HomeMy WebLinkAboutMITIGATION (2) Environmental
Consultants~ inc.
Solving environment-related business problems worhtwide
91'1 South Primrose Avenue · Suite K
Monrovia, Ca[iforrda 91016 USA
626.256.6662 ' 800.477.7411
Fax 626.256.6263
www. deltaer~v, com
April 15, 2004
Project PA24010-1
CalLforrSa Re~onal Water Quality Control Board
CentrM Valley Re, on
1685 B Street
Fresno, California 93706-2020
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Re: FIRST QUARTER 2004 GROUNDWATER MONITORING REPORT
Texaco Service Station
2401 Oak Street
Bakersfield, California
Dear/Viz. Whiting:
On behalf of Eqnilon Enterprises LLC dba Shell 0/2 Products (SHELL), Delta Environmental Consultants, Inc.
(DELTA) [formerly KI-IM Environmental Management, Inc. (KH2VD] has prepared th/s First Quarter 2004
Groundwater Monitoring Report for the above referenced site.
This quarterly report represent DELTA'S professional opinions based upon the currently available/n_formation and
are arrived at in accordance with currently acceptable professional standards. This report is based upon a specific
scope of work requested by the client. The Contract between DELTA and its client outlines the scope of work, and
only those tasks specifically author/zed by that contract or outlined/n this report were performed. This report is
/ntended only for the use of DELTA's CLient and anyone else ~pecifically Listed on th/s report. DELTA will not
~md cannot be liabl-e for unauthorized reliance by any other th/rd party. Other than as contained in th/s para,apb,
DELTA makes no express or implied warranty as to the contents of this report.
If you have a~y questions regarding this site, please contact Brad Clark (DELTA) at (626) 256-6662 or
ti TOnY Palagy/(SHELL) at~(425) 377-85)0.
I De!t~ Enj~roumental Consultants, Inc.~
.E. C55425
/I Staff Geolo~st Senior Projec~ Engineer
Attachment: First Quarter 2004 Groundwater Monitoring Report
I cc: Tony Pata~yi, Shell 0/2 Products US
Howard H. W~es I~, City of Bakersfield Fire Department
A membeT off
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SHELL QUARTERLY STATUS REPORT
April iS, 2004
Station Address:
DELTA Project No.
SHiELL Environmental Engin./Phone No.:
DELTA Site Manager/Phone No.:
Primary Agency/Regulatory ID No.:
Other Agencies to Receive Copies:
2401 Oak Street, Bakersfield, California
PA24010-1
Tony Palagyi/(425) 377-8530
Kathryn Ewing(626) 256-6662
Central Valley RWQCB / John Whiting.
City of Bakersfield Fire Dept./t-Ioward H. Wines III
WORK PERFORMED THIS QUARTER (ITIRST - 2004):
1. Quarterly groundwater monitoring and sampling. Submitted quarterly report.
2. Implemented no-pUrge sampling per CVRWQCB approval letter dated October 10, 2003.
3. Implemented approved site assessment activities per CVRWQCB approval letter dated October 21,
2003.
4.. Submitted "Site Assessment Report" dated February 20, 2004.
WORK PROPOSED FOR NEXT QUARTER (SEcoND - 2004):
1. Quarterly groundwater monitoring and sampling. Submit quarterly report.
Current Phase of Proj eot: Groundwater monitoring
Frequency of Sampling: Quarterly
Frequency of Monitoring: · Quarterly
Is Separate Phase Hydrocarbon Present On-site (Well #'s): [] Yes [] No
Cumulative SPH Recovered to Date: NA
SPH Recov6red This Quarter: None
Sensitive Receptor(s) and ReSPective Direction(s): Nearest field verified well is Well BK060-02 (State Well
Current Remediation Techniques:
Permits for Discharge:
Approximate Depth to Groundwater:
Groundwater Gradient
Current Agency Correspondence:
Summary of Unusual Activity:
No. 29S/27E-25D02M) of the California Water Service
Company in Bakersfield approximately 759 feet East of
the site.
None
None
16.30' to 20.59' · .
South-southeast (~ approximately 0.011 ft/ft
cVRWQCB letter dated January 6, 2004.'
None
/
I<lathrsm Ewing
Site Manager (DELTA)
ATTACI~F,D:
· Table 1 - Historical Groundwater Gauging and Analytical Results
· Table 2 - Additional Chemicals of Concern
· Figure 1 - Site Location Map
· Figure 2 - Groundwater Elevation Contour Map
· Figure 3 - Hydrocarbon Distribution in Groundwater Map
· Figure 4 - TPH-g Concentrations in Groundwater Map
· Figure 5 - Benzene Concentrations in Groundwater Map
· Figure 6 - MTBE Concentrations in Groundwater Map
· Appendix A- Field Data Sheets
· Appendix B - Field Procedures
· Appendix C - Waste Disposal Document
· Appendix D - Laboratory Report and Chain-of-Custody Documents
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TABLES
m m mmm mm m m m mmm m m m m m m m m m m m
HISTORICAL GROUNDWATER GAUGING AND ANALYTICAL DATA
SHELL SERVICE STATION ._
2~401 Oak Street, Ba___kersfield, California
i:i:i~:~r~:i:i:i:i:~i:::: :~t~ :::: ~ ~;~: :}: ================================================================================================================= :::::::::~: :::::::::::::::::::::::::::::::::::::::::::::::: ::::::::
:::::: :~:~:::::::~:~::::::RB~;:::::ff~¢i~i(~::::::::: :::~:~::: :::::::~:~::: :::::~:~:~:~:~::::::: :':: ::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::
::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::: :~:~:~:~:i~&~: :i:~:~: :(~i :?:: :~:::: :i~i:::: ~:::: ~: :::: ~¢~::: :::: :::: :: :~: :?: :: :::: ::
MW-I Top of~asinj elevation~fO: 402.03
3/18/2003 26.81 0.00 375.22
3/~5/2003 28.19 0.00 373.84 ~<1000 ~<50 ~<0.50 ~<1.0 ~<1.0 ~<1.0 ~<1.0 ~<10 ~<2.0 ND<2.0 ~<2.0 ~<10~
6/18/2003 17.70 0.00 384.33 ~<50 ~<0.50 ND<I.0 ~<1.0 ~<1.0 ~<1.0 ~<10 ND<2.0 ~<2.0 ~<2.0
9/3/2003 16.33 0.00 385.70 ND<50 ~<0.50 ~1,0 ND<I.0 ~<1.0 ~<1.0 ~<10 ~2.0 ~<2.0 ~2.0 ~<100
10/21/2003 21.6~ 0.00 380.40 ~<50 ~0.50 ND<I.0 ~<1.0 ND<I.0 ~<I.0 ~<10 ~<2.0 ~<2.0 ~<2.0
1/13/2004 17.6~ 0.00 384.43 ~<50 ~<0.50 ~<1.0 ~<1.0 ND<I.0 ~<1.0 ~10 ~<2.0 ~<2.0 ~<2.0 Pre-pprge sample
1/13/2004 ~<50 ~0.50 ~l.0 ~<1.0 ND<I.0 ~<1.0 ~<10 ~<2.0 ~<2.0 ~<2.0 Post-purge sample
MW-2 Top of~asin~ elevation~t): 404.49
3/18/2003 29.70 0.00 374.79
3/25/2003. 31.02 0.00 373.47 ~<1000 660 ~<0.50 ~1.0 ~<1.0 ~<1.0 ~<1.0 ~<10 ~<2.0 ~<2.0 ~2.0 ~<100
6/18/2003 20.79 0.00 383.70 ~<50 ~<0.50 ~<1.0 ~<1.0 ~<1.0 ~<1.0 ~<10 ~<2.0 ~<2.0 ~<2.0
9/3/2003 19.31 0.00 385.18 ~<50 ~<0.50 ~<1.0 N~I.0 ~<1.0 ~<I.0 ~<10 ~<2,0 ~<2.0 N~2.0 N~100
10/21/2003 24.57 0.00 379.92 ~<50 ~D<0.50 ND<I.0 . ~<1.0 ~<1.0 ND<I.0 ~<10 ~<2.0 ~2.0 ND<2.0
,~/13~004 20.59 ~ 0.00 383.90 ~<50 ~<0.50 ~<1.0 ~<1.0 ~<1.0 ~<1.0 ~<10 ~<2.0 ~<2.0 ~<2.0 Pre-pur~esa~pl~
1/13/2004 __ ~<50 ~0.50 ~<1.0 ~<1.0 ~1.0 ~<1.0 ~<10 ~2.0 ~<2.0 ~2.0 Post-purge sample
MW-3 T~p of easing elevation (ft): 403.43
3/18/2003 28.94 0.00 374.49
3/25/2003 30.27 ~ 0.00 373.16 ND<1000 72 ~<0.50 ~<1.0 ~<1.0 ~<I.0 57 ~<10 ND<2.0 ~<2.0 ND<2.0 ND<100
6/18/2003 20.98 0.00 382.45 ND<50 ~0.50 ~<1.0 ~<1.0 ~<1.0 17 ND<I0 ~<2.0 ~<2.0 ~<2.0
9/3/2003 19.01 0.00 384.42 ~<50 ~<0.50 ~<1.0 ND<I.0 ~<1.0 ~1.0 ~<10 ~<2.0 ~<2.0 ~<2.0 ~<100
10/21/2003 23.89 0.00 379.54 ~50 ~<0.50 N~l.0 ND<I.0 ~<1.0 ~<1.0 ~<I0 ~<2.0 ND<2.0 ~<2.0
_j/13/2004 20.37 0.00 ~ 383.06 ~<50 ~0.50 ND<I.0 ~<1.0 ~<1.0 ~<I.0 ~<10 ~<2.0 ~<2.0 ~<2.0 Pre-purge sample~
1/13/2004 ~<50 ~<0.50 ~<1.0 ~<1.0 ~<1.0 ~<1.0 ~<10 ~2.0 ND<2.0 ~2.0 Post-purge sample
MW-4 T~p of casing elevation (ft): 400.11
3/19/2003 25.42 0.00 374.69
3/25/2003 26.75 0.00 373.36 ~<1000 ~<50 ~0.50 ~<1.0 ND<I.0 ~1.0 7.3 ~<10 ND<2.0 ~<2.0 ~2.0 ND<100
6/18/2003 17.31 0.00 382.80 ~<50 ~0.50 ~1.0 ~<1.0 ND<I.0 ~<1.0 ~<10 ~2.0 ~<2.0 ~<2.0
9/3/2003 15.43 0.00 384.68 ~<50 ~0.50 ~<1.0 ~<1.0 ~<1.0 3.4 ~<I0 ~<2.0 ~<2.0 ND<2.0 ~<100
10/21/2003 20.34 0.00 379.77 ND<50 ~<0.50 ~<l.0 ~<I.0 ND<I.0 ~<1.0 ~<10 ~2.0 ND<2.0 ~<2.0
1/13/2004 16.77 0.00 383.34 ~<50 ~<0.50 ~<1.0 ~<1.0 ~<1.0 ~<1.0 ~<10 ND<2.0 ~<2.0 ~<2.0 Pre-purge sample
MW-5 _Top of casing elevation (ftC: 399.91
3/19/2003 25.03 0.00 374.88
3/25/2003 26.38 0.0O 373.53 ~<1000 ' ~<50 ND<0.50 ND<I.0 ~1.0 ND<I.0 40 ~<10 ~<2.0 ~<2.0 ND<2.0 ~<100
6/18/2003 16.72 0.00 383.19 ND<50 ~<0.50 ~<1.0 ~<1.0 ~<1.0 ~<1.0 ~<10 ~<2.0 ~<2.0 ~<2.0
9/3/2003 15.28 0.00 384.63 ~<50 ~<0.50 ~<1.0 ~<1.0 ~<1.0 ~<1.0 ~<10 ~<2.0 ~<2.0 ~<2.0 ~<100
10/21/2003 19.89 0.00 380.02 ~<50 ~<0.50 ND<I.0 ND<I.0 ~<1.0 ~<1.0 ~10 ~<2.0 ND<2.0 ~<2.0
1/13/2004' 16.30 0.00 383.61 ~<50 ~<0.50 N~I.0 ~<1.0 ~<1.0 ~<1,0 ND<10 ~<2,0 ~<2.0 ~<2.0 Pre-purge sample
Page I of 2
HISTORICAL GROUNDWATER GAUGING AND ANALYTICAL DATA
SHELL SERVICE STATION I
2401 Oak Street, Bakersfield, California
ii ip~i~ i i i i:~i:!:i:i:i:~a.':::: ~;~. ~ .~;i::: ~ :i:i:i:~'i~.'::: :::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::
GW - Groundwater
S~H - Separate-phase hydroc~bons
MSL - Mean sea level
ND - Not detected
u_~ -~an~per billion
~H-D - Total petroleum h~droc~bons ~ diesel
TPH-G - Total petroleum hydrocarbons as gasoline using either EPA Method 8015M or ~e DHS L~T Method
M~E - Me~yl-ten bu~ ether
~A - Te~-bu~l alcohol _
D~PE - Di-isopsopyl ether
E~E - Ethyl-te~ bu~ e~er
T~ - Te~-amyl methyl ether
Su~ey dam provided by ~ Enviromenml M~agement, Inc.
I I I I
Page 2 of 2
TABLE 2~ L I
ADDITIONAL CHEMICALS OF CONCERN
TEXACO SERVICE STATION
2401 Oak Street, Bakersfield, California -- ~--
:::::::::::::::::::::::::::: ::2 {~i~::: (~i~::::;::::::::::: ~i~¢O~}:: 2~:: ~:~:.~i.~i~a).:.:.:.~.:.:.~.:.:.:.:.:.:~:.:.~.:.:.:.:.:.:.~.:.:.:.:.:.~.X.~.~.~.
MW.1
9/3/2003~lO ND<0.10 0.42 17 NDe.50 50 50 ND<I.0 ND<I.0 ND<0.0 16.2 N~0.1 3.63 1.63 29.9 ND<0.005 240 66 6.21 150
1/13/200~ ~ 71 NA 1.0 N~ N~0.50 56 56 N~I.0 N~I.0 N~0.01 NA ~A 0.0128 2.72 33.2 NA 490 140 6.54 300
1/13~004 82 NA~ I.I NA ND<0.50 100 100 ND<I.0 N~I.0 ND<0.01 NA NA 0.0114 2.78 33.6 NA 490 140 6.55 290
MW-2
9B/2003 NA NA N~ NA NA NA NA NA ~ ~NA N~0.0 NA NA NA NA NA NA NA NA NA NA
1/13~004 NA NA NA NA NA NA NA NA NA ND<0.0[ NA NA NA NA ~ NA NA NA NA NA NA ~ple
1/13/2004 NA NA NA NA NA NA NA NA NA ND<0.01 NA NA NA NA NA NA NA NA NA NA P~l-pur~ ~ple
~-3
9/3/2~3 19 I~ 1.50 20 ND<0.50 56 56 ND<I.0 ~1.0 N~0.01 15.7 0.107 4.06 1.66 31.9 ND<0.005 230 74 6.23 130
1/13/2004 67 ] NA 0.54 NA ND<0,50 46 46 ND<I.0 ND<I.0 ND<0.01 NA NA ND<0.005 3.00 30.6 NA 440 120 6.72 260 P~-pu~ ~ple
1/13~0~MW472 ~NA 1.4 NA 0.63 60 ~ 60 N~I.0 ND<I.0 ND<0.01 NA NA 0.114 3.55 31.8/ NA 470 140 6.51 28~
9/3/2003 19 0.95 22 0.56 66 66 N~I.0 ND<I.0 ND<0.01 16.7 0.6 4.14 1.~ 33.1, 0.0467 250 74 6,14 150
1/13~004 48 - NA I 0.65 NA 0,56 26 26 N~I~ N~I.0 N~0.01 N~ NA 0.0337 3.09 27.2} NA 350 98 6~6~ 210
__ MW-5
9/3~003 ~A NA NA NA N~ - NA NA NA NA N~0.01 NA NA NA NA NA NA NA N~ ~ N~
1/13~004 ~NA ] NA NA NA NA NA NA NA NA N~0.01 NA NA _~A NA NA NA NA NA NA NA
Not~:
TKN - Total KjeIdahl Nitm~n ~ ~
TDS - Total Dissolved Solids
NA - Not anal~ ~
NOTES: ~
Addlti~al Chemicals of Concern Anai~uring tho fi~~ for wells MW-I~W-3, and MW~.
Tw~les were ~en on 1/13~0~ for wells MW-I, MW-2, and MW-3. ~e fi~t eo~s~nd to ~¢ p~-purge ~pl¢.
Page 1 of I
Fmcs
i19'~04!00' W !Igz'0~00'' W !!9°02'00'' W WGS84 119°0I'00'' W
119°04'00"
I
DELTA I SHELL OIL PRODUCTS US
ENVIRONMENTAL TEXACO SERVICE STATI'ON
CONSULTANTS INC.I BAKERSFIELD, CALIFORNIA
FIGURE 1
SITE LOCATION MAP
2401 OAK STREET
BAKERSFIELD, CALIFORNIA
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DEISEL
TANK
SLAB
BOOTH
MW-1
W
LEGEND
384.40-- -- --
MW-1 ~ GROUNDWATER MONITORING WELL
LOCATION ANDDESIGNATION
(384.43) GROUNDWATERELEVATION
IN FEET ABOVE MEAN SEA
LEVEL (Ft/MSL)
GROUNDWATER CONTOUR
IN FEET ABOVE MEAN SEA
LEVEL (Ft/MSL)
CONTOUR INTERVAL=0.40 FEET
~III APPROXIMATE GROUNDWATER
FLOW DIRECTION
PLAN~R
EXISTING
SERVATION
WELL
SIGN
/
MW-2
(383.90
DISPENSER
ISLAND
(TYP)
/
(383.06
SLAB
'~ /~" 1~)
PLANTER
4) I
0 30 60
SCALE IN FEET
,Delta
ENVIRONMENTAL
CONSULTANTS INC.
SHELL OIL PRODUCTS US
TEXACO SERVfCE STATION
BAKERSFIELD. CALIFORNIA
FIGURE 2
GROUNDWATER ELEVATION CONTOUR MAP
01/13/04
2401 NORTH OAK STREET
BAKERSFIELD, CALIEORNIA
\\Server\khm_data\Clients~_Shefl%Shell Sites\Z\2401 Oak\2004-XX-X,X_I(~04 Quarterly Report\FIGURE 2(2401)_GROUNDWATER ELEVATION CONTOUR HAP.dwg, Hodel, 3/2212004 5:31:33 PM
MW-1
DATE TPH-q BENZENE MT~E
(~/L)
(.ug/L) OJg/L)
03/25/0.3 ND<50 ND<O,50 ND<I,0
06/'iB/03 ND<50 ND<0.50 ND<I.0
09/05/05 ND<50 ND<0,50 ND<I.0
10/21/03 ND<50 ND<0.50 NO<I.0
1/13/04 ND<50 ND<O.50 ND<I,0
DEISEL
TANK
SLAB
PLANTER
MW-2
'MW-2
TRASH
OFFICE
AND
R.R.-
BOOTH
DISPENSER '~. SLAB
iSLAND
(T'rP)
2~7;, "-'
OBSERVATIONWELL 7
PLANTER
MW-5
DATE ~H- BENZENE MTBE
Cu~/~ O~/L) O-~/L)
05/25/05 ND<50 ND<0.50 40
06/18/03 ND<50 ND<O.50 ND<I.0
09/05/05 ND<50 ND<0.50 ND<I,0
1D/21/OSIND<50 ND<0.50 ND<I.0
1/15/04 ND<50 ND<0.50 ND<I.0
MW-4-
DATE TPH-g BENZENE MTBE
OD/L) (.ug/L) O~g./L)
05/25/05 ND<50 ND<0.50
06/18/05 ND(50 ND(0.50 ND<I.0
09/03/05 ND<50 ND<0.50 3.'3.4
10/21/05 ND(50 ND<0.50 ND<I.0
1/15/04 ND<50 ND<0.50 ND<I.O
MW-5
LEGEND
TPH-g
MTBE
~ug/L
ND<
GROUNOWAI~R MONITORING WELL
LOCATION AND DESIGNATION
TOTAL PETROLEUM HYDROCARBONS
AS GASOLINE
METHYL TERT-BUTYL ETHER
MICROGRAMS PER LITER
NOT DETECTED ABOVE LIMIT NOTEO
0 20 60
I ~
SCALE IN FEET
ADelta
ENVIRONMENTAL
CONSULTANTS INC.
SHELL OiL PRODUCTS US
TEXACO SERVICE STATION
BAKERSFIELD', CALIFORNIA
FIGURE 3
HYDROCARBON DISTRIBUTION
IN GROUNDWATER MAP
2401 NORTH OAK STREET
BAKERSFIELD, CALIFORNIA
\\Server\khm_data\Clients~_Shell~_Shell Sites\2\240~ Oak\2004-x-xx_lQ04 Quarterly Report~FIGURE 3(2401)_HYDROCARBON DISTP,]BUT~ON IN GW MAP.dw9, M~del, 2/g/2004 t0:3t:qB AM
TRASH -
N
S
OFFICE
AND
~ MW-1
DEISELTANKsLAEi CANOPY
LEGEND
~ MW-14~- GROUNDWATER MONITORING WELL
LLI LOCATION AND DESIGNATION
~_ ND<50 TPH-g CONCENTRATIONS IN
CD MICROGRAMS PER LITER C.ucj/L)
x<,' TPH-g TOTAL PETROLEUM HYDROCARBONS
~ AS GASOLINE
0
ND<: NOT DETECTEO ABOVE LIMIT NOTED
PLANTER
ND<50 ~
EXISTli~
"'""-.,...~ER VA TI 0 N
WELL
OISPENSER
ISLAND
(TYP)
PLANTER
SLAB
0 30 60
SCALE IN FEET
Delta
ENVIRONMENTAL
CONSULTANTS INC.
SHELL OIL PRODUCTS US
TEXACO SERVICE STATION
BAKERSFIELD, CALIFORNIA
FIGURE 4
TPH-g CONCENTRATIONS IN
GROUNDWATER MAP
01/13/04
2401 NORTH OAK STREET
BAKERSFIELD, CALIFORNIA
\\Server\khm_data\Clients~.Shell~_Shell Sites\2\2401 Oak\2004-XX-XXjQ04 Quarterly Report\FIGURE 4(2401)_TPH-g CONCEi~m~,AT]ON HAP.dwg, Model, 3/22/2004 5:32:36 PM
TRASH
SLAB
OFFICE
AND
:ANOPY
LEGEND
N
-S
MW-I~ GROUNDWATER MONITORING WELL
LOCATION AN[3 DESIGNATION
ND<0,50 BENZENE CONCENTRATIONS
IN MICROGRAMS PER LITER
(~/L)
ND< NOT DETECTED ABOVE LIMIT NOTED
PLANTER
MW-2
EXISTING
ERVATION
WELL
"~ SIGN
OIS~
ISLAND
(TY~)
SLAB
PLANTER
30 60
,
SCALE IN FEET
ADelta
ENVIRONMENTAL
CONSULTANTS INC.
SHELL OiL PRODUCTS US
TEXACO SERVICE STATION
BAKERSFIELD, CALIFORNIA
FIGURE 5
BENZENE CONCENTRATIONS
IN GROUNDWATER MAP
2401 NORTH OAK STREET
BAKERSFIELD, CALIFORNIA
\\Server\khm_data\Clients~_Shell~_Shell Sites\2\2401 Oak\2004-x-xx_lQ04 Quarterly Report\FiGURE 5(240~,)_BENZENE CONCENTRATION MAP,dwg, Model, 2/5/2004 10:53:27 AH
TRASH -
DEISEL
TANK
SLAB ~
OFFICE
AND
MW- 1
LEGEND
N
~ MW-1 ~ GROUNDWATER MONITORING WELL
LLI LOCATION AND DESIGNATION
ILl ND<I.O MTBE CONCENTRATIONS
r~ IN MICROGRAMS PER LITER
cn Cra/L)
x~ MTBE METHYL TERT-BUTYL
<3~ ETHER
o
ND< NOT DETECTED ABOVE LIMIT NOTED
~NOPY
PLANTER
MW-2
NP<.1,0
EXISTING
'~.~ERVATION
WELL
DISPENSER
ISLAND
(T~)
MW-3
SLAB
'~
PLANTER
0 30 60
SCALE IN FEET
.Delta
ENVIRONMENTAL
CONSULTANTS INC.
SHELL OIL PRODUCTS US
TEXACO SERVICE STAtiON
BAKERSFIELD, CALIFORNIA
FIGURE 6
MTBE CONCENTRATIONS
IN GROUNDWATER MAP
ol/~ 3/04
2401 NORTH OAK STREET
BAKERSFIELD, CALIFORNIA
\\Server\khm_data\Clients~_Shell~_Shell Sites\2\2401 Oak\2004-x-xx_lQ04 Quarterly Relx~t~c]GURE 6(2401)_MTBE ]SOCONCENTRATJON MAP,dwg, Model, 2/5/2004 10:53:46 AM
AP?ENmX A
FIELD DATA SHEETS
WELLHEAD INSPECTION CHECKLIST P~ge , or,
Client~ 5k,~ t~. . Date I - ~- -too,~
Site Address .3 ~ o~ ~- t ¢~ ~ ~$ ~' e~~~
Job Number o~o~ ~- nician ~. ~~.
Well Inspected -
No Corrective
Well ID A:Uon Required
Other AcUon
Water Bailed We~lbox
Cap Lock Taken
From Components Replaced Replaced (explain
Wellbox ' .Cleaned ,,. below)
Well Nol
[nspecf~d
(explain
Submitted
INOTES:
eLAINE TECH SERVICES, IHC.
SAN JOSE SACR,rd,4ENTO LOS ANGELES SAN DIEGO
Site 3 ~q o I o_,~ ~¢ ~+,
WELL GAUGING DATA
Date
Well ID
Size
(in.)
I
Sheen /
Odor
Depth to
hnmiscible
Liquid (ft.)
Ttfickmess
of
Immiscible
Liquid (ft.)
Volume of
Immiscibles
Removed [Depth to water
(mO
ZO
Depth to welt
bottom (ft.)
Survey [
P oLut: TOB
lC,.
Blaine Tech Services~ Inc. 1680 Rogers Ave. San Jose, CA 951'12 (408) 573-0555
WELL MONITORING DATA
Well I.D.: ~. I We5 Dimeter: 2 3 ~ 6 8
TotM Well Dep~ (TD): q a. o~ Dep~ to Water ~T~: ~ ~. a o
Depth to Free Product: ~clmess of Free Product (fee0:
Referenced to: ~ O~d~ D.O. Meter (ffreq'd): vs~ ~c~
DTW with 80% Recharge [(Height of Water Cohmn'x 0.20) + DTW]:
Purge Method:
Bailer · Waterra
Disposable Bailer Peristaltic
Positive Air Displacement Extraction Pump
Electric Submersfble ~ Other
Sampling Method:
Other:.
Bailer
Disposable Bailer
Extraction Port
Dedicated Tubing
Well Diamete~ l{Jultiulier Well Diameter Multlalier
1" 0.04 4"
-- (Gals.) X ' - = - Gals. ~ 2" 0.16 6" 1.47
I ] Case Volume Specified Volumes Calculated Volume 3" 037 Other mflius2 * 0.16'1
Cond. Turbidity
Time Temp (°F) pH (mS or¢[i~;~ (NTUs) Gals. Removed Observations
Bailer lowered. "~. ' below
DTW to obtotn sample
Did well dewater? Yes cl~ Gallons actually evacuated: --
Sampling Date: t. I S. zooq .. Sampling Tkne: totf Depth to Water: ,-,. ~,o
Sample I.D.: ~..~. 1 Laboratory: ~ Columbia Other
EB I.D. (if applicable): @ -a~, Duplicate I.D. (if applicable):
Analyzed for: TPH-G BTEX MTBE TPI-I-D Oxygenates(5) Other:
D.O. (ifreq'd): Pre-purge: ma/[ Post-purge: me/[
O.R.P. (if req'd): Pre-purge: mV Post-purge: mV
Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (800) 545-7558
Screened Interval: IO ' S O Il'well is listed as a no-purge, confirm that water level is below the top
of screen. Otherwise, the well must be purged.
Sampler:
Well I.D.: ,,,,a- ~ Well Diameter: 2 3 d~ 6 8
Total Well Depth (TD): ,~ q .o~, Depth to Water (DTW): t-~. ~,o
Depth to Free Product: Thickness of Free Product (feet):
Referenced to: ~ arade D.O. Meter (if req'd): vs~
DTW with 80% Recharge [(Height of Water Column x 0.20) + DTW]:
Purge Method: Bailer Waterra Sampling Method: Bailer
Disposable Bailer Peristaltic ~¢Disposabl~ Bailer
Positive Air Displacement Extraction Pump Extraction Port
~Eleclric Submersible Other Dedicated Tubing
Other:
Screened Interval: ~ot. $ o' Il'well is listed as a no-purge, confirm that water level is below the-top
of screen. Otherwise, the well must be Eurged.
~ell Di~mete/" /~uJtiplier" Well Diameter MultiPlier
to.,4 (Gals.) X ~ -- &l.~ Gala. 2" 0.t6 6" 1.47
[ 1 C~e yolu~e Spe~fied Volumes CMeulated Volume y' 037 Omer mdi~~ * 0.163
dond. T~bi~
T~xe Temp (°F) I pH (mS or ~) ~s) GMs. Removed Obse~afions
Balier low.ed ~ ' below
~DTW to ubtain sample
Did well dewater? Yes ~ Gallons actually evacuated: ~. g
S~pling Date: I. ~a. o H .. Smpl~g T~e: -ti q ~ Depth to Water: ~ a. ~
S~ple I.D.: ~ _ ~ Laboratm~: ~ Columbia Other
EB I.D. (if applicable): ~ T~,. Duplicate I.D. (if applicable):
~alyzed for: TPH-G B~X MTBE TPH-D Oxygenates (5) Oilier:
mgl ,
D.O. (ifreq'd): Pre-p~ge: 'Li Post-p~ge: ma/L
O.R.P. (ifreq'd): Pre-p~ge: mV Post-purge: mV
Blaine Tech Services~ Inc. 1680 Rogers Ave., San Jose~ CA 95~'i2 (800)545-7558
WELL MONITORING DATA ~,.cIEET
BTS #: o ,a o,, 'a - s ~4. 2.. Site: q .~ ,4 -~, ~-'+o
Well I.D.'
Total Well Depth (TD): ~ q. ~ ~.
Depth to Free Product:
Referenced to: ~ Grade
Date: , _ ,-~ ~ ~ oo .q
Well Diameter: 2 3 ¢I> 6 8
Depth to Water (DTW): ,_ o, s ,~
i Thiclmess of Free Product (feet):
D.O. Meter (if req'd):
YSI HACH
DTW with 80% Recharge [(Height of Water Columnx 0.20) + DTW]:
Purge Method: Bailer Waterra Sampling Method: Bailer
. Disposable Bailer Peristalt/c ~ Disposable Bailer
Positive Air Displacement Extract/on Pump Extraction Port
Electric Submersible ~.Other Oe~,-~,~ DedicatedTuhing
· Other:
Screened Interval: tO' - s o · IfweI1 is listed as a no-purge, confirm that water level is below the..tbp
of screen. Otherwise, the well must be purged.
Well Blame[er' '"~'ultiplier Well Diameter Multiplier
1" 0.04 4" 0.65
-- (Gals.) X ~ = - Gals. z'. 0.16 6'
I Case Volume Specified Volumes Calculated Volume z" o.37 Other rad[u~' · o.~63
Cond. Turbidity
Time Temp (°F) pH (mS or ffe~ (NTUs) Gals. Removed Observations
Bailer low,w~d "~ ' b~low
IDT$¥ to obtain ~ample
Did well dewater? Yes ~ Gallons actually evacuated: ~
Sampling Date: ~. c~. o q Sampling Thne: Io-~o Depth to Water:
Sample I.D.: ~,,,. ~. ~ Laboratory: .~e Columbia Other
Analyzed for: ~ ~-. Mrna TV~-D ~enat~($). ~ ;,, S'o~.,~
EB I.D. (if applicable): ~.,. Duplicate I.D. (if applicable):
Analyzed for: TPH-G BTEX IvlTBE TPH-D Oxygenates (5) Other:
D.O. (ifreq'd): Pre-purge: ms/t. Post-purge: rog/L
O.R.P. (if req'd): Pre-purge: mVI Post-purge: reV'
Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (800) 545-7558
SH:EL= WELL MONITORING DATA ~rlEET
,BTS #: o,~ o, ,~-.~4-
Sampler:
IDate: ,- ,-s-
Well I.D.: m,,s - ~. Well Diameter: 2 3 · 6
Total Well Depth (TD): u ~t. 5', Depth to Water (DTW): 'z o. ~ q
Depth to Free Product: Thiclmess of Free Product (feet):
Referenced to: ~ a~de D.O. Meter (ff req'd): YS~
DTW with 80% Recharge [(Height of Water Colurrm x 0.20) + DTW-]: > ~,. :~ ~
Purge Method: Bailer Waterra Sampling Meflmd: Bailer
Disposable Bailer Peristaltic ~Disposable Bailer
Positive Air Displacement Extraction Pump Extraction Port
~-Etectric Submersible Other Dedicated Tubing
Other:
Screened Interval: to'- $o ' If well is listed as a no-purge, con_firm that water level is below the.t'op
of screen. Otherwise, the well must be purged.
we .Diamete~ l~'uldplier Well Diameter Multlnlier
~" 0.04 4- 0.~
.!. Case Volume Specified Volumes Calculated Volume Y' 0.37 Olher radias~ * 0.163
Cond. Turbidity
Time Temp (°F) pH (mS o~ (NTUs) Gals. Removed Observations
Bailer lowered "~ ' below
DTW to obtain sample
Did well dewater? Yes d~ Gallons actually evacuated:
Sampling Date: I' ~'~- o q Sampling Time: ~'z ~ o Depth to Water:
Sample I.D.: ~. a- Laboratory: ~e Columbia Other
Analyzed for: ~~ ~rm~ 'rP}? $,,, r~.~...
EB I.D. (if applicable): @ ,~ Duplicate I.D. (if applicable):
Analyzed for: TPH-G BTEX MTBE TPH-D Oxygenates (5) Other:
D.O. (ifreq'd): Pre-purge: m~/~ Post-purge:
O.R.P. (ifreq'd): Pre-purge: Il:tV Post-purge: mx/.
Blaine Tech Services, inc. 1680 Rogers Ave., San Jose, CA 95112 (800) 545-7558
I
r ...... MONITORING' ~
SFI~L~ WELL DAT ,,d:EET
Sampler: .,c,_,,,~ /4 -- ~. .,.,,-,, Date: ~_ ,.~. ~oo,~
8
Well I.D.
Total Well Depth (TD): ,j ~. ~..-+
Depth to Free Product:
Referenced to: ~ Grade
Well Diameter: 2 3 t'~ 6
Depth to Water (DTW): -/~>.-~-+
Thickness of Free Product (feet):
D.a. Meter (if req'd):
YSI HACH
i.DTW with 80% Recharge [(Height of Water Column x 0.20) + DTW]:
Purge Method: Bailer Waterra Sampling Method: Bailer
Disposable Bailer Peristaltic ~Disposable Bailer
Positive Air Displacement Extraction Pump Extract/on Port
Electric Submersible ~Other ta~-~-{~ Dedicated Tubing
Other:
Screened Interval: ~o' -' ~o~ If well is listed as a no-Purge, confirm fl~at water level is below the..t'op
of screen. Otherwise, the well must be purged.
I ~w. eil Diamem~ Multiplier Well Diam'et~r Multiplier
' I" 0.04 4" 0.65
~ (Gals.) X. "-- = ~ Gals. 2" 0.16 6" 1.47
1 Case Volume Specified Volumes Calculated Volume 3" 0.37 Other radius~ * 0.163
Cond- Turbidity
Time Temp (°F) pH (mS or~l:l~ (NTUs) Gals. Removed Observations
Bailer lowered '~- ' below
DTW to obtain sample'
Did well dewater? Yes ~ Gallons actually evacuated: ~
Sampling. Date: t- ~'l..: o,~ Samplh~g Time: tav~- Depth to Water:
Smnple I.D.: ~,,.~- :3 Laboratory: ~ Columbia Other
ga~alyzed for: ('?Y~ 6~ MT~. TPn-D ~~: g~,
BB I.D. (if applicable): @ T~= Duplicate I.D. (if applicable):
Analyzed for: TPI-t-G BTEX MTBE TPH-D Oxygenates(5) Other:
D.a. (ifreq'd): Pre-purge: m/L Post-purge: m~/L
O.R.P. (ifreq'd): Pre-pt'ge: mV Post-purge: mV
Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95~12 (800) 545-7558
I
BTS #: o ,q o ~, -~ -
SHEL~ 'WELL MONITORING DATA ,.,I-IEET
Sampler:
Date: ,_,~. ~oo~
Well I.D.: t,-,,.~.- '~ Well Diameter: 2 3 icj> 6 8
Total Well Depth (TD): 't q .3 } Depth to Water (DTW): -, o. -~-~
De~to Free Product: Thickness of Free Product (feet):
~Refere~ce-'~o."-~ qa~:. etude D.O. Meter (ifreq'd): ys~ ~L~C~
!IDTW with 80% Recharge [~-Ieight of Water Column x 0.20) + DTW]: a ~,. ,~
Purge Method: Bailer Waterra Sampling Method: Bailer
Disposable Bailer Peristaltic ~Disposable Bailer
Positive Air Displacement Extraction Pump Extraction Port
~Electric Submersible Other Dedicated Tubing
Othen
Screened Interval: to ' - ~o' IfweI1 is Iisted as a no-purge, confirm that water level is below the...t'op
of screen. Otherwise, tl~e well must be purged.
(Well Diaraeter Mu [ip ie'r Well Diameter . Multiplier
1" 0.04 4"
tP.9 (Gals.)X ~ = ~ ~. ,.~ Gals. 2" 036 ¢' 1.47
I Cas.~ Volum..e . Specified Volumes Calculated Volume _v, 037 Other radlus~ * 0.1~3
Cond.' Turbidity
Time Temp (°F) pH (mS or~"~) (NTUs) Gals. Removed Observations
Bailer lowered ~[ ' below
DTW tn nhtuln rumple
Did well dewater? Yes ~l~ GaIlons actually evacuated:
SamptingDate: ~.~-~.oq SmnplingTime: ~.~:,- Depth to Water:
Sample I.D.: t~,,-, - '~ Laboratory: ~ce Columbia Other
EB I.D. (ifapplicabIe): @ T~..~ Duplicate I.D. (ifapplicable):
Analyzed for: TPH-G BTEX MTBE TPH-D Oxygenates(5) Other:
D.O. (if req'd): Pre-purge: m§/L Post_purge: m§/L
O.R.P. (ifreq'd): Pre-purge: rnV Post-purge: mV
'I
Blaine Tech Services, inc. 1680 Rogers Ave., San Jose, CA 951ff2 (800) 545-7558
WELL MONITORING DATA orIEET
BTS#: o~o,,-~- s~4- ~_ Site: ~.~, -}l -~-~.o
S~pler: S~,, ~ ~ ~ Date: ,_ ,~_ ~
Well I.D.' ~. w Well Dimeter: 2 3 ~ 6 8
Total Well Dep~ (TD): u~. ~ Dep~ to Water ~TW): i ¢.~ ~
Depfl~ to Free Product: ~iclmess of Free Product (feet):
Referenced to: ~ ~d~ D.O. Meter (ifreq'd): YsI ~CH
DTW with 80% Recharge [(Height of Water Column x 0.20) + DTW]:
Purge Method: Bailer Waterra Sampling Method: Bailer
Disposable Bailer Peristaltic ~-Disposable Bailer~gl~
Positive Air Displacement Extraction Pump Extraction Port
Electric Submersible ,~ Other ~--.~ Dedicated Tubing
Other:
Screened Interval: to' o ~ o ' If well is listed as a no-purge, confirm that water level is below the..t'op
of screen. Otherwise, the welI must be purged.
W~'ti'Diamete~ M'ultiplier Well Diameter Multipiler
~ I" 0.04 4" 0.§5
~ (Gals.) X = -- Gals. 2" 0.16 6" 1.47
1 Case Volume Specified Volumes Calculated Volume 3" 0.37 Other radius2 * 0.163
Cond. Turbidity
Time Temp (°F) pH (mS or ~ ('NTUs) Gals. Removed Observations
Bailerlowered '~ 'belm¥
'DTW to 0btaia sample
Did well dewater? Yes ~ Gallons actually evacuated:
Star, piing Date: ~.~$.0,4 SamptingT/me: tt ~S" Depfl~to Water:
Smnple I.D.: ,..~,..., Laboratory: C¢~ii~ Columbia Other
EB I.D. (if applicable): @ ,~ Duplicate I.D. (if applicable):
gmalyzed for: TPH-G BTEX MTBE 'TPH-D Oxygenates (5) Other:
D.O. (if req'd): Pre-purge: mg/L Post-purge:
O.R.P. (/freq'd): Pre-purge: mV Post-purge: mM
Blaine Tech Services~ Inc. 1680 Rogers Ave. San Jose, CA 951~2 (800) 545-7558
SIiE~',,~ W~ELL MONITORING DATA
Date:
Well I.D.' ,,,,,,.,. r Well Dimneter: 2 3 ~D 6
Total Well Depth (TD): ~'l-~t~ Depth to Water (DTW): f G. '~ o
Depth to Free Product: i Thiclcrtess of Free Product(feet):
Referenced to: ~ Grade D.O. Meter (if req'd): YS~
DTW with 80% Recharge [(Height of Water Column x 0.20) + DTW]:
Purge Method: Bailer Waterra Sampling Method: Bailer
Disposable Bailer Peristalt/c ~:Disposable Bailer
Positive Air Displacement Extraction Pump Extraction Port
Electric Submersible ~ Other t.~r~l~ ~ Dedicated Tubing
Other:
Screened Interval: t o' - ~ ~' If well is listed as a no-purge, confirm that water level is below the..t'op
of screen. Otherwise, the well must be purged.
Well Diamete~ l~a, llipl!er Well Diameter,, Multiplier
1" 0.04 4" 0.65
~. Case Volume Specified Volumes Calculated Volume y' 0.ay O~er ~di~~ * 0.1 ~3
Cond. T~bi~W
T~e Temp (°F) pH (mS or ~ ~s) Gals. Removed Obse~afions
Bgller lowered ~ ~ below
DT~ to o~taln snmple
Did wol] dewater? Yes ~ Gallo~s ac~a~y evacuated: ~
Sampl~g Date: ~.~3. os Smnp~g T~e: f~o Dep~ to Water: fG. ~o
S~ple I.D.: ~. ~ Laborato~: ~e Colmbia
'EB I.D. (if applicable): '~ ~ Duplicate I.D. (if applicable) :
'~lalyzedfo?: TPH-G BTEX MTBE TPH-D Oxygenates(5) Oilier:
D.O. (if req'd): Pre-purge: ~/~' Post.pmge: ~/~
O.R.P. (if req'd): Pre-pmge: mV ?ost-pmge: mV
I
Blaine Tech Services, inc. 1680 Rogers Ave., San Jose, CA 95112 (800) 545-7558
FIELD PROCEDURES
I BLAINE
TECH SERVICES,.~
1680 ROGERS AVENUE
SAN JOSE, CA 95112.-1105
(408) 573-7771 FAX
(408) 573-0555 PHONE
CONTRACTOR'S LICENSE #746684
www. blainetech.com
January 29, 2003
Tony Palagyi
Shell Oil Products US
P.O. Box 7869
Burbank, CA 91510-7869
Fkst Quarter 2004 Groundwater Monitoring at
Shell-branded Service Station
2401 Oak Street
Bakersfield, CA
Monitoring performed on January 13, 2004
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Groundwater Monitoring Report 040113-SH-2
This report covers the routine monitoring of grotmdwater wells at this Shell-branded facility. In
accordance with standard procedures that conform to Regional Water Quality Control Board
requirements, routine field data collection includes depth to water, total well depth, thickness of
any separate immiscible layer, water column volume, calculated purge volume (if applicable),
elapsed evacuation time (if applicable), total volume of water removed (if applicable), and
standard water parameter instrument readings. Sample material is collected, contained, stored,
and transported to the laboratoryin conformance with EPA standards. Purgewater (if applicable)
is, likewise, collected and transported to D.K. Environmental.
Basic field' infonnation is presented alongside analytical values excerpted from the laboratory
report in the cumulative table of WELL CONCENTRATIONS. The fidl analytical report for
the most recent samples and the field data sheets are attached to tiffs report.
At a minimum, Blaine Tech Services, Inc. field personnel are certified on completion of a forty-
hour Hazardous Materials and Emergency Response trai~xing course per 29 CFR 1910.120. Field
personnel are also enrolled in annual eight-horn' refresher courses.
Blaine Tech Services, Inc. conducts sampling and docmuentation assi~m~ents of this type as an'
h~dependent tl~ird party. Our activities at this site consisted of objective data and sample
collection only. No interpretation of analytical results, defining of hydrological conditions or
formulation ofrecormuendations was performed
Please call if you have any questions.
Yours truly,
Francis Thie
Vice President
FT/ks
attachments:
Cumulative Table of WELL CONCENTRATIONS
Certified Analytical Report
Field Data Sheets
CC:
Kathryn Ewing
Delta Environmental Consultmats, Inc.
911 S. Primrose Ave., Suite K
Monrovia, CA 91016
BLAINE TECH SERVICES, INC.
METHODS AND PROCEBURES
FOR THE ROUTINE MONITORING OP
· GROUNDWATER WELLS AT SHELL SITES
Blaine TeCh Services, Inc. performs environmental sampling and documentation as'an
independent third party. We specialize in groundwater monitoring assignment, s and intentionally
limit the scope of our services to those Centered on the generation of objective information..
To avoid conflicts of interest, Blaine Tech Services, Inc. personnel do not evaluate or interpret
the information we collect. As a state licensed contractor (C-57 well drilling -water- 746684 )
performing strictly technical services, we do nOt make any professional recommendations and
perform no consulting of any kind.
'SAMPLING PROCEDURES OVERVIEW
SAFETY'
All groUndwater monitoring assignments performed for Shell comply with Shell's safety
guidelir!es,.29 CFR 1910.120 and SB-198 Injury arid Illness PreventiOn I~rogram (IIPP). All
Field Technicians receive, the full 40-hour 29CFR 1910.120 OSHA SARA 'HAZWOPER course,
medical clearance and on-the-job training prior to commencing any work on any Shell site.
INSPECTION AND GAUGING
Wells are inspected prior to evacuation and sampling. The condition of the wellhead is checked
and noted according to a wellhead i ..nspection checklist.
Standard !measurements include the depth to water (DTW) and the total well depth (TD)
obtained with industry standard electronic water level indicators that are graduated in
inbrements of.hundredths of a foot.
The water in each well is inspected for the presence of immiscibleS. When free product is
suspected,' its presence is confirmed rising an eleCtronic interface probe (e.g. MMC). No
samples are collected from a Well containing over two-hundredths'of a foot (0.02')of product.
EVACUATI ON
Depth to water measurements are collecte~l by our personnel prior to purging and minimum
purge volumes are calculated anew for each well based on the height of the water column and
the diameter of the well. Expected purge volumes are never less than three case :volumes and
are set at no less than four case volumes in some jurisdictions.
Blaine Tech Services, Inc. Standard Methods & Procedures Shell Oil Products'US Page 1
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Well purging, devices are selected on the basis of the well diameter.and the total volume to be
evacuated. 'In most cases the well will be purged using an electric submersible pump (i.e.
· Grundfos) suspended near (but not touching) the bottom of the well.
RARAM ETER STAB I LIZATION
Well purging completion standards include minimum purge volumes, but additionally require
stabilization of specific groundwater parameters prior to sample collection. TypiCal groundWater
parameters used to measure stability are electrical conductivity, pH, and temperature.
Instrument readings are obtained at regular intervals during the evacuation process (no less
thar) once per case volume).
Stabilization standards for routine' quarterly monitoring of fuel sites include the following:
Temperature is considered to have stabilized when successive readings do not fluctuate more
than +/- 1 degree Celsius. Electrical conduotivitY is considered stable when suc(~essive
readings are within 10%. pH is considered to be stable when successive readings remain
Constant or vary no more than 0.2 of a pH unit.
DEWATERED WELLS
Normal evacuation removes no less than three Case volumes of water from the well. However,
less water may be remOVed.in cases where the well dewaters and does not immediately
rech'arge.
MEASURING RECHARGE
Upon completion of well purging, a depth to water measurement is collected and notated to
ensure that the well has recharged to within 80% of its static, pre-purge level Prior to sampling.
Wells that dO not immediately show 80% recharge or dewatered wells will be alloWed
minimum of 2 hours to recharge prior to sampling. The water level at time of sampling will be
nOted.
PURGEWATER CONTAINMENT
All non-hazardous purgewater evacuated from each groundwater monitoring well is'captured
and contained in on-board Storage tanks on the Sampling Vehicle and/or special water hauling
trailers. Effluent from the decontamination of reusable apparatus (sounders, electric pUmps and
hoses etc.), cOnsiSting of groundwater combined with deionized water and non-phosphate soap,
is also captured and pumped into effluent tanks.
Non-hazardous purgewater is transported under standard Bill of Lading documentation to a
Blaine Tech Services, Inc. facility before being transported to a Shell approved disposal facility.
Blaine Tech Services, Inc. Standard Methods & Procedures Shell Oil Products US Page 2
SAMPLE COLLECTION DEVICES
All samples are collected using a stainless steel, Teflon or disposable bailers.
SAMPLE CONTAINERs
Sample material' is decanted directly from the sampling bailer into sample containers provided
by the laboratory that will analyze the samples. The transfer of sample material from the bailer
to the Sample container Conforms to specifications contained in the USEPA T.E.G.D. The type
of sample container, material of construction, method of closure and filling requirements are
specific to the intended analysis. Chemicals needed to preserve the samPle material are
commonly placed inside the sample containers by the laboratory or glassware vendor prior to
deliVery of the bottle to our personnel. The laboratory sets the number of re'plicate containers.
TRIP BLANKS
Trip Blanks', if requested, are taken to the site and kept inside the sample cooler for the duration
of the event. They are turned over to the laboratory for analysis with the samples from that site.
DUPLICATES
Duplicates, if reqUested, may be collected at a site. The Field Technician uses their discretion
in chooSing the well at which the Duplicate is collected, typically one suspected of containing
measurable contaminants.' The Duplicate sample is labeled "DUP" and the time of collection is
omitted from the COC, thus rendering the sample blind.
SAMPLE STORAGE'
All sample containers are promptly placed in food grade ice chests for storage in the. field and
transport (direct or via our facility)'to, the designated analytical laboratory. TheSe ice chests
contain'quantities of restaurant grade ice as a refrigerant material. The samples are maintained
in either an ice .chest or a refrigerator until relinquished into the custody of the laboratory Or
laboratory courier. ,
DOCUMENTATION CONVENTIONS
A label must be affixed to all sample containers. In most cases these labels are generated by
our office personnel and are partially preprinted. Labels can also be hand written by. our field
personnel. The site is identified wi[h the store number and site address, as is the particular
groUndwater well from which the sample is drawn (e.g. MW-l, MW-2, S-1 etc.). The time and
date of sample collection along with the initials of the person who collects the sample are
handwritten onto the label.
Chain of Custody records are created using client specific preprinted forms following USEPA
specifications.
Blaine Tectt Services, Inc. Standard Methods & Procedures Shell Oil Products US Page 3
Bill of Lading records are contemporaneous records created in the field at the site whe~-e the
non-hazardous purgewater is ganerated. Field Technicians use preprinted Bill of Lading.forms.
DECONTAMINATION
All equipment is brought to the site in clean and serviceable condition and is cleaned after use
in each well and before subsequent use in any other well. Equipment is decontaminated before
leaving the site.
The primary decontamination device is a commercial steam cleaner. The steam cleaner is de-
tuned to function as a hot pressure washer that is then Operated with high quality deionized
water that is produced at our facility and stored onboard our sampling vehicle. Cleaning is
facilitated by the use of proprietary fixtures and devices included inthe patented workstation
(U.S. Patent 5,535,775) that is ncorporated in each sampling vehicle. The steam cleaner is
used to decon reels, pumps and bailers.
Any Sensitive equipment or pads (i.e. Dissolved Oxygen sensor membrane,, water level
· indicator etc.) that cannot be washed using the high pressure water, will be sprayed with a non-
phosphate soap and deionized water solution and rinsed with deionized water..
DISSOLVED oXYGEN READINGS
Dissolved Oxygen readings are taken pre- and/or post-purge using YSI meters (e.g. YSi Model
54, 58 or 95) or HACH field test kits.
The YSI meters are equipped with a stirring device that enables them to collect accurate in-situ
readings. The probe/stirring devices are modified to allow downho!e measUrements to be taken
from Wells with diameters as Smail as two inches. The probe and reel is decontaminated
between wells as described above. The meter is calibrated between wells as per the
instructions in the operating manual. The probe and stirrer is lowered into the water Column.
· The reading is. allowed t° stabilize prior to collection'.
OXYIDATON REDUCTION POTENTIAL READINGS
All readings are obtained with either Corning Or Myron-L meters (e.g. Corning ORP-65 or a
MyromL Ultrameter GP)..The meter is cleaned between wells as described above. The meter
is calibrated at the start of each day'according to the instruction manual.
FERROUS-IRON MEASUREMENTS
All field measurements are collected at time of sampling With a HACH test kit.
Blaine Tech Services, Inc. Standard Methods & Procedures Shell Oil Products US Page 4
DISPOSAL DOCUMENT
NON-HAZARDOUS WASTE DATA FORM
GI~NI:;RA-r~N G ~I'E'-
WIC~ z.,.{ol
SHELL OIL PRODUC'I-~ US s'~,-¢¢,~(~, cPr
NAME
P.O. BOX 71969
ADDRESS
BURBANKr CA 91510-786c~
PHONE NO: ( )
CONTAINERS: ~o. , VOLUME ~ ~'o ?~-t' , WaeHm
TANK DUMP
TYPE:- Tt~UCK []mUQK [] O,UUS
NON-HAZARDOUS GROUNDWATER
WAbblE DESCRIPTION,
co~apot, m,'~'rs o]= WASTS PPM 99-~O%:!.O
WATER
1
TPH
[] CARTONS [] OTHEP,
PURGED GRouFJ DWATER
ZNCI'DENT# q
BE'SI
4. 7-10'
PROPERTIES: oH__ []
HANDLING INSTRUCTIONS:
XX ~'
SOLID [] UOUIO [] SLUpOE [] SLURRY [] OTHER
24-HOUR EMERGENCY PHONE (1~00) 424-9300
JTH~ GENERATOR CERTIFIES'THAT THE J
WASTE .AS DESCRIBED IS 100~
· NON-HAZARDOUS.
NAME,
ADDRF--.~S.
BREA, CAITFORNZA 92821
OITY, ~TA'TE. ZIP..,
(714) 990~eB55
PHONE NO,. ,
TYPED OR PRI~ ~LL NAME & SIGNA~RE DA~
EPA~' '" '"" .....
~O ~D SONS TRUC~NG, INC. ~.~,
NO.
I
1281 BR~ ~YON'ROAD I FIRST~~E
!1 --a[ml~ ~ , _, ~ ..... _ ;~' u ~ER~'~E.ORDER NO. -
I 20 0
(310) 782-2~5
TRUOK, UNIT I.D, NO. TYPED OR PRINTED FULL NAME & SII~NATURE
NAM~
DATE
D~fK Er~/IRON I~ F__~TAL ~.a,
3630 E, 26TM STREET
ADDRESS
LOS ANGELEs, CA 510023
CITY, ~'trATE, ZIP
(3231 2~-5o56
PHONE NO
.DIGPO~AL.b-rHOD
[] LANDFILL [] OTHER
m
TYPED OR PRINTED FULL NAME & SIGNATURE
GEN OLD/NEW L A TONS
Te~S S B
RTI~D HV-~F
Cm NONE
DISCREFANCY
DATE
APPENDIX D
LABORATORY REPORT AND
CHAIN-OF-CUSTODY DOCUMENTS
Client Reference:
~=a_. l__science
January 20, 2004
Nick Sudano
Blaine lech Services,
20360 Gramercy Place
Torrance, CA @0501-1511
Subject: Cal$cienceWork Order No.:
Client Referenc~
Dear Client:
Enclosed is an analytical re
included in this report were
the attached chain-of-custo,
Unless otherwise noted, all
guidelines established in
ou
operating procedures, and
subcontracted analysis is pr
package. The results in this
reproduction thereof must b
If you have any questions rE
the undersigned.
Cal.~,en cez/~ir.on mental
(.~r~m'°~s' ,nc'
04-01-0549
2401 Oak Street, Bakersfield, CA
Project Manager
Quality Assurance Manager
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
Enclosed is an analytical report for the above-referenced project. The samples
included in this report were received 1/13/2004 and analyzed in accordance with
the attached chain-of-custody,
Unless otherwise noted, all analytical testing was accomplished in accordance with the
guidelines established in our Quality Assurance Program Manual, applicable standard
operating procedures, and other related documentation. The original report of any
subcontracted analysis is provided herein, and follows the standard Calscience data
package. The results in this analytical repeal are limited to the samples tested and any
reproduction thereof must be h~ade in its entirety.
If you have any questions regarding this report, please do not hesitate to contact
alscience
_nvironmental
--ab°ratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project: 2401 Oak Street, Bakersfield, CA
Analytical Report
Date Received: 01/13/04
Work Order No: 04-01-0549
Preparation: N/A
Method: EPA 120.1
Page I of 1
Lab Sample Date Date Date
Client Sample Number Number Collected Matdx Prepared Analyzed QC Batch ID
Parameter Result RI. D._EF Qual Units
Specific Conductance 490 1.0 1 umhos/crn
Para meter Result RI. D._~F Qual U nits
Specific Conductance 440 1.0 1 umhos/cm
I
Parameter Result RI. DF: Qual Units
Specific Conductance 350 1.0 1 umhos/cm
Parameter, Result RI_ D__[F Qual Units
Specific Conductance 490 1.0 1 umhos/cm
I
Parameter Result RI_ D._.~F Qual Units
Specific Conductance 470 1.0 1 umhoslcm
orhng Limit , DF - Dilution Factor , Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427
· TEL: (714) 895-5494
· FAX: (714) 894-7501
I
--~-~- Analytical Report
n_ vironmentai
I L-ab°rat°ries'lnc'
Blaine Tech Services, Inc Date Received: 01/13/64
i 20360 Gramercy Place Work Order No: 04-01-0549
Torrance, CA 90501-1511 Preparation: N/A
Method: EPA 130.2
I Project: 2401 Oak Street, Bakersfield, CA Page 1 of 1
Lab Sample Date Date Date
I Client Sample Number Number Collected Matrix Prepared Analyzed QC Batch ID
Parameter Result RI_
I Hardness, Total 140 2
Parameter Result RL
I Hardness, Total 120 2
Parameter Result RL
Hardness, Total 98 2
Parameter Result RL
I Hardness, Total 140 2
I Parameter Result RL
Hardness, Total 140 2
I Parameter Result RL
Hardness, Total ND 2.0
I
!
7440 lincoln Way, Garden Grove, GA g2841-1427 · ltl[_: (7~4) 895-5494 · FAX: (714) 8~4-7501
1
DF Qual Units
1 mg/L
D.~F Oual Unils
I mg/L
D.__~F Qual Units
1 mg/L
D_.~F Oual Units
1 mg/L
DF Qual Units
I mg/L
D__[F qual Units
1 mg/L
~-a!science
~_nvironmental
iL_ aboratories, inc.'
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received: 01/13/04
Work Order No: 04-01-0549
Preparation: N/A
Method: EPA 150.1
Project: 2401 Oak Street, Bakersfield, CA Page I of 1
Lab Sample Date Date Date
Client Sample Number Number Collected Matrix Prepared Analyzed QC Batch ID
Parameter Result RI_ D._.~F Qual Units
pH 6.54 0.01 1 pH units
Parameter Result RI.. D._~F Qual Units
pH 6.72 0.01 1 pH units
Parameter Result RL DF= 9u~l Units.
pH 6.62 0.01 I pH units
Parameter Result RI- DF Qual Units
pH 6.55 0.01 I pH units
Parameter Result RL D_..EF Qual Units
pH 6.51 0.01 1 pH units
Pt. - Reporting Limit , DF - Dilution Factor , QLm! - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427
· TEL: (714) 895-5494 · FAX: (714) 894-7501
aiscience
- vironmental
--aboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
bate Received: 01/13/04
Work Order No: 04-01-0549
Preparation: N/A
Method: EPA 160.1
Project: 2401 Oak Street, Bakersfield, CA Page 1 of 1
Lab Sample Date Date Date
Clienl Sample Number Number Collected Matrix Prepared Analyzed QC Batch ID
Parameter Result R~L D....[F Oual Units
Solids, Total Dissolved 300 1.0 1 mg/L
Parameter Result RI. D._[F Qual Units
Solids, Total Dissolved 260 1.0 I mg/L
Parameter R~,?,ult RL D,_.~F Qual Units
Solids, Total Dissolved 210 1.0 I mg/L
I
Parameter Result RI.. DF: Qua! Unils
Solids, Total Dissolved 2go 1.0 1 mg/L
Parameter Result RI_ D._[F Qual Units
Solids, Total Dissolved 280 1.0 1 mg/L
J ~ RL - Reporting Limit , DF - Dilution Factor ' , Oual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427
TEL: (714) 895-5494 · FAX: (714) 894-7501
.._a!.science
j _nvironmental
aboratories, inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received: 01/13/04
Work Order No: 04-01-0549
Preparation: N/A
Method: EPA 300.0
Project: 2401 Oak Street, Bakersfield, CA Page 1 of 1
Lab Sample Date Date Date
Client Sample Number Number Collected Matrix Prepared 'Analyzed QC Batch ID
Ii;";:'"' ~/':":::: L!: ~.~i .i:::':".'L:,:.'~:"L..:':.: . -: .... ', ': . !....'.:,-i. :-.::.,::~; : ' ..... .-.' ' .... ' :". · ]:~ L.. '.'.. .: ' · ' '. .... · ': ... · ~'
:MWt!~',(.!~!,P.-~g~)i' :i ::;: .... ::'.: .... ' .: '.: . '~:' :. ~ {: .;:; ?.'~!~054S-1~. ~ · :01..~13104..;'.;:..'~kOaS~ '::i '.'.: i.N,'A': .: ". :. 0~/t3104'~:'.'., '0a~1.~13L01
Parameter Result RL D_..~F Qual Units Parameter Result RI_ DF: Qua._._Jl Units
Chlodde 71 10 10 D mg/L Sulfate 31 10 10 D mg/L
Nitrate (as N) 1.0 0.1 1 mg/L
Parameter Result RI_ DF: Qual Unit,~ .parameter Result RL D~F Oua..__.JI Units
Chloride 67 10 10 D mg/L Sulfate 24 10 10 D mg/L
Nitrate (as N) 0.54 0.10 1 mg/L
[
~ : ~. !~ : , ~ :, , .::; :-::: ,' :~ :..:.';-:...; ~i~:..'~;.:u:.-? ~;::~i.'!~; [i!i~:'='~ ~' ::~:;;:i;:;!'.~i.:..~!/';'!~:': .i: !/'..i!~:.~:: '.: ~,' ?.; :~ .;:~'1..:'." :' : ~ :' .~ "~ .:. :!': :- :i .:"...-:'.rm:i ,: :: -:':'." '.. · -:,. =.. ?'..; '.. '.: ·
Parameter Result RI- DF Qual Units Parameter Result RI- DF Qual Units
Chloride 48 10 10 D mg/L Sulfate 16 10 10 D mg/L
Nitrate (as N) 0.65 0.10 I mg/L
I
Parameter ,Result RI. DF: Oual Units Parameter Result RI_ D_~F (~ual Units
Chloride 82 10 10 D mg/L Sulfate 36 10 10 D mg/L
Nitrate (as N) 1,1 0.1 I mg/L
I
Parameter Result RI_ D._.~F Qual Units Parameter Result RI_ D.._~F Qual Units
Chloride 72 10 10 D mg/L Sulfate 29 10 10 D mg/L
Nitrate (as N) 1.4 0.1 1 mg/L
Parameter Result RI_ DF Qual Units parameter Result R~L D._.~F Qual Units
Chloride ND 1.0 I mg/L Sulfate ND 1.0 1 mg/L
Nitrate (as N) ND 0.10 I mg/L
I
I J . RL- Repoding Limi! , DF- Dilution Factor , QuaJ- Qualifiers
.
7440 Lincoln Way, Garden Grove, CA 92841-1427
· TEL: (714) 895-5494 · FAX: (714) 894-7501
..alscience
-__nvironmental
aborat° ries, Inc.
B~aine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Rec~i'ved: 01/13/04
Work Order No: 04-01-0549
Preparation: N/A
Method: EPA 351.3
Project: 2401 Oak Street, Bakersfield, CA Page 1 of 1
Lab Sample Date Date Date
Client Sample Number Number Collected Matdx Prepared Analyzed QC Batch ID
Parameter Result R__L D._~F Qual Units
Total Kjeldah, I Nitrogen ND 0.50 1 mg/L
Parameter ~ RL D__F .Qua] Units.
Total Kjeidahl Nitrogen ND 0.50 1 mg/L
/
Parameter Result RI_ D._~F Qual Unlts
Total Kjeldahl Nitrogen 0.56 0.50 1 mg/L
I
I
Parameter Result RI. DF: Oual Units
Total Kjeldahl Nitrogen ND 0.50 1 mg/L
Parameter Result RI_ DF: Qua. I Un.Its
Totai Kjeldahl Nitrogen 0.63 0.50 I mg/L
Parameter Result RI_ DF Qual Units
Total Kjeldahl Nitrogen ND 0.50 I mg/L
orhng Limit , DF - Dilution Factor , Qual- Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841~1427
· TEL: (714) 895-5494
· FAX: (714) 894-7501
~-aiscience
~r.n_ vironmentai
~L ab°ratories, Inc.
Blaine Tech' SJ~/ices, I~IcIII
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
' ' Date Received: 01/13/04
Work Order No: 04-01-0549
Preparation: N/A
Method: SM 2320B
Project: 2401 Oak Street, Bakersfield, CA Page 1 of 1
Lab Sample Date Date Date
Client Sample Number Number Collected Matrix Prepared Analyzed QC Batch ID
.......... .:..~, .... .......,,.. ...... . .......... ., ~
Parameter Result RI. D__F QuaJ Units
Hydroxide (as CaCO3) ND 1,0 1 mgic
Parameter Result R__LL DF: Q,'..ual Units
Hydroxide (as CaCO3) ND 1.0 1 mg/L
~.,~g~,~.~i~ ............
Pa~meter Result R~ D~ Qua~ Units
Hyd~xide (as CaCO3) ND 1.0 I mg/L
I
Pa~meter Result R~ D~ Qual Uni~
Hyd~xide (as CaCO3) ND 1.0 1 mg/L
I
Parameter Result R~ D~ Qual Uni~
Hydroxide (as CaCO3) ND 1.0 1
ort~ng Limit , DF - Dilution Factor , Oual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427
· TEL: (714) 895-5494 · FAX: (714) 894-7501
~..~al_science
l~- nvironmental
~-- aboratories, inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received:
Work Order No:
· Preparation:
Method:
01/13~O4
04-01-0549
N/A
SM 2320B
Project: 2401 Oak Street, Bakersfield, CA Page 1 of 1
Lab Sample Date Date Date
Client Sample Number Number Collected Matrix Prepared Analyzed QC Batch ID
I':. ~i~:ii~;~.:~;!; :.iii:!~i ;'i' ili:i;;i':!i;;:;:; :,.'.:: .. ;;..: ... :i, :...!/::.i~:~,~,.~ ;. ;.: ~i~'- :- ~. ~;, '~'::.':;~'-:~:~...~,.... "~ ....... ~:. :~: "'.:~'~' ~ . ......... '~ '~' ": '1
Parameter ,.Result. RL D.._~F Oual Units
Carbonate (as CaCO3) ND 1.0 I mg/L
[.!:~,~c~i~!!-:,~;!',; ~;~i(;~ ~, ~! i·i:' ::!~;~.~·~i!:..i, :::: ;~::'..,, ':.'~i..-~:..!: ;..:i!~~ :-.:,'~'~'.";;' ~ i~ ~, !~i:;; ~ ;:~:, '~¢~,~::,-:: .e.~..,i '.' 'i
Parameter .Result RI. DF: Qual Units
Carbonate (as CaC03) ND 1,0 1 mg/L
~ ~ i~[ ~i ~ !i ii; !ii !i~;!i~ ,!'.;:ii:~!i!;:i:, ~ ,?.' ;..~ :;?:~i;ii:~!~ ii:.!~ ;~ :·'·~ ;~:~ i:,~:~ ~!!i!,~i!H~.~,; ~ ~:.:.,; ~a~: :.: ~ ~:
Parameter Result R_L_L D__E P~a! Un,its
Carbonate (as CaCO3) ND 1,0 1 mg/t.
Parameter ReSult RI. D._~F Qual Unil;s
Carbonate (as CaCO3) ND 1.0 1 mg/L
I
I
I
I
I
I
Parameter Re,~ult RI. D._EF Qual Units
Carbonate (as CaCO3) ND 1.0 1 mg/L
p·
od~ng Limit , DF - Dilution Factor , Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427
· TEL: (714) 895-5494 ° FAX: (714) 894~7501
alscience
.nvironmental
aboratories, Inc.
Analytical Report
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received: 01/13/04
Work Order No: 04-01-0549
Preparation: N/A
Method: SM 2320B
Project: 2401 Oak Street, Bakersfield, CA Page I of 1
Lab Sample -Date Date Date
Client Sample Number Number Collected Matrix Prepared Analyzed QC Batch ID
Parameter Result RI_ D._EF Quat Units
Bicarbonate (as CaCO3) 56 1.0 I mg/L
Parameter Result Ri_ DF Qual ,Units
Bicarbonate (as CaCO3) 46 1.0 1 mg/L
; ;:~:!;~;:i~i'~:i!H;i~i:!~i~{i~iii~[~!H:ii[[!~i~!:i~i~ !~!;~ ;i :'i, ":,i;'~.~i: i:'i!.::!;:'-i:.!;',!~:;~L.;:~'F~;,:.i:.~,:!:-.::..'~/:iL j~;L'..:'...:,"';. ~: i~t~: i ~; '.i:~ ...':~ ::,;.i.; ..... ~ ....... '.~' .-.. .. .... :.....~.
1
Parameter Result Ri_ D.._~F Qual Units
Bicarbonate (as CaCO3) 26 1.0 I mg/L
Parameter Result RI_ DF: Qual Uni!s
Bicarbonate (as CaCO3) 100 5.0 1 mg/L
Parameter Result Ri_ DF' Qual Units
Bicarbonate (as CaCO3) 60 1.0 1 mg/L
orting Limit , DF - Dilution Factor , Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427
· TEL: (714) 895-5494
· FAX: (714) 894-7501
~.alsclence
~E~vironmen~a!
· L_ aboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received: 01/13/04
Work Order No: 04-01-0549
Preparation: N/A
Method: SM 2320B
Project: 2401 Oak Street, Bakersfield, CA Page 1 of 1
Lab Sample Date Date Date
Client Sample Number Number Collected Matdx Prepared Anaty-z_ed QC Batch ID
ti ~i i~ "~.:. ;~.:~'.!! :'; ili:~i!?.~.!.i'~.:,!~i.:i "~.i: :::/:..';:~.;'~.::.~.~ ....?~,;~.!~. :?,~.: !.:.,~,~..,. ~.~:, ,i:~i,~,,~:~..,:~. :. ~,~
Parameter Result RI_ DF Qual Units
Alkalinity, Total (as CaCO3) 56 1.0 1 mg/L
Parameter Result RI_ DF' Qual Units
Alkalinity, Total (as CaCO3) 46 1.0 1 mg/L
Parameter Result RI_ DF' Qual Units
Alkalinity, Total (as CaCO3} 26 1.0 I mg/L
Parameter Result
AJkalinity, Total (as CaCO3) 100 5.0 1 mg/L
Parameter Result RI_ DF Qual ,Uni ,ts
Alkalinity, Total (as CaCO3) 60 1.0 1 mg/L
ep'
od~ng Limit , DF - Dilution Factor , Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427
· TEL: (714) 895-5494
m
· FAX: (714) 894-7501
..aiscience
F-_nvironmental
aboratOries, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 9050'l-15'1 '1
Analytical Report
Date Received:
Work Order No:
Preparation:
Method:
01/13/04
04-01-0549
EPA 3005A Flit.
EPA 601 OB
Project: 2401 Oak Street, Bakersfield, CA Page 1 of 2
Lab Sample Date Date Date
Client Sample Number Number Collected Matrix Prepared Analyzed QC Batch ID
Pa~meter Result R~ DF Qual Uni~
Lead ND 0.0100 I mg/L
parameter Result R~ D~ Qual Uni~
Lead ND 0,0100 1 mg~L
~ammeter Result R~ DF Qual Units
Lead ND 0.0100 1 mg/L
Parameter Result R~ DF Qual Units
Lead ND 0.0100 1 mg/L
Parameter Result R~ DF Qual Units
Lead ND 0,0100 1 mg/L
I
Parameter Result R~ D~ Qual Units
Lead ND 0.0100 1 . mg/L
Pa~meter Result R~ DF Qual Uni~
Lead ND 0.0100 1 m~L
Pa~meter Result R~ DF Qual Units
Lead ND 0.0100 1 mg/L
~ RL - Reporiing Limit , DF - Dilution Factor , Quad - Qualifiers
7440 Lincotn Way, Garden Grove, CA g2841-1427
· TEL: (714) 895-5494 · FAX: (714) 894-7501
mals_cience
. -_nvironmental
aboratories, Inc.
Blaine Tech Services, thc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received:
Work Order No:
Preparation:
Method:
01 / 13/04
04-01-0549
EPA 3010A Total
EPa 6010B
Project: 2401 Oak Street, Bakersfield, CA Page 2 of 2
Lab Sample Date Date Date
Client Sample Number Number Collected Matdx Prepared Analyzed QC Batch ID
Parameter Result RL DF Qual Units P,~rameter ~Result RI_ DF Qual Units
Manganese 0.0128 0.0050 1 mg/L Calcium 43.3 0.1 1 mg/L
Potassium 2.72 0.50 1 mg/L Iron 0.302 0.100 1 mg/L
Sodium 33.2 0.5 1 mg/L Magnesium 9.09 0.10' 1 mg/L
Parameter Result RI. D_.[F Q, ual ~ni~ Parameter .Result RI- DF Qual Units
Manganese ND 0.00500 1 mg/L Calciurn 32.3 0.1 1 mg/L
Potassium 3.00 0.50 I mg/L Iron ND 0,100 1 mg/L
Sodium 30.6 0.5 I mg/L Magnesium 9.82 0.10 1 mg/L
Parameter Result RI_ DF Qual Uni_._.~ P~rameter Result RL DF Qual Units
Manganese 0.0337 0.0050 1 mg/L Calcium 28.1 0.1 1 mg/L
Potassium 3.09 0.50 I mg/L Iron 0.876 0.100 1 mg/L
Sodium 27.2 0.5 1 mg/L Magnesium 7.32 0.10 1 mg/L
Parameter Result RI. DF' Qual Units Paramete~r Result RI_ D._EF Qual Units
Manganese 0.0114 0.0050 I mg/L Calcium 44.4 0.1 1 mg/L
Potassium 2.78 0.50 1 mg/L Iron 0.239 0.100 1 mg/L
Sodium 33.6 0.5 I mg/L Magnesium 9.36 0.10 1 mg/L
Parameter Result RI- DF Qual Units Parameter Result RI_ D._~F ~ual Units
Manganese 0.114 0.005 1 mg/L Calcium 37.9 0.1 I mg/L
Potassium 3.55 0.50 I mg/L iron 1.70 0,10 1 mg/L
Sodium 31.8 0.5 I mg/L Magnesium 11.5 0.1 I mg/L
Parameter Result RI_ DF Qual Units Parameter Result RI_ DF Qual Units
Lead ND 0.0100 1 mg/L Manganese ND 0.00500 1 mg/L
Calcium ND 0.100 1 mg/L Potassium ND 0.500 1 mg/L
Iron ND 0.100 1 mg/L Sodium ND 0.500 1 mg/L
Magnesium ND 0.100 1 mg/L
ortrng Umit , DF - Dilution Factor , Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427
· TEL: (7-14) 895-5494 · FAX: (714) 894-7501
. -a!science
/J -_nvironmentai
aboratories, inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received: 01/13/04
Work Order No: 04-01-0549
PreparatiOn: EPA 5030B
Method: DHS LUFT
Project: 2401 Oak Street, Bakersfield, CA Page I of 3
Lab Sample Date Date Date
Client Sample Number Number Collected Matrix Prepared Analyzed QC Batch ID
Parameter Result RL D.__.~F Oual Uqi.ts
TPH as Gasoline ND 50 I ug/L
Surroqates: REC {%) Contr01
Limits
1,4-Bromofluocobenzene 82 49-133
Parameter Result RI_ DF' Qual Units
TPH as Gasoline ND 50 1 ug/L
Surroqates: REC {%) Contra) Qual
Limits
1,4-Bromofluorobenzene 83 49-133
Parameter Resutt RL D~F Qual Units
TPH as Gasoline ND 50 1 ug/L
Surroaates: REC (%) Control Oual
Limlt~
1,4-Bromofluorobenzene 82 49-133
Parameter Result RL ' D__.EF Oual Uni .ts
TPH as Gasoline ND 50 1 ug/L
SurroRates: ~ Control
Limits
1,4-Bromofluorobenzene 80 49-133
Qual
iding Limit , DF - Dilution Factor , Oual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427
· TEL: (714) 895-5494 · FAX: (714) 894-7501
~=,-alscience
~.____nvironmental
~c_ aboratories, Inc.
Blaine To'ch Services, 'in(:: '
20360 Gramercy Place
Torrance, CA 90501~1511
Analytical Report
Date Received: 01/13/04
Work Order No: 04-01-0549
Preparation: EPA 5030B
Method: DHS LUFT
Project: 2401 Oak Street, Bakersfield, CA
Page 2 of 3
Lab Sample Date Date Date
Client Sample Number Number Collected Matrix Prepared Analyzed QC Batch ID
'',.'.. ........ i.' ..... o,,:,,.o,
Parameter Result Rt_ DF' Qual Units
TPH as Gasoline ND 50 I ug/L
Surrogates: REC (%) Control
.Limits
1,4-Bromofluorobenzene 83 49-133
qual
Parameter Result RI_
TPH as Gasoline ND 50
Surrogates REC (%) Control
Limits
1,4-Bromofluorobenzene 81 49-133
DF Qual Units
I ug/L
Qual
Parameter Result RI_
TPH as Gasoline ND 50
DF' Qual Units
1 ug/L
Surroqates: REC (%) C.q.ntrol.
Limits
1,4-Bromofluorobenzene 82 49-133
Qual
Parameter Result RI_
TPH as Gasoline ND 50
DF ~al Units
I uglL
Surrooates: REC, (%) CoO, trol
Limits
1,4-Bmmofluorobenzene 78 49,133
Q'ual
ortmg Limit , DF - Dilution Factor , Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427
° TEL: (714) 895-5494
FAX:' (714) 894-7501
-_a/s_cience
vironmental
aboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received: " 01/13/04~
Work Order No: 04-01-0549
Preparation: EPA 5030B
Method: DHS LUFT
Project: 2401 Oak Street, Bakersfield, CA Page 3 of 3
Lab Sample Date Date Date
Client Sample Number Number Collected Matrix Prepared Analyzed QC Batch ID
Parameter Result
TPH as Gasoline ND
Surrogates; REC (%)
1,4-Bromofluorobenzene 85
R.__~L D__EF Qual Uni!s
50 1 ug/L
Control
Limits
49-133
Qual
Pa~ ,meter Resplt RL
TPH as Gasoline ND 50
Surroqates: REC (%) Control
Limits
1,4.Bromofluombenzene 84 49-133
DF Qual Units
I ug/L
Qual
J ~ RL - Reporting Limit , DF. Dilution Factor , Oual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427
° TEL: (714) 895-5494
· FAX: (714) 894-7501
~-alscience
~Epvironmentai
~=~ aboratories, Inc.
Analytical Report
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order'No:
Preparation:
Method:
01/1~04
04-01-0549
EPA 5030B
EPA 8260B
Project: 2401 Oak Street, Bakersfield, CA
Lab Sample Date Date
Client Sample Number Number Collected Matrix Prepared
,'.::,!
Page I of 10
Date
Analyzed QC Batch ID
Parameter Result R._~L DF Qual Units Parameter Result R__.~L D.._EF
Acetone ND 10 1 ug/L l,l-Dichloropropene ND 1.0 1
Benzene ND 0.50 1 ug/L c-1,3-Dichloropropene ND 0.50 t
Bromobenzene ND 1.0 1 ug/L t-1,3-Dichloropropene ND 0.50 1
Bromochloromethane ND 1.0 1 ug/L Ethylbenzene ND 1.0 1
Bromodichloromethane ND 1.0 1 ug/L 2.Hexanone ND 10 1
Bromoform ND , 1.0 1 ug/L Isopropylbenzene ND 1.0 1
Bromomethane ND 10 I ug/L p-lsopropyltoluene ND 1.0 1
2-Butanone ND 10 I ug/L Methylene Chlodde ND 10 1
n-Butylbenzene ND 1.0 I ug/L 4-Methyl-2-Pentanone ND 10 1
sec-Butylbenzene ND 1.0 1 ug/L Naphthalene ND 10 1
tert-Butylbenzene ND 1.0 1 ug/l_ n-Propylbenzene ND 1.0 1
Carbon Disuifide ND 10 1 ug/L Styrene ND 1.0 1
Carbon Tetrachloride ND 0.50 1 ug/L 1,1,1,2-Tetrachlo~oethane ND 1.0 1
Chlorobenzene ND 1.0 1 ug/L 1,1,2,2-Tetrachloroethane ND 1.0 1
Chloroethane ND 1.0 1 ug/L Tetrachloroethene ND 1.0 1
Chloroform ND 1.0 1 ug/L Toluene ND 1 .O 1
Chloromethane ND 10 1 ug/L 1,2,3-Trichtorobenzene ND 1.0 1
2-Chlorotoiuene ND 1.0 1 ug/L 1,2,4-Trichlorobenzene ND 1.0 1
4-Chlorotoluene ND 1.0 1 ug/L 1 ,l,l-Trichloroethane ND 1.0 1
Dibromochloromethane ND 1.0 1 ug/L 1,1,2-Trichloroethane ND 1.0 1
1,2-Dibromo-3-Chloropropane ND 5.0 1 ug/L Trichloroethene ND 1.0 1
1,2-Dibromoethane ND 1.0 1 ug/L Trichlorofluoromethane ND 10 1
Dibromomethane ND 1.0 I ug/L 1,2,3-Tdchloropropane ND 5.0 1
1,2-Dichlorobenzene ND 1.0 1 ug/L 1,2,4-Trimethylbenzene ND 1.0 1
1,3-Dichlorobenzene ND 1.0 I ug/L 1,3,5-Trimethylbenzene ND 1.0 1
1,4-Dichlorobenzene ND 1.0 I ug/L Vinyl Acetate ND 10 1
Dichlorodifluoromethane ND 1.0 1 ug/L Vinyl Chlodde ND 0.50 1
1,1.Dichloroethane ND 1.0 1 ug/L p/m-Xylene ND 1.0 1
1,2-Dichloroethane ND 0.50 1 ug/L o-Xylene ND 1.0 1
1, i-Dichloroethene ND 1.0 1 ug/L Methyl-t-Butyl Ether (MTBE) ND 1.0 1
c-1,2-Dichloroethene ND 1.0 1 ug/L Terl-Butyl Alcohol ('TBA) ND 10 1
t-1,2-Dichloroethene ND 1.0 1 ug/L Diisopropyl Ether (DIPE) ND 2.0 1
1,2-Dichioropropane ND 1.0 1 ug/L Ethyl-t-Butyl Ether (ETBE) ND 2.0 1
1,3-Dichloropropane ND 1.0 1 ug/L Terl-AmyI-Methyl Ether (TAME) ND 2.0 1
2,2-Dichloropropane ND 1.0 I ug/L
Surro.qates: REC (%) ConlTol Qual Surro_qates: REC {%) Control
Limits
Dibromofluoromethane 100 84-120 Toluene-d8 100 91-109
1,4--Bromofluorobenzene 100 84-108
.~ Units
ug/L
ug/L
ug/L
ug/L
ugJL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/l_
ug/L
ug/l_
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Qual
~ PI_- Reporling IJmit , DF - Dilution Factor , Qual- Qualifiers
7440 Lincoln Garden Grove, CA 92841-1427
Way,
· TEL: (714) 895-5494
· FAX: (714) 894-7501
!
pvironmentai
I raboraton'es, Inc.
Analytical Report
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project: 2401 Oak Street, Bakersfield, CA
Date Received: 01/13/04
Work Order No: 04-01-0549
Preparation: EPA 5030B
Method: EPA 8260B
Page 2 of 10
Lab Sample Date Date Date
Client Sample Number Number Collected Matrix Prepared Analyzed QC Batch ID
!~;2(~i~!~.,ge):~,:..:~::.:.~,::.~.i~ ~:~.. :::. ~ ~i: :~ !~::: !: ;. :.04~0549~2: -~,' ~O~fl~ .','. ~us ..:~...:~.~NIA .... .. -'.0~1~/15/0~:. 040115L01
Parameter Result RI. DF Dual Units Parameter Result RI. D._~F Oual Units
Acetone ND 10 I ug/L 1,1.Dichloropropene ND 1.0 I ug/L
Benzene ND 0.50 1 ug/L c-l,3-Dichloropropene ND 0.50 1 ug/L
Bromobenzene ND 1.0 I ug/L t-1,3-Dichloropropene ND 0.50 1 ug/L
Bromochloromethane ND 1.0 1 ug/L Ethylbenzene ND 1.0 1 ug/L
Bromodichloromethane NO 1.0 1 ug/L 2-Hexanone ND 10 1. ug/L
Bromoform ND 1.0 1 ug/L Isopmpytbenzene ND 1.0 1 ug/L
Bromomethane ND 10 1 ug/L p-lsopropyltoluene ND 1.0 1 ug/L
2-Butanone ND 10 1 ug/L Melhylene Chlodde ND 10 I ug/L
n-Butylbenzene ND 1.0 1 ug/L 4-Methyl-2-Pentanone ND 10 I ug/L
sec-Butylbenzene ND 1.0 1 ug/L Naphthalene ND 10 1 ug/L
tert-Butylbenzene ND 1.0 1 ug/L n-Propylbenzene ND 1.0 I ug/L
Carbon Disulfide ND 10 1 ug/L Styrene ND 1.0 I ug/L
Carbon Tetrachlodde ND 0.50 1 ug/L 1,1,1,2-Tetrachloroethane ND 1.0 I ug/L
Chlorobenzene ND 1.0 1 ug/L 1,1,2,2-Tetrachloroethane ND 1.0 I ug/L
Chloroethane ND 1.0 1 ug/L Tetrachloroethene ND 1.0 1 ug/L
Chloroform ND 1.0 I ug/L Toluene ND 1.0 1 ug/L
Chloromethane ND 10 1 ug/L 1,2,3-Tdchlorobenzene ND 1.0 1 ug/L
2-Chlorotoluene ND 1.0 1 ug/L 1,2,4-Trichlorobenzene ND 1 ;0 I ug/L
4-Chlorotoluene ND 1.0 I ug/L 1,1,1-Tdchloroethane ND 1.0 1 uglL
Dibromochloromethane ND 1.0 I ug/L. 1,1.,2-Tdchloroethane ND 1.0 I ug/L
1,2-Dlbromo-3-Chloropropane ND 5.0 1 ug/L Trichloroethene ND 1.0 I ug/L
1,2.Dibromoethane ND 1.0 1 ug/L Trichlorofl uoromethane NO 10 I uglL
Dibromomethane ND 1.0 1 ug/L 1,2,3~Trichlompropane ND 5.0 1 ug/L
1,2-Dich~orobenzene ND 1.0 I ug/L 1,2,4-Trimethylbenzene ND 1.0 1 ug/L
1,3-Dich/orobenzene ND 1.0 I ug/L 1,3,5-Trimethylbenzene ND 1.0 1 ug/L
1,4-Dichlombenzene ND 1.0 1 ug/L Vinyl Acetate ND 10 1 ug/L
Diqhlorodifluoromethane ND 1.0 1 ug/L Vinyl Chloride ND 0.50 1 ug/L
1,1-Dichloroethane ND 1.0 1 ug/L p/m-Xylene ND 1.0 I ug/L.
1,2-Dichloroethane ND 0.50 1 ug/L o-Xylene ND 1.0 1 uglL
1,1-Dichloroethene ND 1,0 1 ug/L Methyl-t-Butyl Ether (MTBE) ND 1.0 1 ug/L
c-l,2-Dichlor0ethene ND 1.0 1 ug/L Tert-Butyl Alcohol (TBA) ND 10 I ug/L
t-1,2-Dichloroethene ND 1.0 1 ug/L Diisopropyl Ether (DIPE) ND 2.0 I ug/L
1,2-Dichloropropane ND 1.0 1 ug/L Ethyl-t-Butyl Ether (ETBE) ND 2.0 I ug/L
1,3-Dichloropropane ND 1.0 1 ug/L Te~t-AmyI-Methyl Ether (TAME) ND 2.0 1 ug/L
2,2-Dichloropropane ND 1.0 I ug/L
Surro,qates: REC (%) Control Qual Surrogates: REC (%) Control Oual
Limits
Dibromofluoromethane 103 84.120 Toluene-d8 97 91-109
1,4-Bromofluorobenzene 100 84-108
I
I
RI_. Reporting Limit , DF - Dilution Factor , Oual - Qualifiers
7440 Lincoln Garden Grove, CA 92841-1427
Way,
· TEL: (7t4) 895-5494 · FAX: (714) 894-7501
I
I
I
I
I
I
I
I
:1
I
!
I
I
I
I
I
-_nvironmental
--aboratories, Inc.
AnalYtical Report
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received: 01/13/04
Work Order No: 04-01-0549
Preparation: EPA 5030B
Method: EPA 8260B
Project: 2401 Oak Street, Bakersfield, CA
Page 3 of 10
Lab Sample Date Date Date
Client Sample Number Number Collected Matrix Prepared Analyzed QC Batch ID
Parameter Result RI_ DF :Qual Units Parameter Result R~L DF Oual Units
Acetone ND 10 1 ug/L 1,1.Dichloropropene ND 1,0 1 ug/L
Benzene ND 0,50 I ug/L c-1,3Oichlompropene ND 0.50 1 ug/L
Bromobenzene ND 1.0 I ug/L t-1,3-Dichloropropene ND 0.50 1 ug/L
Bromochloromethane ND 1.0 1 ug/L Ethylbenzene · ' ND 1.0 1 ug/L
Bromodichloromethane ND 1.0 1 ug/L. 2-Hexanone ND 10 1 ug/L
Bromoform ND 1.0 1 ug/L Isopropylbenzene ND 1.0 I ug/L
Bromomethane ND 10 I ug/l_ p-isopropyltoluene ND 1.0 I ug/L
2-Butanone ND 10 I ug/L Methylene Chloride ND 10 I ug/L
n-Butylbenzene ND 1.0 1 ug/L 4-Methyl-2-Pentanone ND 10 1 ug/L
sec-Butylbenzene ND 1.0 1 ug/L Naphthalene ND 10 1 ug/L
tert-Butylbenzene ND 1.0 1 ug/L n-Propylbenzene ND 1,0 I ug/L
Carbon Disulfide ND 10 1 bg/L Styrene ND 1.0 1 ug/L
Carbon Tetrachloride ND 0.50 1 ug/L 1,1,1,2-Tetrachloroethane ND 1.0 1 ug/L
Chlorobenzene ND 1.0 1 ug/L 1,1,2,2-Tetrachloroethane ND 1,0 1 ug/L
Chloroethane ND 1.0 1 ug/L Tetrachloroethene ND 1.0 1 ug/L
Chloroform ND 1.0 1 ug/L Toluene ND 1.0 1 ug/L
Chloromethane ND 10 1 ug/L 1,2,3-Tdchlorobenzene ND 1.0 1 ug/L
2-Chlorotoluene ND 1.0 1 ug/L 1,2,4-Trtchlorobenzene ND 1.0 1 ug/L
4-Chlorotoiuene ND 1.0 I ug/L 1,1,1-Trichloroethane ND 1.0 I ug/L
Dibromochloromethane ND 1.0 1 ug/L 1,1,2-Trichloroethane ND 1.0 1 ug/L
1,2-Dlbromo-3-Chlompropane ND 5.0 I ug/L Trichloroel~ene ND 1.0 1 ug/L
1,2-Dibromoethane ND 1.0 1 ug/L Trichlorofluoromethane ND 10 1 ucj/L
Dibromomethane ND 1.0 1 ug/L 1,2,3-Trichloropropane ND 5.0 1 ug/L
1,2-Dichlorobenzene ND 1.0 I uglL 1,2,~Tdmethylbenzene ND 1.0 I ug/t.
1,3-Dichlorobenzene ND 1.0 1 ug/L 1,3,5-Tdmethylbenzene ND 1.0 1 ug/L
1,4-Dichlorobenzene ND 1.0 1 uglL Vinyl Acetate ND 10 1 ug/L
Dichlorodifluoromethane ND 1.0 1 ug/L Vinyl Chloride ND 0.50 1 ug/L
1,1 -Dichloroethane ND 1.0 I ug/L p/m-Xylene ND 1.0 1 ug/L
1,2-Dichloroethane ND 0.50 1 ug/L o-Xylene ND 1.0 I ug/L
1,1-Dichloroethene ND 1.0 I ug/L Methyl-t-Butyl Ether (MTBE) ND 1.0 I ug/L
c-l,2-Dichloroethene ND 1.0 1 ug/L . Ted-Butyl Alcohol (TBA) ND 10 1 ug/L
t-l,2-Dichloroethene ND 1.0 1 ug/L Diisopropyl Ether (DIPE) ND 2.0 1 ug/L
t ,2-Dichloropropane ND 1.0 1 ug/L Ethyl-t-Butyl Ether (ETBE) ND 2.0 1 ug/L
1,3-Dichloropropane ND 1.0 1 ug/L Tert-Amyl-Methyl Ether (TAME) ND 2.0 1 ug/L
2,2-Dichloropropane ND 1.0 1 ug/L
Surrogates; REC (%) Control Qual Surroflate~; REC {%) .Control Qual
Limits
Dibromofluoromethane gg . 84-120 Toluene-d8 100 91-109
1,4-Bromofl uorobenzene 101 84-108
ortlng Limit , DF - Dilution Factor , Oual- Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427
u
· TEL: (714) 895-5494
· FAX: (714) 894-7501
nvironmental
~ Analytical Report
~-- aboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Method:
Project: 2401 Oak Street, Bakersfield, CA
Lab Sample
Client Sample Number Number
Parameter , RestJlt RL D~ Qual Units
Acetone ND 10
ug/L
Benzene ND 0.50 1 ug/L
Bmmobenzene ND 1.0 1 ug/L
Bromochlorome~ane ND 1.0 1 ug/L
Bromodichloromethane ND 1.0 1 ug/L
Bromoform ND 1.0 1 ug/L
Bromomethane ND 10 1 ug/L
2-Butanone ND 10 I ug/L
n-Butylbenzene ND 1.0 I ug/L
sec-Butylbenzene ND 1.0 1 ug/L
tert-Butylbenzene ND 1.0 1 ug/L
Carbon Disulfide ND 10 1 ug/L Styrene
Carbon Tetrachloride ND 0.50 1 ug/L 1,1,1,2-'
Chlorobenzene ND 1.0 1 uglL 1,1,2,2-'
Chloroethane ND 1.0 1 ug/L Tetrachl
Chloroform ND 1.0 1 ug/L Toluene
Chloromethane ND 10 I ug/L
2-Chlorotoluene ND 1.0 I ug/L
4-Chlorotoluene ND 1.0 I ug/L
Dibromochloromethane ' ND 1,0 1 ug/L
1,2-Dibromo-3-Chloropropa ne ND 5.0 1 ug/L
1,2-Dibromoethane ND 1.0 I ug/L
Dibromomethane ND 1.0 1 ug/!-
1,2-Dichlorobenzene ND 1.0 1 ug/L
1,3-Dichlorobenzene ND 1.0 I ug/L
1,4-Dichlorobenzene ND 1.0 1 ug/L
Dichlorodifluorometh ane ND 1.0 1 ug/L
1,1-Dichloroethane ND 1.0 1 ug/L
1,2-Dichloroethane ND 0.50 1 ug/L
1,1-Dichloro~thene ND 1.0 1 ug/L
c-1,2-Dichloroethene ND 1.0 1 ug/L
t-1,2-DichlOroethene ND 1.0 1 ug/L
1,2-Dichloropropane ND 1,0 1 ug/L
1,3-Dichloropropane ND 1.0 ' 1 ug/L
2.,2-Dichloropropane ND 1.0 1 uglL
Surroqates; REC (%) Control Qual Surrogates:
Limits
Dibromofluoromethane 100 8-~'-120 Toluene-d8
t ,4-Bromofluorobenzene 99 84-108
7440 Lincoln Way, Garden Grove, CA 92841-1427
Date Received:
Work Order No:
Preparation:
01/13/O4
04-01-0549
EPA 5030B
EPA 8260B
Page 4 of 10
Date Date Date
Collected Matrix Prepared Analyzed QC Batch ID
..: · . . ...... .....
Parameter
1,1-Oichloropropene
c-1,3-Dichior0Propene
t-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene
p-lsopropyttoluene
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
n-Propylbenzene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachlomethene
1,2,3-Trichlorobenzene
1,2,4-Tdchlorobenzene
1,1,1-Trichloroethane
1,'I ,2-Tdchloroethane
Tdchloroethene
Tric~lorofluorometha ne
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl Acetate
Vinyl Chloride
p/m-Xylene
o-Xylene
Methyl-t-Butyl Ether (MTBE)
Tert-Butyl Alcohol (TBA)
Diisopropyl Ether (DIPE)
Ethyl-l-Butyl Ether (ETBE)
Tert-AmyI-Methyl Ether (TAME)
Result RL D_[F Qual Unit._._~s
ND 1.0 I ug/L
ND 0,50 1 ug/L
ND 0.50 1 ug/L
ND 1.0 1 ug/L
ND 10 I ug/L
ND 1,0 1 ug/L
ND 1.0 I ug/L
ND 10 I ug/L
ND 10 1 ug/L
ND 10 1 ug/L
ND 1.0 1 ug/L
ND 1.0 1 ug/L
ND 1.0 1 ug/L
ND 1.0 1 ug/L
ND 1.0 I ug/L
ND 1.0 1 ug/L
ND 1.0 1 ug/L
ND 1.0 I ug/L
ND 1.0 1 ug/L
ND 1.0 1 ug/L
ND 1.0 1 ug/L
ND 10 I ug/L
ND 5.0 1 ugfL
ND 1.0 I ug/L
ND 1.0 I ug/L
ND 10 I ug/L
ND 0.50 I ug/L
ND 1.0 1 ug/L
ND 1.0 1 ug/L
ND 1.0 1 ug/L
ND 10 1 ug/L
ND 2.0 I ug/L
ND 2.0 1 ug/L
ND 2.0 1 ug/L
REC {%) Co,ntro,
100 91-109
Qual
· TEL: (714) 895-5494 · FAX: (714) 894-7501
,,alscience
J ._n vironmental
aboratories, Inc.
Analytical Report
Blaine Tech Services, Inc Date Received: 01/13/04
20360 Gramercy Place Work Order No: 04-01-0549
Torrance, CA 90501-1511 Preparation: EPA 5030B
Method: EPA 8260B
Project: 2401 Oak Street, Bakersfield, CA Page 5 of 10
Lab Sample Date Date Date
Client Sample Number Number Collected Matdx Prepared Analyzed QC Batch ID
....... ' ......... ,~;,,~;,;i~ .......... "' ,, ',,' ............................................. 'ii '':' ..... ,,'~t" ' ,,,,, ', ......... ,,' ' ..
Parameter Result RI. DF Qual Units Parameter Result RI. DF Qual Units
Acetone ND 10 1 ug/L 1,1-Dichloropropene ND 1.0 I ug/L
Benzene ND 0.50 1 ug/L c-1,3-Oichloropropene ND 0.50 I ug/L
Bromobenzene ND 1,0 1 ug/L t-1,3-Dichloropropene ND 0.50 1 ug/L
Bromochloromethane ND 1.0 I ug/L Ethylbenzene ND 1.0 1 ug/L
Bromodichloromethane ND 1.0 I ug/L 2-Hexanone ND 10 1 ug/L
Bromoform ND 1.0 1 ug/L Isopropylbenzene ND 1.0 1 ug/L
Bromomethane ND 10 1 ug/L p-lsopropyltoluene ND 1.0 1 ug/L
2-Rutanone ND 10 1 ug/L Methylene Chloride . ND 10 I ug/L
n-Butytbenzene ND 1.0 1 ug/L 4-Methyl-2-Pentanone ND 10 1 ug/L
sec-Butylbenzene ND 1.0 1 ug/L Naphthalene ND 10 1 ug/L
tert-Butylbenzene ND 1.0 1 ug/L n-Propylbenzene ND 1.0 1 uglL
Carbon Disulfide ND 10 1 ug/L Styrene ND 1.0 1 ug/L
Carbon Tetrachloride ND 0.50 1 ug/L 1,1,1,2-Tetrachloroethane ND 1.0 1 ug/L
Chlorobenzene ND 1.0 I ug/L 1,1,2,2-Tetrachioroetha ne ND 1.0 I ug/L
Chloroethane ND 1.0 I ug/L Tetrachloroethene ND 1.0 I ug/L
Chlorofom3 ND 1.0 1 ug/L Toluene ND 1.0 I ug/L
Chloromethane ND 10 1 ug/L 1,2,3-Trichlorobenzene ND 1.0 1 ug/L
2-Chlorotoluene ND 1.0 1 ug/L 1,2,4-Trichlorobenzene ND 1.0 1 ug/L
4-Chlorotoluene ND 1.0 1 ug/L 1,1,1-Tdchloroethane ND 1.0 1 ug/L
Dibromochloromethane ND 1.0 1 ug/L 1,1,2-Trichloroethane ND 1.0 1 ' uglL
1,2-Dibromo-3-Chloropropane ND 5.0 1 ug/L Trlchloroethene ND 1.0 I ug/L
1,2-Dibromoethane ND 1.0 1 ug/I. Trichlorofiuoromethane ND 10 I ug/L
DIbromomethane ND 1.0 1 ug/L 1,2,3-Tdchloropropane ND 5.0 1 ug/L
1,2-Dichi0robenzene ND 1.0 I ug/L 1,2.4-Trimethylbenzene ND 1.0 1 ug/L
1,3-Dichlorobenzene ND 1.0 I uglL 1,3,5-Tdmethylbenzene ND 1,0 1 ug/L
1,4-Dichlorobenzene ND 1.0 I ug/L Vinyl Acetate ND 10 1 ug/L
Dichlorodifluoromethane ND 1.0 1 ug/L Vinyl Chlodde ND 0.50 1 ug/L
1,1-Dichloroethane ND 1.0 t ug/L p/m-Xylene ND 1.0 I ug/L
1,2-Dichloroethane ND 0.50 1 ug/L o-Xylene.. ND 1.0 1 uglL
1,1-Dichloroethene ND 1.0 1 ug/L Methyl-t-Butyl Ether (MTBE) ND 1.0 1 uD/L
c-'J ,2-Dichloroethene ND 1.0 1 ug/L Tert-Butyl Alcohol (TBA) ND 10 1 ug/L
t-l,2-Dichloroelhene ND 1,0 1 ug/L Diisopropyt El~er (DIPE) ND 2.0 1 ug/L
1,2-Dichloropropane ND 1.0 1 ug/L Ethyl-t-Butyl Ether (ETBE) ND 2.0 1 ug/L
1,3-Dichloropropane ND 1.0 1 ug/L Tert-AmyI-Methyl Ether (TAME) ND 2.0 1 ug/L
2,2-Dichloropropane ND 1.0 1 ug/L
Surro,qates: RFC (%) Control Oual Surro.qates: EEC (%) Control Qual
Limits
DIbmmofluoromethane 102 84-120 Toluene-d8 97 91-109
1,4-Bromofluorobenzene 98 84-108
ort:ng Umit , DF - Dilution Factor , Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427
· TEL: (714) 895-5494
· FAX: (714) 894-7501
I
-alscience
m nvironmental
,,. ~ .... Analytical Report
I b aDorarones, inc.
Blaine Tech Services, Inc Date Received: 01/13/04
· 20360 Gramercy Place Work Order No: 04-01-0549
· Torrance, CA 90501-1511 Preparation: EPA 5030B
Method: EPA 8260B
I Project: 2401 Oak Street, Bakersfield, CA Page 6 of 10
Lab Sample Date . .. Date Date .......
· Client Sample Number, Number Collected Matnx Prepared Analyzed
_ Parameter .R~ult RL DF QUal Unit~ Parameter Result RL DF Qual Units
B ND 10 1 ND 1.0 1
Acetone
u~I/L
1,1-Diahloropropene
u~/L
· Benzene ND 0.50 1 ug/L c-1,3-Dichloropropene ND 0.50 I ug/L
Bromobenzene ND t .0 1 ug/I. t-l,3-Dichloropropene ND 0.50 1 ug/L
Bromochloromethane ND 1.0 1 ug/L Ethylbenzene ND 1.0 1 ug/L
Bromodichloromethane ND 1.0 1 ug/L 2-Hexanone ND 10 1 ug/L
· Bromoforrn ND 1.0 1 ug/L .Isopropylbenzene ND 1.0 1 ug/L
~ Bromomethane ND 10 1 uglL p-lsopropyltoluene ND 1.0 1 ug/L
2-Butanone ND 10 1 ug/L Methylene Chloride . ND 10 1 . ug/L
I~ n-Butylbenzene ND 1.0 1 ug/L 4-Methyl-2-Pentanone ND 10 1 ug/L
· sec-Butylbenzene ND 1.0 1 ug/L Naphthalene ND 10 I ug/L
~ tert-Butylbenzene ND 1.0 I ug/L n-Propyll~nzene ND 1,0 I ug/L
- Carbon Disulfide ND 10 1 ug/L ~ Styrene ND 1.0 1 ug/L
__ Carbon Tetrachloride ND 0.50 1 ug/L 1,1,1,2-Tetrachloroethane ND 1.0 1 ug/L
Chlorobenzene ND 1.0 I ug/L 1,1,2,2-Tetrachloroetha ne ND 1.0 1 ug/L
· Chloroethane ND 1.0 I ug/L Tetrachloroethene ND 1.0 1 ug/L
Chloroform ND 1.0 1 ug/L Toluene ND 1.0 I ug/L
Chloromethane ND 10 1 ug/L 1,2,3-Trichlorobenzen e ND 1.0 I ug/L
· 2-Chlorotoluene ND 1.0 1 ug/L 1,2,4.T richlorobenzene ND 1.0 1 ug/L.
B 4-Chlorotoluene ND 1.0 1 ug/L 1,1,1-Tfichloroethane ND 1.0 1 ug/L
Dibromochloromethane ND ' 1.0 1 uglL 1,1,2-Trichloroethane ND 1.0 1 ug/L
1,2-Dibromo-3-Chlorop ropa ne ND 5.0 1 ug/L Trichloroethene ND 1.0 1 ug/L
B~ 1,2-Dibromoethane ND 1,0 1 u§/L Trichlorofluoromethane ND 10 1 ug/L
· Dibromomethane ND 1.0 I ug/L 1,2,3-Tdchloropropane ND 5.0 1 ug/L
· 1,2-Dichlorobenzene ND 1.0 1 ug/L 1,2 4-Trimethylbenzene ND 1.0 1 ug/L
' 1,$-Dichlorobenzene ND 1.0 I ug/L 1,3,5-Trimethylbenzene ND 1.0 1 ug/L
1,4-Dichlorobenzene ND 1.0 1 ug/L Vinyl Acetate ND 10 1 ~ ug/L
· Dichlorodifluoromethane ND 1.0 1 ug/L Vinyl Chloride ND 0.50 1 . ug/L '
· 1,1-Dichloroethane ND 1.0 1 ug/L p/m-Xytene ND 1.0 1 ug/L
~' 1,2-Dichloroethane ND 0.50 I . ug/L o-Xylene ND 1.0 1 ug/L
1,1-Dichloro~thene ND 1.0 1 ug/L Melhyl-toButyl Ether (MTBE) ND 1.0 t ug/L
lEI c-l,2-Dichloroethene ND 1.0 1 'ug/L Tart-Butyl Alcohol (-FBA) ND 10 I ug/L
· t-l,2-Dichloroethene ND 1.0 1 ug/L Diisopropyl Ether {DIRE} ND 2.0 1 ug/L
~ 1,2-Dichloropropane ND 1.0 1 ug/L Ethyl-t-Butyl Ether (ETBE) . ND 2.0 1 uo/L
1,3-Dichloropropane ND 1.0 1 ug/L Tert-AmyI-Methyl Ether (TAME) ND 2.0 1 ug/L
i 2,2-Dichloropropane ND 1.0 1 ug/L
· Surroclates: REC i'%} Control Qual Surroqntes: REC {%) Control Qual
-- Limits
Dibromofluoromethane 101 '--~'~'20 Toluene-d 8 100 91 -109
I 1,4-Brom ofluorobenzene 102 84-108
!
alscience
n vironmental
· --aborato es, Inc.
Analytical Report
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project: 2401 Oak Street, Bakersfield, CA
Date Received:
Work Order No:
Preparation:
Method:
01 / 13/04
04-01-0549
EPa 5030B
EPA 8260B
Page 7 of 10
Lab Sample Date Date
Client Sample Number Number Collected Matrix Prepared
Date
Analyzed
.: o!/14/o4
QC Batch ID
'1
I
I
I
!
i
I
!
i
I
I
I
I
Parameter Result RI_ D__~F Qual Units Parameter Result
Acetone ND 10 1 ug/L 1,1-Dichloropropene ND
Benzene ND 0.50 1 ug/L c-1,3-Dichloropropene ND
Bromobenzene ND 1.0 1 ug/L t-1,3-Dichloropropene ND
Bromochloromethane ND 1.0 1 ug/L Ethylbenzene ND
Bromodichloromethane ND 1.0 1 ug/L 2-Hexanone ND
Bromoform ND 1.0 I ug/L Isopropylbenzene ND
Bromomethane ND 10 I ug/L p-lsopropyltoluene ND
2-Butanone ND 10 1 ug/L Methylene Chloride ND
n-Butylbenzene ND 1.0 I ug/L 4-Methyl-2-Pentanone ND
sec-Butylbenzene ND 1.0 1 ug/L Naphthalene ND
tert-Butylbenzene ND 1.0 1 ug/L n-Propylbenzene ND
Carbon Disulfide ND 10 1 ug/L Styrene ND
Carbon Tetrachloride ND 0.50 1 ug/L 1,1,1,2-Tetrachloroethane ND
Chlorobenzene ND 1.0 1 ug/L 1,1,2,2-Tetrachioroethane ND
Chloroethane ND 1.0 1 ug/L Tetrachloroethene ND
Chloroform ND 1.0 1 uglL Toluene ND
Chloromethane ND 10 1 ug/L 1,2,3-Trichlorobenzene ND
2.Chlorotoluene ND 1.0 I ug/L 1,2,4-Trlchlo~obenzene ND
4-Chlorotoluene ND 1.0 I ug/L 1,1,1-Trichloroethane ND
Dibromochlommethane ND 1.0 1 ug/L 1,1,2.Tdchloroethane ND
1,2-Dibromo-3-Chloropropane ND 5,0 I ug/L Trichloroethene ND
1,2-Dibromoethane ND 1.0 I uglL Tdchlorofluoromethane ND
Dibromomethane ND 1.0 1 ug/L 1,2,3-Trichloropropane ND
1,2-Dichlombenzene ND 1.0 1 ug/L 1,2,4-Trimethylbenzene ND
1,3-Dichlorobenzene ND 1.0 1 ug/L 1,3,5-Trimethylbenzene ND
1,4-Dichlorobenzene ND. 1.0 1 ug/L Vinyl Acetate ND
Dichlorodifluoromethane ND 1.0 1 uglL Vinyl Chloride ND
1,1-Dichloroethane ND 1.0 1 ug/L p/m.Xylene ND
1,2-Dichloroethane ND 0,50 1 ug/L o-Xylene ND
1,1-Dichloroethene ND 1.0 1 ug/L Methyl-t-Buty~ Ether (MTBE) ND
c-1,2-Dichloroethene ND 1.0 I ug/L Ted-Butyl Alcohol (TBA) ND
t-1,2-Dichloroethene ND 1.0 I ug/L Diisopropyl Ether (DIPE) ND
1,2-Dichloropropane ND 1.0 1 ug/L Ethyl-t-Butyl Ether (ETBE) ND
1,3-Dichloropropane ND ' 1.0 1 ug/L Tert-AmyI-Methyl Ether (TAME) ND
2,2-Dichloropropane ND 1.0 1 ug/L
Surrogates: REC (%) Control Qual Surrogates; REC {'%)
Limits
Dibromofluoromethane 101 84-120 Toluene-d8 94
1,4-Bromofluorobenzene 99 84-108
RI_ DF Qual Units
1.0 I uglL
0.50 1 ug/L
0.50 I ug/L
1.0 I ug/L
10 1 ug/L
1.0 I ug/L
1.0 I ug/L
10 1 ug/L
10 1 ug/L
10 1 ug/L
1.0 I ug/L
1,0 1 ug/L
1.0 1 ug/L
1.0 1 ug/L
1.0 I ug/L
1.0 I ug/L
1.0 1 ug/L
1.0 1 ug/L
1.0 1 ug/L
1.0 1 ug/L
1.0 1 ug/L
10 1 ug/L
5.0 I ug/L
1.0 I ug/L
1.0 1 ug/L
10 I ug/L
0.50 1 ug/L
1.0 I ug/L
1.0 1 ug/L
1.0 I ug/L
10 I ug/L
2,0 I ug/L
2.0 1 ug/L
2.0 1 ug/L
~.ontrol
91-109
Qual
ortlng Limit , DF - Dilution Factor , Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427
· TEL: (714) 895-5494
· FAX: (714) 894-7501.
-_als=cience
vironmen tal
aboratories, inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received: 01/13/04
Work Order No: 04-01-0549
Preparation: EPA 5030B
Method: EPA 8260B
Project: 2401 Oak Street, Bakersfield, CA Page 8 of 10
Lab Sample Date Date Date
Client Sample Nurnber Number Collected Matrix Prepared Analyzed QC Batch ID
i: ..... .' :1
param, ete[ Result RI. D._.~F Qual Units Parameter Result RI_ D__~F Qual ~
Acetone ND 10 1 ug/L 1 ,l-Dichloropropene ND 1.0 1 ug/L
Benzene ND 0.50 1 ug/l_ c-1,3-Dichioropropene ND 0.50 I ug/L
Bromobenzene ND 1.0 1 ug/L t-1,3-Dtchloropropene ND 0.50 I ug/L
Bromochlorornethane ND 1.0 1 ug/L Ethylbenzene ND 1.0 1 ug/L
Brornodichloromethane ND 1.0 1 ug/L 2-Hexanone ND 10 1 ug/L
Bromoform ND 1.0 I ug/L Isopropylbenzene ND 1.0 I ug/L
Bromomethane ND 10 I ugfL p-lsopropyltoluene ND 1.0 I ug/L
2-Butano~e ND 10 1 ug/L Methylene Chloride ND 10 I ug/L
n-Butylbenzene ND 1.0 1 ug/L 4oMethyl-2-Pentanone ND 10 1 ug/L
sec-Butylbenzene ND 1,0 1 uglL Naphthalene ND 10 1 ug/l.
tert-Butylbenzene ND 1.0 1 ug/L n-Propylbenzene ND 1.0 I ug/L
Carbon Disulfide ND 10 1 ug/L Styrene ND 1.0 1 ug/L
Carbon Tetrachlodde ND 0,50 1 ug/L 1,1,1,2-Tetrachloroethane ND 1.0 1 ug/L
Chlorobenzene ND 1,0 I ug/L 1,1,2,2-Tetrachioroethane ND 1.0 1 ug/L
Chloroethane ND 1.0 I ug/L Tetrachloroethene ND 1.0 I ug/L
Chloroform ND t .0 '1 ug/L Toluene ND 1.0 1 ug/L
Chloromethane ND 10 1 ug/L 1,2,3-Trichlorobenzene ND 1.0 1 uglL
2-Chlorotoluene ND 1.0 1 ug/L 1,2,4.Trichlorobenzene ND 1.0 1 ug/L
4-Chlorotoluene ND 1.0 1 ug/L 1,1,1-Trichloroethane ND 1.0 1 ug/L.
Dibromochloromethane ND 1.0 I ugJL 1,1,2-Trichloroethane ND 1.0 I ug/L
1,2-Dibromo-3-Chloropropane ND 5.0 1 ug/L Tdchloroethene ND 1.0 1 ug/L
1,2-Dibromoethane ND 1.0 1 ug/L Tdchlorofluoromethane ND 10 1 ug/L
Dibromomethane ND 1.0 1 ug/L 1,2,3-Tdchloropropane ND 5.0 1 ug/L
1,2-Dichlorobenzene ND 1.0 1 ug/L 1,2,4-Tdmethylbenzene ND 1.0 1 ug/L
1,3-Dichlorobenzene ND 1.0 I ug/L 1,3,5-Tdrnethylbenzene ND 1.0 1 ugfL
1,4-Dichlorobenzene ND 1.0 1 ug/L Vinyl Acetate ND 10 I ug/L
Dichlorodifluoromethane ND 1.0 1 ug/L Vinyl Chloride ND 0.50 I ug/L.
1,1-Dichloroethane ND 1.0 I ug/L p/m-Xylene ND 1.0 1 ug/L
1,2-DichloroebSane ND 0.50 I ug/L o-Xylene ND 1.0 1 ug/L
1,1-Dichloroethene ND 1.0 1 ug/L Methyl-t-Butyl Ether (MTBE) ND 1.0 1 ug/L
c-1,2-Dichloroethene ND 1.0 1 ug/L Ted-Butyl Alcohol ('F'BA) ND 10 1 ug/L
t-1,2-Dichloroethene ND 1.0 1 ug/L Diisopropyl Ether (DIPE) ND 2.0 1 ug/L
1,2-Dichloropropane ND 1.0 1 ug/L Ethyl-t-Butyl Ether (ETBE) ND 2.0 I ug/L
1,3-Dichloropropane ND 1.0 1 ug/I. Tert-AmyI-Methyl Ether (TAME) ND 2.0 I ug/L
2,2-Dichloropropane ND 1.0 1 ug/L
Surrogates: REC (%). Controt ' Qual Surroqates: REC {%) Control Qua!
Limits
Dibromofl uoromethane 1 O0 84-120 Tol uene*d8 99 91-109
1,4-Bromofluorobenzene 101 84-108
o~ng Limit , DF - Dilution Factor , Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427
· TEL: (714) 895-5494 · FAX: (714) 894-7501
~ra!science
~E~vironmental
i--a~to~es, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-151
Analytical Report
Date Received: 01113/04
Work Order No: 04-01-0549
Preparation: EPA 5030B
Method: EPA 8260B
Project: 2401 Oak Street, Bakersfield, CA Page 9 of
Lab Sample Date Date Date
Client Sample Number Number Collected Matrix Prepared Analyzed QC Batch ID
10
Parameter Result RI_ DF Qual .Units Parameter Result R~L DF Qpal Units
Acetone ND 10 1 ug/L 1 .l-Dichloropropene ND 1.0 1 ug/L
Benzene ND 0.50 1 ug/L c. 1,3-Dichloropropene ND 0.50 1 ug/L
Bromobenzene ND 1.0 I ug/L t-1,3-Dichloropropene ND 0.50 1 ug/L
Bromochloromethane ND 1.0 1 ug/L Ethylbenzene ND 1.0 1 ug/L
Bromodichloromethane ND 1.0 1 ug/L 2-Hexanone ND 10 1 ug/L
Bromoform ND 1.0 1 ug/L Isopropylbenzene ND 1,0 I ug/L
Bromomethane ND 10 1 ug/L p-lsopropyltoluene ND 1.0 I ug/L
2-Butanone ND 10 1 ug/L Methylene Chloride ND 10 1 ug/L
n-Butylbenzene ND 1,0 1 ug/L 4-Methyl-2-Pentanone ND 10 1 ug/L
sec-Buty~benzene ND 1.0 I ug/L Naphthalene ND 10 I ug/L
tert-Butylbenzene ND 1.0 1 ug/L n-Propylbenzene ND 1.0 1 ug/L
Carbon Disutfide ND 10 1 ug/L Styrene ND 1.0 I ug/L
Carbon Tetrachlodde ND 0.50 1 ug/L 1,1,1,2-Tetrachloroethane ND 1.0 1 ug/L
Chlorobenzene ND 1.0 1 ug/L 1,1,2,2-Tetrachloroetha ne ND 1.0 1 ug/L
Chloroethane ND 1.0 1 ug/L Tetrachloroethene ND 1.0 1 ug/L
Chlorofon~ ND 1.0 1 ug/L Toluene ND 1.0 I ug/L
Chloromethane ND 10 I ug/L 1,2,3-Trichlorobenzene ND 1.0 1 ug/L
2-Chlorotoluene ND 1.0 1 ug/L 1,2,4-Trichlorobenzene ND 1.0 1 ug/L
4-Chlorotoluene ND 1.0 1 ug/L 1,1,1-Trichloroethane ND 1.0 1 ug/L
Dibromochloromethane ND 1.0 1 ug/L 1,1,2-Tdchloroethane ND. 1.0 1 ug/L
'l,2-Dibromo-3-Chloropropane ND 5.0 1 ug/L Trichloroethene ND 1.0 1 ug/L
1,2-Dibromoethane ND 1.0 1 ug/L Trichlorofluoromethane ND 10 1 ug/L
Dibromomethane ND 1.0 1 ug/L 't ,2,3-Trichloropropane ND 5.0 1 ug/L
1,2-Dichlorobenzene ND 1.0 1. ug/L 1,2,4-Trimethylbenzene ND 1.0 1 ug/L
1,3-Dichlorobenzene ND 1.0 1 ug/L 1,3, 5--Trimethylbenzene ND 1.0 1 ug/L
1,4-Dichlorobenzene ND 1.0 1 ug/L Vinyl Acetate ND 10 1 ug/L
Dichlorodifluoromethane ND 1.0 1 ug/L Vinyl Chloride ND 0.50 1 ug/L
1,1-DlchJoroethane ND 1.0 1 ug/L p/m-Xylene ND 1,0 1 ug/L
1,2-Dlchloroethane ND 0.50 I ug/L o-Xylene ND 1.0 1 ug/L
1,1-Dichloroethene ND 1.0 I ug/L Methyl-t-Butyl Ether (MTBE) ND 1.0 1 ug/L
c-l,2-Dichloroethene ND 1.0 I ug/L Tert-Butyl Alcohol (TBA) . ND 10 I ug/L
t-1,2-Dichloroethene ND 1.0 I ucj/L Diisopropyl Ether (DIPE) ND 2.0 I ug/L
1,2-Dichloropropane ND 1.0 1 ug/L Ethyl-t-Butyl Ether (ETBE) ND 2.0 1 ug/L
1,3-Dichloropropane ND 1.0 1 ug/L Tert-Amyl-Methyl Ether (TAME) ND 2.0 1 ug/L
2,2-Dichloropropane ND 1.0 I ug/L
Surrooates: _REC {%) Control Qual Surrofl. ates: REC (%) _Control Qual
Limits
Dibromofluoromethane 98 84-120 Toluene-d8 100 91-109
1,4-Bromofluorobenzene 99 84-108
RL - Repoding Limit , DF - Dilution Factor , Oual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427
· TEL: (714) 895-5494 · FAX: (714) 894-7501
als_cience
r_nvironmental
j aboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received: 01/13/04
Work Order No: 04-01-0549
Preparation: EPA 5030B
Method: EPA 8260B
Project: 2401 Oak Street, Bakersfield, CA Page 10 of
Lab Sample Date Date Date
C~ient Sample Number Number Collected Matdx Prepared Analyzed QC Batch ID
10
Parameter Result RI_ D_~F Qual
Acetone ND 10 t
Benzene ND 0.50 1
Bromobenzene ND 1.0 1
Bromochloromethane ND 1.0 1
Bromodichloromethane ND 1.0 1
Bromoform ND 1.0 1
Bromomethane ND 10 1
2-Butanone ND 10 1
n-Butylbenzene ND 1.0 1
sec-Butylbenzene ND 1.0 1
tert-Butylbenzene ND 1.0 1
Carbon Disulfide ND 10 1
Carbon Tetrachloride ND 0.50 1
Chlorobenzene ND 1.0 1
Chioroethane ND 1.0 1
Chloroform ND 1.0 1
Chloromethane ND 10 1
2-Chlorotoluene ND 1.0 1
4-Chlorotoluene ND 1.0 1
Dibromochloromethane ND 1.0 1
1,2-Dibromo-3-Chloropropane ND 5.0 1
1,2-Dibromoethane ND 1.0 1
Dibromomethane ND 1.0 1
1,2-Dichlorobenzene ND 1.0
1,3-Dichlorobenzene ND 1.0 1
1,4-Dichiorobenzene ND 1.0 1
Dichlorodifluoromethane ND 1,0 1
1,1 -Dichloroethane ND 1.0 1
1,2-Dichloroethane ND 0.50 1
1,1-Dichloroethene ND 1.0 1
c-1,2-Dichloroethene ND 1.0 1
t-1,2-Dichloroethene ND 1.0 1
1,2-Dichloropropane ND 1.0 1
1,3-Dichloropropane ND 1.0 1
2,2-Dlchloropropane ND 1.0 1
Surro,qates: REC (%) Control Qual
Limits
Dibromofiuoromethane 104 84-120
1,4-Bromofluorobenzene 104 84-108
Units Parameter Result RI.. DF Qual Units
ug/L 1,1-Dichloropropene ND 1.0 1 ug/L
ug/L c-1,3-Dichloropropene ND 0.50 1 ug/L
ug/L t-1,3-Dichloropropene ND 0.50 1 ug/L
ug/L Ethylbenzene ND 1.0 I ug/L
ug/L 2-Hexanone ND 10 1 ug/L
ug/L Isopropylbenzene ND 1,0 1 ug/L
ug/L pqsopropyltoluene ND 1,0 1 ug/L
ug/L Methylene Chlodde ND 10 1 ug/L
ug/L 4-Methyl-2-Pentanone. ND 10 I ug/L
ug/L Naphthalene ND 10 I ug/L
ug/L n-Propylbenzene ND 1,0 I ug/L
ug/L Styrene ND 1.0 I ug/L
ug/L 1,1,1,2-Tetrachloroethane ND 1.0 1 ug/L
ug/L 1,1,2,2-Tetrachloroetha ne ND 1.0 1 ug/L
ug/L Tetrachloroethene ND 1.0 I ug/L
ug/L Toluene ND 1.0 1 ug/L
ug/L 1,2,3-Trichlorobenzene ND 1.0 I ug/L
ug/L 1,2,4-Trichlorobenzene ND . 1.0 I ug/L
ug/L 1,1,1-Tdchloroethane ND 1.0 I ug/L
ug/L 1,1,2-Tdchloroethane ND 1.0 1 ug/L
ug/L Trichloroethene ND 1.0 1 ug/L
ug/L Trichlorolluoromethane ND 10 1 ug/L
uglL 1,2,3-Trichloropropane ND 5.0 I ug/I.
uglL 1,2,4-Tdmethylbenzene ND 1.0 I ug/L
ug/L 1.3,5-Trimethylbenzene ND 1.0 1 ug/L
ug/L Vinyl Acetate ND 10 1 ug/L
ug/L Vinyl Chloride ND 0.50 1 ug/L
ug/L p/m-Xylene ND 1.0 I ug/L
ug/L o-Xylene ND 1.0 1 ug/L
ug/L Methyl-t-Butyl Ether (MTBE) ND 1.0 1 ug/L
ug/L Tert-Butyl Alcohol (TBA) ND 10 I ug/L
ug/L Diisopropyl Ether (DIPE) ND 2.0 1 ug/L
uglL Ethyl-t-Butyl Ether {ETBE) ND 2.0 1 ug/L
ug/L Tert-AmyI-Methyl Ether (TAME) ND 2.0 1 ug/L
ug/L
Surroqates: REC (%) Control
Toluene-d8 101 91-109
orting Limil , DF - Dilution Factor , Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427
Qual
· TEL: (714) 895-5494 · FAX: (714) 894-7501
~,~lscience
~ nvironmental
i_ aboratories, Inc.
Quality Control - Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project: 2401 Oak Street, Bakersfield, CA
Date Received: 01/13/04
Work Order No: 04-01-0549
Preparation: N/A
Method: EPA 120.1
Date Date Duplicate Batch
Quality Control Sample ID Matrix Instrument Prepared: Analyzed: Number
l~i;~;~il;.::.;;.;:~.:i..i:~:'~:~!:::i:.'::.:..¢ ,:.:.i'.:..::. ;'.. ;=::' :i. ,i;':,:. . :.:; :~:.-i.i':::'!:;' '. '?: ,,~::'" '""" i, · ':, "" :;'::,, ;;i; .... ,' '
Parameter Sample C0nc DUP Conc ~ RPD CL
Specific Conductance 950 960 1 0-25
7440 Lincoln Way, Garden Grovel CA 92841-1427 · TEL: (714) 895-5494 ·
Qualifiers
FAX: (714) 894-7501
· ~nvironmental Quality Control - Duphcate
I j~aboratories, Inc.
_
I Blaine Tech Services, Inc " Date Received: 01/'13/04
20360 Gramercy Place Work Order No: 04-01-0549
· Torrance, CA 90501-1511 Preparation: N/A
[] Project: 2401 Oak Street, Bakersfield, CA Meth°d:, EPA 130.2
I Duplicate Batch
· Quail' Control Sam le ID Matdx In trument Date Date Number
[Y p S~ Prepared: Analyzed:
Parameter Sample Oonc DUP Conc RPD PD L Qualifi~r~
I Hardness, Total 98 96 2 0-25
I~~ 7440 Lincoln Way, Garden Grove, CA g2841-1427
· TEL: (714) 895-5494 · FAX: (714) 894-7501
I
. ~alscience
~nvironmental
~--ab°ratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project: 2401 O
Quality Control Sample ID
Parameter
Quality Control - Duplicate
2401 Oak Street, Bakersfield, CA
Matrix
Samole Conc
6.22
Date Received: 01/13/04
Work Order No: 04-01-0549
Preparation: N/A
Method: EPA 150.1
Date Date Duplicate Batch
Instrument Prepared: Analyzed: Number
Dup C0nc,. RPD RPD CL
6.22 0 0-25
Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841:1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
~.~aiscience
~_nvironmental
~.~ aboratOries, Inc.
Quality Control - Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project: 2401 Oak Street, Bakersfield, CA
Date Received: 01/13/04
Work Order No: 04-01-0549
Preparation: N/A
Method: EPA 150.1
Date Date Duplicate Batch
Quality Control Sample ID Matrix Instrument Prepared: Analyzed: Number
t:i~i~i~);ii!~ ;?!?.~:' ii;'.~! ii:. :i:! ii f':.i,!'.?:-i:i': :~. ?~': ?:' !.:, :i: i: i:i.?.~!i:~-"~: :.:i' ::' :' :i: ?!'f.'-:~.:.!~i:.'.~:~'~i~i!: i:i;i'?i~ii.i~!~.~ ;.': !...:.o~,!.,~,,,~:-. '..: ..,,,r~.~'",~:,. '1
Parameter Sample Cea3_q_ DUP Conq RPD RPD CL~
pH 6,51 6,53 0 0-25
Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427
· TEL: (714) 895-5494 · FAX: (714) 894-7501
~r_als_cience
EEpvironmental
[J~ aboratories, Inc.
Quality Control - Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project:
2401 Oak Street, Bakersfield, CA
Date Received: 01/13/04
Work Order No: 04-01-0549
Preparation: N/A
Method: EPA 160.1
Date Date Duplicate Batch
Quality Control Sample ID Matdx Instrument Prepared: Analyzed: Number
Parameter Sample C0nc DUP Conc RP._..._~D RPD CL, .qualifier~
Solids, Total Dissolved 270 270 0 0-25
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
~alscience
~-__nvironmental
~r---aboratories, Inc.
Quality Control - Spike/Spike Duplicate
Blaine Tech Services, Inc
20360 Gramercy PEace
Torrance, CA 90501-1511
Project: 2401 Oak Streetr Bakersfield~ CA
Quality Control Sample ID Matrix
Date Received: 01/13/04
Work Order No: 04-01-0549
Preparation: N/A
Method: EPA 300.0
Date Date MS/MSD Batch
Instrument Prepared Analyzed Number
Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers
Chloride 100 98 50-150 2 0-25
Nitrate (as N) 101 101 50-150 I 0-25
Sulfate 98 96 50-150 1 0-25
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
~F._nvironmental Quality Control - LCSILCS Duplicate ~ aboratories, Inc.
Blaine Tech Services, Inc Date Received: N/A
20360 Gramercy Place Work Order No: 04-01-0549
Torrance, CA 90501-1511 Preparation: N/A
Method: EPA 300.0
Project: 2401 Oak Street, Bakersfield, CA
Date Date LCS/LCSD Batch
Quality Control Sample ID Matrix Instrument . Prepared Anatyzed Number
Parameter LCS %REC LCSD %REC %REC CL RPD RPD CL Qualifier~
Chloride 101 100 80-120 1 0-25
Nitrate (as N) 102 102 80-120 0 0-25
Sulfate 102 104 80-120 2 0-25
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
Caiscience
~.~ n vironmental
~ aboratories, Inc.
Quality Control - Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project: 2401 Oak Street, Bakersfield, CA
Quality Control Sample ID
Date Received:
Work Order No:
Preparation:
Method:
Date Date
Matrix Instrument Prepared: Analyzed:
01/13/04
04-01-0549
N/A
EPA 351.3
Duplicate Batch
Number
Parameter ~.ample Conc DUP Conc RPD RPD CL
Total Kjeldahl Nitrogen 0.56 0,56 0 0-25
Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
~nvironmental Quality Control - Duplicate
~- aboratories, Inc.
,,
'
Blaine Tech Services, Inc Date Received: 01/13/04
20360 Gramercy Place Work Order No: 04-01-0549
Torrance, CA 90501-1511 Preparation: N/A
Method: SM 2320B
Project: 2401 Oak Street, Bakersfield, CA
Date Date Duplicate Batch
Quality ~trol Sample ID Matrix Instrument Prepared: Analyzed: Number
........ :..::.. ............... ~ ;. ~,.~ ................................. .... ......... ~..., ~.,..,,;,. ..... ......~.,.....:.; ;:.~.,.. ........ ~.: ~:.. ..... ..:.~.....::..:... .......... ,...:........:':,O~:~Ad<
Parameter. Sample Conc DUP Conc RPD RPD GL Qualif~r~
Alkalinity, Total (as CaCO3) 56 54 4 0-25
Bicarbonate (as CaCO3) 56 54 4 0-25
Carbonate (as CaCO3) ND ND NA 0-25
Hydroxide (as CaCO3) ND ND NA 0-25
I .
/~/~j~/J~ j~ ~j~ 7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 ·
FAX: (714) 894-7501
~alscience
~, nvironmental
-~- aboratories, Inc.
Quality Control - Spike/Spike Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project: 2401 Oak Streetr,BakersfieldI CA
Quality Control Sample ID Matrix
Date Received:
Work Order No:
Preparation:
Method:
Date Date
Instrument Prepared Analyzed
01 / 13/O4
04-01-0549
EPA 3010A Total
EPA 601 OB
MSIMSD Batch
Number
Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers
Lead 98 97 80-120 1 0-20
7440 Lincoln Way, Garden Grove, CA 92841-1427
· TEL: (714) 895-5494
FAX: (714) 894-7501
I
~_n vironmental
I ~aboratories, lnc.
I Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
I Project: 2401 Oak Street, Bakersfiefd, CA
I Quality Control sample ID
I Parameter
Lead
I IrCo;~cium
Magnesium
Sodium
I
I
I
i
I
I
I
I
Quality Control - LCS/LCS Duplicate
Date Received:
Work,Order No:
Preparation:
Method:
N/A
04-01-0549
EPA 3010A Total
EPA 6010B
Date Date LCS/LCSD Batch
Matrix Instrument Prepared Analyzed Number
101
100
99
98
102
96
95
LCS %REC LCSD %REC %REC CL RPD RPD CL Qualifier8
101 80.120 ~1 0-20
100 80-120 0 0-20
99 80-120 0 0-20
98 80.120 0 0-20
101 80-120 O 0-20
98 80-120 2 0-20
97 80-120 2 020
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
~_aiscience
~F-_nvironmental
#~ aboratories, Inc.
Quality .Control - Spike/Spike Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project: 2401 Oak Street~ Bakersfield~ CA
Quality Control Sample ID Matrix
Date Received: 01/13/04
Work Order No: 04-01-0549
Preparation: EPA 5030B
Method: DHS LUFT
Date Date MS/MSD Batch
Instrument Prepared Analyzed Number
Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers
TPH as Gasoline 90 93 70-112 4 0-17
I
I
I
7440 Lincoln Way, Garden Grove, CA92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
· ~a!science
~.nvironmental
~-aboratories, Inc.
Quality Control - Spike/Spike Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project: 2401 Oak Street~ Bak,e[$field~ CA
Quality Control Sample ID Matrix
Date Received: 01/13/04
Work Order No: 04-01-0549
Preparation: EPA 5030B
Method: DHS LUFT
Date Date MS/MSD Batch
Instrument Prepared Analyzed Number
Parameter MS %REC MSD %REC %REC CL RP,D RPD CL C~ualifiers
TPH as Gasoline 86 90 70-112 4 0-17
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
~,-_als_cience
~vironmental
~.- aboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-15t 1
Quality Control - LCS/LCS Duplicate
Project: 2401 Oak Street, Bakersfield, CA
Date Received: N/A
Work Order No: 04-01-0549
Preparation: EPA 5030B
Method: DHS LUFT
Date Date LCS/LCSD Batch
Quality Control Sample ID Matrix Instrument Prepared Anaryzed Number
I:..~~.!~!,.~.,:. ,i~:~i.:.i~. !~: '", :,i? i:.;i~:.:.::?,~!,.. ?i~.~a~i:.~:...?;~!, i? !,~,~,~'.3~ i..:.~?.:. :,::: ..~,~.~:[.~ .. i:~ .i.., ~?ii~ ii:,:~i~i: ~.-::" :'i' :.?~"~,,, '. i."' -...~ ~:: ']
Parameter LCS %REC LCSD %REC. %REC CL RPD RPD CL Qu~31ifiers
TPH as Gasoline 98 96 72-114 1 0-10
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
~.nvironmental
i~l..aboratories, lnc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project: 2401 Oak Street, Bakersfield, ,,CA
Quality Control Sample ID Matrix
Parameter
TPH as Gasoline 96
Quality Control - LCS/LCS Duplicate
LCS %REC
Date Received: N/A
Work Order No: 04-01-0549
Preparation: EPA 5030B
Method: DHS LUFT
Date Date LCS/LCSD Batch
Instrument Prepared Analyzed Number
LCSD %REC %REC CL RPD RPD CL Qualifiers
96 72-114 '1 0-10
7440 Lincoln Way, Garden Grove, CA 92841-1427
· TEL: (714) 895-5494 · FAX: (714) 894-7501
alscience
_nvironmental Quality Control - LCS/LCS Duplicate
aboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project: 2401 Oak Street, Bakersfield, CA
Date Received: N/A
Work Order No: 04-01-0549
Preparation: EPA 5030B
Method: - EPA 8260B
Date Date LCSfLCSD Batch
Quality Contmt Sample 1D Matrix Instrument Prepared Analyzed Number
Parameter
Benzene
Carbon Tetrachloride
Chlorobenzene
1,2-Dichlorobenzene
1,1-Dichloroethene
Toluene
Tdchtoroethene
Vinyl Chloride
Methyl-t-Butyl Ether (MTBE)
TeK-Butyl Alcohol (TBA)
Diisopropyl Ether (DIPE)
Ethyl.t-Butyl Ether (ETBE)
Tert-AmyI-Methyl Ether (TAME)
Ethanol
LCS %REC LCSD %R. EC %REC CL RPD RPD CL
96 96 67-117 0 0-5
103 101 77-137 2 0-9
98 98 89-113 0 0-5
99 99 90-114 0 0-8
108 104 81-129 4 0-15
98 97 BB-118 2 0-71
100 98 67-121 1 0-21
101 99 71-131 3 0-34
104 97 65-125 6 0-49
110 95 38-140 15 0-98
96 93 77-119 2 0-53
100 98 73-121 2 0-31
99 96 71 - 119 3 0-33
101 90 54-132 12 0-55
Qualifiers
7440 Lincoln Way, Garden Grove, CA92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
,I
!
I
I
I
I
I
I
I
I
~-aiscience
~F-n_vironmentai Quality Control - LCS/LCS Duplicate
E--aboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project: 2401 Oak Street, Bakersfield, CA
Date Received: N/A
Work Order No: 04-01-0549
Preparation: EPA 5030B
Method: EPA 8260B
Date Date LCS/LCSD Batch
Quality Control Sample ID Matrix Instrument Prepared Analyzed Number
Parameter LCS %REC L¢$D,%REC %REC CL RPD RPD CL
Benzene 94 94 87-117 1 0-5
Carbon Tetrachlodde 109 107 77-137 I 0-9
Chlorobenzene 98 100 89-113 I 0-5
1,2-Dichlorobenzene 100 100 90-114 1 0-8
1,1 -Dichloroethene 113 106 81-129 6 0-15
Toluene 96 97 88-118 I 0-71
Trichlor0ethene '103 105 67-121 2 0-21
Vinyl Chloride 97 90 71-131 8 0-34
Methyl-t-Butyl Ether (MTBE) 103 106 65-125 2 0-49
Ted-Butyl Alcohol (TBA) 84 89 38-140 5 0-98
Diisopropyl Ether (D[PE) 94 92 77-119 2 0-53
Ethyl-t-Butyl Ether (ETBE) 101 101 73-121 1 0-31
Tert-AmyI-Methyl Ether (TAME) 98 99 71-I 19 1 0-33
Ethanol 70 93 54-132 27 0-55
Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
~-alscience
~--- _n vironmental
· ~--aboratories, inc.
Quality Control - Spike/Spike Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
2401 Oak Street~ Bakersfield~ CA
Project:
Quality Control Sample iD Matrix
Date Received: 01/13~04
Work Order No: 04-01-0549
Preparation: EPA 5030B
Method: EPA 8260B
Date E~ate M~/~SD B;tch
Instrument Prepared Analyzed Number
Parame. ter MS %REC MSD %REC %REC CL RPD RPD CL Q~ualifiers
Benzene 94 95 84-120 0 0-13
Carbon Tetrachloride 102 106 72-132 3 0-15
Chlorobenzer{e 98 99 87-117 I 0-12
1,2-Dichlombenzene 98 99 86-116 I 0-13
1,1-Dichloroethene 106 104 77-137 I 0-15
Toluene 96 96 85-121 0 0-15
Trichtoroethene 99 100 66-120 1 0-13
Vinyl Chloride 96 99 68-140 3 0-'~6
Methyl-t-Butyl Ether (MTBE) 98 106 68-128 7 0-18
Tort-Butyl Alcohol (TBA) 97 119 30-156 21 O-Z6
Diisopropyl Ether (DIPE) 92 94 75-123 3 0-14
Ethyl-t-Butyl Ether (ETBE) 98 102 66-132 4 0-33
Tert-AmyI-Methyl Ether (TAME) 96 100 59-131 4 0-47
Ethanol 91 108 20-176 17 0-42
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 ·
FAX: (714) 894-7501
J rnvironmental Quality Control - Spike/Spike Duplicate
Blaine Tech Services, Inc Date Received: 01/13/04
20360 Gramercy Place Work Order No: 04-01-0549
Torrance, CA 90501-1511 Preparation: EPA 5030B
Method: EPA 6260B
Project: 2401 Oak Street, Bakersfield, CA ,
Date Date MS/MSD Batch
Quality Control Sample ]D Matrix Instrument Prepared Analyzed Number
Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers
Benzene 95 93 84-120 2 0-13
Carbon Tetrachl0ride 111 105 72-132 5 0.15
Chlorobenzene 100 99 87-117 1 0-12
1,2-Dichlorobenzene 99 99 86-116 0 0-13
1,1-Dichloroethene 117 108 77-137 8 0.15
Toluene 94 95 85-121 0 0-15
Trichloroethene 104 104 66.120 0 0-13
Vinyl Chloride 98 96 68-140 2. 0-16
Methyl-t-Butyl Ether (MTBE) 106 104 68-128 2 0-18
Ted-Butyl AlcohoJ (TBA) 84 95 30-156 13 0-26
Diisopropyl Ether (DIPE) 95 91 75-123 4 0-14
Ethyl-t-Butyl Ether (ETBE) 102 99 66-132 3 0.33
Tert-Amyl-Methyl Ether (TAME) 97 97 59-131 0 0-47
Ethanol 72 79 20-176 10 042
I~ 7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
~_als_cience
~-_ nvironmental
~ abOratories, Inc.
Glossary of Terms and Qualifiers
Work Order Number: 04-01-0549
Qualifier Definition
D
E
ND
The sample data was reported from a diluted analysis.
Concentration exceeds the calibration range.
Not detected at indicated reporting limit.
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494
· FAX: (714) 894-7501
WORK ORDER #:
Cooler I of /
SAMPLE RECEIPT FORM'
CLIENT:~ ~~_._,~ ~
TEMPERATURE - SAMPLES RECEIVED BY:
CALSClENCE COURIER:
~ Chilled, cooler with temperature blank provided.
cchilled, cooler without temperature blank.
hilled and placed in cooler with wet ice.
__ Ambient and placed in cooler with wet ice.
__ Ambient temperature.
_._~_ o C Temperature blank..
CUSTODY SEAL INTACT:
Sample(s): __ Cooler:__ No (Not In~act) '
LABORATORY (Other than Calscience Courier):
__ ° C Temperature blank.
° C IR thermometer.
SAMPLE CONDITION:
Yes
Chain-Of-Custody document(s) received with samples ......................... ~ ....... __
Sample container label(s) consistent with custody papers ..................... ,,~--~.. ...... __
Sample container(s) intact and good condition ........ ~ .......................... ~. ...... __
Correct containers for analyses requested ......................................... / .......
Proper preservation noted on sample label(s) .......................... · ........... f
Tedlar bag(s) free of condensation ..........................................................
COMMENTS:
__ Ambient temperature.
Initial:
Not Applicable (N/A):
Initial:
No
N/A
SHELL Chain Of Custody Record
~.b,,er~,,~,on (,r ~=~): Shell Project Manager to be invoiced: ......
.................. ..~... ............ ~..
Blaine Tech Se~lces, Inc. BTST 2401 Oak Street, Bakersfield Pending
20360 Gramercy Place, Torrance, CA 90501-15~1
~CT co~c~ ~-~v ~"~.~ ~}: Brltney O underso~ 626-256-66~ b~underson~d~l~aenv.com BTS
TURNAROUND TIME (~SINESS DAYS):
~ to ~AYS ~ ~A~ D ~ ~OU~ ~ ~ HOU~ D ~ HOUND LE~T~N ~ ~OU~ REQUESTED ANALYSIS
~ ~-RW~B RE.ATilT ~ U~AG~: Genera[ Minerals
' ' ~ - ~ FIELD NOTES:
GC/MS MT~ CONFIR~ON:. HIGHE~ ~HIGHE~ per ~Rl~ , ~L ~ ~ ~ ~ ~ Co.~iner~r.e~ative
SPECIAL INSTRUCT~NBO~'NoTEs: 'CHECK~XIFEDDIS~EED~ ~ [ ~ ~ ;~ ~ ~ ~ ~ or PlO Readlngs
HN~ poly's were fleta filtered prior to prfle~ation ; .- .° ~ ' ~ --~ ~ ~ ~ or Labomto~ Not.
~.~[~Field Sample IdentEication M~.~
.... . ._
SHELL Chain Of Custody Record
Lab Identlfic~tlon (1! necessary): Shell Project Manager to be invoiced:
Blaine tech Se~lces, Inc. BTST 2401 Oak Street, Bakersfield Pending
. "' ~: " '- I ~0~T~.o~'
20360 Gramercy Place, Torrance, CA 90~1-1Sll ' ,
mo~m ~T (~v ~ ~ ~e~ ~): Briery Gunderson 626-256~662 bgunderson~delt ~nv.com JBTS
Nick Sudano s~P~ ~u~ {~: .
310-782-2465 310-782-2958 nsudano~blainet ech.com ~[~ ~
TURNAROUND TiME (BUSIN~S~ DAYS):
~ [0 DAYS ~ 5 DAYS ~ ~ HOU~ ~ 48 HOU~ ~ ~4 ~U~ ~S~ 2~ ~U~ REQUESTED ANALYSIS
~ ~ - R~ RE~RT ~AT ~ U~ AG~: Genial Minerals
B~SMTaE~NFIR~TION:HIGHE~ HIGHE~.rBOR, NG .... ~L .... ~ ~ ~~ ~ FIELD NOTES:
SPECIAL INSTRUCTIONS OR NO~S: ' CH~CK ~X IF E~ IS ~ NEEDED ~ ~ ~ ~ -: g ~ ~ { ,. Conainar~r. ew~lVOor PlO readings
'Must state whether bicarbonate Is reposed as elthe~ calcium car~n~e [
DATE ~ME
~:~'~
DISTRI~TION: ~i/e ~ ~1 t~ ~ean t0 Far. Y~10w ~n( ~ lO ~OR~