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HomeMy WebLinkAboutRISK MANAGEMENTRisk Management and Prevention Plan ARGO CHEMICAL TABLE OF CONTENTS PART ONE---PURPOSE I. Purpose II. III. IV. CERTIFICATION Introduction Certification Revision RecOrd. ,Page 1 Page 2 Page 3 Page 4 II. -III. IV, V. PART TWO---RMPP Background Description of AHM Accidents .Equipment Report ............ Procedures Report ...... . .... Design, Operating & Maintenance Control Systems ....... VI. Detection, Monitoring, or Automatic Control Systems VII. Proposed Risk Reduction Measures VIII. Emergency Plans 'IX. X. XI. XII. Auditing:Programs Inspection Programs RMPP Implementation RMPP Recordkeeping "Page 1 Page,t5 Page 7 Page'8 Page.9 Page 10 Page. Il Page 14 page 16 Page 17 Page 18 20 PART THREE---HAZARD IDENTIFICATION 'II. III. IV. Purpose Physi'cal Data for Sulfuric Acid Unloading Procedures Hazard Identification Page 1 ,Page 2 :Page 3 ,Page 4 i ARGO CHEMICAL TABLE OF CONTENTS PART FOUR---RISK AND COSEQUENCE ANALYSIS III. IV. VI. purpose- Risk Analysis Matri× Risk Analysis of Equipment Failure Page 1 Page 3 Page 4 Consequence Analysis of Equipment Failure .... Page 5. Risk Analys'is o'f Human Failure Consequence Analysis of Human failure Conclusion-' Page 6 Page 7 Page 8 PART FIVE---APPENDIX I. Emergency.Action Plan II. ARCttIE Model Results-- III R'isk Analysis Matrix IV. Unloading o'f Hazardous Chemical Form 'V. Safety Meetings .Schedule 199:5 VI. Materlal Safety Data Sheet VIIi. Hazardous Material Management Plan VIII. Safety Equipment Checklist (Monthly) Page 1 Page 10 Page 20 Page 21 Page 22 -LPage 23 --Page 27 page 30 O _~. 0 ARGO CHEMICAL 'Risk Management and Prevention Plan I. pUrpose The Risk Management and Prevention PI'an of Argo Chemical is designed to evaluate the facility in handling Acutely Hazardous Materials (AHM) identified by the Administering Agency, minimize any releases of AHM, and to protect public health and safety and the environment from releases that do occur. -The main emphasis of the RMPP is on total system safety and reliability. -1- ARGO CHEMICAL II. Introduction The RMpp .has 'been requested pursuant to Section 25534 of Chapter 6.95 Article 2 of the California.Health & Safety Code by the City of Bakersfield Fire Department to reduce the risk of and'prevent accidents involving AHM. A Risk.Management and PreVention Plan (RMPP) is defined as all of the operational and administrative programs of a business which are designed to prevent releases of AHM, including, but not limited to, programs on design safety of new and existing equipment, safe operating procedures, istandard operating procedures, preventive maintenance programs, 'operator training and accident investigation procedures, risk assessment for unit operations or operating alterna'tives, emergency response planning, and internal or external audit procedures .to ensure that these programs are 'being executed as planned. This definition is used 'in the State of California, Governor's Office of Emergency Services document entitled "Guidance for the Preparation of a Risk Management and Prevention Program, November 1989. This RMPP is based upon Argo Chemical's use of concentrated sulfuric acid and chlorine gas. -2m ARGO CHEMICAL III. Certification Section 25534 (j) of the Cali'fornia Health & Safety Code requires that the RMPP and any revisions be certified as complete by a qualified person and the facility operator. Section 25532 (.f).of the California Health & Safety Code defines a qualified person is qualified to attest, at a minimum, to the validity of the hazard and operability studies done pursuant to Section 25534, and the relationship 'between the corrective steps taken by the handler following the studies and those hazards which were identified in the HazOp studies. I', Roland Mater, safety consultant, certify to the validity of this RMPP document as pursuant to the requirements of Section 25534 of Chapter 6.95 of the'California tealth & Safety Code. Roland Maier-~-Safety Consultant 'Steve Schmedding---Operations Manager ARGO CHEMICAL IV. Revision Record Revision # Pages Affected Date of Revision Signature of Person Making Revision ARGO CHEMICAL Background A. General Business Information Name and Location a. : Argo. Chemical Company, Inc. 100 Quantico Ave. Bakersfield, California 93307 (805) 322-2222 Nature of business a. . Argo Chemical is an industrial chemical distributor, specializing in water treatment and cleaning solutions. -Blending of'chemicals is.provided for special applications. Description of AHM Used Chlorine-Gas a. Argo has elected to modify the handling 'procedures to offloading the product rather than storage on the property. .The cylinders will be 'transferred to the delivery trucks from the supplier's 'trucks and taken to the clients. There will not be any storage-of the cylinders' at our facility. There will be storage of the empty chlorine cylinders, until the subsequent transfer of full Cylinders and the empty cylinders wil'l be returned to the supplier. The empty cylinders will be clearly marked and stored in a cylinder basket with chains to bind the cylinders· b. This procedure takes place approximately twice a month and consists of 10 (150 lb) cylinders each delivery. This method has been discussed with the AA. '2. Concentrated Sulfuric Acid(93%) a. Sulfuric acid is a highly corrosive, clear, colorless to' cloudy liquid. It causes severe burns or irritation on skin contact. Sulfuric acid is not flammable but highly reactive with water and : organic materials with evolution of heat. Reacts with many metals, releasing hydrogen. Since sulfuric acid has a minimal risk of exposure due to the vapor pressure of <lmmHg @ 100 F., the primary concern is from the liquid: Sulfuric acid has complete solubility in water. ARGO CHEMICAL Sulfuric acid is subject to the reporting requirements of the Superfund Act of 1986. There is approximately one load delivered each month with '3000 gallons delivered. A spill or release which equals or exceeds 42 gallons of liquid, is a significant, reportable release. II. ARGO CHEMICAL Description of AHM Accidents A. .Accidents at this Facility An employee was burned on his leg with sulfuric acid on July'lB, 1991 at the Argo facility. He was filling drums from the tanker truck when he overfilled the drum and the acid contacted his leg. Inadequate personal protection was worn at the time of the accident. The employee was wearing the 'acid resistant boots with an overcoat. This was the required protection .at the time of the accident. However, because of 'the incident, acid resistant.pants were added to the personal protective clothing to alleviate any openings in the overcoat/boots arrangement. The underlying.causes o.f the accident were: a. Too much pressure on the discharge hose when filling the drums. b· Not enough personnel involved in the process. c. The repetitive nature of the task causing human error. d. Inappropriate personal protective clothing' with the overcoat· Measures taken to prevent occurrences: a. ·Gravity,flow tankers to discharge the liquid. b. More personnel involved in the process, a stand-by, someone to assist with moving the discharge hose, and the truck driver. c. Requiring the full acid suit when unloading along with goggles, face shield, and boots. d. Safety meeting held before unloading of sulfuric acid to familiarize personnel with product, safety procedures, responsibilities of each person, and to handle any concerns that may arise. Accident Investigation Procedures a..When the cause of the'accident .has been determined, a method Shall be developed to ensure that the accident will not recur. b. System designs, operating and maintenance procedures that need updating or alteration shall be noted, and a time schedule set'for implementation of improvements. -5- ARGO CHEMICAL Source of-Historical Accident Data a. Argo's in-house data is being used. Since its inception in 1980, Argo has approximately 260,000 manhours worked with 1 injury concerning sulfuric acid. b. These manhours are based on an average of 45 hrs/wk and 51 weeks per year. Release reporting procedures a. Pursuant to Section 25507 of Chapter 6.95 Article 1 of the California Health & Safety Code, releases of AHM that may threaten human life, health, and safety or the environment or exceed the reportable quantity must be reported. When a reportable release occurs, the following people must be notified immediately: 1. Bakersfield City Fire Department Hazardous Material Division (805.) 326-3979 2. CA Office of Emergency Services' (800) 852-7550 b. The Safety Director is responsible for reporting a release· ARGO CHEMICAL III. EquiPment Report A. Nature, Age, & Condition The supplier of the sulfuric acid uses their own trucks and trailers which are under their safety, program guidelines. The vehicles meet all applicable laws and regulations pertaining to their use, through DOT and CHP inspections which are required by law. The supplier assures Argo that these inspections are part. of their on-going safety program. A copy of the inspections are kept on the vehicle during operation. a. The hoses and valves are inspected prior to. each load being delivered. b. The drivers go through a thorough safety program upon employment, to insure safety awareneSs. The supplier of the poly-drums, which are intended for highly corrosive acid use, are tested, maintained, and certified by the supplier according to the applicable regulations and guidelines set forth by.'the appropriate regulatory agency, which is the Department of Transportation. These are maintained by Waymire Drum as part of their safety program. -7- ARGO CHEMICAL IV. Procedures Report Offloading procedures The Safety Director conduct"§ a safety meeting .prior to.the offloading of the concentrated sulfUric acid. This is essential to review with the employees the hazards associated with sulfuric acid and the offloading procedures. The MSDS is reviewed during'the meeting. The tanker truck delivering the product is a bottom-dump gravity flow tanker and it arrives @ 6:00 AM to alleviate the heat. This allows the sulfuric acid to stay relatively cool and the employees to work more effectively. All employees involved with the offloaffing are required to wear appropriate personal protective equipment: a. Full acid-resistant suits consisting of pants and overcoat b. Rubber boots c. Hard hats with face shield and chemical goggles Breaks are generally taken after six (6) drums are filled, but earlier if necessary. Each of the employees involved in the offloading are taught all of the various tasks involved. This allows for better job awareness, less complacency due to the repetitive nature of the tasks, and more knowledge for hazard identification and correction.-, The truck driver of the product also is involved in the safety meeting, required to wear the appropriate safety apparel, and maintain a stand-by position at the truck. The offloading takes place outside of the wareh6use. The sulfuric acid is transferred into 55 gallon poly drums, banded and stored on pallets. -8- ARGO CHEMICAL Design, Operating & Maintenance Control Systems A. The offloading Procedures used by Argo to offload sulfuric acid and store empty chlorine gas cylinders do not necessitate any design controls. Operating controls 1. Appropriate labeling of the poly drums. Safety meetings reiterating job awareness and safety. Rotating personnel to the various tasks associated-with the off loading procedures. Maintenance of equipment is the responsibility of the suppliers and is verified by the Safety Director by inspection documentation by the supplier. The safety equipment is maintained on a' monthly basis· An employee is assigned .to inspect all of the safety equipment monthly, completing any repairs, cleanings, or adjustments necessary. The forklifts are checked daily by the operators and annually are serviced by the manufacturer's service representative. Each of the drivers have attended a certification Class by the forklift distributor and will attend any refresher courses required. -9- ARGO CHEMICAL VI. Detection, Monitoring, or Automatic Control Systems 'A. Primarily, the detection and-monitoring system is facilitated by the uSe of a flotation device placed down in the drum approximately 6 inches below the top of the drum." The flotation device, usually cork or rubber, is attached to a wire that forms a triangle which is placed on the top.of the bung opening. As the liquid contacts the.flotation device, the liquid is swirling, the triangle will move around noticeably and the employee shuts off the valve stopping the flow of sulfuric acid into thedrum. Bo Ce Secondarily, the detection and monitoring system is facilitated by the use of a stand-by person as an integral part of the procedure. The truck driver is also used in this capacity. There is not an automatic control device applicable in'the offloading procedures used by Argo Chemical. -10- ARGO CHEMICAL VII. PropoSed Risk Red¢ction Measures A', Written Operating Procedures All employees are trained in the offloading procedures as part of the orientation and on-going-safety program. Ail employees involved and the truck driver conduct a safety meeting prior to offloading the liquidl This helps to ensure a safe and efficient offloading occurs. The safety program applies to sulfuric acid and chlorine gas. B. Increased Inspections An inspection is completed after each unloading by the Safety Director. A review of the procedures is part of the agenda of the Safety Committee. A review by'a safety consultant is completed once a year to ensure the. validity and efficiency of the program. Labeling 1. :Labeling and warning signs are an effective means-of communicating hazards to new employees and/or visitors to the facility. Emergency responders will need to know the contents and types of materials present'at the facility. Argo Chemical meets the guidelines for the appropriate Right-to-Know laws· De Safety & Training Program Employees will receive training under the safety program. Program is described in Section XI. ,2. Release prevention and emergency response training will .reduce the risk of releases and minimize the consequences of releases -11- ARGOCHEMICAL Fire Prevention Plan Employee safety training Housekeeping practices to remove combustible materials Fire extinguishers "No Smoking" signs are posted where appropriate Reduction of Consequence to Neighboring Homes or Businesses 1. Because of the low vapor pressure (< lmmHg @ 100 degrees F), there is a negligible risk to neighboring homes and businesses. To lessen any chance, .only qualified-and trained employees, are authorized to assist in the offloading of the sulfuric acid. The release of any sulfuric acid would be retained in the containment basin and would be neutralized by soda ashland plenty of wa'teri.~ Essentially no atmospheric dispersion occurs for unheated sulfuric acid as the ARCHtE air dispersion model depicts (the referenced model is located in the appendices). ARGO CHEMICAL Sulfuric Acid (SA) Training Required / Date Completed Emp 1 oyee Name I I I I i SA IResp. Hand 1 i ng I Fire Safety I Emerg.l Evac.l Spilll I Notif.l Proc.l Proc.l ! I I I I I I ! I I I I I I I I I I I I I I I I + 4. I I I I I I I I I I I I I I I I I I I I , I I I I I I I I I I I I I I ~- + 4- I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I 1 I I I I I I I I I I -I I I ! I I I I I I I I I I I I I I I I I -I I I I I I I : ........ q 4. ~ 4. 4. + I I I I I I I I I I I I I I I 1 4. 4- ...... + I I I I I I I I I I I + 4- ...... + I I I I I I 1 I I I I I I I I 4' 4- ...... -I' I I I I I I I I I I I I I I I I I I I I I I I ! I I I I I I I I I I I I I I I I I '1 I I I I I I I I I I I I I I I I I t + 4. I I I I I I I I I I I I ARGO CHEMICAL VIII. Emergency Plans Argo Chemical has reviewed the Cai-OSHA-standards (CCR, Title 8, SeCtions 3220 and 3221), and has implemented the required emergency action and'fire prevention measures. General evacuation procedures are to be' used whenever there is an emergency situation occur. All employees and visitors-to the facility are to cooperate and comply with the evacuation procedures and go to the designated check-in area. The specific steps are in the emergency plan located in the appendix of this document. D. Fire and/or Earthquake Use water spray only to keep fire-exposed container cool. Do not use a solid water stream near ruptured container. Significant Spills '3. Cleanup procedures for a sulfuric acid release will mitigate the'effects of the release. a. Sulfuric acid is soluble in water at all proportions b. Soda ash (1:1 ratio) and lime (2:1 rKtio) will neutralize sulfuric acid c. Dilute with plenty of water d. During a release, the Safety Director will attempt to stop the leak, if possible in a safe manner e. The in-house vacuum pump will not be used" for these spilIs During the neutral'ization phase of the cleanup, water should be sprayed in a heavy mist rather than a steady stream. The asphalt in the unloading area is bermed and slOped to troughs which run to the containment basin. The containment basin will hold 5000 gallons of liquid. This should be enough to allow cleanup procedures to begin. There is usually 10 pallets of soda ash and 4 pallets of lime in stock at all times (1 pallet = 2400 lbs.) ARGO CHEMICAL In all emergency situations, the Safety Director will follow the procedures outlined in the Emergency-Plan. Since all of the employees are aware of the Emergency Plan, anyone may start the evacuation procedures to begin. The Safety Director and. the managers.are the on!'y ones authorized to. call in a cleanup contractor. Emergency Responders When a reportable release occurs, the following people need to be notified immediately: 'a. Bakersfield-City Fire Department Hazardous Materials Division Telephone (-805) 326-3979 b. California Office of Emergency Services Telephone (800) 852-7550 -15- ARGO CHEMICAL IX. Auditing Programs 'The purpose of the auditing system is to ensure the sulfuric acid procedures are operating and maintained in a manner that provides the minimum risk to employees, the general public, the environment, 'and the public safety. B. Other goals of the auditing system are: Pinpoint actual and potential safety.hazards due to design~, location, operation, and maintenance of the sulfuric acid processes. .2. Provide a means of Objectively defining needs for fiPgiading and modifying. Provide a means of objectively assessing and documenting plant safety. 4. Provide' feedback on safety issues. Ce The Argo Chemical sulfuric acid audit will be done on a yearly basis and will be an integral part of the Argo Safety Committee agenda. After each unloading, the Safety Director inspects the safety equipment to verify it functioned properly and was cleaned and stored.' All of the safety equipment is inspected monthly as part of.the audit system. This form is listed in the appendix. -16- ARGO cHEMICAL Inspection Program An inspection program is necessary for the asseSsment of hazards present in the facil!.ty duri'ng the offloading process. The person responsible must be familiar with the process and procedures being scrutinized. Hazards, deficiencies, unusual observations or occurrences must be recognized and recorded during the inspection. Potential hazards identified through. the inspection will be assessed and assigned priorities for correction. Action will then be taken to reduce the risk presented by the identified hazards according to the prioritization completed. The Safety Director is responsible for inspecting the facility during the offloading and transporting of the sulfuric acid. C~ The inspection mechanism is an on-going process used after each unloading of the sulfuric acid takes place. Do A monthly inspection by a qualified employee. assures that all of the safety equipment is functioning properly and ready for use. E e. Annually a consultant will inspect the safety .equipment, auditing system, .offloading procedures, and all phases of the safety program at ARGO. -.17.-. ARGO CHEMICAL XI. RMPP A. Implementation Personnel ReSponsible for RMPP Implementation 1. The title of each 'person responsible for RMPP implementation duties are listed below, along with their .respective responsibilities: Title RMPP Implementation Responsibilities Operating Manager Safety Director All Employees Supervise audits, inspections, and recordkeeping, responsible for RMPP implementation Supervise operating and maintenance training, emergency response training, inventory control and labeling Complete emergency response.and evacuation training B. Implementation Schedule Pro~ram Inspection Program Sulfuric Acid Audit RMPP Recordkeeping Safe Operating ProcedUres Training Evacuation Training Emergency Response Training Labeling Respiratory Elimination CYlinder Training of' Full Chlorine Storage Date of Full On-Going July 1992 July 1992 May 1992 Implementation April 1992 July 1992 On-Going August 1992 January 1993 -18- ~60 CHemICaL Training Program for R~PP implementation The R~PP training Program must ensure that standard operating procedures are easily understood by all affected employees. Training should be able~t° provide a continuity of safety despite employee turnover or changes in personnel. Training ensures that programs and plans will work effectively as designed when they are utilized. -19- ARGO CHEMICAL XII. RMPP Recordkeeping B. Recordkeeping, required by RMPP legislation. ( Chapter 6.95, Section 25534), ensures that the RMPP programs are implemented and maintained. Accident Reports Documentation of accidents is necessary to prevent reoccurrence. This is a means of identifying potential hazards, though, not the most efficient method. Argo Chemical's safety program would rather be pro-active than reactive. Training records Training records will be kept to ensure that each employee receives required training. All employees must be trained in evacuation procedures, emergency response, and handling of the AHM. Affected employees need more specific training in the offloading and. handling procedures associated with the sulfuric acid. D~ Audit Records The audit records are necessary to ensure that .the operating , maintenance, and training procedures and programs are providing, the minimum risk to the employees, the general public, the environment, and the public safety. By using the audit records, effective assessment and evaluation processes can initiated. This is also'an opportunity for the Argo Chemical and the AA to evaluate the effectiveness of the entire program. Inspection Records Inspection records should be made on a regular basis to ensure that appropriate safety features are operational. The results-of all inspections are analyzed to identify deviations from safe operations and to Supplement safety audits. -20- ARGO 'CHEMICAL Safety Meetings Warehouseman and truck drivers, those employees involved in the unloading of the sulfuric acid, have safety meetings every 10 working days ~nd before EACH load of acid is unloaded. Management, salespeople, and office personnel not directly involved with the unloading of the acid. have safety meetings every'quarter and are aware of the unloading process. -21- ARGO CHEMICAL RMPP--Hazard Identification .The Risk Management and Prevention Program of Argo Chemical is designed to evaluate the facility in handling Acutely Hazardous Material's (AHM) identified by the Administering Agency, minimize any releases of AHM, and'to protect public health and safety and the environment from releases that do'occur. The main emphasis of the RMPP is on total system safety and reliability. The RMPP has been developed for the risks and risk environment at the Argo Chemical facility at 100 Quantico Ave., Bakersfield, California. The AHM (Acutely Hazardous Materials) identified by theAdministering Agency (AA) are concentrated sulfuric acid and chlorine Sas.. The chlorine sas requirement for the RMPP has been substantially reduced in response to the modifications previously discussed with the AA. The first phase of the RMPP, hazard identification, will address only the concentrated sulfuric acid. The purpose of the hazard identification is to identify possible accidents, releases, and spills of the AHM. The procedural recommendations for development of the hazard and operability studies are based on those set forth in the. 19.85 Guidelines for Chemical Hazard Evaluation Procedures prepared. by the Center for Chemical Process Safety of the American 'Institute of Chemical Engineers (AIChE). The "What-if" and Human Error analyses are being used for this pro.cess. This hazard identification process is for concentrated sulfuric acid Sulfuric acid is a highly corrosive, clear, colorless to Cloudy liquid. Sulfuric acid causes severe burns or irritation on skin contact. If ingested, can cause irritation and severe burns to throat, mouth, and stomach. Inhalation of fumes or mists can cause irritation or corrosive burns to the upper respiratory system. Long-term exposure to high levels··of acid fumes may cause erosion of teeth followed by jaw necrosis, bronchial irritation, coughing, and bronchial pneumonia, or gastrointestinai disturbances. Sulfuric acid is not flammable but highly reactive and capable of igniting f-inely divided combustible materials on contact. Reacts violently with water and organic materials with evOlutioq...of heat. Extremely hazardous in contact with many materials, particularly carbides, chlorates, fulminates, nitrates, pictrates, powdered metals and other combustibles. Attacks many metals, releasing hydrogen. -1- ARGO CH£MICAL The physical data for concentrated sulfuric acid, or oil of vitriol, is it contains approximately 93.2% by weight of H2SO4 by weight (CAS No. 7664-93'9). T. he OSHA P£L is lmg/M3 and the ACGIH TLV is lmg/M3. The. reportable quantity is 1000 lb./454 kg. Sulfuric acid is subject to the reporting requirements' of section 313 of Title III of t.he Superfund Amendments and Authorization Act of 1986 and 40 CFR part 372. The molecular weight is 98.08, boiling point is 529 degrees F approx., and the melting point is -20 degrees' @93% and 30 degrees @ 98%. Specific gravity is 1.835-1.844, vapor density is 3.4, and vapor pressure for 78% - 100% is less than 1 mmHg @ 100 degrees F. Sulfuric acid has complete Solubility in water. Personal protective equipment should be worn at all times when handling this material. At A~go Chemical, employees who handle this material are trained in handling concentrated sulfuric acid by the Safety Director. An MSDS is discussed prior to handling. During the unloading of the concentrated sulfuric acid, each employee is wearing full protective suits, rubber'gloves, headgear with face shield and goggles. These are the safety instructions required of all employees handling this material. Sulfuric acid should be protected from physical damage.. Store in a cool, well-ventilated area away from combustibles and reactive chemicals. Keep containers in upright pos'ition. If a leak or spill occurs, dilute small leaks cautiously with plenty of water. Neutralize with alkali such as soda ash or lime. Adequate ventilation is required for soda ash NEUTRALIZATION due to release of CO2 gas. Major spills must be diked and neutralized with soda ash. Do not wash into . storm or Sanitary sewer system. Disposal of sulfuric acid is subject .to Federal, State and local regulations. · Concentrated sulfuric acid is EPA hazardous'waste No. D002 (corrosive) if discarded. At Argo. Chemical concentrated sulfuric acid is transported to the Bakersfield facility by tanker truck. There is appr'oximately one load delivered each month from the supplier. The Supplier generally uses their own chemical truck or provides another transport vehicle. Argo Chemical requests gravity-flow, bottom dump transport tanker trucks to deliver the material to their facility. This facilitates less pressure on the discharge hose. E~g.h_~load.is appr0~imately...3.000 gallons and is_deli'vered..at 6.:O0'AM when ~"'~emp~rature is cooler and it is safer to deliver. ........ · -Each of the emplOyees dnloading the material are wearing acid_resistant protective Suits, rubber gloves and boots, safety face shields and goggles. The employees are required to review the MSDS before unloading the material. This is accomplished by having a safety meeting before the material is unloaded to review all"the pertinent safety information and Company safety rules. The Safety Director conducts the meeting. ARGO CHEMICAL In identifying the hazards associated with concentrated sulfuric acid, the release and spill of the material is of primary concern. Since sulfuric acid has a minimal risk of exposure from fumes and gas, due.to the vapor pressure of <1 mmHg @ 100 degrees F., the primary' concern is from the liquid. The liquid presents a hazard to the employees when unloading the material from the truck. When the truck is being unloaded, there are various ways that a release of the chemical could occur. The procedures for the unloading of the truck are part of the safety program at Argo Chemical.. When the bottom-dump tanker truck pulls into the facility, it is intentionally planned for 6:00 AM to lessen the effect of the heat on the chemical. The truck driver is required to stay by the discharge valve at the bottom of the tanker. The driver is required to wear personal protective equipment as are the employees unloading the material. The truck provides a fifteen (15) foot hose, two (2) inches in diameter, which is manufactured for sulfuric acid use. At the end of the acid unloading hose is a stainless steel ball valve to regulate the amount of liquid being dispensed. An Argo employee handles the hose at the ball valve to regulate the flow and to. shut off when'the individual drums reach the desired amount. Another employee helps this individual move the hose from a position of'five (5) feet up-stream of the ball valve at the discharge end of the hose. This individual is responsible for the majority of the actual lifting and moving of the hose. This allows the employee handling the valve at the end of the hose to direct his attention to the unloading of the material. Both of these employees are wearing full acid-resistant pants and jackets, rubber gloves, rubber boots, hard hat with full face shield and chemical goggles to facilitate the safety of the people involved. A third employee is. strictly a stand-by, watching the operation from a safe distance. This employee is responsible for observing the operation for any splits or ruptures in the hose, drums or leaks from the valves. He is capable of notifying the driver to shut-off the main discharge valve at the tanker. There is a fourth employee that removes the full drums after sealing the drum-by inserting the bung. This employee also brings in empty drums to be filled. The drums are loaded on a pallet before they are filled. After the drums are filled and sealed, they are then banded together and removed by forklift to the storage area. The third and fourth employees are also wearing the appropriate personal protective equipment as the two employees handling~the discharge hose. Each of the employees will take. a turn at each of the tasks involved in unloading the tanker truck to gain the necessary knowledge of identifying any areas where there could be possible hazards and for job awareness. ARGO CHEMICAL The employees take a break after six drums are filled, generally, but sooner if warranted for 'safety. All of the unloading procedures are done outside of the warehouse, to the south of the facility, to allow more access for the forklift. This also is near the access to the spill containment basin. At Argo Chemical sulfuric acid is not dispensed in any mixing or blending operations. The operations are limited to filling of the. barrels, storage and delivery to the clients. The concentration of the liquid remains constant with the delivered proportion. The.hazards identified with the equipment during the unloading procedures are: I. Main discharge valve 3. 4. 5. Chemical hose (2") Ball valve at the end of the discharge hose Poly-drum used for the sulfuric acid Forklift . The hazards associated with human error during the unloading procedures are: 1. Failure to manipulate the valves Failure to observe a hazard by stand-by Overfilling the drums 4.. Poor forklift oPeration There are hazards associated with the storage and delivery of the concentrated 'sulfuric acid. Duri'ng the normal storage time of the liquid, on pallets in poly-drums specifically for acid use, the drums are sealed and stored outside the warehouse. The material is loaded on the flatbed trucks by forklift for delivery to the customers. The drums are unloaded by'customer., if they have their own forklift, or by drum doily. The Argo truck drivers are trained and certified in the use of forklifts. They have a MSDS in their trucks for concentrated sulfuric acid on all deliveries. They are required to.wear a hardhat with face shield, chemical goggles, rubber gloves and rubber boots. It is not required to wear the acid-resistant suits unless there is a spill or leak. During the loading and/or unloading of the poly-drums of concentrated sulfuric acid, there is the chance .of forklift operator error. The forklift fork could strike the.side of the drum. The drums are manufactured to absorb this type of operational error. The. drums are inspected and -4- ARGO CHEMICAL certified by the manufacturer periodically. The hazard of the c'rushed nutshells, identified in an earlier correspondence, being stored adjacent to the sulfuric acid has been..alleviated by removing the hazard to a safer location on the northwest side of the property. This should remove the possible chance of combustion between the nutshel'ls and the sulfuric acid ~in the case of a spill or release. '- '' In the. eVent-of a natural disaster, as identified in the Emergency Action Plan, the procedures would be the same for sulfuric acid. The main emphasis would be placed on earthquake and fire emergency scenarios. In the case of an earthquake, there wOuld be minimal damage to the poly-drums of sulfuric'acid. The drums are banded together on pallets and they have enough flexibility to endure a major earthquake. The employees would call 911 and evacuate the area and allow the emergency responders to assess the damage and plan an appropriate course of action. In the event that an immediate response was not possibl'e, ihe Safety Director and the management would assess the situation and attempt to minimize any immediately dangerous situation until'the emergency personnel could-arrive at the facility. In the event .of a fire at the Argo facility, 911 Would- be initiated and the area would be evacuated in the proximity of Ihe fire..' Argo's emergency action plan woUld be initiated. Water is located at various locations at the facility, inside and outside the warehouse. The drums of ~sulfuric acid are approx, sixty (60) feet from the warehouse and one hundred twenty (120) feet from the stor'ed flammables. Water would be sprayed on the drums of sulfuric acid to minimize the effect of the heat on the sulfuric acid. '.The response time of the Virginia Ave. Fire st'ation has been very short and this should minimize most of the catastrophic situations which may occur. -5- ARGO CHEMICAL RMPP--Risk and. Consequence Analysis The Risk` Management'and Prevention Program of Ar$o Chemical is designed to evaluate the facility in handling Acutely Hazardous Mat. erials (AHM) identified by the Administering Agency (AA), minimize.any releases of AHM, and to protect public health and safety and the environment.from releases that do occur. The main emphasis of the RMPP is on total system safety and reliability. The RMPP has been developed for the risks and risk environment at the Argo Chemical facility at 100 Quantico Ave., Bakersfield, California. The AHM identified by the AA .are concentrated sulfuric acid and chlorine gas. The chlorine gas requirement for the RMPP has been substantially reduced in response to the modifications previously discussed with the AA. The risk and consequence analysis, as the hazard identification did, will address only the concentrated sulfuric acid. The purpose of the risk and consequence analysis'is to examine and/or prioritize potential accidents in terms of their probability of occurrence, to evaluate the consequences and impacts associated with the occurrence of the accidents, and to combine these results to provide a measure of overalt risk associated with the accident scenarios being studied.. The risk and consequence analysis permits examination and/or prioritization of accident scenarios in terms of overall "risk". The hazard identification process identified various hazards'associated with equipment failure and human error during the unloading and handling of the concentrated sulfuric acid. The'hazards identified with equipment failure during the unloading procedures are: I. Main discharge valve 2. Chemical Hose 3. Ball valve at the end of the discharge hose 4. Poly-drum used for storage of sulfuric acid 5. Forklift The hazards associated with human error during the unloading procedures are: 1 Failure to manipulate the valves 2. Failure to Observe a haZard by stand-by Observer 3. Overfilling the drums Poor forklift operation ARGO.CHEMICAL Probabil'istic assessment of accident potential can provide a good idea of the.likelihood that a potential accident will actually take place. At Argo Chemical we have looked-at the hiStorical accident data to develop a safety and heal'th program which has addressed many of these scenarios a few years ago. Assessing the hazards associated with equipment failure in the unloading of the concentrated sulfuric acid assisted in the safety guidelines used to unload the AHM. Initially , the AHM was unloaded by pressurizing the tanker truck and pumpi'ng the concentrated sulfuric'acid into poly,drums with 5-15 lbs. of pressure; This process unloaded the tanker substantially quicker, yet proved to be more hazardous to the employees unl.oading'the AHM. Because of this, Argo Chemical decided to .request gravi, ty'~flow, bottom dump transport vehicl.es. This "new" procedure exposes the workers longer to the concentrated .sulfuric acid, yet in a less hazardous environment. There were .procedures developed to alleviate the time spent actually exposed to the sulfuric acid while unloading. More employees were used to unload the AHM and training became an' integral part of-the'unloading process. - Acid releases from the tanker could be a maximum of 3000 gallons if the dr. iver could not manipulate the discharge valve on the tanker outlet. An acid release from the fifteen feet hose woulfl conStitute 40 gallons and could be neutralized by soda ash and diluted With water. Any .. reportable release of sulfuric acid, that could be diked, would be. washed into the concrete containment basin that has a capacity of 4500 gallons. The appropriate agencies would be contacted and disposal procedures wouild be initiated with the consultation of the agencies responding. The ARCHIE program was used to assess the vapor dispersion and fire impacts associated with releases of concentrated sulfuric acid into the environment, specifically the ARGO Chemical facility. The explosion impacts were not applicable to sulfuric acid. The results of the model are in the appendix of this document. -2- Attachment' 1 RISK ANALYSIS MATRIX LOW MEDIUM HIGH Severity of.-'Consequences Due to AHM Combinations of Conclusions From Risk Analysis that Identify Situations-of Major Concern Combinations that Identify Situations of Considerable Concern Combinations of Concern Which may Require Planning for Cr6dible Events Release (From RMPP Guidance for the PreParation of a Risk Management and Prevention prOgram, November, 1989, California Office of Emergency Services.) LOW: MEDIUM: HIGH: QUALITATIVE DEFINITIONS OF PROBABILITY OF OCCURRENCE : Probability of occurrence considered unlikely during thc expected lifetime of the facility assuming normal operation and maintenance. Probability of occurrence considered possible during the expected lifetime of thc facility. Probability of occurrence considered sufficiently high to .assume event will occur during the expected lifetime of thc facility LOW: MEDIUM: HIGH: .DEFINITIONS OF SEVERITY OF CONSEQUENCES TO PEOPLE Chemical is expected to move into thc surrounding environment in negligible concentrations. Injuries expected only for exposure over extended periods or when individual personal health conditions create complications. , Chemical is expected to move into thc surrounding environment in concentrati°ns sufficient to cause serious injuries and/or deaths unless prompt and cffcctive corrective action is taken. Death and/or injuries expected Only for cxpbsurc over extended periods or when individual pc~rsonal health conditions created complications. Chemical is expected to move into thc surrounding environment in concentrations sufficient to cause serious injuries and/or dcaths upon exposure. Large numbers of pc.opic expected to bc affected. (From the EPA Technical Guidance for Hazard Analysis, 1987) ARGOCHEMICAL Assessing the-various accident scenarios'which may take place during un'loading, with respect to equipment failure, and the consequences assOciated with each of the individual areas of concern is of primary.concern to Argo Chemical. Using the "What-if" approach.to address the aforementioned equipment failures: What-if Main discharge valve closed or clogged Main discharge valve will not close Chemical hose leaks Ball valve closed or clogged Ball valve will not close Poly-drum leaks Forklift malfunctions Risk Analysis Consequence Product will not- discharge Product'will.'discharge Product will disCharge Product will not discharge Product will discharge Product will spill Product may Spill Probabi 1 ity Low ' I ! I I Low , I Low ' , I I Low ' I Low ' I , I. Low ' , I Low ' Assessing the various scenarios individually, the main discharge valve is checked before and after each load is delivered by the supplier. Also, with the new regulations and much-needed emphasis on chemical safety, the trucks are being equipped with an internal pneumatic shut-off valve which helps to mitigate a catastrophic spill. The hoses and ball valves are also checked before and after eaCh load by the supplier,and again here at ARGO by the Safety Director. With new technology concerning poly-drums, they are made safer. When we complete a drum the bung is inserted in the drum and the six full drums are banded before being moved. The forklift is maintained on a daily basis by ARGO's employees and periodically by the manufacturer's service representative. -4- ARGO' CHEMICAL Analyzing each of the consequences, on-site and off-site, produces the following results: I I I I What-if Main discharge.valve closed or clogged Main discharge valve will not close Chemical hose leaks Bal'l valve closed or clogged Ball valve wil,1 not close Poly-drum leaks Forklift malfunctions On-Site Consequence Low Medium Low Low Low Low Low Off-S te Consequence Low! Medium Low Low Low Low Low Since sulfuric acid has a very low vapor pressure (0.004 mmHg @ 68 degrees F), there is negligible voltility and therefore a low rating for the on-site and off-site consequences, With the safety programs of ARGO Chemical.and their respective supPliers; SoCal Trucking and Scholle Corp. for the sulfuric acid, Waymire Drum for 'the poly-drUms and PowerLift for the forklift, and the "new" strength of the chemical safety legislation and laws, there is reason to state that is unlikely an equipment failure would occur. In'the case of a major spill at the facility, where the possibility of fillin~ the containment basin would exist, Argo has a sump pump that would remove excess precipitation from the secondary containment basin. Also, the spill would be diked immediately to allow flow into the containment basin without the need for excess water. As the Archie program depicts, a 25,000 sq. f.t. evaporation pool size would include the paved surface and the containment basin. The appropriate agencies would assist in the cleanup and disposal of the spilled liquid. Furthermore, as the ARCHIE model predicts dispersion distances that do not exceed Argo's property line, a vulnerability zone diagram will not be necessary. ARGO CHEMICAI, Addressing the hazards associated with human error by usi~,,' the "What-if" a~o' ~n- a~h ,,:ith the human erro~~ technique ~o analyze the inherent hazards during t'he unloading of the concentrated sulfuric acid produces the following results: Wh'a t-i f Failure to manipulate the valves 'Failure to observe by stand-by Overfilling the d I' il Ill ~ Poor forklift opera t ion Cons eqllence Product will not discharge Product will discharge Product will discharge Product wilt spill from drum Probabi 1 i Low Low Med i um Low Becuse of ARGO's training program and new unloading procedures, ~v'hict~. were mentioned-in the RMPP section of this document, there is justification to state that it is unlikely a ~,pii!.l wi-Il occur b:~cause of' human error. [['he pre-unloading safety meeting which identifies and reviews all of' the tasks involved and the hazard:--, associated with each, should greatly mitigate any human error during the unloading phase. Secondly, thc tr~in[ng of the emp!c, yees in the hazards associated with sulfuric acid, reviewing the MSDS, having morc frcquent breaks az, deemed nece:.,sary, and the use of the personal protective wear also helps reduce the chance of a spi I 1, ARGO CHEMICAL;!}~ Analyzing each of the consequences, on-site and off-site, produces the following results: What-if Failure tc: manipulate the valves Failure to observe bi' stand-by Overfill. ins the drums Poor forklift epera t ien On-Site Coils equence L o w '.. Low Off-Site Consequence Low Low Med i um Low Lo w Low I 1 l + Sulfuric acid has a very low vapor pressure (0.004 mmHg no a~mospheric dispersion occurs for unheated sulfuric acid. Sulfuric acid is soluble in water in ail proportions. If sulfuric acid is spilled, it is neutralized with soda ash and diluted with plenty of wa~er. The on-site and off-site consequences wout~ '¢,~ minimal and ne~"i*ible respectively -7- ARGO CHEMICAL:~., An effective training program can alleviate many of the problems associated with human error failure. A safety meeting prior to the.unloading process identifies these hazards and alerts the employees to the consequences associat'ed with the hazards. The Safety Director informs each of the employees involved with the unloading process of their respective duties initially. Each of the tasks will be performed by all of the employees involved. The truck driver is notified of his duties and responsibilities. The employees are rotated through ail of the jobs to offset any loss of. concentration .due to the repetitiveness of the task. The MSDS is covered during the safety.meeting by the Safety Director. At Argo Chemical, we are confident these safety meetings help. insure the safety of our employees. Breaks taken by the personnel.involved are initiated-by any -person feeling a break is needed for safety reasons. The Safety Director is in the area during the unloading to insure every detail is being covered. An on-going maintenance and trai.ning program are integral components of an effective safety program. All of our employees are trained in the use of a forklift by a certified instructor. The forklifts are serviced regul, arly and inspected prior to use daily. Each of the employees are trained in CPR/ First Aid and in-the use of the various' respirators used on our site. The training program is essential to our business, as the safety of our employees is our main concern and priority. The probability of a sulfuric acid'release due to human error was found to be minimal. The supervised transfer of the liquid from the tanker to the drums and the safety procedures reduced the risk of a release or spill. Qualified, well-trained personnel also reduced the risk of human errors in normal, maintenance, and emergency operations at the Argo Chemical facility. It must be realized, however, that the most frequent'types of spills or discharges have .relatively minor consequences, and that more serious accidents will generally have lower probabilities of' occurrence. In summary, the probability of a major or minor §pill or r'elease of' sulfUric acid at Argo Chemical's facility would be minimal.~-.The severity of consequences from a sulfuric acid rTl-ease or spill are expected to be low. '--8-- WA S HIN(.i'I'I'~ l'! AL STREET YAMPA ST WI ~ICO EASTER ltASI. E1 I AV I. OIJEI_I A DR AVE TA ST ~Rt. JSHST m m COURT I']1 HEIVEYST z InO REVERLEY ! HATES AVE ,>BURNETT£ -1- P M( LAII ST AVl:. ST ARGO CHEMICAL EMERGENCY ACTION.PLAN our Emergency Action Plan has been designed to ensure employee safety'in the event of a major disaster. The Safety Director shall.review all aspects of this plan at least once each year, and shall ensure that the plan has been properly communicated to all employees. Further, all aspects of our plan shall be reviewed periodically by the Safety Committee, who shall make necessary revisions, additions, and deletions a.s needed. Our current Emergency Action Plan encompass the following elements: 1 Fire 2 Earthquake 3 Facility Damage 4 Flooding 5 Vapor Release / Substance Spill 6 Transportation or Equipment Accident 7 Any Immediate Danger to Safety and Health Any changes'made to the overall plan or to any element of the' plan shall be posted on the Company "safety board" for a period of thirty (30) days and discussed at all safety meetings. ARGO CHEMICAL Facili'ty Evacuation Procedures In the' event of an emergency that requires 'an evacuation, basic procedures need to be followed at all times: 1. The Safety'Director, .Tim Quinn, is responsible to initiate the evacuation pro.cedures. 2. Call 911 as sOon as. possible, from the facility, if safely able to, or from the designated check-in location. 3~ Under normal conditions, the chain of authority for purposes.of .initiating an evacuation are: a. Safety. Director, Tim Quinn b. owners, Steve Schmedding or Mark Rodgers c. Any employee aware of the need Circumstances requiring an evacuation include, but are not limited to: a. Fire/smoke b. Flood Earthquake Toxic (Chemical) spill; gases, fumes, etc. Explosion Structural damage Any immediate danger to health and safety Onca a decision has been made to order an evacuation, every possible means may be used to announce the initiation of 'the "company evacuation procedure". This includes, but is not limited to: a. Public address system (phone) b. Portable/stationary radio system Audible/electronic alarm system Person-to-person/word of mouth Any other means available -2- ARGO CHEMICAL During an evac'uation, al'l persons~on company property and/or within company facilities are to cooperate and comply immediately· Persons outside the facility-are to remain outside the structures, and are to assemble in .the designated check-in area. Persons inside the facility are to leave the premises, without delay, by using the nearest available exit, or a safe alternate exit (posted near each lobby and work area is an exit.plan). All employees are to leave the facilities in a calm and orderly manner,' and once outside, they are to assemble in the designated check-in area. The designated check-in area will be in the front of the property (Quantico Ave. side), at the NE corner. If that location is not safe, the alternate check'in area will be the SE corner of the property. The supervisory staff will be responsible for recording the number of employees present and report this information to the Safety Directors. a.. .Steve Schmedding .... warehouse personnel b. Mark Rodgers marketing-personnel c. -Faye Tillman office personnel Once all employee counts have been received, and if that count fails to correspond to the number of employees on duty. a roll call shall be initiated to identify those missing. Every attempt shall be made to ascertain the last known location of Person(s) not accounted for. This information shall be relayed to the Safety Director, Tim Quinn, so that rescue operations can be initiated at the earliest possible opportunity. Rescue operations will ONLY be initiated with the help of the responding, local authorities. If injured persons have been identified on-site, first aid shall be administered by a certified first-aid employee awaiting the arrival of outside emergency services. -3- ARGO CHEMICAL 11. If all personnel have been accounted for and no injur'ies exist, the Safety Director shall survey the situation, evaluate the circumstances,'and prioritize the actions to be taken, with a focus on CONTROL- CONTAINMENT-CONFINEMENT!! 12. Re-entry into the facility will not be authorized until approved by local authorities and/or Safety Director. 13. KeeP.main entrances to the work area clear of people so that emergency vehicles will have quicker access to the emergency. . '14. The Safety Director will be responsible for assuring that the water, gas and electrical main shut-offs are closed and any other potential hazards are shut off or neutralized, .if safely possible. Do not allow untrained employees to participate in the control of the emergency. The following is additional information for specific disasters and/or'emergencies: - EARTHQUAKE: The actual movement of the ground in an earthquake is seldom the direct cause of injury or death. Most casualties result from. falling objects and debris , such as falling plaster or steel and-flying glass. If indoors, stay away from windows and get under a table, desk or stand in a corner. If outdoors, move to an open area away from buildings, trees, walls, and powerlines. If. driving, stop and stay in your vehicle until the shaking stops. Avoid stopping near trees, powerlines and overpasses. Also, be aware there will be after-shocks as nearly as powerful as the original quake. FLOODING: If a workplace becomes flooded, move to higher ground. If outside, do not try to drive through a flooded area. If inside,.turn off all electrical equipment and evacuate the facility to higher'ground.- FACILITY STRUCTURAL DAMAGE: Structural damage may rupture a gas line or Shut off electrical power. ~If inside, evacuate the structure immediately AWAY from the damage. If outside, do not enter the damaged facility. If driving near the structure, pull over and stop. Turn off your engine, and evacuate the area. Remember to inform the Safety Director of the damage and any potenfial hazards near the structural damage. -4- 4'. ' ARGO CHEMICAL FIRE: · When a threat of fire occurs in any situation, evacuate to the designated check-in area. If inside a facility that is in flames move to the nearest exit to evacuate the area. If an employee becomes engulfed in flames DO NOT LET THEM RUN, lay'them down on the ~floor .or ground and wrap them in a jacket, fire blanket, throw rug, etc., and roll them on the surface to ext'inguish the flames. If an employee suffers burns, protect the area from contamination and keep them calm. There should be a certified first aid employee at the workplace that can assume the responsibilties for the care of the burned person until emergency personnel arive. Do not move the injured employee unless there is a threat of danger. .Again, contact the Safety Director or other authorized supervisory personnel to begin the company emergency procedures. TOXIC (CHEMICAL) SPILL OR RELEASE: GASES, FUMES, ETC. Early detection is crucial with a vapor release. The area is to be evacuated and evacuation.procedures initiated immediately. Identify the chemical, contact the local~ authorities, and consult the appropriate MSDS to become aware of the characteristics of the chemical. Do not attempt controlling the release without being trained and consulting the MSDS sheet. Shut off the source of the leak and evacuate downwind of the release. Do not attempt to dike, spray, or. sweep up a spill without being trained and consulting the appropriate MSDS sheet. · A substance spill requires specialized training for any form of control. Shut · off the source.of the spill, if possible, and evacuate downwind of the spill. TRANSPORTATION OR EQUIPMENT ACCIDENT: During a transportation accident the engine is to turned off and the vehlcle evacuated. If an employee becomes trapped inside or underneath a'vehicle or piece of equipment, the supervisor is to stay with the trapped employee and to send another employee to call the Safety Director to contact the' local authorities of the accident. if an accident occurs during the operation of a machine, the main Power switch to that piece of equipment is to'be shut off immediately. All employees not involved in the accident are to be evacuated from the area. The supervisor is to 'stay with the employee and send another employee to contact -the Safety Director. The Safety Director will contact the authorities and begin evacuation procedures for that area. '--5-- ARGO CHEMICAL FACILITY DISASTER PROCEDURES 'We recognize the possibility that a natural or man made disaster could occur at any time, with or without warning. We also recognize that a disaster may be so catastrophic that damage may occur to utilities, communication lines and transportation routes. Furthermore, the demand for emergency services (police- fire-medical-etc.) may be so overwhelming.that we may have to temporarily provide essential services ourselves. While our primary concern shall be for the safety and well-being of our own employees, if we are fortunate enough to receive outside aid in any.form, we shall accept it graciously and cooperate with regulatory and emergency service agencies completely. This includes, but is not limited to, assisting and supporting: Law enforcement personnel 2 Fire department personnel 3 Local and state government agencies 4 Ambulance, paramedic and medical personnel 5 Water, gas and electric company personnel 6 'CAL/OSHA, RCRA, NIOSH, or EPA officials and personnel 7 Red Cross personnel 8 Any 'ot'hers providing assistance To'the degree possible, the Safety Director shall be responsible for coordinating the response of emergency personnel from outside the facility. Other employees shall assume full responsibility for performing emergency assignments to the best of their ability, considering the existing circumstances. The' Safety Director, with-help and support from supervisory staff, shall first attempt to establish an emergency control center from which to organize operations, collect data and otherwise direct'essential activi'ties on a priority basis. While the following'list is a suggested guideline, the Safety Director will have the full authority for establishing his own priorities. / I. Evaluate the overall situation as quickly as possible. 2. Implement a facility evacuation, if appropriate. 3. Designate an Emergency Command center. ARGO CHEMICAL- o Mobilize first aid and .rescue teams. Establish/re-establish communications. Request outside emergency service, if available. Assess damage to utility systems, and shut down damaged/dangerous systems. Assign/reassign functions to employees, as necessary. Assess damage to hazardous materials and take appropriate action. Establish appropriate security measures. Re-evaluate damages. REMEMBER THAT OUR PRIORITY OBJECTIVE IS TO PROTECT LIFE AND SAFETY; NOT TO MINIMIZE PROPERTY LOSS AND DAMAGE!! SET PRIORITIES ACCORDINGLY!! -7- ARGO CHEMICAL METHODS FOR REPORTING EMERGENCIES · In the event'of an emergency at our facility, it shall be ~the responsibility of the person'observing or discovering the' emergency to ensure that the emergency is immediately reported to the appropriate person. If, for any r.eason, this is not possible, the reporting person shall immediately call 911 and explailn the nature of the emergency to the Emergency Operator. Be sure to remain on the phone, so that' you may provide both accurate and essential information. To summon an ambulance for a medical emergency dial 911. To summon Law Enforcement Emergency Assistance dial 911. To summon Fire'Department Emergency Personnel dial 911. Non-emergency phone numbers of importance: 3. 4. 5. 6'. 8. 9. 10. 11. 12. 13. 14. 15 16 17 18 19 20 21 22. 23. 24. 25. 26. 27. 28, 29. 30. 31. Arvin Substation KCSO 854-2211 Arvin Fire Depar.tment 854-5517 Arvin Animal Control 854-3134 Arvin Police Department ................. 854-3128 Bakersfield Police DePartment ........... 327-7'111- Bakersfield Fire Department .......... .--324-4542 Hazardous Materials Division 326-3979 Bakersfield CAL/OSHA ....... 395-2718 Bakersfield Dept. of Motor Vehicles ..... 395-2825 California Highway Patrol ..... 327-1069 CAL/OSHA Consultation (209)454-1295 Delano Police Department 725-3277 Kern County Sheriff's Department 861-3110 Kern County Fire Department ............. 861-2577 Hazardous Materials Division 861-2761 Kern County District Attorney 861-2421 Kern County Emergency Medical Services--861-3200 Kern County Environmental Services ...... 861-3636 Kern County Health Department ........... 861-3621 Kern County Mental Health Services 861-2825 Kern County Medical Center ............... 326-2000 McFarland Police Department 792-2121- Memorial Hospital 327-1792 Mercy Hospital 328-5223 San Joaquin Community Hospital 326-4107 Shafter Police Department ............... 746-6341 Shafter Fire Department ................. 746-3933 Taft Police Department .................. 763-3101 Taft Fire Department .................... 7-65-4136 Tehachapi Fire Department ......... 822-2240 -Tehachapi Substation KCSO 822-2222 Wasco Fire Department ........... 758-6448 Wasco Substation KCSO 758-5166 -8- ARGO CHEMICAL FACILITY FLOOR PLAN POLICY' If there are evacuation procedures initiated, ali employe'es who are in-the office area of the facility, shall evacuate the facility using the main entrance in the front of the building. I£ unable to exit through the front double doors,'then proceed to the door into the warehouse area and proceed to the nearest avai'lable exit door, either to the north, south, or east' After exiting the building, proceed to the check-in area at the NE corner of the facility. All employees in the warehouse area and yard areas will evacuate the area via the safest route away from the emergency, unless there have been specific directions given by the Safety Director. Immediately upon reaching the check-in area, evacuation procedures will be followed. A detailed floor plan drawing shall be marked to specifically identify the locations of all major safety points, including but not limited to: All exits All first aid equipment 3. All fire extinguishers and other fire equipment' 4. A'll alarms and alarm stations 5. All hazardous materials storage areas 6. All disposal locations (dumpsters, containers, etc.) Once completed, the diagrams shall be prominently affixed to key locations through-out the facility, reflecting escape and evacuation routes. !. In the lobby and reception area 2. In all secluded and isolated areas Adjacent to all common areas In all hallways, aisles, pathways, etc On the company "safety board" On all common bulletin/information areas HAZARDOUS MATERIAL ADDRESS \ LOCATION DATE OF ASSESSMENT NAME OF DISK FILE = sulfuric acid = 100 Quantico = 3-23-93 = ARGO2.ASF ******* DISCHARGE RATE/DURATION ESTIMATES Liquid discharge from nonpressurized container Average diScharge rate = 1732.2 lbs/min Duration of discharge = 26.'1 minutes Amount discharged = 45042 lbs State of material = Liquid ******* LIQUID POOL SIZE. ESTIMATES Evaporating pool area = 25000 ft2 ******* LIQUID POOL EVAPORATION RATE/DURATION ESTIMATES Vapor evolution rate ~= .013 Evolution duration = 3680082 lbs/min minutes ******* TOXIC VAPOR DISPERSION ANALYSIS RESULTS Downwind distance to concentration of 2 ppm -- at groundleve! = 36 feet N~te: Minimum computable, answer is 33 feet! Actual hazard distance may be less. See attached table(s) for further details. TOXIC VAPOR DISPERSION ANALYSIS RESULTS Downwind Distance (feet) (miles) Groundlevel Concentration (ppm). Source Height Concentration (ppm) Initial Evacuation Zone Width* (feet) 32 .01 2.5 2.5 130 33 .01 2.5 2.5 130 33 .01 2.5 2.5 130 33 .01 2.4 2.4 120 34 .01 2.4 2.4 120 34 .01 2.3 2.3 120 34 .01 2.3~ 2.3 120 34 .01 2.3 2.3 120 35 .01 2.2 2.2 .120 35 .01 2.2 2.2 110 35 .01 2.2 2.2 110 36 .01 2.1 2.1 110 36 .01 2.1 2.1 110 36 .01 2.1 2.1 99 36 .01 2 2 1 *Usually safe for < 1 hour release. Longer releases or sudden wind shifts may require a larger width or different direction for the evacuation zone. See Chapters 3 and 12 of the guide for details. Source height specified by the user for this scenario was 0 feet. TOXIC VAPOR DISPERSION ANALYSIS RESULTS Downwind Distance Contaminant Arrival Time Contaminant Departure Time at Downwind Location at Downwind Location (feet) (miles) (minutes) (minutes) gw__'- 32 01 .1 3680082 33 .01 .1 3680082 33 .01 .1 3680082 33 .01 .1 3680082 34 .01 .1 3680082 34 .01 .1 3680082 34 .01 .1 3680082 34 .01 .1 3680082 35 .01 .1 3680082 35 .01 .1 3680082 35 .01 .1 3680082 36 .01 .1 3680082 36 .01 .1 3680082 36 .01 .1 3680082 36 .01 .1 3680082 CAUTION: See guide for assumptions used in estimating these times. INPUT PARAMETER SUMMARY PHYSIOCHEMICAL PROPERTIES OF MATERIAL NORMAL BOILING POINT = MOLECULAR WEIGHT LIQUID SPECIFIC GRAVITY VAPOR PRES AT CONTAINER TEMP VAPOR PRES AT AMBIENT TEMP TOXIC VAPOR LIMIT 529 degrees F = 98.08 = 1.8 = .001 psia = .052 mm Hg = .0011 psia = .052 mm Hg = 2 ppm CONTAINER CHARACTERISTICS CONTAINER TYPE TANK DIAMETER TANK LENGTH TOTAL WEIGHT OF CONTENTS LIQUID HEIGHT IN CONTAINER DISCHARGE HOLE DIAMETER DISCHARGE COEFFICIENT OF HOLE = TEMP OF CONTAINER CONTENTS = = Horizontal cylinder = 4.2 feet = .40 feet = 45042 lbs = 1.9 feet = 2 inch(es) 1 75 ~' degrees F ENVIRONMENTAL/LOCATION CHARACTERISTICS AMBIENT TEMPERATURE = 75 WIND VELOCITY = 6.7 ATMOSPHERIC STABILITY CLASS = C LIQUID CONFINEMENT AREA = 25000 VAPOR/GAS DISCHARGE HEIGHT = 0 degrees F mph sq ft feet KEY RESULTS PROVIDED BY USER INSTEAD OF BY EVALUATION METHODS NONE OBSERVED KEY RESULTS OVERRIDDEN BY USER AT SOME POINT AFTER COMPUTATION NONE OBSERVED HAZARDOUS MATERIAL ADDRESS \ LOCATION DATE OF ASSESSMENT NAME OF DISK FILE sulfuric acid 100 Quantico 3-23-93 ARGO2.ASF ******* DISCHARGE RATE/DURATION ESTIMATES Liquid discharge from'nonpressurized container Average discharge rate = Duration of discharge = Amount discharged = State of material = ******* LIQUID POOL SIZE ESTIMATES Evaporating pool area = 1732.2 lbs/min 26.1 minutes 45042 lbs Liquid 25000 -ft2 ******* LIQUID POOL EVAPORATION RATE/DURATION ESTIMATES Vapor evolution rate = .013 Evolution duration = 3680082 ******* TOXIC VAPOR DISPERSION ANALYSIS RESULTS DoWnwind distance to concentration of 20 ppm -- at groundlevel = 33 feet Note: Minimum computable answer is 33 feet! Actual hazard distance may be less. lbs/min minutes · INPUT PARAMETER SUMMARY PHYSIOCHEMICAL PROPERTIES OF MATERIAL NORMAL BOILING POINT = MOLECULAR WEIGHT LIQUID SPECIFIC GRAVITY VAPOR PRES AT CONTAINER TEMP VAPOR PRES AT AMBIENT TEMP TOXIC VAPOR LIMIT 529 = 98.08 = 1.8 = .001 = .052 = .0011 = .052 =' 20 CONTAINER CHARACTERISTICS, CONTAINER TYPE = TANK DIAMETER = 4.2 TANK LENGTH - 40 TOTAL WEIGHT OF CONTENTS = 45042 LIQUID HEIGHT IN CONTAINER = 1.9 DISCHARGE HOLE DIAMETER = 2 DISCHARGE COEFFICIENT OF HOLE = 1 TEMP OF CONTAINER CONTENTS = 75 degrees F psia mm Hg psia mm Hg ppm Horizontal cylinder feet feet lbs feet. inch(es) degrees F ENVIRONMENTAL/LOCATION CHARACTERISTICS AMBIENT TEMPERATURE = 75 WIND VELOCITY = 6.7 ATMOSPHERIC STABILITY CLASS = C LIQUID CONFINEMENT AREA = 25000 VAPOR/GAS DISCHARGE HEIGHT = 0 degrees F mph sq ft feet KEY RESULTS PROVIDED BY USER INSTEAD OF BY EVALUATION METHODS NONE OBSERVED KEY RESULTS OVERRIDDEN BY USER AT SOME POINT AFTER COMPUTATION NONE OBSERVED HAZARDOUS. MATERIAL ADDRESS \ LOCATION DATE OF ASSESSMENT NAME OF DISK FILE = sulfuric aCid = 100 Quantico Ave. = 3-23-93 = ARGO3.ASF *** SCENARIO DESCRIPTION tanker release ******* DISCHARGE RATE/DURATION ESTIMATES Liquid discharge from nonpressurized container 'Average discharge rate = 1732.2 Duration of discharge = 26.1 Amount discharged = 45042 State'of material = 'Liquid **'***** LIQUiD~POOL SIZE ESTIMATES Evaporating pool area = 25000 lbs/min minutes lbs ft2 ******* LIQUID POOL EVAPORATION. RATE/DURATION ESTIMATES vaPor evolution rate = .01 Evolution duration = 4676863 lbs/min minutes ******* TOXIC VAPOR DISPERSION ANALYSIS RESULTS Downwind distance t° concentration of 20. ppm -- at grOundlevel = 33 feet Note: Minimum computable answer is 33 feet! Actual hazard distance may be less. INPUT PARAMETER SUMMARY PHYSIOCHEMICAL PROPERTIES OF MATERIAL NORMAL BOILING POINT = MOLECULAR WEIGHT LIQUID SPECIFIC GRAVITY VAPOR PRES AT CONTAINER TEMP .VAPOR pRES AT ~AMBIENT TEMP TOXIC VAPOR LIMIT 529 degrees F = 98.08 = 1.8 = .001 psia = ~052 mm Hg = .0011 psia = .052 mm Hg = 20 'ppm CONTAINER CHARACTERISTICS CONTAINER TYPE = TANK DIAMETER = 4.2 TANK LENGTH = 40 TOTAL WEIGHT OF CONTENTS = 45042 WEIGHT OF LIQUID = 45042 LIQUID HEIGHT IN CONTAINER = 1.9 WEIGHT OF GAS UNDER PRESSURE = 0 TOTAL CONTAINER VOLUME = 3141 = 23497 LIQUID VOLUME IN CONTAINER = 401.1 = 3000 DISCHARGE HOLE DIAMETER = 2 DISCHARGE COEFFICIENT OF HOLE = 1 TEMP OF CONTAINER CONTENTS = 40 Horizontal cylinder feet feet ~lbs lbs feet lbs ft3 .gals ft3 gals inch(es) degrees F ENVIRONMENTAL/LOCATION CHARACTERISTICS AMBIENTTEMPERATURE = 40 WIND VELOCITY = 4.5 ATMOSPHERIC STABILITY CLASS = C LIQUID CONFINEMENT AREA = 25000 VAPOR/GAS DISCHARGE HEIGHT = 0 degrees F mph sq ft feet KEY RESULTS PROVIDED BY USER INSTEAD OF BY EVALUATION METHODS NONE OBSERVED KEY RESULTS OVERRIDDEN BY USER AT SOME POINT AFTER COMPUTATION NONE OBSERVED HAZARDOUS MATERIAL = sulfuric acid ADDRESS \ LOCATION = 100 Quantico Ave. DATE OF ASSESSMENT = 3-23-93 NAME OF DISK FILE = ARGO3.ASF *** SCENARIO DESCRIPTION tanker release ******* DISCHARGE RATE/DURATION ESTIMATES Liquid discharge from nonPressurized container Average discharge rate = 1732.2 Duration of discharge = 26.1 Amount discharged = 45042 State of material = Liquid ******* LIQUID POOL SIZE ESTIMATES Evaporating pool area = 25000 ft2 ******* LIQUID POOL EVAPORATION RATE/DURATION ESTIMATES Vapor evolutiOn rate = .01 Evolution duration = 4676863 " ******* TOXIC VAPOR DISPERSION ANALYSIS RESULTS Downwind distance to concentration of 2 ppm -- at groundlevel = 38 feet Note: Minimum computable answer is 33 feet! Actual hazard distance may be less. See 'attached table(s) for further details. lbs/min minutes lbs lbs/min. minutes )wnwind Distance (feet) (miles) TOXIC VAPOR~DISPERSION ANALYSIS RESULTS Groundlevel Source Height Initial Evacuation Concentration Concentration Zone width* (ppm) (ppm) (feet) 32 .01 · ' 2.7 33 .01 2.7 33 .01 2.6 34 · .01 2.5 34 .01 2.5. 34 .01 2.4 35 .01 2~4 35 ' .01 2.3 35 .01 2.3 36 .01 2.2 36 .01 2.2 37 .01 2.2 37 .01 2.1 37 ,01 2.1 38 .01 2 2.7 130 2.7 130 2.6 130 2.5 130 2.5 130 2.4 130 2.4 120 2.3 120 2.3 120 2.2 120 2.2 120 2.2 110 2.1 110 2.1 110 2 1 *Usually safe' for < 1 hour release. Longer releases or sudden wind shifts may require a larger width or different direction for the evacuation zone. See Chapters 3 and 12 of the guide for details. Source height specified by the user for this scenario was 0 feet. Downwind Distance TOXIC VAPOR DISPERSION ANALYSIS RESULTS Contaminant Arrival Time ................... at Downwind Location (feet) (miles) ('minutes) 32 .01 .1 4676863 33 .01 .1 4676863 33 '01 .1 4676863 34 .01 .1 4676863 34 .01 .1 4676863 34 .01 ..1 4676863 35 .01 .1 4676863 35 .01 ~ .1 4676863 35 .01 .1 4676863 36 .01 .1 4676863 36 .01 .1 4676863 37' .01 .1 4676863 37 .01 .1 4676863 37 .01 .1 , 4676863 38 .01 .1~ 4676863 Contaminant Departure Time at Downwind Location (minutes) CAUTION: See guide for assumptions used in estimating these times. INPUT PARAMETER SUMMARY PHYSIOCHEMICAL PROPERTIESOF MATERIAL NORMAL BOILING POINT = MOLECULAR WEIGHT LIQUID SPECIFIC GRAVITY VAPOR PRES AT CONTAINER TEMP VAPOR PRES AT AMBIENT TEMP TOXIC VAPOR LIMIT 529 degrees F = 98.08 = 1.8 = .001 psia = .052 mm Hg = .0011 psia = .052 mm Hg = 2 ppm CONTAINER CHARACTERISTICS CONTAINER TYPE = TANK DIAMETER = 4.2 TANK LENGTH = 40 TOTAL WEIGHT OF CONTENTS = 45042 WEIGHT OF LIQUID = 45042 LIQUID HEIGHT IN CONTAINER = 1.9 WEIGHT OF GAS.UNDER PRESSURE = 0 TOTAL CONTAINER VOLUME = 3141 LIQUID VOLUME IN CONTAINER = 23497 = 401.1 = 3000 = 2 1 40 DISCHARGE HOLE DIAMETER DISCHARGE COEFFICIENT OF HOLE = TEMP OF CONTAINER CONTENTS = 'ENVIRONMENTAL/LOCATION CHARACTERISTICS AMBIENT TEMPERATURE = 40 WIND VELOCITY = 4.5 ATMOSPHERIC STABILITY CLASS = C LIQUID CONFINEMENT AREA = 25000 VAPOR/GAS DISCHARGE HEIGHT = 0 Horizontal cylinder feet feet lbs lbs feet lbs ft3 gals ft3 gals inch(es) degrees F degrees F mph sq ft feet KEY RESULTS PROVIDED BY USER INSTEAD OF BY EVALUATION METHODS NONE OBSERVED KEY RESULTS OVERRIDDEN BY USER AT SOME POINT AFTER COMPUTATION NONE OBSERVED Attachment 1 RISK ANALYSIS MATRIX Combinations of Conclusions From Risk Analysis that Identify Situations of Major Concern Combinations that Identify · Situations of Considerable Concern Combinations of Concern Which may Require Planning for Credible Events LOW MEDIUM HIGH Severity of Consequences Due to AHM Release (From I~MPP Guidance for the Preparation of a Risk Management and.Prevention Program, November, 1989, California Office of Emergency Services.) LOW:. MEDIUM: HIGHi -LOW: MEDIUM: HIGH: · (From the EPA Technical Guidanccfor Hazard Analysis, 1987) QUALITATIVE DEFINITIONS OF PROBABILITY OF OCCURRENCE Probability of occurrence considered unlikdy during the expected lifetime of the facility assuming normal operation and maintenance. ': . Probability of occurrence considered possible during the expected lifetime of thc facility. Probability of occurrence considered sufficiently high to assume event will occur during the expected lifetime of the facility DEFINITIONS OF sEVERITY OF CONSEQUENCES TO PEOPLE . . Chemical is expected to move into the surrounding environment in negligible concentrations. Injuries expected Only for exposure over extended periods or when individual personal health conditions create complication~ , Chemical is expected to move into the surrounding environment in concentrations sufficient to cause serious injuries and/or deaths unless prompt and effective corrective action is taken. Death and/or injuries expected only for expbsure over extended periods or when individual personal health conditions created complications. Chemical is expected t0 move into 'the surrounding environment in concentrations sufficient to cause serious injuries and/or deaths upon exposure. Large numbers of people expected to be affected. ' AR~O CHEMICAL UNLOADING OF HAZARDOUS CHEMICALS The procedures for the unloading of hazardous chemicals are: 1. Pre-unloading safety meeting o Check for gravity flow or low pressure tankers Two people drumming at one time a. The first drumming, second tending hose Both of these individuals in personal protective equipment', suitable for material (full suit, rubber gloves and boots, face shield and goggles) ~ 4. Third person is stand-by and will be rotated o Driver of supplier MUST stay with truck, in personal protective equipment at main discharge valve while unloading material Length of time between rotations of shift, will vary with temperature, individuals, et'c., with the safety of the personnel the primary concern ¸. A review, of the MSDS for the product A review of each of the tasks involved with the unloading Name of hazardous chemical being'unloaded Name of person going over procedures Persons attending the pre-unloading'safety review: Driver!s Signature Da(e AtlRO CtlI~II C~L -MEI~;TING ,~tII~DULI~ ( 1.997 ) Ao Commencing on the fourth (4th) Tuesday of ,,each quarterly month: 1. ~anuary 28, ].997 2. April 22, 1997 3. July 22,-1997 4. Octol~r 28, 1997 II. B. Meetings will be in the Conference Room at 8:30 '~a~_~eo_p_l~ Mana~nt Meetings A~ CommenCing on the first (lst) Monday of each quarterly month: 1. January 6, 1997 2. April 7, 1997 3. July 7, 1.997 4. October 6, 1997 B.. Meetings will 'be in the Conference Room at 9:30 a.m. III. Office personnel Meetings Commencing on the third (3rd) Hednesday of each quarterly mon~: 1. January 15, 1997 2. April 16, 1997 3.-., · July lO, 1997 4. October 15, 1997 IV. B. Meetings will be in the Conference Room at 8:30 a.m. Personnel'in Hazardous Envi~~ A. Commencing on the first &thirdHedne~day fi~¢~ month: 2. 3. 4. 5. 6. 7. 6. 9. ' 10. 11. 12. January 8 & 9.2, 1997 February 5 & 19, 1997 March 5 & 19, 1997 April 2 & 23, 1997 May 7 & 21, 1997 June 4 & 25, 1997 July 9 & 23, 1997 Auamst 6 & 20, 1997 September 3 & 24, 1997 october 8 & 22, 1997 November' 5 & 19, 1997 December 3 & 1~, 1997 Meetings to be in Conference Rm or Warehouse; 8:00 a.m. ARGO CHEMICAL SAFETY MEETINGS SCHEDULE (1993) I. Safe~y Committee Meetinqs Commencing on the third (3rd) Tuesday Of each quarterly month: 1. January 19, 1993 2. April 20, 1993 3. July'20, 1993 4. October 19, 1993 B. Meetings will be in the conference room at 8 AM II. Salespeople and Manaqement' Meetings Commencing on the first (l~t) Monday of each quarterly month: 1. January 4, 1993 2. April 5, 1993 3. July 5, 1993 4. October 4, 1993 B. Meetings will be in the conference room at 8 .AM III. Offic~ Personnel Meetings A o Commencing on the third (3rd) Wednesday of each quarterly month: 1. January 20., 1993 2. April 14, 1993 3. July 14, 1993 4. October Z0, '1993 B. Meetings will be in the Conference room at 8 AM IV. Personnel in More Hazardous Environment. Meetings Ao 4. 5. 6. 7. 8. Commencing on every other Wednesday of each month: January 6 & 20, 1993 February 3 & 17, 1993 March 3, 17 & 31, 1993 April 14 & 28, 1993 May 12 & 26, 1993 June 9 & 23, 1993 .July 7 &'21, 1993 August 4 & 18, 1993 9. .'September 1,.15 & 29, 1993 10. October 13 & 27, 1993 ................. 1'1. November 10 &'24, 1993 ' 12. December 8 & 22, 1993 B. · Meetings will be in the conference room or the warehouse at 8 AM ARGO CHEMICAL Date: Safety Equipment Checklist I. Safety Showers A. Southside B. SW Corner C. NW Corner II~ Fire Extinguishers A', Time Clock B. south Wall C. West Wall III. Forklifts A. Nissan 1. Backup Alarm 2. Lights 3. Maintenance B. Datsun 1. Backup Alarm 2. Lights 3. Maintenance IV. Respirators A. Ful l~Face 1. 2. 3. 4. 5. 6. Pass Fail Needs Repair Comments ARGO CHEMICAL IV. V o VI. Respirators (con~.) B'. Half-Face 1. 3 4. 5. Misc Safety Equipment' A. H o Generaq Safety Appearance & Observations VII,. person CondUcting Safety Equipment Audit: Scholle Cor ration 1200.West North Avenue, Emergen~cyi Te. lephone · Chemtrec (~00) 42.~-9300 · Northlake, IL 60164/Te1.(708) 562-7290 ~..~' ~3an: 1'991 PLANTS: Northlake, IL (708) 562-7290 / Rancho Dominguez (Compton, CA) (213) 53~-1600./Atlanta, GA (404) 761-3134 / Dallas, TX (214) 278-9545 Material Safety Data 'Sheet -Suffuric Aci- " ~ ...... L-'--'----(I-~I~SO4 ~ 93.19%) This Material Safety Data Information Sheei is principally directed to mhnagerial,'safety, hygiene and m~ic. al personnel. The description of physical, chemical and toxicological properties and handling advice is based on elperi~hen{ai results and past experience. It is intended as a starting point for the development of health and safety procedures. DOT LABELING Shipping Name: Sulfuric acid REQUIREMENTS: Class: Corrosive material .~_? .......... - --~. =U. 12CNO.:: -~ .... UN.!330 ...... ~ _ ~ .... ._- HAZARDOUS INGREDIENTS/IDENTITY Sulfuric Acid - 66° Baume (Mineral Acid, Oil of Vitriol, H2SO4, suiphuric acid) 40 CFR Part 372.45 Notification: OSHA ACGIH CAS PEL TLV '.NUMBER lmg/M3 : lmg/M3 - 7664-93-9 Concentrated sulfuric acid contatns approximately 93.2% by weight of H2SO4 by weight (C~s NO. 7664-93-9%) and is subject to the reporting requirements of section 313 of Title III of the superfund amendments and authorization act of 1986. It is also subject to the reporting requirements of 40 CFR part 372. PHYSICAL & CHEMICAL CHARACTERISTICS: Formula: Formula Weight: Physical State/ Description: Boiling Point: Flash Point: Freezing Point,: Odor: pH: H2SO4 98.08 Clear, colorless to cloudy liquid. - 93 % = 529 °F approx. · Not applicable 93% = -20 °F (-28.9 °C) approx. 98% = 30°F (- 1.1 °C) approx. None .:. .... · Eess than '1 (1% aqueous solution) Specific Gravity:~ : -' 78% = 1.7 (water = 1) .~82 ' 100% = 1.8 (water = 1) Vapor Density~ ·3.4 (air, = I at boiling point of sulfuric acid) Vapor PressUre: ~'"'78% to 100% = Less than I mmHg at 100°F (37.8°C) I Water Solubility: Soluble in ali proportions. Reportable Quantity: 1,000 1b./454 kg. Scholle Emergency Telephone Chemtrec (800) 424-9300 Corporation/200West North Avenue, Northlake, IL 60164/Teli (708)562-7290 Jan. 1991 FIRE & EXPLOSION DATA: PHYSICAL HAZARDS: (REACTIVITY DATA) Flash Point: Auto-Ignition Temperature: Extinguisher Media: Special Fire Fighting Procedures: Unusual Fire and Explosion Hazards: Stability: Conditions to Avoid: Incompatibility: (Materials to Avoid) Hazardous Decomposition Products: Hazardous Sulfuric Acid (HzSO4 -- 93.19%) N/A N/A Dry chemical or CO: small fires. Water fog, large fires'. Do not direct water into acid tanks. Cool outside of tank __~with ,w. ater._W~ear f, uJI-face,, self-~cont_ained~_rgsp!Lat0r, rubberized outer wear, gloves, boots. Sulfuric acid will not burn but can start fires with organic material, nitrates, carbides, chlorates and metal powders. Flammable hydrogen gas can form when acid contacts most metals. Hydrogen may accumulate in containers, avoid ignition sources, spill over into sewers may generate hydrogen gas or toxic sulfides. Addition of water to acid causes heat and possible splattering. Stable Contact with metals, organics. Strong corrosive agent will attack most metals. Contact with organics, nitrates, carbides, chlorates, etc. may cause ignition. Allyl compounds and aldehydes undergo polymerization -- possibly violent. Sulfur oxides at high temperature. Reacts with above to form hydrogen cyanide and hydrogen sulfide. HEALTH HAZARDS: ' Pbly~rn~fi~tiO'n~.~ -~Will ~Nft-O¥cffr~ ..... Conditions to Avoid: Acute: .Signs and Symptoms of Exposure: Medical Conditions Generally Aggravated by Exposure: All contact with organic substances and most metals. 3rd degree burns. S~vere respiratory, skin and eye irritant. Bronchitis Laryngeal and pulmonary edema may result. Prickling or burning sensation of skin and mucous membranes. Coughing, sneezing, tightness of chest, difficulty in breathing. Any pre-existing respiratory disease, for example emphysema. 2 Scholle Emergency Telephone . Chemtrec (800) 424-9300 orporauon/200 West North Avenue, Northlake, IL 60164/Tel. (708) 562-7290 Jan. 1991 HEALTH HAZARDS (continued): Chemical Listed as Carcinogen or Potential Carcinogen: National Toxicology Program: I.A.R.C. Mon0gr__aphs: .. OSHA: CAL/OSHA: Prop65: Emergency and First Aid Procedures: Sulfuric Acid (H2SO4 -- 93.19%) No No No No No Speed in removing a~id is essential. Treat most urgent symptoms first: cessation of breathing, eye injury, skin contact, shock. Seek medical assistance even if injury appears slight. Give physician detailed account of incident. RECOMMENDATIONS TO PHYSICIAN: ROUTES OF ENTRY: While the patient is being transported to a medical facility, apply compresses of iced water. If medical treatment must be delayed., immerse the affected area in iced water. If immersion is not practical, comPresses of iced water can be applied. Avoid freezing tissues. , Note to Physician: Continued washing of the affected area with cold' or iced water will be helpful in removing the last traces of sulfuric acid. Creams or ointments should not be applied before or during the washing phase of the treatment. Inhalation: Eyes: Skin: Ingestion: Conditions Aggravated by: Remove from exPosure. CPR, if indicated. Give oxygen. Flush immediately with large amounts of water for at least 15 minutes. Hold eyelids open during flushing. Flush immediately with large amounts of water. Remove contaminated clothing and shoes (this can be done while under shower). Do not induce vomiting. Give large amounts of milk, milk of magnesia or table oil or fresh eggs. Use water when nothing else is available. Rinse mouth often. Individuals with pre-existing disease of the lungs may have increased susceptibility to the toxicity of excessive exposures. 3 -Scholle ~ .Emergency Telephone Chemtrec (800) 424-9300 Corporation./200West North Avenue, Northlake, IL 60164/Tel. (708) 562-7290 Jan. 1991 SPECIAL PRECAUTIONS AND SPILL/LEAK PROCEDURES: sPECIAL PROTECTION INFORMATION/CONTROL MEASURES: P}'~cautions t6"" ....... , b~' Taken in Handling and Storage: See Sections 4 and 5. Do not store near organics. '. ..... . Hydrogen may be generated inside drums and tanks; avoid flames and sparks. Other' Precautions: Steps to be Taken in Case Material is Released or Spilled: Waste Disposal Methods (Consult Federal, State and Local Regulations): Sulfuric Acid (H2SO4 -- 93.19%) Never add water to Containers of acid. For spills, beware of acid reaction in sewers' that may produce -flammabl~ hydrogen' ~h~ '6r t0xi~:~ su-Ifii:liss.~- : -' Wear full acid-protective gear. Remove sources of ignition. Neutralize gpill with lime or soda ash, flush to waste water treatment system. Dike large spills. Do not wash into storm or sanitary sewer system. Flush as above. Neutralize with lime or soda ash. Approx. 15 lb,/gal. Consult regulations. EPA hazardous waste DOOO2 - corrosive and DOOO3 - reactive if discarded. Respiratory Protection: When needed use NIOSH or MSHA approved half or full-face mask with acid gas cartridge. For high concentrations, use self-contained breathing unit. ? Ventilation: Required Local Exhaust: Yes Mechanical: Ventilate storage tanks before entry. rrotectlve taioves: l~unDer Eye Protection: Other Protective Clothing or Equipment: Work/Hygienic Practices: Maintenance of Contaminated Equipment: Labeling Priority: Chemical goggles or full-face shield. Rubber safety shoes/boots. Rubber apron or full suit if splashes likely. Prohibit smoking. Provide safety showers/eye washes near work site. Train employees in chemical handling practices. Use same precautions as in "Special Precautions" above. Corrosive FORM #860228-2 Bakersfield Fire Dept. Hazardous Materials Division 2130 "G" Street Bakersfield, CA. 93301 HAZARDOUS MATERIALS MANAGEMENT PLAN INSTRUCTIONS: 2. 3. 4. To avoid further action, return this form within 30 days of receipt. TYPE/PRINT ANSWERS IN ENGLISH. Answer the questions below for the business as a whole. Be brief and concise as possible. SECTION 1' BUSINESS IDENTIFICATION DATA BUSINESS NAME: ARGO. CHEMICAL, INC. LOCATION: 100 QUANTICO AVE. MAILING ADDRESS: 100 QUANTZCO AVE. CITY: BAKERSFIELD STATE: 'CA. ZIP: 93307 PHONE: 805-322-2222 DUN & BRADSTREET NUMBER' N/A SIC CODE'. N/A PRIMARY ACTIVITY: CHEMICAL WHOLESALE DISTRIBUTION OWNER' INCORPORATED MAILING ADDRESS: 1 00 QUANTICO:..'AVE~.. BAKERSFIELD, .CA. 93307 SECTION 2: EMERGENCY NOTIFICATION: CONTACT TITLE BUS. PHONE 24 HR. PHONE 1. MARK T. RODGERS PRES. 322-2222 834-5618 2. STEVEN J. SCHMEDDING V.P. 322-2222 398-8934 'l~akerstield Fire Dept. Hazardous Materials Division HAZARDOUS MATERIALS MANAGEMENT PLAN SECTION 3: TRAINING: NUMBER OF EMPLOYESS: 1 o MATERIAL SAFETY DATA SHEETS ON FILE: BRIEF SUMMARY OF TRAINING PROGRAM: WEEKLY 3 0 DAY YES SAFETY AND TRAINING MEETING FOR MATERIAL HANDLING'PERSONNEL INITIAL TRAINING PERIOD FOR NEW MATERIAL HANDLING PERSONNEL SECTION 4: EXEMPTION REQUEST: I CERTIFY UNDER PENALTY OF PERJURY THAT MY BUSINESS IS EXEMPT FROM THE REPORTING REQUIREMENTS OF CHAPTER 6,95 OF THE "CALIFORNIA HEALTH & SAFETY CODE" FOR THE FOLLOWING REASONS: WE DO NOT HANDLE HAZARDOUS MATERIALS. WE DOHANOLE HAZARDOUS MATERIALS, BUT THE QUANTITIES AT NO TIMEEXCEED THE MINIMUM REPORTING QUANTITIES. OTHER (SPECIFY REASON) SECTION 5: CERTIFICATION: I, MARK m_ Ro~n~...~ CERTIFY THAT THE ABOVE INFOR- MATION IS ACCURATE. I UNDERSTAND THAT THIS INFORMATION WILL BE USED TO FULFILL MY FIRM'S OBLIGATIONS UNDER THE "CALIFORNIA HEALTH AND SAFETY CODE" ON HAZARDOUS MATERIALS (DIV. 20 CHAPTER 6.95 SEC. 25500 ET AL.) AND THAT INACCURATE INFORMATION CONSTITUTES PERJURY. TITLE DATE FD1590 Bakersiield Fire Dept. Hazardous Materials Division HAZARDOUS MATERIALS MANAGEMENT PLAN Facility Unit Name: . ARGO CHEMICAL~ INC. SECTION 6: NOTIFICATION AND EVACUATION PROCEDURES: Ao AGENCY NOTIFICATION PROCEDURES: CALL VIRGINIA COLONY FIRE STATION (861-2541) CALL 911 EMPLOYEE NOTIFICATION AND EVACUATION' NOTIFY ALL PERSONNEL TO EVACUATE PLANT. TO THE EAST THEN'NORTH ON QUANTICO AVE. NOTIFY FIRE DEPT. EXIT PLANT & OFFICES TO AREA FREE OF .SMOKE c PUBLIC EVACUATION' PER GOVT. AGENCY. EMERGENCY MEDICAL PLAN: CALL 911 PROVIDE INITIAL FIRST AID Bakersfield Fire Dept. Hazardous Materials Division HAZARDOUS. MATERIALS MANAGEMENT PLAN sEcTION 7: MITIGATION, PREVENTION AND ABATEMENT PLAN: A, RELEASE PREVENTION STEPS' MATERIALS STORED IN SEALED CONTINERS AND DOT APPROVED CONTAINERS RELEASE CONTAINMENT AND/OR MINIMIZATION: ALL HAZARDOUS MATERIALS STORED IN DYKED CONTAINMENT AREAS CLEAN-UP PROCEDURES: IF PRODUCT IS SPILLED PICKUP WITH VACUUM PUMP AND RECLAIM SECTION 8: UTILITY SHUT-OFFS (LOCATION OF SHUT-OFFS AT yOuR FACILITY): NATURAL GAS/PROPANE: NORTH EAST CORNER OFFICE BUILDING ELECTRICAL: NORTH EAST CORNER WAREHOUSE WATER:' NORTH EAST CORNER OF PROPERTY SPECIAL: LOCK BOX: .YES/NO IF YES, LOCATION' SECTION 9: PRIVATE' FIRE PROTECTION/WATER AVAILABILITY: A, PRIVATE FIRE PROTECTION: 4 - 2A10BC FIRE EXTINGUISHERS (1- CENTER OF EAST WHSE..WALL, 1- SOUTH ROLLUP DOOR, 1- SOUTHWEST ROLLUP DOOR , 1- FORKLIFT B. WATER AVAILABILITY (FIRE HYDRANT): FIRE HYDRANT EAST SIDE OF QUANTICO - DIRECTLY ACROSS FROM SOUTH EAST CORNER OF PROPERTY 4. PO1590