T7-2 TANK 4 T10-2 TI-6 T4-6 T7-6 T10-6 T5-2 T8-2 T11-2 T5-6 T8-6 T11-6 DISPENSERS D2-2 D2-6 SPOIL PILES SP1 SP2 D3-2 N/A D3-6 N/A D4-2 D4-6 D5-2 D5-6 N/A T3 -2 T6-2 T9-2 T 12-2 N/A N/A T3-6 T6-6 T9-6 T12-6 N/A i N/A 3 2 CONVENIENCE MARKET SPOIL PILE 2 )[ 2 ~, 5 I~ 8 t, 11 42' 5&' PARKING 9 5PACES 9'x20' I HANDICAP 14'x20' / / / / I / / / / / / ~ /, , I I I I I I II I I I __ I I I I I I I i I I I I I I I II I I I /, , I I I I I I I / I II I I I /, , I I I ' ' I I I I / / I / / A.P.N.:01-005403-025-0 J DAlE J REVISIONS SCALE: F: l 1" = lOFT I °'~d4 o2 o, CONVENIENCE SIORE FOR: .C:)HEET NO. s.!  BAKERSFIELD, CALIFORNIA 933 OP APPENDIX A LABORATORY REPORTS I I I I I I I I I I I I I I I I I I I Certified Analytical Report .Laboratories, Inc. Cover Report RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MAEAMMA Project Number: COC Number: BCL Number:' Cover- Page I of 1 Zool~-© 04-02683 This report contains the analytical results for the samples received under chain of custody by BC Laboratories, Inc. The samples were logged into the Laboratory Information Management System (LIMS) and BC Lab numbers were assigned to each sample. The result of the temperature check, condition of the samples and any other discrepancies were recorded on the cOoler receipt form. All applicable quality control procedures met method-specific acceptance criteria, except as. noted on the following analytical and quality control reports. This report shall not be reproduced except in full, without written approval of the laboratory. California DOHS Certification #1186 Authorized Signature All rexu t listed iq this report are for the exclusive use of the submitting part>,, BC Laboratories, Inc. assumes no responsibil ty for repollr alteration detaz0h~oczb, lrd party Printed 07jl~o'~l:'~jO~Cl~.rtlB]tilZ~ersfield, CA 93308 * (661)32%4911 * Fax(661)32% 1918 * www.bcla~'s.comu°'u/ui3'5 ~ interpretation. Laboratories, Inc. Chain of.Custody Form 9504 ' ~eport To: 0 A & J ~t~ . Client: r'N"I,kI~ ~-"~J. ~. Prqject ~: ~t~ 0 I Attn: ~{~ ~~. Project mame~~~~ Street Address: 2[0~ ~~ Project Code: Ci~, State, gip:~~ ~ ~! Sa~pler(s): ~~~ ~4'~}'~{'~ Phone~q ~5 % Fax~ [[3 ~ Samgpl? Matrix m~ Are there any tests ~th 'g' ' Email Addr{~s: ~ - - ~'~,Q ~(}. or equal to 48 hours? ttal ~: ~~0 ~'~ J ~.~ ~'%' ~ ~ ~ yes o Submi ~ ~ ~ ¢ ~ ~ * Standard Turnaround = 15 work days ': ' ' ::' ' 'i ~ -~~]: * ~otes ___ ' [ I I ~ DI~TRIBUTION Ill/ Sample Disposal ~ Special RepoSing ,  Report Drin~ng ~ ~aw Data Same as above Wate~t~ FO~? ~ Re~rn to Client Disposal by lab ~ ~chive: Months_~ . ~ Q~ ~ WIP Dat~ Time Client: ~Yes ~No Date T~e //37 , Address1 Send Co~y to State of ~ 2. ~li~.ishea ~y Ti~e ~ate Ci~: ~ State Zip cat ~ _ _ Attn: ~ Yes~o 3. Reliaqaished ~y Date . ?ime ~. [eceivea ~y ~ate ] ?ime POg: BC Laboratories, Inc. - 4100Atlas Ct. - Bakersfield, CA 93308 - 661.32'~ - BC LABORATORIES INC. SAMPLE RECEIPT FORM Rev. No. 10 01/21/04 Page Submission #:C'~-~.~~ I Project Code: I TB Batch # SHIPPING INFORMATION ~ ';x,~HIPPING CONTAINER Federal Express [] UPS [] Hand Delivery Ice Chest/l~ None [] BC Lab Field Service [] Other [] (Specify) Box 'E3 Other [] (Specify). Refrigerant: Ice Blue Ice [] None [] Other [] Comments: CustodySeals:,ceChestCl I IContainersCl D None)l~ Comments: ntact? Yes []No [] Intact? Yes [] Nq All samples received? Yes~i~ No[] All samples containers intact? Yes/C~No [] Description(s) match COC? Y~,,~ No [] I SAMPLE NUMBERS QTGENERAL MINERAL/GENERAL PHYSICAL PT PE UNPI~.ESER. VED (2'1' INORGANIC CIIEbIICAL METALS PT INORGANIC CHEMICAL METALS PT CYANIDE PT NITROGEN FORMS PT TOTAL SULFIDE 2oz. NITILkTE / NITRITE 100mi TOTAl. ORGANIC CARBON QT TOX PT CtlEMICAI, OXYGEN DF. MAND :PtA PHENOJACS 40_.mi VOA VIAL TRAVEL BLANK 40n'd VOA VIAL QT EPA 413.1,413.Z~418.1 PT ODOR RADIOLOGICAL BACTERIOLOG ICA L 40 mi VOA VIAL- 5114 QT EPA 508/608/8080 QT EPA 515.1/8150 QT EPA 525 QT EPA $~5 TRAyEL BLANK 100mi EPA 5;47 100mt EPA 531.1 QT EPA 548 QT EPA 549 QT EPA 632 QT EPA 801 StOl Q'F QA/QC ~)1' ANIBER 32 OZ. JAR SOIL PCB VIAIr PLASTIC BA.(; .FERROUS IRON ENCORE IH:\DOCS/WPSO\LAB DOCS\FORrvlS\SAMREC 2.WPD ] Laboratories, Inc RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number iReceive Date/Time 03/16/2004 @ 11:38 .......... Project Number ;;0150 iSampling Date/Time 03/16/2004 @ 10:30 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point iSP 1 SOIL PILE-TANKS Sample Matrix Soil ................................ Sampled By iK. Malamma . BCL Sample ID 04-02683-1 Benzene ~ < PQL ~ Ag/kg ~ 0:005 0.00036 ~ 8021B ~03/17/04 ~03/17/04 03:03 HKS GO-V8 1 i 302-100442 . ND ~ S09 %i~ ................. ~~ ~ mg/kg 0.005 0.0040 8021B !03/17/04 i03/17/04 03:03 ~ HKS GC-V8 I 1 1~02-100~"--~ ........ ~ ..... ~--'~F ...... ~i~;~;;~; ...................... [--- < POL i me/kg I o.oo5 0.~18 ~ 8021B 03,17,04 103,17,04 o3:o3 ! HKS GC-V8 1 13o2-1oo~4~._L___~ .......... ~ ....... M~(~~ .............. ~---%-- [ me/kg ~ 0.02 ~ 0.00056 ~ 8021B }03/17/04 J 03/17/04 ~03:03 HKS 60-V8 I I 302-10044~__.L__~_P ......... 5~?_ ......... Total Xvlenes j < PQL i me/kg ] 0.01 I 0.0098 I 8021B ; 03/17/04 ~ 03/17/04 ~03:03 I HKS / GC-V8 1 302-100442 : ND ; s09 Gasol ne Range Organ cs (C4 - I ' ~ ~ ' ' ' C12) ~ < PQL i me/kg I 1 ~ 0.046 I 8015M t03/17/04 ~ 03/17/04 I03:03 I HKS I ec-v8 ; 1 ~ 302-100442 Su[ro~ate.~aompounds ........................... [ ............... ~ ..................................................................... [; ......................... ~ .......................................................... .----.-.. - ............ .--.--.---...-.--- ...-. ....... ~ ..................... ......-. . .-.. a a a-Trifluorotoluene 34 ~ % 70-130 8021B 03/17/04 03/17/04 03:03 I HKS GC-V8 ! I i 302-100442 a,a.a-Tnfluorotoluene (8015 . , ~ ' Surrogate) 49 % 70-130 i 8015M ~ 03/17/04 ~ 03/17/04 03:03 HKS GC-V8 1 302-100442 I { .s09 tlag E~lanations 09 IThe ~ recovery on the sample for this compound was not within the control limits. C ifica ion California DOHS ,~¢!esulLst,sted #1 186 m this report are for the exclusive use of thc submitting party.. BC Laboratories, Inc. assumes no respoosibility for report alteration, separation, deMachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-t918 * www.bclabs.com Printed 03/22/2004 08:42:03 04-02683-1 Laboratories, Inc RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number ___ Receive Date/Time 103/16/2004 @ 11:38 Project Number ;200150 Sampling Date/Time 03/16/2004 @ 10:45 Sampling Location 3ELLE TERRACE Sample Depth --- Sampling Point SP 2 SOIL PILE-DISPENSERS Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02683-2 Benzene ] < PQL I mg/kg 0.005 I 0.00036 8021B ~ 03/17/04 03/17/04 10:08 HKS GC-V8 [ 1 302-10044_2 ,__,_N_D____[ T01uen~- .......... ~ <PQL mg/k; / 0005 I 00040 8021B 03/17/04 03/17/04 10:08I HKS GC-V8~ 1_ 302-100442_[____N~ -Eth--vl%e%~;~-~ ...... --~----< pQ----~- 1- rng/k~--~ I -0 00-'-~-~ [ --~-0018 i 8021~ 103/17/04 !03/17/04 10:08 HKS GO-V8 / 1 302-100442 ...... '" ...................... ~" ...... ? ' ! I I ' Methyl t-buty ether < PQL mg/kg 0.02 t 0.00056 8021B I 03/17/04 03/17/04 10:08 HKS GO-V8 I 1 302-10044_2__L___N__D~_£[ ~;~a~-~/~-~n-e~ .......................... 0 010 ! mg/kg 0 01 0.0098 I 8021B 03/17/04 03/17/04 10:08 HKS GO-V8 [ I 302-10044~ ...................... ~ '" [ i I ' I [ Gasol ne Range Organics (C4 - ! ' I I I ' I C12) I 1 7 I rng/kg I 1 i 0 046 i 8015M I 03/17/04 103/17/04 10:08 HKS I 6C-V8 I 1 I 302-100442 ~:;~ :::::::::::::::::::::::::::::::::::::: ................... ~;:::::~ :::::::::::::::::::::::::::::::::::: ................. ;t:- ....................... i:;i::i55~:;:i?,~;i~i~i~!~}::;!iii!!;:~il:! ~ i~i?.!:.~;~i;~:i;;i;;i!fiii::~ !~(: I.~ ~:;!:Ra~;i:; .............................. a a a-Trfuoroto uene ' I 88 % [ 70-130 8021B 03/17/04 03/17/04 10:08 I HKS GC-V8 ! 1 I 302-100442 a a a-Tr fluorotoluene (8015 I I ' I ' I S'u~rogate) i 114 % 70-130 , 8015M 103/17/04 103/17/04 10:081 HKS I GC-V8I 1 1302-100442 California DOHS Certification #1186 All results listed in this repo~X are for the exclusive use of the submitting party.. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/22/2004 08:42:09 04-02683-2 Laboratories, Inc II 1 1 1 mu~ I RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number --- Receive Date/Time 03/16/2004 @ 11:38 Project Number 200150 Sampling Date/Time 03/16/2004 @ 10:30 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point SP 1 SOIL PILE-TANKS Sample Matrix Soil _ Sampled By K. Ma aroma BCL Sample ID 04-02683-1 Benzene < PQL I mg/kg 0.005 0.00036 8021B 03/17/04 ~ 03/17/04 03:03 HKS GO-V8 I 302-100442 ND S09 _~ T~luene < PQL mg/kg 0.005 0.0040 8021B 03/17/04 03/17/04 03:03 HKS CC-V8 1 302-100442 ND S0g Ethylbenzene ~ < PQL mg/kg 0.005 0.0018 8021B 03/17/04 03/17/04 03:03 HKS CC-V8 ~ 1 302-100442 ND s0g Methyl t-butyl ether ~ < PQL mg/kg 0.02 0.00056 8021B 03/17/04 03/17/04 03:03 HKS CC-V8 1 302-100442 ND S0g Total Xylenes ~ < PQL mg/kg 0.01 0.0098 8021B 03/17/04 03/17/04 03:03 HKS CC-V8 1 302-100442 ND S0g Gasoline Range Organics (C4 - ~C12) < PQL mg/kg 1 0.046 8015M 03/17/04 03/17/04 03:03 HKS CC-V8 I 302-100442 ND S0g a,a,a-Trifluorotoluene 34 % 70-130 8021B 03/17/04 03/17/04 [03:03 HKS CC-V8 I 302-100442 s09 ~a,a,a-Trifluorotoluene (8015 Surrogate) 49 % 70-130 8015M 03/17/04 03/17/04 03:03 HKS CC-V8 1 302-100442 s09 Flag ~xplanations I S09 IThe surrogate recovery on the sample for this compound was not within the control limits. Alt results li~sted tt,t) ~ r~g,ort are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibili .ty for report alteration, separation, detachment or third party interpretation. California DOHS Certificatton ~-i q ~o 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Pr'inted 03/18/2004 14:24:33 04-02683-1 Laboratorie& Inc l 1 I / ~ge I RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number --- Receive Date/Time 03/16/2004 @ 11:38 Project Number 200150 Sampling Date/Time 03/16/2004 @ 10:45 Sampling Location BELLE TERRACE Sample Del~th --- Sampling Point SP 2 SOIL PILE-DISPENSERS Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02683-2 Benzene < PQL mg/kg 0.005 0.00036 8021B 03/17/04 03/17/04 110:08 HKS GC-V8 1 302-100442 ND Toluene < PQL mg/kg 0.005 0.0040 8021B 03/17/04 03/17/04 10:08 HKS GC-V8 I 302-100442 ND Ethylbenzene < PQL mg/kg 0.005 0.0018 8021B 03/17/04 03/17/04 10:08 HKS GC-V8 1 302-100442 ND _Methyl t-butyl ether < PQL mg/kg 0.02 0.00056 8021B 03/17/04 03/17/04 10:08 HKS GC-V8 1 302-100442 ND Total Xylenes 0.010 mg/kg 0.01 0.0098 I 8021B 03/17/04 03/17/04 10:08 HKS GC-V8 1 302-100442 ND Gasoline Range Organics (C4 - C12) 1.7 mg/kg 1 0.046 I 8015M 03/17/04 03/17/04 10:08 HKS GC-V8 1 302-100442 ND a,a,a-Trifluorotoluene 88 % 70-130 8021B 03/17/04 03/17/04 10:08 HKS GC-V8 1 302-100442 a,a,a-Trifluorotoluene (8015 Surrogate) 114 % 70-130 8015M 03/17/04 03/17/04 10:08 HKS GC-V8 1 302-100442 California DOHS C~t~tk~ ~¢~ 86on are for tbe exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibib~ for report alteration, separation, detachment or flfird party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/18/2004 14:24:43 . 04-02683-2 I I I I I I I I I Certified Analytical Report Laboratories, Inc. Cover Report Cover - Page 1 of 1 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Project Number: COC Number: BCL Number: 04-02683 Dear Mr. Malamma: This report contains the analytical results for the samples received under chain of custody by BC Laboratories, Inc. The samples were logged into the Laboratory Information Management System (LIMS) and BC Lab numbers were assigned to each sample. The result of the temperature check, condition of the samples and any other discrepancies were recorded on the cooler receipt form. All applicable quality control procedures met method-specific acceptance criteria, except as noted on the following analytical and quality control reports. This report shall not be reprodUced except in full, without written approval of the laboratory. California DOHS Certification #1186 Authorized Signature All re,:uit listed iq this report are for the exclusive use of the submitting party, BC Laboratories, Inc. assumes no responsibility for report alteration, detachment or third party interpretation. ~ ~ ersfield, CA * * Printed 0:J/~/~3,C~.~a~ ' 93308 * (66i)32%491t Fax(661)327-1918 www.bclabs, coO4-02683 ~ Laboratories, Inc RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA I cedl~ed 1 Analytical Fuel Identification / Quantitation Summary EPA Method 8015M) CCC Number --- Receive Date/Time 03/16/2004 @ 11:38 Project Number 200150 Sampling Date/Time 03/16/2004 @ 10:30 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point SP 1 SOIL PILE-TANKS Sample Matrix Soil Sampled By IK. Malamma BCL Sample ID 04-02683-1 Diesel Range Organics (C12- C24 < PQL mg/kg 10. 3. I 8015M 03/17/04 03/18/04 13:01 MAA GC-12A 1 Tetracosane I 97 % 46-137 8015M 03/17/04 i03/18/04 13:01 MAA GC-12A 1 California DOHS Certification #1186 All results listed in this report are for the exclusive usc of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/25/2004 10:03:45 04-02683-1 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification /Ouantitation Summary (EPA Method 8015M) coC Number_ I--- Receive Date/Time i03/16/2004 @ 11:38 Project Number 200150 Sampling Date/Time 03/16/2004 @ 10:45 Sampling Location BELLE TERRACE Sample Depth --- S__ampling Point SP 2 SOIL PILE-DISPENSERS Sample Matrix Soil Sampled By I K. Malamma BCL Sample ID 04-02683-2 :; ;; ~ii ~:;: ~i~ ~; :~: ~ :~:~: ~: ::~:; :;~: ~:~ :~: ~:~: i:': i:: ::: ::~: i: i:i:~: ~ ;ii :~:~: :; ;;: ::: i:: ~:~ :~: ~:;: i: ;::~:~ :i: ;;: i: ~:': ?i :i:: :~: i:i::~ :~: i:~: ~: i:~ :;~:~: ~:~ :~: ~:~: ~:::~: ~:~:~ ......................................................................................... · ........................................................................................................... ::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::: :::::::::::::::::::::::::::::::::::::::::::::::::::: ::~ii?:i!i~ii!iliiiil ....................................... !~R~i~!~:!: ........................................ :;!~:![h~I~:;i:i:i:!~ ......................... !i!i ~!i !i:.i!~i! i!i~i ii~ ii!~!:~!i I::} i !i!i!i!i!~:g!!!!!!!ii!i!~!~!!~!i!i :i:i::~:!:!?!:!:!:~a D!:!:!:i:!?i~:::!:::! Diesel Range Organics (C12- C24 15 I mg/kg 10. 3. 8015M ~ 03/17/04 03/18/04 13:26 MAA GC-12A I I A52 Tetracosane 106 % 46-137 8015M 03~17104 03/18/04 13:26 MAA I GC-12A 1 Flag_ 1 Explanations A52 ~~m not typical of diesel. California DOHS Certification #1186 All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/25/2004 10:03:49 04-02683-2 ~ Laboratories, Inc RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 8015M) CCC Number ___ --~ Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 09:50 Sampling Location BELLE TERRACE Sample Dap.th --- Sampling Point T~-6 TK 3-9-6' Sample Matrix Soil Sampled By IK. '~a~am~-~a BCE Sample ID 04-02749-32 Diesel Range Organics (C12- C24j < PQL mg/kg 10. 3. 8015M 03/18/04 03/19/04 22:09 MAA I GC-,12A I 1. I Tetracosane f 79 ! % I 46-137 8015M I03/18/04 !03/19/04 122:09 MAA GC-12A 1. California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Printed 03/23/2004 1 6:47:45 41oo Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327- 918 * www.bclabs.com 04-02749-32 ._~~ Laboratomes, Inc RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 8015M) COC Number --- Receive Date/Time '03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 09:45 ..... Sampling Location BELLE TERRACE Sample Depth --- Sampling Point T9-2 TK 3-9-2' Sample Matrix Soil ..................... Sampled By K. Malamma BCL Sample ID 04-02749-31 Diesel Range Organics (C12- C24 < PQL mg/kg 10. 3. ] 8015M 03/18/04 03/19/04 20:31 MAA '"'"~C-12A"'""'1. '"' "'I ' t ' Tetracosane I 100 % 46-137 8015M 103/18/04 103/19/04 20:31 I M~'"'"l'";'~Ci~"-"l ........ i"; ............................................ I : .......... California DOHS Certification #1186 Al! results listed in riffs report are for the exclusive use of the submitting party. DC Laboratoffes, Irtc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Printed 03/23/2004 16:47:37 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com 04-02749-31 ._~_.~ Laboratortes, Inc RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Ouantitation Summary 'EPA Method 8015M) COC Number --- Receive Dat~fTime 03/17/2004 @ 11:40 Project Numbe~- 200150 Sampling Date/Time 03/17/2004 @ 09:44 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point T6-6 TK 2-6-6' Sample Matrix Soil Sampled By IK. Malamma BCL Sample ID 04-02749-30 Diesel Range Organics (C12- C241 < PQL I me/kg ! 10. I 3. I 8015M 03/18/04 t 03/19/0420:06 MAA GC-12A 1. Tetracosane / 95 ........... i .............. ;~ ................ t ................ ~;2'i'~'¢ ............................ l'"'""~;i;~"'-'"l";;ii";>;;~'""l ;;;'i';>;;i'""i'~;i;';'"t--"~"l GC-12A '"'"'i. I ", California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of thc submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/23/2004 16:47:29 04-02749-30 ~ Laboratortes, Inc RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Ouantitation Summary (EPA Method 8015M) COC Number I'-- Receive Date/Time 03/17/2004 @ 11:40 Project Number~ 200150 Sampling Date/Time 03/17/2004 @ 09:42 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point T6-2 TK 2-6-2' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-29 Diesel Range Organics (C12- C24t < PQL mg/kg 10. I 3. ~ 8015M 03/18/04 103/19/04 , 19:41 MAA GC-12A I 1. i! Tetracosane 101 I % 46:137 I 8015M 103110104103119104 19:41 MAA GC-12A, 1. California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the submitting party. BC Laboratoffes, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/23/2004 16:47:20 O4-02749-29 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Ouantitation Summary (EPA Method 8015M) COC Number .._ Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 09:40 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point T3-6 TK 1-3-6' Sample Matrix Soil ............. Sampled By K. Malamma BCL Sample ID 04-02749-28 Diesel Range Organics (C12- C24', < PQL mg/kg 10. I 3. 8015M 03/18/04 I 03/19/04 19:16 MAA I GC-12A 1. I I Tetracosane 98 I % 46-137 8015M 03/18/04 03/19/04 19:16 MAA GC-12A 1. California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the submitting party. BC Labomto~es, hlc. assumes no responsibility for report alteration, separation, detachment or third party interpretation, 4100 Atlas Court * Bakemfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/23/2004 16:47:11 04-02749-28 a a c RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 8015M) COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Da, te/Time 03/17/2004 @ 09:37 _Sampling Location BELLE TERRACE Sample Depth --- _Sampling Point iT3-2 TK 1-3-2' Sample Matrix Soil Sampled By IK. Malamma -- BCL Sample ID 04-02749-27 Diesel Range Organics (C12- C24t < PQL I mg/kg I 10. 3. 8015M 03/1e/04 103/19/04 18:52 Tetracosane t i 102 I % I 46-137 t 8015M 03/18/041103119104 18:52 California DOHS Certification #1186 Al! restdts listed in this report are for the exclusive use of the submitt/ng party. BC Laborato~es, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Printed 03/23/2004 16:47:02 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com 04-02749-27 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary 'EPA Method 8015M) COC Number _ ;~ Receive Date/Time 03/17/2004 @ 11:40 Project Number 0150 Sampling Date/Time 03/17/2004 @ 09:33_ Sampling Loca_tion BELLE TERRACE Sample Depth --- _ Sampling Point ~T~-6 TK 1-1-6' Sample Matrix. Soil Sampled By - tK. ~a-~am-~a tBCL Sample ID 04-0274-~-2~6 Diesel Range Organics (012- C24t < PQL i mg/kg 10. 3. I 8015M 03/18/04 103/19/04 18:27 MAA GC-12A 1. Tetracosane I 99 I % I 46-137 I 8015M 03/18/04 I 03/19/04 18:27 MAA GC-12A 1. California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the submitting party. BC Laboratorles, [nc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Printed 03/23~2004 1 6:46:53 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com 04-02749-26 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 8015M) COC Number --- Receive Date/Time t03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 09:30 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point T1-2 TK 1-1-2' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-25 Diesel Range Organics (C12- C24' < PQL I mg/kg 10. 3. 8015M 03/18/04 03/19/04 118:02 MAA I GC-12A 1. Tetracosane 96 % I 46-~3~ I ~0=5M [03/18/04 03/19/04 18:021 MAA IGC-12A I ~' California DOHS Certification #1186 Al! results listed in this report are for the exclusive use oft. he submitting party. BC Laboratories, Inc. assumes no responsibility for report aJterarion, separat/on, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/23/2.004 16:46:45 04-02749-25 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST, BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 8015M) CDC Number I--- IReceive Date/Time 03/17/2004_2_11~:_4_0- Project Number 200150 Sampling Date/Time 03/17/2004 ~_09:~2_5_ Sampling Location BELLE TERRACE Sample Depth --- _ Sampling Point T2-6 TK 1-2-6' Sample Matr. ix Soil .............................. Sampled By K. Malamma . BCL Sample ID 04-02749-24 ..................... ;~I.-....,,........,...:;:.. ..... ~i[ ................................ y _..~.~it .............................. ii .............. ....~ ...................... ........... .............. ;.~.: ......~ ....... ...-........... Diesel Range Organics (C12- C24t < PQL mD/kg 10. I 3. 8015M 03/18/04 03/19/04 17:37 MAA I GC-12A I 1. Tetracosane 99 I % 46_137 I 8015M t03,18,04 103,49,04 17:37 M~ I GC-12A I 1. , I California DOHS Certification #1186 Al! results listed in this report are for the exclusive u.se of the submitting party. BC Laborato~es, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation Printed 03/23/2004 16:46:36 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com , 04-02749-24 a a c RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 8015M) COC Number t--- I Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 09:22 Sampling Location BELLE TERRACE Sample Depth --- _Sampling Point T2-2 TK 1-2-2' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-23 Diesel Range Organics (C12 - C24' < PQL I mg/kg 10. 3. 8015M 03/18/04 03/19/04 ~ 17:13 MAA I GC-12A 1. T..etracosane j 101 I % j 46-137 J 8015M j03/18/04 03/19/04 17:13 MAA IGO-12A 1. California DOHS Certification #1186 Al! results listed in this report are for the exclusive use oft. he submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Printed 03/23/2004 1 6:46:27 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com 04-02749-23 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary 'EPA Method 8015M) COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 09:20 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point T5-6 TK 2-5-6' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-22 Diesel Range Organics (C12- C24 < PQL mg/kg 10. 3. 8015M 03/18/04 ! 03/19/04 16:48 I MAA GC-12A Tetracosane 96I % 1 46-137 t8015M 03,18104 03/~9/04 16:48 California DOHS Certification #1186 Al! results listed in dtis report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printe6 03/23/2004 16:46:19 04-02749-22 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 8015M) COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 09:17 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point___ T5-2 TK 2-5-2' Sample Matrix Soil ~Sampled By K. Malamma BCL Sample ID 04-02749-21 Diesel Range Organics (C12- C24 < PQL I mg/kg 10. I 3. 8015M 03/18/04 03/19/04 10:57 MAA GC-12A 1. I Tetracosane I 100 I % 46-137 8015M t03/18/04 103/19/04 10:57 MAA I GC-12A 1. , California DOHS Certification #1186 All results listed in'this report are for the exclusive use of the submitting party. BC Labomto~es, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Printed 03/23/2004 16:46:10 4~00 Atlas Court* Bakersfield, CA 93308* (661) 327-4911 * FAX (661) 327-1918' www.bclabs.corn 04-02749-21 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 8015M) COC N umber --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 09:15 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point T4-6 TK 2-4-6' Sample Matrix Soil ,Sampled By K. Malamma BCL Sample ID 04-02749-20 Diesel Range Organics (C12 - C24~ < PQL mg/kg I 10. I 3. 8015M 03/18/04 03/20/04 10:55 M~ GC-I~ 1. Tetracosane J 90 % J 46-137 , 8015M 03/18/04 03/20/04 10:55 M~ GC-12A 1. j California DOHS Certification//1186 Al! r¢suJts listed ~ this report ate for the exc]usive use o£ thc submJttin~ path,. BC Laboratories, [~c. assumes no respons~.b~.]i~ for report ~iteradon, separafioQ, detachment or third parb, [u[¢rprctafion. Printed 03/23/2004 1 6:46:02 4100 Atlas Court * Bakersfield, CA 93308 * (661) 32%4911 * FAX (661) 32%1918 * www.bclabs.corn 04-02749-20 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 80-15M) COC Number ;-~ Receive Date/Time 03/17/2004 @ 11:40 Project Number 0150 Sampling Date/Time 03/17/2004 @ 09:10 ,Sampling Location BELLE TERRACE Sample Depth --- Sampling Point T4-2-TK 2-4-2' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-19 Diesel Range Organics (C12- C24 < PQL I mg/kg 10. t 3. 801§M 03/18/04 03/20/04 10:30 MAA GC-12A 1. Tetracosane 97 J % I 46-137 8015M ll03/18/04 j03/20/04 10:30 I MAA GC-12A 1. I California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report a teration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www,bclabs.com Printed 03/23/2004 16:45:53 04-02749-19 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Ouantitation Summary (EPA Method 8015M) COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 09:05 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point T8-6 TK 3-8-6' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-18 Diesel Range Organics (C12- C24t < PQL mg/kg 10. 3. t 8015M 03/18/04 i 03/20/04 10:06 MAA GC-12A 1. Tetracosane I 96 % I 46-137 8015M 103/18/04 103/20/04 110:06 i MAA GC-12A t 1. , California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the subnfitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Printed 03/23/2004 16:45:44 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com 04-02749-18 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 8015M) COC Number --- Receive Date/Time 03/17/2004 @ 11:40 ............. Project Number 200150 Sampling Date/Time 03/17/2004 @ 09:02 Sampling Location BELLE TERRACE Sample Depth Sampling Point T8-2 TK 3-8-2' Sample Matrix Soil Sampled By K. Malamma IBCL Sample ID 04-02749-17 Diesel Range Organics (C12- C24t < PQL I mg/kg I 10. 3. 8015M 03/18/04 103/20/04 09:41 MAA GC-12A 1. I ii:iii:i:i:i:ii:i:i:i:iii?i:i:i:i:i:i:i:i:i:i:i:::i:i:i:i:i:ii:i:i:iii:ii:i:i:ii:i:i:iiii:i:i:i:i?i:i:i:i:::i:i~:i:;!:ii:!:~?!:!~:i:!~i::i::i:::~ii:::i:i:i::i:i:i:i:i:i:i:i?i:::i:i:i:i:i:i:i[i:i:i:i:i~:i~:iii:i~!~:i:!:!:i~i:ii:ii:i:i:i:~:i:i:i:i:i:i:3i:~:i~:!:!~:!~::i~ :::::::::::::::::::::::::::::::::::::::::::::::::: ........... ~-:~:- ............................. -~-: ................................ ~iiil~!iii!i':~ ~ !!:.!!!!!!!!!!!~!!!!¥:~!i ':~' ................................... i:!:!R~i~$i:3i~ ii:i:i:!!~:;!~:!:i:iiiiiii;iiiili~iii~i~!!~:!:!li~[i~JlA' 3: iilili i? ii!ii iii : ::::: Tetracosane i 103 % 46-137 t 8015M ,03/18/04 03/20/04 09:41 MAA I GC-12A 1. · California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the submiuing party. BC Laboratodes, Inc. assumes no responsibility for repor~ alteration, separation, detachment or third party interpretation. Printed 03/23/2004 16:45:35 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com 04-02749-17 ~ Laboratortes, Inc 1 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Ouantitation Summary (EPA Method 8015M) COC Number l--- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @_08~.'5_8- Sampling Locat_ion BELLE TERRACE Sample Depth --- __ Sampling Point T7-6 TK 3-7-6' __ Sample Matrix Soil Sampled By J K. Malamma BCL Sample ID 04-02749-16 Diesel Range Organics (C12- C24j < PQL mg/kg 10. I 3. 8015M 03/18/04 03/20/04 09:16 MAA GC-12A I 1. Tetracosane 99 I % 46-137 I 8015M t03/18/04 03/20/04 09:16 MAA I GC-12A 1. California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the subrnitth~g party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/23/2004 16:45:27 04-02749-16 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 8015M) COC Number --- Receive Date/Time 03/17/2004 @ 11:40 _Project Number 200150 Sampling Date/Time 03/17/2004 @ 08:55 _Sampling Location BELLE TERRACE Sample Depth --- Sampling POint T7-2 TK 3-7-2' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-15 Diesel Range Organics (C12 - C24 < PQL mg/kg 10. I 3. 8015M 03/18/04 103/20/04 07:37 MAA GC-12A 1. I Tetracosane 104 I % I 46-137 8015M !03/18/04 t03/20/04 07:37 t MAA GC-'12A 1. I California DOHS Certification #1186 Al! results listed in fl~is report are for the exclusive use of the submit~g party. DC Laborato~es, inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/23/2004 16:45:18 04-02749-15 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / OuantitatiOn Summary 'EPA Method 8015M) COC Number I_._ Receive Date/Time 03/17/2004 @ 11:40 Project Numbe_r_ 200150 __ Sampling Date/Time 03/1~ Sampling Location BELLE TERRACE Sample Depth --- Sampling Point T12-6 TK 4-12-6' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-14 Diesel Range Organics (C12- C24 < PQL mg/kg 10. ~ 3. 8015M 03/18/04 03/20/04 07:13 M~ GC-12A 1. Tetracosane 82 % 46-~37 80~5M 103/~8/04 ¢03/20/04 07:~3 M~ GC-~2A ~. California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for repor~ alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.corn Printed 03/23/2004 16:45:10 · 04-02749-14 a ~ c RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 8015M) COC Number --- Receive Date/Time t03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 08:40 Sampling Location BELLE TERRACE Sample Dep{h --- Sampling Point T12-2 TK 4-12-2' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-13 Diesel Range Organics (C12- C24j < PaL mg/kg j 1'0. t 3. 8015M 03/18/04 03/20/04 106:48 I MAA GC-12A 1. Tetracosane I 101 % I 46-13~ I 8015M t03/18/04 103~20z04 10~:4~ u~ GC-12A 1. I California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the subm/tting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/23/2004 1~:45:01 04-02749-13 a a c RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 8015M) COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 08:30 _Sampling Location BELLE TERRACE Sample Depth --- . ..... Sampling Point T11-6 TK 4-11-6' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-12 Diesel Range Organics (C12 - C24 < PQL mg/kg 10. ~ 3. 8015M 03/18/04 03/20/04 ~06:23 M~ ~ GC-12A 1. Tetracosane i 100 % 46-137 j 8015M 03/18/04 ~03/20/04 06:23 M~ GC-12A 1. California DOHS Certification #1186 Al! results listed in dds report are for the exclusive use of the submitting party. BC Laboratoffes, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Printed 03/23/2004 1 6:44:53 4~oo Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com 04-02749-12 Laboratories, Inc RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 8015M) COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 08:25 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point T11-2 TK 4-11-2' Sample Matrix Soil Sampled By IK. Malamma BCL Sample ID 04-02749-11 Diesel Range Organics (C12- C24J < PQL mg/kg 1 10. 3. 8015M 03/18/04 I 03/20/0405:59 MAA GC-12A 1. , Tetracosane I 91 ~ % I 46-137 ! 8015M ~03/18/04 03/20/04 05:59 M~ GC-12A 1. I I California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the submitting party. BC Laborato~es, Inc. assumes uo responsibility for report alteration, separation, detachment or third party interpretation. Printed 03/23/2004 1 6:44:44 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com 04-02749-11 B~~'-ll 1 / l, / 1 Laboratortes, Inc RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Ouantitation Summary (EPA Method 8015M) COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 1200150 Sampling Date/Time 03/17/2004 @ 08:20 Sampling Location BELLE TERRACE Sample Depth .... Sampling Point IT10-6 TK 4-10-6' Sample Matrix Soil Sampled By K. Malamma BCL Sample'lD 104-0274~ Diesel Range Organics (C12- C24: < PQL ] mg/kg I 10. 3, I 8015M i03/18/04 03/20/04 05:34 I MAA [ GC-12A ~otracosane I 99 I % I 46-137 ................... l"'"'";;~;i';'~' .......... 0';;18;;4'"'1";~;~'~;~,'"' '0;i'3'4 ....... ~ ............ ;'~':i'~A'"l 1. ........................... 1 California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the subnfi.vting party. BC Laborato~es, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 32%4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/23/2004 16:44:36 04-02749-10 a at c RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 8015M) COC Number Receive Date/Time 03/17/2004 @ 11:40 Project Number ;'~0150 Sampling Date/Time 03/17/2004 @ 08:1~5 .............. Sampling Location BELLE TERRACE Sample Depth --- __ Sampling Point T10-2 TK 4-10-2' Sample Matrix Soil Sampled By IK. Malamma B.CL Sample ID 04-02749-9 Diesel Range Organics (C12 - C24', < PQL rog/kg 10. 3. 8015M 03/18/04 03/19/04 23:48 MAA GC-12A 1. !:ii~iii~iii?ii:;ii;:iii~iii~ii~i:ii!~ii~:!:i:i:%~?E~:~?::~i~.~:i~ .;:i~;~i:~¢~:~:; ~f~ ~~:~E:~:~f~;:~:::::::::~ :::::::::::::::::::::::::::::::::::::::::::::: F Tetracosane 95 i %46-~37 8015M 03/18/04 t03/~e/04 23:48 M~60-~2A I ~. California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the subnfitting party. DC Laboratories, inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Printed 03/23/2004 16:44:27 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.corn 04-02749-9 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 8015M) COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ _0_7:~5~0 ................ Sampling Location BELLE TERRACE Sample Depth Sampling Point D2-6 DISPENSER #2-6' Sample Matrix !Soil Sampled By IK. Malamma BCL Sample ID 104-02749-8 !i¢-b:.~i~fi~:~i::!i!i!:::i!::i!i!i!:i:i:::::::::::::-:::::~ ....................... ::::::::::::::::::::::::::::::::::::::::::::::::::::::: i¥i~!!iiiiiii!R~l:~:ii:::iiii~iii;ili;i~i31:i;::!!ilU~!i~::ili::!31!;i !i;;il;~iii~;~ii!iii::iliiiii~iliM~i~ili::!ililili;ili ::ii~t~8i~i;i:i! ~iiiiiililili~ililili~ii! ~i~iiii~i~"I~iii !iiii~i~:~i!ii~:~i!!!! 6i~i~ill Diesel Range Organics (C12- C24t < PQL mg/kg 10. 3. 8015M 03/18/04 03/20/04 05:09 MAA GC-12A 1. I · ................ ~::..~i~P.: ii~Rbn::::::~ ............................ :i:i:i:i::li~:fifb~::;::;;: ........... QE~:ilili!iiiiiii:i!i:~:i:::i:i::!i! ~!::i%!!iM. Bi!!!:!i!i!!i!i!i!i!i!i:i!i :iii!i%i~!~:::::::.:.:::.;::::::::: Tetracosane 75 % 46-137 8015M 03/18/04 03/20/04 05:09 MAA GC-12A 1. California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.corn Printed 03/23/2004 16:44:18 04-02749-8 a at c RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA · Fuel Identification / Ouantitation Summary (EPA Method 8015M) COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number' 200150 Sampling Date/Time 03/17/2004 @ 07:45 Sampling Location BELLE TERRACE Sample Depth --- _Sampling Point D2-2 DISPENSER #2-2' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-7 Diesel Range Organics (C12- C24' < PQL mg/kg 10. I 3. I 8015M 03/18/04 I 03/20/04 04:45 MAA GC-12A I 1. Tetracosane / 93 % 45-137 8015M 03/18/04 03/20/04 '04:451 MAA i GC-12A I 1. I California DOHS Certification #1186 Al! results listed in fids report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for repor~ alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/23/2004 16:44:09 04-02749-7 a a c RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 8015M) COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 07:40 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point D5-6 DISPENSER #5-6' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-6 Diesel Range Organics (C12- C24 < PQL I mg/kg 10. I 3. 8015M 03/18/04 03/20/04 04:20 MAA GC-12A I 1. Tetracosane I 68 I % 46-137 8015M 03/18/04 103/20/04 O4:2O MAA California DOHS Certification #1186 At! results list¢c't i. this report are for [be ~×clusiv¢ usc of~¢ subrrd~n~ par~. BC Laboratodes, ~nc. assumes ~o responsibility £or report ~]teradon, sepa~do., detachment or ~{rd party iuterpret~tio.. Printed 03/23/2004 16:44:01 4~00 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.corn 04-02749-6 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 8015M) COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 07:39 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point D5-2 DISPENSER #5-2' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID t04-02749-5 Diesel Range Organics (C12- C24 19 mg/kg 10. I 3. 8015M 03/18/04 03/20/04 I03:55 MAA GC-12A I 1. I A52 IChromatogram not typical of diesel. California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the submitting party BC Laboratories, Inc. assumes no re~onsibility for report alteration, separation, detachment or third party interpretation. Printed 03/23/2004 16:43:52 4~ oo Arias Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www. bclabs, com 04-02749-5 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 8015M) COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 07:30 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point D3-6 DISPENSER #3-6' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID t04-02749-4 ,Diesel Range Organics (C12- C24 < PQL mg/kg 10. 3. 8015M 03/18/04 03/20/04 102:16 MAA GC-12A 1. Tetracosane ! 85 I % t 46-137 I 8015M 03/18/04 03/20/04 '02:161 MAA GC-12A 1. California DOHS Certification #1186 Al! results listed in this report are for the exclusive ~e of[he submJtdn8 party. DC Labormo~es, ~c. assumes no re~onsibflity Jo]' report alteration, separation, detachment or third par~ interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www,bclabs.com Printed 03/23/2004 16:43:44 04-02749-4 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Quantitation Summary (EPA Method 8015M) COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 07:27 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point D3-2 DISPENSER #3-2' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-3 Diesel Range Organics (C12- C24 <PQL I mg/kg I 10. I 3. I 8015M t03/18/04 03/20/04 101:52 MAA GC-12A 1. California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the s~bmitfing party. BC Laboratories, Inc. assumes no responsibility for report alteration, separatqon, detachment or third party interpretation. Printed 03/23/2004 16:43:35 4~00 Atlas Co,an * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com 04-02749-3 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Ouantitation Summary (EPA Method 8015M) COC Number 1--- I Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 iSampling Date/Time 03/17/2004 Sampling Location BELLE TERRACE Sample Depth --- __ Sampling Point D4-6 DISPENSER//4-6' Sample Matrix Soil ........................ Sampled By K. Malamma BCL Sample ID 04-02749-2 Diesel Range Organics (O12- C24t < PQL mg/kg 10. I 3. I 8015M 03/18/04 03~20~04 01:27 MAA GC-12A 1. metracosane I 74 i % 46-137 1801SM o3118104 o312o1o4 01:27 MAA GC-12A California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the submitting party. BC Laborato~es, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Printed 03/23/2004 16:43:27 4200 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com 04-02749-2 _~.~ Laboratortes, Inc RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Fuel Identification / Ouantitation Summary (EPA Method 8015M) CdC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 07:20 Sampling Location BELLE TERRACE Sample Depth --- _Sampling Point D4-2 DISPENSER #4-2' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-1 Diesel Range Organics (O12- 024 < PQL mg/kg 10. 3. 8015M I 03/18/04 i03/20/04 01:02 MAA GC-12A 1.0 Tetracosane 90 { % 46-137 8015M 03/18/04 103/20/04 101:02 MAA GC-;~2A 1.0 California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of file submitting party. DC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Printed 03/23/2004 16:43:23 4~00 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com 04-02749-1 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number --- IReceive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 09:15 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point T4-6 TK 2-4-6' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-20 Benzene i < PQL mg/kg 0.005 0.00036 8021B 03/18/04 03/18/04 21:17 HKS GC-V8 1 302-100443 Toluene / < PQL mg/kg 0.005 0.0040 8021B 03/18/04 03/18/04 21:17 HKS GC-V8 1 ~ 302-100443 i' Ethylbenzene~L < PQL I mg/kg 0.005 0.0018 8021B 03118104 03/18/04 21:17 HKS GC-V8 1 I 302-100443 Methyl t-butyl ether { < PQL mg/kg 0.02 0.00056 8021B t 03/18/04 03/18/04 21:17 HK'S GC-V8 I 302-100443 .L Total Xylenes < PQL mg/kg 0.01 0.0098 8021B~ 03/18/04 03/18/04 21:17 HKS GC-V8 I 302-100443 I ND Gasoline Range Organics (C4 - C12) < PQL mg/kg 1 0.046 8015M I 03/18/04 03/18/04 21:17 I HKS GC-V8 1 302-100443 a,a,a-Trifluorotoluene 92 i , % 70-130 8021B 03/18/04 !03/18/04 21:17 HKS GC-V8 1 302-100443 a,a,a-Trifluorotoluene (8015 Surrogate) 114 % 70-130 8015M 03/18/04 03/18/04 21:17 HKS I GC-V8 1 302-100443, j ,, California DOHS Certification #1186 All results listed in Qtis report are for the exclusive use of the submitting party. BC Laboratories, ~c. assumes no re~onsibility for report alteration, separation, detachment or third party interpretation. Printed 03/24/2004 16:00:37 4~00 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com 04-02749-20 Laboratortes, Inc 1 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVlN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number 1-" Receive Date/Time 03/17/2004 @ 11:40 Project Number 1200150 Sampling Date/Time 03/17/2004 @ 09:10 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point. TK~a~aKm2~4a-2' Sample Matrix Soil Sampled By BCL Sample ID 04-02749-19 Benzene [ < P~QL I mg/kg 0.005 0.00036 __8021B 03/18/04 03/18/04 20:47 HK8 GO-V8 1 302-100443 t ND Toluene [ < PQL ! mg/kg · 0.005 0.0040 8021B 03/18/04 03/18/04 !20:47 HK8 GO-V8 1 [ 302-100443 ND Ethylbenzene r-- - I t ' < PQL mg/kg t 0.005 _ 0.0018 8021B I 03/18/04 03/18/04 20:47 HKS GO-V8 1 1 302-100443 I ND Methyl t-butyl ether _ < PQL mg/kg 0.02 0.00056 8021B 03/18/04 03/18/04 120:47 ~HKS GC-V8 1 302-100443I ND Total Xylenes < PQL I mg/kg 0.01 0.0098 8021B 03/18/04 03/18/04 i20:47 HKS GC-V8 1 302-100443 i ND Gas°line Range Organics (64- i t C12) < PQL rog/kg 1 0.046 8015M 03/18/04 03/18/04 20:47 HKS GC-V8 I 302-100443 ND a,a,a-Trifluorotoluenea'a'a-Tr~iflu°r°t°luene (8015 92 % i 70-130 8021B 03/18/04 03/18/04 20:47 HKS GC-V8 [ I 302-100443 S. urrogate) 116 % 70-130 8015M 03/18/04 03/18/04 20:47 HKS GC-V8 1 302-100443 California DOHS Certification #1 186 All re§ults listed in this report are for the exclusive use of the submitting party. BO Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas C0tLrt * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * v,,ww.bclabs.com Printed 03/24/2004 16:00:2~ 04-02749-19 Laboratortes, Inc l RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 09:05 Sampling Location,BELLE TERRACE Sample Depth I-- Sampling Point IT8-6 TK 3-8-6' Sample Matrix Soil Sampled By IK. Malamma BCL Sample ID 0~-02749-18 Benzene < PQL mg/kg 0.005 0.00036 I 8021B 03/18/04 I 03/18/04 18:17 HKS GC-V8 1 302-100443_ ND ! S09 302-100443 Toluene < PQL rog/kg 0.005 0.0040 8021B 03/18/04 03/18/04 18:17 HKS GC-V8 1 Ethylbenzene _ < PQL I mg/kg 0.005 0.0018 8021B 03/18/04 03/18/04 18:17 HKS GC-V8 I 1 302-100443~ND Methyl t-butyl ether I < PQL mg/kg 0.02 0.00056 8021B 03/18/04 03/18/04 18:17 HKS GC-V8' 1 302-100 ND I S09 Total Xylenes < PQL mg/kg 0.01 0.0098 8021B 03/18/04 03/18/04 18:17 HKS GC-V8 1 302-1004431 ND 1 S09 Gasoline Range Organics (C4.~ ~i C12) < PQL mg/kg I 0.046 8015M 03/18/04 03/18/04 18:17 HKS GC-V8 1 302-100443 ND - a,a,a-Trifluorotoluene 42 % 70-130 8021B 03/18/04 03/18/04 18:17 HKS GC-V8 1 302-100443 S09 a,a,a-Trifluorotoluene (8015 Surrogate) 53 % j 70-130 8015M 03/18/04 03/18/04 18:17 HKS GC-V8 1 302-100443 s09 Flag Explanations S09 IThe surrogate recovery on the sample for this compound was not within the control limits. California DOHS Certification #1186 ' . AIl results listed in this report are for the exclusive use of'the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteradon, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/24/2004 16:00:16 04-02749-18 l,a ora orie s, IncII 1 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number --- Receive Date/Time 03/17/2~0_04~_1_~1:4~.0_ Project Number 200150 iSampling Date/Time 103/17/2004~ 09~:0__2 Sampling Location BELLE TERRACE !SamPle D.epth~ --- __ Sampling Point T8-2 TK 3-8-2' ~Sample Matrix Soil Sampled By K. Ma[aroma IBCL Sample ID 04-02749-17 Benzene ' [ii:!i <POe mg,kg' 0'.005 0.00036' 8021B 03,18,04 0'3,18,04 17:47 HAS Ge-v8 1 302-100443 ' N~) , Toluene __ < PQL ~ mg/kg 0,005 I 0.0040 8021B 03/18/04 03/18/04 17:47 HKS GC-V8 1 302-100443 T ND I Ethylbenzene < PQL mg/kg 0.005 0.0018 8021B 03/18/04 03/18/04 17:47 HKS GC-V8 I 302-100443 ND I IMethyl t-butyl ether < PQL rog/kg 0.02 0.00056 8021B 03/18/04 03/18/04 17:47 HKS GC-V8 1 302-100443 ND Total Xylenes < PQL mg/kg 0.01 0.0098 8021B 03/18/04 03/18/04 17:47 HKS GC-V8 1 302-100443 ND Gasoline Range Organics (C4 - IC12) < PQL mg/kg 1 0.046 8015M 03/18/04 03/18/04 17:47 HKS GC-V8 1 302-100443 I ND .~ ~ ~ ~4~ ~:~ ~? ~;~:~m~::~:m~.~:: :~::~??~::;~::~l~:;:::;~::~:.!~?:~?:~?:~ :~?:~::~:~:~?.::~?:::~ I · 'a,a,a-Tr~fluorotoluene 95 ~ % j 70-130 8021B I03/18/04 03/18/04 17:47 HKS [ GC-V8 1 302-100443 ~ a'a'a-Triflu°r°t°luene (8015 I [ Surrogate) 121 % 70-130 8015M 03/18/04 ,03/18/04 17:47 HKS GC-V8 ~ I 302-100443 ific ti n #.1186 California DOHS ~¢~,,~u ~,~i[c~,. tn,s ~epon a,,~ for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93305 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/24/2004 16:00:06 04-02749-17 1 1 1 l l RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number i--- Receive Date/Time __ 03/17/2004 ._~1_1_:_4_? Project Number 1200150 Sampling Date/Time 03/17/2004 @ 08:58 Sampling Location BELLE TERRACE __ Sample Depth --- _ Sampling Point T7-6 TK 3-7-6' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-16 _B_enzene < PQL mg/kg 0.005 0.00036 8021B 03/18/04 03/18/04 17:17 HKS GC-V8 1 302-100443 ND Toluene t < PQL mg/kg 0.005 0.0040 8021B ,03/18/04 03/18/04 17:17 HKS GC-V8 1 302-100443 I ND -, Ethylbenzene < PQL mg/kg 0.005 0.0018 8021B 03/18/04 03/18/04 17:17 HKS GC-V8 1 302-100443 ND Methyl t-butyl ether < PQL mg/kg 0.02 0.00056 8021B 03/18/04 03/18/04 17:17 HKS GC-V8 1 302-100443 ND Total XylenesI < PQL rog/kg 0.01 0.0098 8021B I 03/18/04 03/18/04 17:17 HKS GC-V8 1 302-100443 _! ND Gasoline Range Organics (C4 - C12) < PQL rog/kg I 0.046 8015M i= 03/18/04 03/18/04 17:17 HKS GC-V8 1 302-100443 I ND a,a,a-Trifluorotoluene (8015~ I Surrogate) 110 % 70-130 8015M 03/18/04 03/18/04 17:17 HKS GC-V8 1 302-100443 California DOHS Certification #1186 All results listed in this report are for the exclusive use of'the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661 ) 327-1918 * www.bclabs.com Printed 03/24/2004 15:59:56 04-02749-16 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number Receive Date/Time 03/17/2004 @ 11:40~ P~roject Number ;-~0150 Sampling Date/Time 03/17/2004 @ 08:55 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point T7-2 TK 3-7-2' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-15 Benzene < PQL mg/kg I 0.005 0.00036 8021B 03/18/04 03/18/04 16:47 HKS GC-V8 1 302-100443 ND Toluene < PQL mg/kg 0.005 0.0040 8021B 03/18/04 03/18/04 16:47 HKS GC-V8 1 302-100443 ND .... Ethylbenzene Methyl t-butyl ether Total Xylenes < PQL Gasoline Range Organics (C4 - C12) I <PQL mg/kg 1 0.046 t 8015M 03/18/04 03/18/04 16:471 HKS GC-V8 1 302-100443 a,a,a-Trifluorotoluene 90 % a,a,a-Trifluorotoluene (8015 Surrogate) 112 % 70-130 ~ 8015M 03/18/04 , 03/18/04 16:47 HKS GC-V8 1 302-100443 California DOHS Certification #1186 All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 3274911 * FAX (661) 327-1918 ~ xvww.bclabs.com Printed 03/24/2004 15:59:46 04-02749-15 Laboratories, Inc RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number --- Receive Date/Time ~03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 06:45 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point T12-6 TK 4-12-6' Sample Matrix ISoil Sampled By K. Ma~amma BCL Sample ID 04-02749-14 Benzene <PQL mg/kg 0.005 0.00036 Toluene Ethylbenzene Methyl t-butyl ether Total Xylenes Gasoline Range Organics (C4 - C12) I <PQL mg/kg I 1 I 0.046 i 8015M 03/18/04 03/18/04 16:17 HKS 6C-V8 1 302-100443 ND a,a,a-Trifluorotoluen_e 80 % j 70-130 I 8021B 103/18/04 03/18/04 16:17 HKS GC-V8 1 302-100443 a,a,a-Trifluorotoluene (8015 ' Surrogate) 98 % 70-130 8015M 103/18/04 03/18/04 16:17 HKS GC-V8 California DOHS Certification #1186 ~t~l results hsted in this report are for the exclusive use of the submitting par~y. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918" www.bclabs.com Printed 03/24/2004 15:59:36 04-02749-14 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD. CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number I--- ;Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Samphng Date/Time 03/17/2004 @ 08:40 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point IT12-2 TK 4-12-2' Sample Matrix Soil Sampled By IK. Malamma BCL Sample ID 04-02749-13 Benzene I < PQL rng/kg 0.005 0.00036 "~021B ¢03/18/04 ;03/18/04 i5:47' HKS . GO*V8 1 _~ 302-100443 i ND Toluene <PQL , mg/kg 0005 0.0040 8021B ~03/18/04 03/18/04 1547 HKS GO-V8 1-/s02-1oo443 ~~ ..... ~QL mg/kg 0.005 0.0018 8021B 03/18/04 03/18/04 15:47 ,KS ~ GO-V8 1 302-10044~-'~----~ Methyl t-butyl ether < PQL rog/kg 0 02 0 00056 ~ 8021B I 03/18/04 03/18/04 1547 HKS I GC-V8 ~t~,Xy,~,~ ' I <PQ~ mg/~g ~ 0.0, 0.00eSl 8021B ~03/18/04 t03/18/04 15:47 HKS GO-V8 ~ 302-100443 ~'~'~-~_ Z %_._. Gasolin~ Rang~ O~ganics (C4 - ' I ~ ' C12) <PQL ~ rog/kg 1 0.046 8015M 03/18/04 J03/18/04 15:47 HKS a,~,a-Trifluorotoluene 100 % 70-130 8021B 03/18/04 ~ 03/18/04 15:47 HKS GO-V8 1 302-100443 a,a,a-Trifluorotoluene (8015 Surrogate) 126 %'~ 70-130 8015M 03/18/04 03/18/04 15:47 HKS GC-V8 1 302-100443 California DOHS Certification #1186 All results listed ir~ this report are for the exclusive Use of the submitting party. BC Laborator/es, h~c. assumes no responsibility for report a~teradon, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * w~'w.bc]abs.corn Printed 03/24/2004 15:59:26 04-02749-13 ~ Laboratortes, Inc RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number I-" Receive Date/Time 03/17/2004 @ 1~1:_4__0 Project Number 200150 Sampling Date/Time 103/17/2004 @ 08:3__0~ Sampling Location BELLE TERRACE Sample Depth --- _ Sampling Point T11-6 TK 4-11-6' Sample Matrix Soil K. Malamma Sampled By BCL Sample ID 104-02749-12 Benzene i <PQL [ mg/kg 0.005 0.00036 80218 03/18)04 03/18/04 15:17 HKS GC-V8 j_~_. 302-100443~ ND ~-- <PQL mg/kg 0.005 0,0040 8021B 03/18/04 03/18/04 15:17 HKS GC-V8 t 1 , 302-100443 ~~n~-~-- <PQL rng/kg '0.005 0.0018 8021B 03/18/04 03/18/04 15:17 ,KS GC-V8-~---~I -~~'-~ Methylt-buty'et~r <PO' I rog/kg 0.02 0.00058 t 6021B ~03/18/04 03/18/04 15:17 .KS GO-V6 I 1 302-100443 Tota Xyle,es .... < PQ~~/k-'~-- 0 01 0 0098 8021B }03/18/04 03/18/04 15'17 HKS GC-V8 "~---~2-~- Gasoline Range Organics (C4 - ! ~ · I I i C12) I < PQL j rog/kg 1 0.046 [ 8015M t03/18/04 f 03/18/04 15:17 HKS GC-V8 I 1 ) 302-100443 I ND a,a,a-Trifluorotoluene 101 __ % ~_ 70-130 8021B 03/16/04 03/16/04 15:17 IlKS Ge-V6 1 302-100443 a,a,a-Trifluorotoluene (8015 I 03/18/04 Surrogate) 129 % 70-130 8015M 03/18/04 15:17 HKS GC-V8 1 302-100443 California DOHS Certification #1186 All re§ults listed in this report are for the exclusive use of'the subm/tt/ng part3,. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-.4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/24/2004 15:59:16 04-02749-12 aboratortes, Inc l 1 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons ~ 03/17/2004 COC Number I--- Receive Date/Time @ 11:40 Project Number 1200150 Sampling Date/Time 103/17/200~4 @~08_'._2_5 Sampling Location BELLE TERRACE Sample Depth i--- Sampling Point T11-2 TK 4-11-2' Sample Matrix Soil Sampled ByK' Malamma BCL Samp e ID 04-02749-11 Benzene < PQL rog/kg 0.005 0.00036 8021B 03/19/04 03/19/04 06:17 HKS GC-V8 1 302-100443 ND Toluene < PQL mg/kg 0.005 0.0040' 8021B 03/19/04 03/19/04 06:17 HKS GC-V8 1 302-100443 ND Ethylbenzene < PQL mg/kg I 0.005 0.0018 8021B 03/19/04 03/19/04 06:17 HKS GC-V8 1 302-100443 ND Methyl t-butyl ether < PQL mg/kg , 1 0.02 0.00056 8021B 03/19/024 03/19/04 06:17 HKS GC-V8 1 302-100443 ND __ Total Xylenes < PQL mg/kg 0.01 0.0098 8021B 03/19/,04 03/19/04 06:17 HKS GC-V8 1 302-100443 ND Gasoline Range Organics (C4 - C12) < PQL mg/kg 1 0.046 8015M 03/19/04 03/19/04 06:17 HKS GC-V8 1 302-100443 ND a,a,a-Tdfluorotoluene 94 % 70-130 8021B 03/19/04 03/19/04 06:17 HKS GC-V8 I 302-100443 a,a,a-Trifluorotoluene (8015 Surrogate) 116 % 70-130 8015M :03/19/04 ~ 03/19/04 06:17 HKS GC-V8 1 302-100443 California DOHS C.-..'xertification #1186 ~ results, listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * vcww.bclabs.com Printed 03/24/2004 15:59:07 04-02749-11 Laboratortes, Inc RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number ~--- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 08:20 Sampling Location BELLE TERRACE ISample Depth --- Sampling Point T10-6 TK 4-10-6' Sample Matrix Soil Sampled By I K. Malamma BCL Sample ID 04-02749-10 Benzene < PQL mg/kg' 0.005 0.00036 8021B 03/18/04 03/18/04 14:17 HKS GC-V8 1 302-100443 ND S09 Toluene < PQL mg/kg 0.005 0.0040 8021B 03/18/04 03/18/04 14:17 HKS GC-V8 1 302-100443 ND I $09 Ethylbenzene < PQL mg/kg 0.005 0.0018 8021B 03/18/04 03/18/04 14:17 HKS GC-V8 1 302-100443 ND S09 Methyl t-butyl ether < PQL mg/kg 0.02 0.00056 8021B 03/18/04 03/18/04 14:17 HKS GC-V8 1 302-100443 ND ___ S09 Total Xy!enes < PQL mg/kg 0.01 0.0098 8021B 03/18/04 03/18/04 14:17 HKS GC-V8 I 302-100443 ND S09 Gasoline Range Organics (C4 - C12) < PQL mg/kg 1 0.046 8015M 03/18/04 , 03/18/04 14:17 HKS GC-V8 1 302-100443 ND SOO a,a,a-Trifluor0t0'l'uene' , 38 .................. % ......... 70-1'30 8021B 03/18/04 0~/i8/04" 'i'4'i'i7' '"~'KS ' GC-V8 i I 30~-'i~0443 [ S09 ~,a;~:~;ifl~7or~toluene (8015 t. ' -- Surrogate) I 51 t % I 70-130 I 8015M I03/18/04 103/18/04 14:17 HKS GC-V8 I I 302-100443 [ [ S09 I Flag I Explanations S09 [The surrogate recovery on the sample for this compound was not within the control limits. California DOHS Certification #1186 All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/24/2004 15:58:57 04-02749-10 Laboratortes, Inc RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 08:15 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point T10-2 TK 4-10-2' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-9 Benzene < PQL mg/kg 0.005 0.00036 8021B 03/18/04 03/18/04 13:47 HKS GC-V8 I 302-100443 ND Toluene < PQL mg/kg 0.005 0'.0040 8021B 03/18/04 03/18/04 13:47 HKS GC-V8 1 302-100443 ND Ethylbenzene < PQL mg/kg 0.005 0.0018 8021B i 03/18/04 03/18/04 13:47 HKS GC-V8 1 302-100443 ND Methyl t-butyl ether < PQL ! mg/kg 0.02 0.00056 i 8021B 03/18/04 03/18/04 13:47 HKS GC-V8 1 302-100443 ND Total Xylenes < PQL mg/kg 0.01 0.0098 8021B 03/18/04 03/18/04 13:47 HKS GC-V8 1 I 302-100443 I ND Gasoline Range Organics (C4 - i j [ C12) I < PQL j rog/kg I 0.046 8015M 03/18/04 03/18/04 13:47 HKS GC-V8 I 302-100443 I ND a,a,a-Trifluorotoluene (8015 iI [ ''! Surrogate) 120 ! % 70-130 I 8015M 03/18/04 103118104 13:47 HKS GC-V8 1 302-100443 I California DOHS Certification #1186 All results listed in this report are for the exclusive use of the submitth~g party. BC Laboratories, Inc. assumes no responsibility for repori alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/24/2004 15:58:46 O4-O2749-9 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA 1 Purgeable Aromatics and Total Petroleum Hydrocarbons . COC Number --. Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 07:50 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point D2-6 DISPENSER #2-6' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 104-02749-8 Benzene < PQL mg/kg 0.005 0.00036 6021B 03/19/04 03/19/04 17:54 HKS GC-V8 1 302-100443 ~ ND Toluene I < PQL mg/kg 0.005 0.0040 8021B 03/19/04 03/19/04 17:54 HKS GC-V8 1 302-100443 ND ~ 17:54 Ethylbenzene I < PQL mg/kg I 0.005 0.0018 8021B 03/19/04 03/19/04 HKS GC-V8 1 302-100443 ND Methyl t-butyl ether < PQL mg/kg I 0.02 0.00056 8021B 03/19/04 03/19/04 17:54 HKS GC-V8 1 302-100443 ND Total Xylenes I < PQL rng/kg t 0.01 0.0098 8021B 03/19/04 , 03/19/04 17:54 HKS GC-V8 I 1 302-100443 ND Gasoline Range Organics (C4 / C12) < PQL mg/kg . 1 0.046 I 8015M 03/19/04 03/19/04 17:54 HKS GC-V8 I 302-100443 ND a,a,a-Trifluorotoluene I 106 I % 70-130 I 8021B 03/19/04 03/19/04 17:54 HKS GC-V8 1 302-100443 17:54 , a,a,a-Trifluorotoluene (8015 I I I Surrogate) 130 % 70-130 I 8015M 03/19/04 03/19/04 t HKS GC-V8 1 302-1004431 California DOHS Certification #1186 All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661)327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/24/2004 15:58:37 04-02749-8 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 07:45 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point D2-2 DISPENSER #2-2' Sample Matrix Soil Sampled By K. Malarnma BCL Sample ID 04-02749-7 Benzene <PQL mg/kg 0.005 0.00036 8021B 03/18/04 03118/04 09:46 HKS Toluene < PQL mg/kg 0,005 0.0040 8021B 03/18/04 03/18/04 09:46 HKS G.C-V8 1 Ethylbenzene Methyl t-butyl ether Total Xylenes I < PQL mg/kg 0.01 0.0098 8021B 03,18,04 03,18,04 09:46 HKS GC-V8 I 302-100443 ~_ N~D ..... Gasoline Range Organics (C4 - C12) < PQL I mg/kg I 0.046 8015M 03/18/04 i 03/18/04 09:46 HKS GC-V8 I I 302-100443 I ND _a,a,a-Trifluorotoluene 72 % 70-130 8021B 03/18/04 03/18/04 09:46 HKS GC-V8 1 'a,a.a-Trifluorotoluene (8015 Surrogate) 92 California DOHS Certification #1186 All results listed in dfis report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FA..',((661) 327-1918 * www.bclabs.com Printed 03/24/2004 15:58:27 04-02749-7 a i c RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number I--- Receive Date/Time 03/17/2004 @ 11:40 Project Number 1200150 Sampling Date/Time 03/17/2004 @ 07:40 Sampling Location /BELLE TERRACE Sample Depth --- Sampling Point [D5-6 DISPENSER #5-6' Sample Matrix Soil Sampled By IK. Malamma BCL Sample ID 104-02749-6 Benzene ~ < PQL ~ mg/kg 0.005 0.00036 8021B 03/18/04' 03/18/04 09:16 HKS GC-V8 I 302-100443 Toluene ~ < PQL ~ mg/kg 0.005 0.0040 8021B 03/18/04 03/18/04 09:16 HKS GC-V8 1 302-100443 Ethylbenzene < PQL ~ mg/kg 0.005 ~ 0.0018 ~ 8021B 03/18/04 03/18/04 09:16 HKS I GC-V8 1 302-100443 ND Methyl t-butyl ether < PQL I mg/kg 0.02 0.00056 ~ 802~B 03/18/04 03/18/04 09:16 HKS GC-V8 ~ 1 302-100443 Total Xylenes < PQL mg/kg 0.01 0.0098 8021B 03/18/04 03/18/04 09:16 HKS GC-V8 ] I 302-100443 ND Gasoline Range Organics (C4 - C12) ' < PQL mg/kg 1 0.046 8015M 03/18/04 03/18/04 09:16 HKS GC-V8 1 302-100443 ND a,a,a-Trifluorotoluene 80 % 70-130 8021B 03/18/04 03/18/04 09:16 HKS GO-V8 1 302-100443 a,a,a-Trifluorotoluene (8015 Surrogate) 102 % 70-130 8015M 03/18~04 03/18/04 09:16 HKS GC-V8 1 302-100443 California DOHS Certification #1 186 All results listed in this report, are for the exclusive use of the submitting party. BC Laboratories, [nc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court" Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.corn Printed 03/24/2004 15:58:18 04-02749-6 ra i RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COc Number i--- Receive Date/Time 03/17/2004 @ 1 1:40 Project Number 200150 Sampling I~ate/Time 03/17/2004 @ 07:39 !Sampling Location BELLE TERRACE Sample Depth --- Sampling Point D5-2 DISPENSER #5-2' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-5 Benzene ~ < PQL mg/kg I 0.005 0.00036 8021B 03/18/04 03/18/04 01:13 HKS GC-V8 1 302-100443 I ND Toluene < PQL mg/kg 0.005 0.0040 8021B 03/18/04 03/18/04 01:13 HKS GC-V8 1 302-100443 ND Ethylbenzene < PQL mg/kg 0.005 0.0018 8021B 03/18/04 03/18/04 01:13 HKS GC-V8 1 302-100443 ND Methyl t-butyl ether < PQL mg/kg 0.02 0.00056 8021B 03/18/04 03/18/04 01:13 HKS GC-V8 1 302-100443 ND Total Xylenes < PQL mg/kg 0.01 0.0098 8021B 03/18/04 03/18/04 01:13 HKS GC-V8 1 302-100443 ND Gasoline Range Organics (04 - 012) < PQL mg/kg 1 '0.046 8015M 03/18/04 03/18/04 01:13 HKS GC-V8 1 302-100443 ND a,a,a-Trifluorotoluene 96 % 70-130 8021B 03/18/04 03/18/04 01:13 HKS GO-V8 1 302-100443 a,a,a-Trifluorotoluene (8015 Surrogate) 121 % 70~130 8015M 03/18/04 03/18/04 01:131 HKS GC-V8 , 1 302-100443 California DOHS Certification #1186 All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/24/2004 15:58:07 04-02749-5 a i c RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total. Petroleum Hydrocarbons COC Number ~ Receive Date/Time 03/17/2004 @ 11:40 Project Number ;-~0150 Sampling Date/Time 03/17/2004 @ 07:30 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point D3-6 DISPENSER #3-6' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-4 Benzene < PQL mg/kg 0.005 0.00036 8021B 03/18/04 03/18/04 08:46 HKS GC-V8 1 302-100443 ND I Toluene < PQL mg/kg 0.005 0.0040 8021B 03/18/04 03/18/04 08:46 HKS GC-V8 1 302-100443 ND Ethylbenzene < PQL mg/kg 0.005 0.0018 8021B 03/18/04 03/18/04 08:46 HKS GC-V8 1 302-100443 ND _~. Methyl t-butyl ether < PQL mg/kg 0.02 0.00056 8021B 03/18/04 03/18/04 08:46 HKS G,C-V8 1 302-100443 ND __J Total Xylenes < PQL I mg/kg 0.01 0.0098 8021B 03/18/04 03/18/04 08:46 HKS GC-V8 1 302-100443 ND Gasoline Range Organics (C4 - I C12) < PQL mg/kg 1 0.046 8015M 03/18/04 03/18/04 08:46 HKS GC~V8 1 302-100443 a,a,a-Trifluorotoluene 78 % 70-130 8021B 03/18/04 03/18/04 08:46 HKS GC-V8 1 1302-100443 a,a,a-Trifluorotoluene (8015 I Surrogate) 98 % 70-130 8015M I 03/18/04 03/18/04 08:46 HKS GC-V8 I 1 302-100443 California DOHS Certification #1186 All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/24/2004 15:57:58 04-02749-4 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 07:27 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point D3-2 DISPENSER #3-2' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-3 Benzene < PQL mg/kg 0.005 0.00036 8021B .03/18/04 03/18/04 00:13 HKS GC-V8 1 302-100443 ND Toluene < PQL rng/kg 0.005 0.0040 8021B 03/18/04 03/18/04 00:13 HKS GC-V8 1 302-100443 ND Ethylbenzene I < PQL I mg/kg 0.005 0.0018 8021B 03/18/04 03/18/04 00:13 HKS GC-V8 1 302-100443 ND Methyl t-butyl ether < PQL mg/kg 0.02 0.00056 8021B 03/18/04 03/18/04 00:13 HKS GC-V8 1 302-100443 ND Total Xylenes I < PQL mg/kg 0.01 0.0098 8021B 03/18/04 03/18/04 00:13 HKS GC-V8 1 302-100443 ND Gasoline Range Organics (C4 - ' C12) I < PQL mg/kg 1 0.046 8015M 103/18/04 03/18/04 00:13 HKS GC-V8 I 1 302-100443 ND a,a,a-Trifluorotoluene 93 ! % I 70-130 I 8021B 03/18/04 03/18/04 00:13 HKS GC-V8 1 302-100443 ~ a,a,a-Trifluorotoluene (8015 . Surrogate) 117 % 70-130 8015M 103/18/04 03/18/04 00:13 HKS GC-V6 I 302-100443 California DOHS Certification #1186 All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 "FAX (661) 327-1918 * www.bclabs.com Printed 03/24/2004 15:57:48 04-02749-3 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number ..- P, eceive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time '03/17/2004 @'07:25 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point D4-6 DISPENSER #4-6' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-2 Benzene < PQL rng/kg 0.005 0.00036 8021B 03/17/04 03/17/04 23:43 HKS GC-V8 1 302-100443 ND Toluene < PQL rng/kg 0.005 0.0040 8021B 03/17/04 03/17/04 23:43 HKS GC-V8 1 302-100443 ND Ethylbenzene i < PQL rng/kg 0.005 0.0018 8021B 03/17/04 03/17/04 23:43 HKS GC-V8 1 302-100443 Methyl t-butyl ether < PQL ~ mg/kg I 0.02 0.00056 I 8021B. 03/17/04 03/17/04 23:43 HKS GC-V8 1 302-100443 ND Total Xylenes , < PQL i mg/kg I 0.01 0,0098 I 8021B 03/17/04 ,03/17/04 23:43 HKS GC-V8 I 302-100443 Gasoline Range Organics (C4 - I C12) < PQL mg/kg I I 0.046 8015M 03/17/04 I 03/17/04 23:43 HKS GC-V8 I 302-100443, ND a,a,a-Trifluorotoluene I 101 % 70-130 8021B 03,17,04 03,17,04 '~;~'; .......... ~'~;'"'"'""")"'";~:';;'-'"'1 ............ i .................. a,a,a-Trifluorotoluene (8015 Surrogate) 129 % 70-130 8015M 03/17/04 03/17/04 23:43 HKS GC-V8 1 302-100443 California DOHS Certification #1186 All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/24/2004 15:57:37 04-02749-2 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons ~,eceive Date/Time 03/17/2004 @ 11:40 COC Number --- Project Number 200150 Sampling Date/Time 03/17/2004 ~ 07:20 Sampling Location BELLE TERRACE Sample Depth --- _ .......................... Sampling Point D4-2 DISPENSER #4-2' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-0274~-1 Benzene I < PQL mg/kg 0 005 0 00036 8021B 03/17/04 03/17/04 23:13 HKS ,I GC-V8 I 302-100443 ~_____N__D ~T~-;~; .............. < PQL mg/kg 0 005 0 0040 8021B 103/17/04 03/17/04 23:13 HKS ! GC-V8 ~ 1 302-100443_L_ N_~_ ~;~; ..... < PQL mg/kg 0 005 0~0018 I 8021B ~03/17/04 03/17/04 23:13 HKS GC-V8 I I 302-100443 &___~ '-MAF;;~;-; .... ~ <POL ~ mglkg 002 0.00056 I 80~1~ [03/~7/04 03/~7/04 123:~31 HAS Ge-v8 1 3o2-1oo443~_. ND ~gFX;~gg ....... <PQL i rog/kg 001 0.0098 I 8021B 103/17/04 03/17/04 23:13 HKS GC-V8 ~ I ~~-', Gasoline Range Organics (C4 - I ~ C12) < PQL [ mg/kg 1 0 046 8015M 03/17/04 03/17/04 23:13 HKS GC-V8 1 302-100443 I ND ....... : ..................................................... ~::":":: ::~:::::':'::::::'::::::~ :':'?:~:: :::':'::~:::':':'":~::~ ~:~:::~:: :: ::1::~ A~:~t~'~::~::~ ~:~: :;~ ~ ~ ~:Bfi:i[~::~ ~?~ ~i ~:~ ~::~ ;~;~:~ ::~ ~ ~;;~:~::~::~:::::~ ~:-~:~ A~;A~{;~i~i~:::::: ~:i:i~:~::~ ::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::: S:u:rrogate:.::~ompound:-::~;::.:::: ................................. :..; ................. ..... ........................ :,- ........ , ;.,..:. .......................... ,.....,.,.....,.....,-.: ............................................................ ,-,-,-,-,-,-, .......................................... · ...... ~ , . . a a a-Trifluoroto uene I 80 % 70-130 8021B 03/17/04 03/17/04 23:13 HKS GC-V8 I" 302-100443 r o I . I ............ ' Surrogate) I 101 ~ Yo 70-130 8015M ~ 03/17/04 ~ u3/1//u4 z~:~d ~ - i - California DOHS Certification #1186 All results listed in this report are for the exclusive use of fl~e submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/24/2004 15:57:32 04-02749-1 m Certified Analytical Report Cover- Page 1 of 1 Laboratories, Inc. ~ (~ ~ ~ ~ ~ l Cover Report ~. ~ MAR 29 2004 mm RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Project Number: '- COC Number: BCL Number: 04-02749 Dear Mr. Malamma: This report contains the analytical results for the samples received under chain of custody by BC Laboratories, Inc. The samples were logged into the Laboratory Information Management System (LIMS) and BC Lab numbers were assigned to each sample. The result of the temperature check, condition of the samples and any other discrepancies were recorded on the cooler receipt form. m m m m m All applicable quality control procedures met method-specific acceptance criteria, except as noted on the following analytical and quality control reports. m This report shall not be reproduced except in full, without written approval of the laboratory. I I I I m i California DOHS Certification #1186 I Authorized Signature All re.-;uh listed iQ tbi:~ report are ibr the exclusive use of the submitting party, BC Laboratories, Inc. assumes no respons b ty for repo~l alteration detac e ' ' ' ersf' , , · , t t d party]nterpretat~on Pnnted 0~):~0~'.45~.~l~ ]eld, CA 93308 (66t)327-4911 Fax(661)327-1918* www.bclabs.co~-6ff~'~ ' Laboratories, Inc; :Chain of Form I ] Custody 10 0 3 8 Attn: ~-'~[K~ ~M/~~ Project Name:~J~[~'-~Yrax_~.._. Comments: Street Address: 2 1 ~)~"~ ~ Project Code: ~<~ ~' ~;~ ~~ Ci~,State, Zip: ~p.~ q33~{ Sampler(s): ~ ~~~  ~ any tests with holding ti .... less Email Address: ~ '~ ~.~.~'~:~ ;~L Sample Matrix Submittal g: ~ ~~ ~ ~ =~ ~ Yes NO J l] I~JJ -3~ ~ ~ Notes I ' ~ ~ ~ ot~ U~-~ Tkq-lO-~' -~ ~3111~{0~{5 x x x'  Sample Disposal Special Reporting Report Drin~ng ~ Same as above Waters~mt~ Form? ~ Return to Client ~ Disposal by lab ~ ~chive: Months .......... ~C ~WIP ~ ~aw Data 1. Rel~~ ~ ,Date/ / mTime ~ive0 B~. I J Date Time Client: ~Yes ~No ~/~ ~/[~[~[{[~ ~~ Address: " ~d By Send Copy to State of ~ 2. Re~nqmshed By Date Time Date Time City: State Zip CA? . . .  ' Time Attn: ~ Yes 0 3. Relinquished By Date Time 3. Received By Date · PO~: ' BC Laboratories, Inc. - 4100 Atlas Ct. - Bakersfield, CA 93308 - 661.327.4911 - Fax: 661.327.1918 - www.bclabs, corn m mm mm m m mm m m m mm mm m m mm m m m m m Laboratories, Inc. Chain of Custody Form ~ 0 0 3 9 ! Client:~%Xi~ ~/x~. ~'~ Project#:2~[~0 ~---'e~.. ' ( m nttn: ~{~ ~~ Project Name: ~t~~ Street Address: ~3 ~0~ Project Code: Ci~, State, Zip:~[~F0 ~ %3~l Sampler(s): )~~~ ~;~ / Phone:3 ~ ~ ~ ~ Fax:~ ~ ~L~ Email Address:~ ~ 'z~'~"~:~ ..... ~)~" ~ ~ ~=~=~ ~ 'or equal ~s? Submittal g: O~ ~~~ [ $ ~ ~~~ ~ ~ Standard Turnaround = 15 work days ,, m mmmlmii )m )m m minim I) m ~)~ ~ ~~ ~ Notes ~b T~t-5-~ ~ ~Jl(~ I Special Reporting ~ ~ Same as above Report Drin~ng Sample Disposal Waters ~tateFo=? ~ Return to Client ~ Disposal by lab ~ ~chive: Months .......... ~ OC ~ ~IP ~ aaw Data Client: ~Yes ~No Date - ]Time ~d~ Address: Send Cop~o State of ~. Ren~h~ By ]Time ~iwa By Date Time Ci~: ~ State ~ Zip CA? Attn: = ~ Yes ~o 3. Relinquished By Date Time 3. Received By Date [ Time POg: BC Laboratories, Inc. - 4100 Atlas Ct. - Bakersfield, CA 93308 - 661.327.4911 - Fax: 661.327.1918 - www.bclabs.com Laboratories, Inc. ' Chain of Custody Form ~~. ~:~1~ Project#: ~ttn: ~[~ ~ ~~ Project Name~ [~f~ omments: Street Address: ~(6 3 ~ ~ Project Code: caw, State, ZiP: ~ ~O ~ ~3~0( Sampler(s):~/~ ~ Phone:3Z~/~% Fax:~q~(7% ~ .... ~ ~~ any tests ~lding times less than ' l~ ~ .. Sample matffix . Arethere or equalm4~s? · Email Address: ~ ~ .~. ~ge~: :~ Submittal ~ ~ ~~ ~ ~' ]1 1 II ~ ~ 7 ~ Standard Turnaround = 15 work days ~ ~5~ Other ~ Notes / ' I I I I I I I I ~ I Report Drin~ng Sample Disposal ~ Special Reporting ~ Same as a~o~e ~t~r. ~o~* E ~e~,o ~,~.~ ~i.~os~,~,~ E ~c~,w: ~o.,~. ......... Elient: ~Yes ~No Date Time ~ddress: ~ ggD ' 2. fieiM, i~h~ ~y ~ime ~ea ~y ~te ~im. Send Copy to State of Oity: __ State ~ Zip Ch? N , ~tt~: ~ Yes~No 3, Reliaquished By Date ~ Time 3. Received By Date Time POg: BC Laboratories, Inc. - 4100 Atlas Ct. - Bakersfield, CA 93308 - 661.327.4911 - Fax: 661.327.1918 - www.bclabs, com sAMPLE RECEIPT FORM Rev. No. 10 0~,~1/04 page~of'~ 'BC LABORATORIES INC. SHIPPING INFORMATION~ ~ SHIPPING CONTAINER Federal Express O UPS Q Hand Delivery~ Ice Chest~ None U BC Lab Field Service Q Othe~ Q (Specify)-- Box '~ Other Q (Specify) Refrigerant: Ice'{~. Blue Ice [] None [] Other [] Comments: Itntact?Yes E) No intact? Yes E3 No samples received? Yes/~ No El tx, COC Received ,~YES [] NO SAMPLE CONTAINERS All samples containers intact? Yes~'[ / No [3 Description(s) match COC? YesJ~']/No E] ~ Temperature: "[~ · ~ °C - QT GENERAL MINERAL/GENERAL PHYSICAL PE UNPRESERVED INORGANIC CIIEMICAL METALS PT INORGANIC CHEMICAL blETALS qlDE FORMS ~ITRATE / NITRITE 00mi TOTAL ORGANIC CARBON :N DEMAND PHENOLICS VGA VIAL TRAVEL BLANK VGA V1AL 413.1,413.1~ 418.1 )DOR i0 mi VGA VIAL- 504 'glS0 ' EPA 525 525 TRAVEL BLANK 00mi EPA 547 00mi EPA 531.1 548 EPA 549 EPA 632 EPA 80155'1 OZ. JAR OZ. JAR OIL SLF'. E V I'.' PCB VIAly LASTIC BAG ENCORE ~-~:.,.,~r~,.-..-'~--..¢;-'~:L :.~-~_, , ~..,~, .z~--. ' '~.~F'.': :.- ';':':",~-~?r; ': 5~.~..~'&t;~ -~.'-e"~t~'~ !- ~ ':'~.~!~. E. ~,~ ..... .~" ~,Z:;~.~'" ,~--. 'T.~.; ..... t ~ :. ,,;v ~F,~:~W£~, . · BC LABO"ATORIES INC. SAMPLE RECEIPT FORM Rev. No. 10 0~121i04 Page ~ Of..~_ SHIPPING INFORMATION,., SHIPPING CONTAINER Federal Express E3 UPS ~ Hand Delivery~ Ice Chest~ None BC Lab Field Service ~ Other ~ (Specify)-- Box '~ Other Q (Specify). Refrigerant: Ice~ Blue Ice ~ None ~ Other ~ Comments: I Intact?Yes DNo D Intact? Yes ~ No COC ReCeived ~ce Chest ID ~ff~ Emissivity ~il. Date/Tim~ YES ~ NO Thermqmeter ID~ Analyst Init ~,,, SAMPLE NHMgERS QT GENERAl. MINERAL/ GENERAL PHYSICAL PT PE UN~RESEEVED 'QT INORCA~IC EII~MIEAL METALS PT INORGANIC CHEMICAL METALS PT CYAN/DE NITROGEN FORMS PT PT TOTAL SULFIDE 2oz. NIT~&TE / NITRITE 100mi TOTAL ORGANIC CARBON QT TOX PT CHEMICAL OXYGEN DEMAND  PtAPRENOLICS t0ml VOA VIAL T~VEL BLANK 40mi VOA VIAL t ~ ~ ~1 ~ ~ ( ~ ) ( QT EPA 413.1~ 413.2~ 418.1 PT ODOR ~DIOLOGICAL BACTE~IOLOG IC~L 40 mi VOA VIAL- 504 QT [PA ~08160818080  QTEPASIS'I/8150 QT EPA 525 QT EPA ~25 TRAVEL BLANK  190mi EPA 547 100mi EPA 531.1 ~T EPA 548 ~ OT EPA 549 ~ OT EPA632 Q~ EPA 8015M Ot QA/QC ~ OTAblBER . . 8 OZ. JAR m 32 OZ. JAR PCB VIAI~ m PLASTIC BAG  FERROUS IRON E~CO~E BC LABORATORIES INC. SAMPLE RECEIPT FORM Rev. ~o. l0 0~12~104 Page Of. Submission #:(~5~,_ ~(~.~L~ I Project Code: I TB Batch. Federal Express BC Lab Field Service Q Other O (Specify) Box O Other O (Specify). Refrigerant: Ice~ Blue Ice ~ None ~ Other ~ Comments:. Custod~ Seals: Ice Chest ~ Containers ~ ~one Comments: [ntact? Yes ~ No Intact? Yes 0 No All samples received? Yes No O All samples containers intact? Yes No ' .COC Received IceChestlD ~' Emissivity ~ Date/Ti~[ ~ ~ Temperature= ~°C-~ C~'r i~ ~ YES ~ NO Thermometer ID: - I ~ 0~?~ Analyst Init OT GENERAL MINERAL/ GENERAL PHYSICAL PT PE UNPRESERVED QT INORGANIC CIIEMICAL ~'1E'I'ALS PT INORGANIC CHEMICAL METALS :PT CYANIDE PT NITROGEN FORMS PT TOTAL SULFIDE' 2oz. NIT~'I'E / NITRITE 100mi TOTAL ORGANIC CARBON Q~ox 40~t VOA VIAL T~VEL I ~ eT EPA 413.1~ 41~.2~ 418.1 ~ PT ODOR ~DIOLOG ICA L ~ BACTERIOLOGICAL I ~0 mi VOA VIAL- 504 QT EPA 508/608/8080 ~ OT EPA 515rl/8150 ~ eT EPA 525 QT EPA 525 TRAVEL BL.4HK ~ 100mi EPA 547 ~ 100mi EPA 531.1 ~T EPA 548 ~ ~T EPA 549 I bT EPA 632 QT EPA 8015M ~ eT OA/OC 8 OZ. JAil ~ ~2OZ. JAR, PCB VIAI~ ~LASTIC It/kG ~ ~EIIROUS IIRON ENCORE  >mments: P BC LABORATORIES INC. SAMPLE RECEIPT FORM Rev. No. 10 01121104 Page Submission #: (~)4 ~..~),71T-49 IPr°joct Code: I TB .Batch# SHIPPING INFORMATION~ ~ ~HIPPING CONTAINER Federal Express [] UPS [] Hand Delivery ~, Ice c;hestIL~ None [] BC Lab Field Service [] Other [] (Specify). Box [] Other [] (Specify) Refrigerant: lc Blue Ice [] None [] Other [] Comments: Custody Seals: Ice Chest [] [] Containers [] Non Comments: ntact?Yes []No Intact? Yes [] No All samples received7 Yes~/ Non All samples containers intact? Yes~,. No E~ Description(s) match COC? Yes~ Ice Chest ID j~.~/~)' Emissivity ~ Date/Time?~ COC Received ~ Temperature: ~;C .W(D Cgtl ii e. LrI Analyst Init ._~ YES [] NO Thermometer ID: , ~ SAMPLE NUMBERS OT GENERAL MINERAL/GENERAL PHYSICAL :PT PE UNPRESER¥'ED INORGANIC CIIEMICAL METALS PT INORGANIC CtlEMICAL METALS PT CYANIDE PT N. ITROGEN FORMS PT TOTAL SIJI~FIDE 2oz. NITRA'[E / NITRITE 100mi TOTAL ORGANIC CARBON QT TOX PT CHEMICAL OXYGEN DEMAND I!PtA PHENOLICS 40mi VOA VIAL TRAVEL BLANK 40mi VOA VIAL ~ ~ ~ ~ ~ ~ ~ I QT EPA 413.1~ 413.2~ 418.1 .... PT ODOR RADIOLOGICAL BACTERIOLOGICAl. 40 mi VOA VIAL- 504 QT EPA 508/608/8080 QT EPA 5.15.1/8150 '¥ QT EPA 515 OT EPA 515 TRAVEL BLA~qK, 100mi EPA 547 100mi EPA 531.1 ~,. QT EPA 548 a~ OT EPA 5.49 I QT ~pA 632 · QT ~/'A ~015hl -- OTQA/QC , I OTAblBER 8 OZ. ,JAil _ 32 OZ. JAil ~ ,pcb V/AI.r PLASTIC BAG FERROUS ENCORE . :omments: 'amole Numbe¥ino G~m'nl~cI-Bg: ':.' ;:~:?¢)':~!:;,i.~. ~ ~ ; ':::'"D~ib')Yi~::;c.:~J:¢:'~."/IC,~;''~ I'~[LY:.~'~''('ccf': ?.';: ;':-::'~ "';'"?!';;'": ~:` {:;-: ':(''~" Laboratortes, Inc RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons _C_._O._C~N_u_m_~e~r .... i'" Receive Date/Time 03/17/2004 @ 11:40 Project Number 1200150 Sampling Date/Time 03/17/2004 @ 09:50 Sampling Location IBELLE TERRACE Sample Depth --- - Sampling Point .... IT9-6 TK 3-9-6' Sample Matrix Soil .................................. Sampled By IK. Malamma BCL Sample ID 104-02749-32 Benzene < PQL I mg/kg 0.005 0.00036 8021B 03/19/04 03/19/04 05:17 HKS GC-V8 1 302-100442 I ND Toluene < PQL mg/kg 0.005 0.0040 8021B 03/19/04 03/19/04 05:17 HKS GC-V8 1 302-100442 ND Ethylbenzene < PQL mg/kg 0.005 0.0018 8021B 03/19/04 03/19/04 05:17 HKS GC-V8 1 302-100442 ND ----~- Methyl t-butyl ether < PQL mg/kg 0.02 0.00056 8021B 03/19/04 03/19/04 05:17 HKS GC-V8 I 302-100442 Total Xylenes < PQL mg/kg 0.01 0.0098 8021B 03/19/04 03/19/04 05:17 HKS GC-V8 1 302-100442 mglkg 1 0.046 , 8015M Gasoline Range Organics (C4 - C12) < PQL 03/19/04 03/19/04 05:17 HKS GC-V8 1 302-100442 ND a,a,a-Trifluorotoluene 91 % 70-130 8021B 03/19/04 03/19/04 05:17 HKS GC-V8 1 302-100442 a,a,a-Trifluorotoluene (8015 Surrogate) 113 % 70-130 8015M 03/19/04 03/19/04 05:17 HKS GC-V8 1 302-100442 California DOHS Certification #1 186 Al! results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakemfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/2412004 16:02:36 04-02749-32 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total PetroleUm Hydrocarbons COC Number i--- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 09:45 Sampling Loca_tion BELLE TERRACE Sample Depth Sampling Point T9-2 TK 3-9-2' Sample Matrix Soil ........................ Sampled By IK, Malamma BCL Sample ID 04-02749-31 Benzene < PQL rng/kg 0.03 0,0018 8021B · 03/19/04 03/19/04 19:24 HKS GC-V8 5 302-100442 ND Toluene < PQL rng/kg 0,03 0,020 8021B 03/19/04 03/19/04 19:24 HKS GC-V8 5 302-100442 ND Ethylbenzene < PQL rng/kg 0,03 0.0086 8021B 03/19/04 03/19/04 19:24 HKS G(~-V8 5 302-100442 ND Methyl t-butyl ether < PQL mg/kg 0,1 0.0028 8021B 03/19/04 03/19/04 19:24 HKS GC-V8 5 302-100442 ND _~. Total Xylenes < PQL I rog/kg 0,05 0,049 8021B 03/19/04 03/19/04 19:24 HKS GC-V8 I 5 302-100442 ND Gasoline Range Organics (C4 - C12) < PQL mg/kg 5 0.23 8015M 03/19/04 03/19/04 19:24 HKS GC-V8 5 302-100442 ND ~t~ .......................................................... ~:~:~!~:~:~p ..................................... ~:R~::~:~:i:i: ........................... ~;~'ti~i~:i:i-~:! ........................ ~:i~;;~ii~if:i%~%~;~:~;;~:~ :::::::::::::::::::::::::::::::::::::::::::::::::::::: a,a,a-Trifluorotoluene 104 % 70-130 8021B 03/19/04 03/19/04 19:24 HKS GC-V8 5 302-100442 ~ ,a,a,a-Trifluorotoluene (8015 I iSurrogate) 130 % 70-130 8015M 03/19/04 03/19/04 19:24I HKS I GC-V8 5 302-100442 Comments PQL's and MDL's are raised due to sample dilution. California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for reporl alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/24/2004 16:02:26 04-02749-31 Laboratories, Inc l / 1 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number I'-' I Receive Date/Time 03/17/2004 @ 1.1_:__4_0_ Project Number 200150 Sampling Date/Time 03/17/2004 @?_9i_4_`4 Sampling Location iBELLE TERRACE Sample Depth --- _ Sampling Point T6-6 TK 2-6-6' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 104-02749-30 . .. .. :!~:!:!:!~ D;~I'~!~:~,!:!~ ![~}~t~i i~:i¢:.~A~:$Iyg[ii:~iii~ggiii:ii!ii[D]l~I[b'fi~ii: Benzene < PQL mg/kg I 0.005 0.00036 8021B 03/19/04 03/19/04 04:17 HKS GC-V8 I 1 302-100442 ND !Toluene < PQL mg/kg 0.005 0.0040 8021B 03/19/04 03/19/04 04:17 HKS GC-¥8 I 302-100442 ND Ethylbenzene < PQL mg/kg 0.005 0.0018 8021B 03/19/04 03/19/04 04:17 HKS GC-V8 1 302-100442 ND Methyl t-butyl ether < PQL mg/kg 0.02 0.00056 8021B 03/19/04 03/19/04 104:17 HKS GC-V8 I 302-100442 ND Total Xylenes __ < PQL i mg/kg 0.01 0.0098 8021B 03/19/04 03/19/04 04:17 HKS GC-V8 I 302-100442 ND _ I Gasoline Range Organics (C4 - C12) ~ < PQL mg/kg 1 0.046 8015M 03/19/04 03/19/04 04:17 HKS GC-V8 I 302-100442 ND a,a,a-Trifluorotoluene L-_ 102 t % 70-130 ! 8021B 03/19/04 03/19/04 04:17 HKS GC-V8 1 302-100442 ! ........... a,a,a-Trifluorotoluene (8015 I I t I ~i I' Surrogate) i 126 I % 70-130 8015M !03/19/04 !03/19/04 04:17 HKS SC-V8 1 302-100442 I California DOHS Certification #1186 All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661)327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/24/2004 16:02:16 04-02749-30 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 09:42 Sampling Location BELLE TERRACE Sample Del~th --- Sampling Point T6-2 TK 2-6-2' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-29 Benzene < PQL mg/kg 0.005 0,00036 8021B 03/19/04 03/19/04 03:47 HKS GC-V8 I 302-100442 ND Toluene < PQL mg/kg 0.005 0.0040 8021B 03/19/04 03/19/04 03:47 HKS GC-V8 1 302-100442 ND Ethylbenzene < PQL mg/kg 0.005 0.0018 8021B 03/19/04 03/19/04 03:47 HKS GC-V8 1 302-100442 ND Methyl t-butyl ether < PQL I mg/kg 0.02 0.00056 8021B 03/19/04 03/19/04 03:47 HKS GC-V8 1 302-100442 ND Total Xylenes < PQL mg/kg 0.01 0.0098 8021B ,03/19/04 03/19/04 03:47 HKS GC-V8 1 302-100442 ND Gasoline Range Organics (C4 - i -- C12) < PQL ' mg/kg I 1 0,046 ~ 8015M t03/19/04 j03/19/04 03:47 HKS SC-V8 I 302-100442 ND a,a,a-Trifluorotoluene 99 % 70-130 8021B 03/19/04 03/19/04 03:47 HKS GC-V8 I 1 302-100442I a,a,a-Trifluorotoluene (8015 , Surrogate) 123 I % 70-130 8015M 03/19/04 03/19/04 03:47 HKS GC-V8 1 302-1004421 California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the submitting party. BC Laboratories, hic. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Printed 03/24/2004 1 6:02:06 4]00 Adas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com , 04-02749-29 a at c RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COc Number --- Receive Date/Time ~03/17/2004 @ 11:40 Project Number 1200150 Sampling Date/Time 03/17/2004 @ 09:40 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point T3-6 TK 1-3-6' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04~02749-28 Toluene <PQL ] mg/kg 0.005 0.0040 8021B 03/19/04 03/19/04 01:17 HKS I GC-V8 1 302-100442 L -~ .... Ethylbenzene -- I <PQL I mg/kg 0.005 0.0018 8021B 03/19/04 03/19/04 01:17 HKS GC-V8 1 302-100442~ Methyl t-butyl ether I < PQL i mg/kg 0.02 0.00056 ~ 8021B ~ 03/19/04 03/19/04 01'17 HKS GC-V8 I 302 100442 Total Xylenes j < PQL I mg/kg 0.01 0.0098 8021B 103/19/04 03/19/04 01'17 HKS I GC-V8 i 1 302-100442- Gasoline Range Organics (04 - ' 0~ I 012) <PQL mg/kg 1 0.046 I 8015M '03/19/ 03/19/04 01:17 I HKS GC-V8 I 1 302-100442 ND a a a-Trifluorotoluene (8015 I I ] I Surrogate) I 108 ! % I 70-130 I 8015M 103/19/04 103/19/04 01:17i HKS I GC-V8 , 1 1302-100442 ] California DOHS Certification #1 186 Al! results listed in this report are for thc exclusive use of the submitting party. BC Laboratories, ~c. assumes no responsibility for report alteration, separation, detachment or third par~y interpretation. 4]00 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/24/2004 16:01:56 04-02749-28 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number --- Receive Date/Time 103/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 09:37 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point IT3-2 TK 1-3-2' Sample Matrix !sOil Sampled By IK. Malamma BCL Sample ID 04-02749-27 ~enzene <,Q' m9,k, 0.005 0.00036 I 6021. 03/19,04 03,19,04 00:47 'HKS Toluene ~ < PQL ~ mg/kg 0.005 0.0040 8021B 03/19/04 Ethylbenzene <PQL mg/kg I 0.005 0.0018 ~ 8021B 03/19/04 '03/19/04 ~00:47 HKS GC-V8 1 302-100442 { N~ } ............. Meth~-butyl ether < PQL mg/kg 0.02 0.00056 ~ 8021B ~03/19/04 03/19/04 00:47 HKS GC-V8 1 302-1004~~ .... Total Xylenes < PQL mg/kg 0.01 0.0098 ~ 8021B 03/19/04 03/19/04 00:47 HKS GC-V8 ~ 1 302-100442 j-~---~ ........... Gasoline Range Organics (~ - ~ ~ I ~ c~2) <~QL ~ ~/~ ~ ~ ~.0~ J ~O~SM ~03/~/0~ ~03/~/0~ 00:~7~ HKS J GC-V~ a,a,a-Trifluorotoluene 95 % 70-130 8021B 03/19/04 03/19/04 00:47 HKS GC-V8 1 302-100442 a,a,a-Trifluorotoluene (8015 Surrogate) 118 % 70-130 8015M ~ 03/19/04 03/19/04 00:47 HKS GC-V8 1 302-100442 California DOHS Certification #1 186 All results listed in this report are for the exclusive use of[he submitting party. BC Laboratories, inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/24/2004 10:01:47 04-02749-27 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 09:33 S~ampling Location BELLE TERRACE Sample Depth --- Sampling Point T1-6 TK 1-1-6' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-26 Toluene ~' < PQL mg/kg 0.005 0.0040 8021B ~ 03/19/04 03/19/04 18:24 HKS GC-V8 Ethylbenz~e ~ < PQL I mg/kg 0.005 0.0018 8021B ~03/19/04 , 03/19/04 18:24 HKS SC-V8 , 1 Methyl t-butyl ether ~ < PQL ! mg/kg 0.02 0.00056 8021B 03/19/04 03/19/04 18:24 HKS GC-V8 Total Xylenes ~ < PQL mg/kg 0.01 0.0098 8021B j 03/19/04 03/19/04 18:24 ~ HKS GC-V8 1 C12) I < PQL i mg/kg 1 0 046 8015M ~03/19/04 I 03/19/04 18:24 I HKS GC-V8 ] I ] 302-100442 I ND 8,e,e-Trifluorotoluene i q0~ I 8,e,e-Trifluorotoluene (80~5 I % 70-~0 802~B 0~/~0/04 ~ 0~/~/04 q8:~4 HKS ~G-V8 Surrogate) q~ % 70-~0 I 80~5M 0~/q0/04 : 0~/~/04 q8:24 HKS ~C-V8 q ~0~-~0044~ California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the submitting party. DC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Printed 03/24/2004 16:01:37 41o0 Atlas Court * Bakemfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com 04-02749-26 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number i'" Receive Date/Time 03/17/2004 @ 11:40 P__roject Number 1200150 Sampling Date/Time 03/17/2004 @ 09:30 S~ampling Location BELLE TERRACE Sample Depth --- ~Sampling Point T1-2 TK 1-1-2' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-25 ..................................................................................fl [ iii i!iii!i?. ii? iiiii Benzene_ < PQL I mg/kg 0.005 0.00036 8021B I 03/18/04 03/18/04 23:47 HKS GC-V8 I 302-100442 I ND Toluene < PQL mg/kg 0.005 0.0040 8021B03/18/04 03/18/04 23:47 HKS GC-V8 1 302-100442i -~ND Ethylbenzene <PQL I rog/kg 0.005 0.0018 8021B 03/18/04 03/18/04 23:47 HKS i GO-V8 i 1 302-100442 J Methylt-butylether I <PQL i rog/kg 0.02 0.00056 8021B 03/1.8/04 03/18/04 123:47 HKS GO-V8 I 1 i3o2-1oo442 --'~_ ._.~_ Total Xylenes .... < PQL mg/~g 0,01 0.0098 8021B 03/18/04 03/18/04 23:47 __HKS GC-V8 I I I 302-100442 ND Gasoline Range Organics (C4 - t I C12) < PQL ~ mg/kg 1 0.046 i 8015M 103/18/04 I 03/18/04 23:47 i HKS GC-V8 1 302-100442 ND :::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::: ::::::::::::::::::::::::::::::::::::::::::::::::::::::::: :: ~ ~ a,a,a-Trifluorotoluene 95 % 70-130 I 8021B 03/18/04 j03/18/04 23:47 HKS GC-V8 1 302-100442 j a,a,a-Trifluorotoluene (8015 Surrogate) 115 % 70-130 8015M 03/18/04 03/18/04 23:47 HKS GC-V8 1 302-100442 California DOHS Certification #1 186 Al! results listed in d~is report are for the exclusive Use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/24/2004 16:01:27 04-02749-25 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number --- Receive Date/Time 103/17/2004 @_!__1:40~ ........... Project Number 200150 iSampling Date/Time 103/17/2004 @ 09:25 Sampling Location BELLE TERRACE Sample Depth !--- __ Sampling Point T2-6 TK 1-2-6' Sample Matrix iSoil Sampled By K. Malamma BCL Sample ID 04-02-~2-2~,- Benzene I < PQL i mg/kg I 0.005 0.00036 8021B 03/18/04 i03/18/04 23:17 HKS GC-V8 1 302-100442 ~ ND J ............ Toluene I < PQL i mg/kg 0.005 0.0040 8021B 03/18/04 ~03/18/04 23:17 HKS GC-V8 i 1 302-100442 Ethylbenzene < PQL mg/kg 0.005 0.0018 8021B 03/18/04 03/18/04 23:17 HKS GC-V8 1 302-100442 N~D___ ~Methyl t-butyl ether < PQL mg/kg 0,02 0.00056 I 8021B 03/18/04 ~ 03/18/04 23:17 HKS GC-V8 1 302-100442 ND Total Xylenes < PQL rog/kg 0.01 0.0098 8021B 03/18/04 03/18/04 23:17 HKS GC-V8 1 302-100442 ND __ Gasoline Range Organics (C4 - C12) < PQL mg/kg 1 0.046 8015M 03/18/04 03/18/04 23:17 HKS GC-V8 1 302-100442 ND a,a,a-Trifluorotoluene 75 % 70-130 8021B 03/18/04 03/18/04 23:17 HKS GC-V8 1 / 302-100442 a,a,a-Trifluorotoluene (8015 Surrogate) 90 % 70-130 8015M 103/18/04 03/18/04 23:17 HKS GC-V8 I I 302-100442 I California DOHS Certification #1 186 Ali results ]isled in dds report, are £or the exclusive usc o£the submittQ~8 party. BC Laboratories, [nc. assumes no responsibility for report a]~.eradon, separation, detachment or t~i.z-d party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/24/2004 16:01:17 04-02749-24 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number I--- Receive Date/Time 03/17/2004 @ 11:40 Project Number 1200150 Sampling Date/Time 03/17/2004 @ 09:22 Sampling Location IBELLE TERRACE Sample Depth l--- _ Sampling Point T2-2 TK 1-2-2' Sample Matrix Soil Sampled By K. Ma aroma BCL Sample ID 04-02749-23 Benzene < PQL mg/kg 0.005 0.00036 8021B 03/18/04 I 03/18/04 22:47 HKS GC-V8 I 302-100442 ND Toluene < PQL mg/kg 0.005 0.0040 8021B '03/18/04 03/18/04 22:47 HKS GC-V8 1 302-100442 ND Ethylbenzene < PQL mg/kg 0.005 0.0018 8021B 03/18/04 03/18/04 22:47 HKS GC-V8 I 302-100442 ND Methyl t-butyl ether , < PQL mg/kg 0.02 0.00056 8021B 03/18/04 03/18/04 22:47 HKS GC-V8 1 302-100442 ND . TotaIXylenes < PQL rog/kg 0.01 0.0098 8021B 03/18/04 03/18/04 22:47 HKS GC-V8 1 302-100442 ND Gasoline Range Organics (C4 - C12) < PQL rng/kg 1 0.046 8015M 03/18/04 03/18/04 22:47 HKS GC-V8 I 302-100442 ND a,a,a-Trifluorotoluene I 74 t % I 70-130 I 8021B 03/18/04,03/18/04 22:47 HKS I Gc-v8 a,a,a-Trifluorotoluene (8015 t I Surrogate) I 92 f % I 70-130 i 8015M i03/18/04 103/18/04 22:47 HKS I GO-V8 ! 1 302-100442 California DOHS Certification #1186 Al! results listed in dds report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. Printed 03/24/2004 1 6:01:07 4~00 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com 04-02749-23 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 09:20 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point T5-6 TK 2-5-6' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-22 Benzene < PQL mg/kg 0.005 0.00036 8021B 03/18/04 03/18/04 22:17 HKS GC-V8 1 302-100442 ND Toluene < PQL mg/kg 0.005 0.0040 8021B 03/18/04 03/18/04 22:17 HKS GC-V8 I 302-100442 ND Ethylbenzene < PQL rog/kg 0.005 0.0018 8021B 03/18/04 03/18/04 22:17 HKS GC-V8 I 302-100442 ND__.i Methyl t-butyl ether < PQL rog/kg 0.02 0.00056 8021B 03/18/04 03/18/04 22:17 HKS GC-V8 1 302-100442 ND ]'o__tal Xylenes < PQL mg/kg 0.01 0.0098 8021B 03/18/04 03/18/04 22:17 HKS GC-V8 I I 302-100442 ND Gasoline Range Organics (C4- I I ' .... q- ........... C12)/ < PQL{ mg/kg 1 0.046 8015M 03/18/04 03/18/04 22:17 HKS GC-V8 1 302-100442 ND a,a,a-Trifluorotoluene j 84 % 70-130__ 8021B 03/18/04 03/18/04 22:171 HKS GC,-V8 I 1 302-100442 a,a,a-Triflu0rotoluene (8015 I ' j I ~ J Surrogate) I 106 % 70-130 ! 8015M 03/18/04 ~03/18/04 22:17 HKS GC-V8 1 1302-100442 , California DOHS Certification #1186 Al! results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-4911 * FAX (661) 327-1918 * www.bclabs.com Printed 03/24/2004 16:00:57 04-02749-22 RAM ENVIRONMENTAL ENGINEERING 2103 20TH ST. BAKERSFIELD, CA 93301 Attn: KEVIN MALAMMA Purgeable Aromatics and Total Petroleum Hydrocarbons COC Number --- Receive Date/Time 03/17/2004 @ 11:40 Project Number 200150 Sampling Date/Time 03/17/2004 @ 09:17 Sampling Location BELLE TERRACE Sample Depth --- Sampling Point '1'5-2 TK 2-5-2' Sample Matrix Soil Sampled By K. Malamma BCL Sample ID 04-02749-21 Benzene I < PQL mg/kg 0.005 0.00036 8021B 03/19/04 03/19/04 12:18 HKS GC-V8 1 302-100442 ~ ND ~_ j ....... Toluene < PQL mg/kg 0.005 0.0040 8021B 03/19/04 03/19/04 12:18 HKS GC-V8 I 302-100442 Ethylben~ene < PQL mg/kg 0.005 0.0018 8021B ~ 03/19/04 03/19/04 12:18 HKS GC-V8 1 302-100442 ND ~ .......... Methyl t-butyl ether < PQL mg/kg 0.02 0.00056 8021B ~ 03/19/04 03/19/04 12:18 HKS GC-V8 I ~ 302-100442 N~ ...... ~ ........... Total Xylenes < PQL mg/kg 0.01 0.0098 8021B 03/19/04 03/19/04 12:18 HKS GC-V8 I ~ 302-100442 Gasoline Range Organics (C4 - J ...... ~ .............. C12) j <PQL ~ mg/kg 1 0.046 8015M 03/19/04 03/19/04 12:18 HKS GC-V8 I 302-100442 ~ ND [ ~ ~p:::~::::::~; ::::::::::::::::::::::::::::::::::::::::::::::::::::::: ~;:~n:~:~:~:~:~ ......................................... :::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::: a,a,a-TriflUorotoluene 95 ! % 70-130 ~ 802~ 03/~9/04J03/~9/04 12:18 HKS IGC-V8 ~ I 302-100442 a,a,a-Trifluorotoluene (8015 12:18 I Surrogate) 120 , % 70-130 8015M 03/19/04 03/19/04 HKS GC-V8 1 1302-100442 , California DOHS Certification #1186 All results listed in this report are for the exclusive Use office submitting party. DC Laboratories, Inc. assumes no responsibility for report a teration, separation, detachment or third party interpretation. 4100 Atlas Court * Bakersfield, CA 93308 * (661) 327-49] 1 * FAX (661) 327-1918 * www.bclabs.com Printed 03/2472004 16:00:47 04-02749-21 I I '1 I I I I I I I I I I I I I I I I APPENDIX B SAMPLING PLAN JACO Oil - Belle Terrace and Stine - Summary Sampling Plan RAM Project #200150, Task 1 - Confirmation Soil Sampling TASK OBJECTIVE: Sample soils at 2-feet and 6-feet below bottom grade of USTs, piping, and dispensers, as necessary, for analysis of TPH-g, TPH-d, MTBE, and BTEX on a rush basis. SOIL SAMPLE ANALYSES Laboratory analysis will be conducted by an environmental testing laboratory certified by the State of California for the tests to be performed. Test methods and criteria are as follows: · TPHg and TPHd by Modified EPA Method 8015 · BTEX and fuel oxygenates by EPA Method 8260 · Analytical Laboratory - BC Laboratories, Bakersfield CA · Rush sample turnaround time - 24 hr results. · Report results to Kevin Malamma, RAM Environmental Engineering SOIL SAMPLING PROTOCOL Soil sampling will be conducted in accordance with RAM Environmental Engineering Services Standard Soil and Groundwater Sampling Protocols (RAM, 2003) and will incorporate the following project specific criteria. Sampling Locations Sample locations will be as follows: 12,000 gallon UST - 3 sample locations 10,000 gallon UST - 2 sample locations Connecting Pipes - sample locations at Tees and 90s as verified in the field Dispensers - 1 sample location per unit Soil Confirmation Information Sample at 2-feet and 6-feet below bottom of hole for USTs, Dispensers, and Connecting Piping - · Use backhoe or excavator bucket for excavation of samples · Push brass sleeve into excavated soil to completely fill sleeve · Use Teflon seal and plastic caps to seal sleeve · Indicate direction of sample collection on sleeve (arrow) · Monitor soils and void space with hand held PID or equivalent Equipment: · Brass Sleeves · Teflon seals and Plastic caps · Disposable gloves, baggies, permanent marking pens, sample labels, COC forms, Field Log forms, residuals (IDR) labels · PID, HNU or OVM meter for monitoring work space for volatiles I 2000 04 150 SummarySamplingPlan I I I I I I I I I I I I I I · Personal Protective Gear per Standard Health and Safety Protocols for fuel impacted groundwater. · Three (3) 5-gallon steel buckets with secure lids for disposal of rinse and purge water. · Pre-chilled non-water cooling material for sample storage/shipping container. Sampling Procedure Once the equipment is removed, the first soil removed should be sampled using the handheld meter and the meter reading recorded. Soil should be returned to the excavation. The backhoe can excavate a bucket's width to 2-feet bgs, bringing the soil to a safe ground level away from the pit. A brass sleeve, properly capped on one end, will be hand pushed into the soil in the backhoe bucket (at the point closest to the teeth of the bucket). The sleeve will be properly sealed and a directional arrow drawn to indicate the sample direction. The soil (and the void space) in the bucket will be monitored with the handheld meter and the results recorded. Sample Identification and Labeling Complete sample label information and sample chain of custody information prior to collection of each sample, leaving sampling time for notation just after collection. Label, bag, and place in foam holders in sample shipping container. Fill other containers supplied by laboratory, and label and store in the same manner. Check/complete the chain-of-custody form and sample logs, and secure the sample storage/shipping container until delivered to the laboratory. Sample container should be kept cool with pre-chilled non-water icing material. 2000 04 150 SummarySamplingPlan