HomeMy WebLinkAboutMITIGATION
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. .. COMBINING OUR
RESOURCES TO
ENHANCE OUR
SERVICES. ..
I Delta
Environmental
WÂ Consultants, Inc.
ENVIRONMENTAL
MANAGEMENT, INC.
July 15, 2003
KHM Project D80-5321
Mr. John D. Whiting
, California Regional Water Quality Control Board
Central Valley Region
1685 E. Street
Fresno, Califomia 93706-2020
Re: SHELL GRASP MONITORING REPORT
Shell Service Station
5321 Stockdale Highway
Bakersfield, California
Dear Mr. Whiting:
On behalf of Equilon Enterprises LLC dba Shell Oil Products (SHELL), KHM
Environmental Management, Inc. (KHM) has prepared this Second Qparter 2003 Groundwater
Monitoring ReportJor the above referenced site.
If you have any questions regarding this site, please contact Brad Clark at (626) 256-6662 or
Tony Palagyi (425) 377-8530.
~
tchen Tagav'ilk ~
oject Manager
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-
Sincerely,
KHM Environmental Management, Inc.
Attachment: Second Quarter 2003 Groundwater Monitoring Report
cc: Tony Palaygi, Shell Oil Products US
Isabel Mejia, Shell Oil Products US
Steve Underwood, City of Bakersfield Fire Department
6284 San Ignacio Avenue' Suite E
San Jose, California 95119 USA
408.224.4724 . Fax: 408,224.4518
800,477. 7411
911 South Primrose Avenue' Suite K
Monrovia, California 91016 USA
626,256,6662 . Fax: 626,256.6263
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July 15, 2003
SHELL QUARTERLY STATUS REPORT
Station Address:
KHM Project No.
SHELL Environmental Engin./Phone No.:
KHM Project Manager/Phone No.:
Primary Agency/Regulatory ID No.:
Other Agencies to Receive Copies:
5321 Stockdale Highway
D80-5321
Tony Palaygi/(425) 377-8530
Gretchen Tagavilla / (626) 256,6662
CVRWQCB/ Jo1m Whiting
City of Bakersfield Fire Department
WORK PERFORMED THIS QUARTER (SECOND - 2003):
1. Quarterly groundwater monitoring and sampling. Submitted quarterly report.
2. Submitted Site Assessment Report.
3. Received agency letter from CVRWQCB on July 3,2003.
WORK PROPOSED FOR NEXT QUARTER (THIRD - 2003):
1. Quarterly groundwater monitoring and sampling.
2. Prepare and submit response to CVRWQCB agency letter.
Current Phase of Project: Groundwater monitoring
Frequency of Sampling: Quarterly
Frequency of Monitoring: Quarterly
Is Separate Phase Hydrocarbon Present On-site (Well #'s): 0 Yes IZI No
Cumulative SPH Recovered to Date: NA
SPH Recovered This Quarter: None
Sensitive Receptor( s) and Respective Direction( s):
Nearest field verified well is Well CBK 06-01 (State Well No.
30S/27E-03B02 M) of the City of Bakersfield approximately
825 feet South of the site. '
Current Remediation Techniques:
Permits for Discharge:
Approximate Depth to Groundwater:
Groundwater Gradient
Current Agency Correspondence:
Summary of Unusual Activity:
None
None
129.59' to 130.76'
South @ approximately 0.015 ft/ ft
Agency letter from the Central Valley RWQCB dated July 3, 2003.
None
~J~
~chen Tagavilla .
oject Manager (KH1\í1)
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ATTACHED:
· Table 1 -Groundwater Gauging and Analytical Results
· Figure 1 - Site Location Map
· Figure 2 - Groundwater Elevation Contour Map
· Figure 3 - Hydrocarbon Distribution in Groundwater Map
· Figure 4 - TPH-G Concentration Map
· Figure 5 - Benzene Concentration Map
· Figure 6 - MTBE Concentration Map
· Appendix A - Field Data Sheets
· Appendix B - Field Procedures
· Appendix C - Laboratory Report and Chain-of-Custody Documents
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TABLE
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TABLE 1 I
HISTORICAL GROUNDWATER GAUGING AND ANALYTICAL DATA
SHEL SERVICE STATION I
5321 Stockdale Highway, Bakersfieid, California
\ \
DATE DEPTH SPH GWELEV. . TPH-D TPH~G BENZENE TOLUENE ,,·.,ETHYL~ TOTAL MTBE TBA DlPE ETBE TAME ETHANOL COMMENTS
TOGW THlCKN. (feet relative BENZENE XYLENES 8260 8260 8260. 8260 8260 8015
(feet) ¡feet) to MSL) (ug/L) (ug/L) (ug/L) (ueIL) (ueIL) (Ul!/L) , (ueIL) hl!uL) (ueIL) (ug/L) (ueIL) (ug/L)
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MW-l Top of casin!! elevation (ft): 386.61
3/17/2003 129.17 0,00 257.44
3/2512003 129.38 0.00 257.23 ND<IOOO ND<50 ND<O,50 ND<LO ND<LO ND<LO ND<LO ND<10 ND<2.0 ND<2.0 ND<2.0 ND<100
6/19/2003 130,76 0.00 255.85 ND<50 ND<0.50 ND<LO ND<LO ND<LO ND<LO ND<10 ND<2.0 ND<2,O ND<2,O No purge sample
.
MW-2 Top of casin!! elevation (ft): 386.06
3/17/2003 128.64 0,00 257.42
3125/2003 128.84 0.00 257,22 ND<1000 ND<50 ND<0.50 ND<LO ND<LO ND<LO ND<LO ND<10 ND<2,O ND<2,O ND<2,O ND<100
6/19/2003 130.27 0,00 255.79 ND<50 ND<0.50 ND<LO ND<LO ND<LO ND<LO ND<10 ND<2,O ND<2,O ND<2,O No purge sample
MW-3 ~p of casin!! elevation (£I): 386.34
--
3/1712003 128,30 0.00 258.04
3125/2003 128.45 0,00 257.89 ND<1000 ND<50 ND<0.50 ND<1.0 ND<LO ND<LO ND<LO ND<10 ND<2.0 ND<2.0 ND<2,O ND<100
6/19/2003 129.82 0.00 256.52 ND<50 ND<O,50 ND<LO ND<LO ND<LO ND<LO ND<lO ND<2,O ND<2.0 ND<2.0 No purge sample
MW-4 Top of casin!! elevation (ft): 386.57
3/1712003 128.17 0.00 258.40
3125/2003 128.25 0,00 258.32 ND<IOOO ND<50 ND<O,50 ND<LO ND<LO ND<LO ND<LO ND<IO ND<2.0 ND<2.0 ND<2.0 ND<IOO
6/19/2003 129.59 0.00 256.98 ND<50 ND<O,50 ND<LO ND<LO ND<LO ND<LO ND<lO ND<2.0 ND<2.0 ND<2.0 No purge sample
Notes:
GW - Groundwater
SPH - Separate-phase hydrocarbons
MSL - Mean sea level
ND - Not detected
.':':gIL - parts per billion
TPH-D - Total petroleum hydrocarbons as diesel
TPH-G· Total petroleum hydrocarbons as gasoline
MTBE, Methyl-tert butyl ether
TBA - Tert'butyl alcohol
DlPE - Di,isopropyl ether
ETBE - Ethyl,tert butyl ether
TAME - Tert-amyl methyl ether
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K:\Clients'-Shell\_ShelJ GRASP\_GRASP Siles\532I Stockdale\2003-07-31_GRASP Monitoring Report\Table I (5300)
Page 1 of 1
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SHELL OIL PRODUCTS US
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CONTOUR MAP 06/19/03
5321 STOCKDALE HIGHWAY
BAKERSFIELD, CALIFORNIA
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K:IClients\..Shell\..Shell GRASP\..GRASP SIteslS321 Stockdalel2003,07,15_GRASP Monitoring Report\FIGURE 3(532ILHYDROCARBON DISTRIBUTION IN GW MAP,dwg, Model, 7/15/2003 I:S6:52 PM
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K:IClients'-Shell'-Shell GRASP,-GRASP SiteslS321 Stockdale\2003,07'15_GRASP Monitoring ReportlFIGURE 6(S321LMTBE CONCENTRATION MAP.dwg. Model, 7/15/2003 2:11:25 PM
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ApPENDIX A
FIELD DATA SHEETS
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WELLHEAD INSPECTION CHECKLIST
Page -L of ~
~!J./ /
)' 121 S f1c.t..t£..k
Job Number O?ð'Jq-ßF~l
Client
Site Address
Well Inspected -
No Corrective
Well 10 Action Required
11l.J ..., X
¡MI.J-~ X
¡VI t,¡- J X
Mf,.¡ "lj X
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NOTES:
Date
!lw'lrr - gCA.~U"S Ç.'eIJ
f
t!tq/ðJ
Technician
J1f
Water Bailed Wellbox Other Action
From Components Cap Lock Taken
WeJlbox Cleaned Replaced Replaced (explain
bBlow)
Welf Not
Inspected
(explaIn
bBlow)
Repair Order
Submitted
BLAINE TECH SERVICES, INC,
SAN JOSE
VIW\', .blainetech .CQm
SACRAMENTO
LOS ANGELES
SAN DIEGO
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SHELL WELL MONITORING DATA SHEET
-f1 F-2
Site:
Date:
Sampler:
Well LD.:
Total Well Depth (TD): J117. £{4
Well Diameter: 2 3 L . 6 8
Depth to Water (DTW): 11 (). -rt
Depth to Free Product: Thickness-.ofFree Product (feet):
Referenced to: pd]:J Grade D.O. Mcler (ifreq'd): ysr HACH
DTW with 80% Recharge [(Height of Water Column x 0.20) + DTW]:
Sq~pling Method:
Bailer
~ Bailt?
Extraction Port
Dedicated Tubing
Purge Method: Bai1er
Disposable Bailer
Middleburg
EI erSl e
Other:
Well Diameter Multiplier Well Diameter Multiplier
1" 0.04 4" 0.65
(Gals.) X Gals. 2" 0.16 6" 1.47
= rndius2 · O. t 63
I Case Volume Specified Volumes Calculated Volwne 3' 0.37 Other
Condo Turbidity
Time Temp C)F) pH (mS or ¡@ (NTUs) Gals. Removed Observations
Qð8' b7·1 ?'L ~q5 q - c kt;..t,' I'tO ock,
.
"
Did well dewater? Yes No Gallons actually evacuated: -
Sampling Date: ,Irq/f» Sampling Time: &fð't Depth to Water: -
Sample LD.: Mw- ( Laboratory: Kiff ~~ Other
Analyzed for: Tt!fØ ~ MTBE TPH-D O~: o)ç~~
EB I.D. (if applicable): @ Duplicate I.D. (if applicable):
Time
Analyzed for: TPH-G BTEX MTBE TPH-D Other:
D.O~ (ifreqtd): mg/L Post-purge: 'mg
Pre~purge: IL
O.R.P. (ifreq'd): Pre-purge: mV Post-purge: mV
Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (800) 545~7558
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SHELL WELL MONITORING DATA SHEET
BTS #: 01ðf,., ¡Cf-f] F-2 Site: 'f 1lfo I g-¡O
Sampler: flF Date: 6/1'1/0;
Well J.D.: {V\V-2- ,^,ell])iarneter: 2 3 <.f) 6 8
-
Total Well Depth {TD): ¡l.fÇ.31 Depth to Water (DTW): /30.2.+
Depth to Free Product: Tbiclrness..ofFree Product (feet):
Referenced to: 1Ø Grade D.O. Mète~ (ifreq'd): YSl HACH
DTW with 80% Recharge [(Height of Water Column x 0.20) + DTW]:
Purge Met1lOd:
S,!,~pIing Method:
Bailer .
~~
Extraction Port
Dedicated Tubing
Bailer
Disposable Bailer
Middleburg
El erst e
1\0
, Wnterra
s ¡tic
Extraction Pump
Other
pCA,.~t.
Othe.r;
-
Well Diameter Multiplier Well Diameter Multiplier
I" 0.04 4" 0.65
(Gals.) X Gals. 2" 0.16 6" 1.47
=
1 Case Volume Specified Volumes Calculated Volume ]" 0.37 Other rndius1 * 0.163
Comi. Turbidity
TÌme Temp eF) pH (mS or ¡@ (NTUs) Gals. Removed. Observations
'iff 'i· t¡ :¡..D ~1-'1 12... -- I deú. f'. {If þ It tl,J
,
"
,
Did well dewater? Yes No Gallons actually evacuated: .-
Sampling Date: '/I&t/o 3 Sampling Time: '1 (8' Depth to Water: -
Sample LD.: Mlt-2.. Laboratory: Kiff ~ciëñct) Other
Analyzed for: T¡4Í9 ~ MTBE TPH-D ~; ð?f~'{ h'14 feet
@ .....
EB J.D. (if applicable): . Time Duplicate I.D. (if applicable):
Analyzed for: TPH-G BTEX MTBE TPH-D Other:
D.G: (ifreq'd): Pre:.purge: mg/L Post-purge: 'mg
It
O.R.P: (ifreq'd): Pre-purge: mV Post-purge: mV
Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (800) 545-7558
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SHELL WELL MONITORING DATA SHEET
BTS #: O]8/., ¡q-fl F-1. Site: 'f 1t(o 187-0 ,
Sampler: IJ.F Date: 6/1'1/03
Well J.D.: Mw-3 Well Diameter: 2 3 @) 6 8 ~
Total WeB Depth (TD): LfS,1I Depth to Water (DTW): I ~q·Kl.
Depth to Free Product: Thiclrness-.ofFree Product (feet):
Referenced to: p@? Grade D.O. Mète,r (ifreq'd): YSI HACH
DTW with 80% Recharge [(Height of Water Column x 0.20) + DTW]:
Purge Method:
. Waterra
s a tic
Ex:traction Pump
Other
pc,\ I'!J to
SÜ'lT1pling Method:
Bailer
Bailer
Disposable Bailer
Middleburg
El em e
YlO
~
Extraction Port
Dedicated Tubing
Other:
WolI Diameter Multiplier Well Diameter Multiplier
1" 0.04 4" 0.65
(Gals.) X Gals_ 2" 0.16 6" 1.47
= ¡¡¡dius1 . 0.163
1 Case Volume Sp'ecified Volumes Calculated Volume 3" 0,37 Other
Cond. . Turbidity
Time Temp eF) pH (mS or @ (NTUs) Gals. Removed Observations
~1l , t~l( 1.' 313 6 - c/~¡¡".l'· rw odJJt·
-
Did well dewater? Yes No Gallons actually evacuated: ----
Sampling Date: G!rc¡!O) Sampling Time: q J ( Depth to Water: -
Sample LD.: MI..I-) Laboratory: Kiff ~ Other
Analyzed for: I~ 4ÛÈ:x MTBE TPH-D O¿!)pr: () k y,qcltlbfe;s
- @
EB I.D. (if applicable): Tim. Duplicate I.D. (if applicable):
Analyzed for: TPH·G BTEX MTBE TPH·D Other:
.'
D.G: (ifreq'd): Pre;.purge: mC/L Post-purge, mg/L
O.R_P. (ifreq'd): Pre-purge: mY Post-purge: mY
Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (800) 545-7558
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SHELL WELL MONITORING DATA SHEET
BTS #: 0$ f -I] f-Z Site:
Sampler: 11 Date:
Well I.D.: (v\. \,J - l Well Diameter: 2 3 cD 6 8
Total Well Depth (TD): J l.11I. 62 Depth to Water (DTW): Or ~ )
Depth to Free Product: Thickness-.ofFree Product (feet):
Referenced to: p@ Grade D.O. Mete~ (ifreq'd): YSI HACH
DTW with 80% Recharge [(Height of Water Column x 0.20) + DTW]:
Purge Method:
. Waterra
s altic
Extraction Pump
Other
ptA.r.!~
Sampling Method:
Bailer
~ailer
Extraction Port
Dedicated Tubing
Bailer
Disposnble Bailer
Middleburg
EI ers! e
1\0
Other:
Well Diameler MuItilJlier Well Diameter MulriDlier
I" 0.04 4" 0.65
(Gals,) X GalS. 21t 0.16 6" 1.47
= ¡¡¡dius' . 0.163
1 Case Volume Sp'ecified Volumes Calculated Volume 3" 0.37 Other
Condo Turbidity .
Time Temp IF) pH (mS or ¡@ (NTUs) Gals. Removed Observations
'1L{g ''l.g :¡rO 3/g 11 - c I R/Á~' ¡to odo,
"
Did well dewater? Yes No Gallons actually evacuated: -
Sampling Date: {lrq(oJ Sampling Time: qf(~ Depth to Water: -
Sample I.D.: Mv -t¡ Laboratory: l(iff ~ Other
Analyzed for: TPlØ ~ MTBE TPH-D 0l:!lÞ: O>í Y'1 e..,c.r /tz.J
EB LD. (if applicable): @ Duplicate I.D. (if applicable):
Time
Analyzed for: TPH-G BTEX MTBE TPJ'I-D Other:
D.O. (ifreq'd): Pre;..purge: mg/L Post-purge: m'f,/L
O.R.P. (ifreq'd): Pre-purge: mV Post-purge: mV
Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (800) 545-7558
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ApPENDIX B
FIELD PROCEDURES
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BLAINE 1680 ROGERS AVENUE
TECH SERVICES"" SAN JOSE, CA 95112-1105
(40B) 573-7771 FAX
(408) 573-0555 PHONE
CONTRACTOR'S LICENSE #746684
www.blainetech.com
July 10, 2003
Tony Palagyi
Shell Oil Products US
P.O. Box 7869
Burbank, CA 91510-7869
Second Quarter 2003 Groundwater Monitoring at
Shel1-branded Service Station
5321 Stockdale Highway
Bakersfield, CA
Monitoring performed on June 19,2003
Groundwater Monitoring Report 030619-BF-2
This report covers the routine monitoring of groundwater wel1s at this Shell-branded facility. In
accordance with standard procedures that confol1n to Regional Water Quality Control Board
requirements, róutine field data collection includes depth to water, total well depth, thiclmess of
any separate Ì1IDniscible layer, water COlU1IDl volume, calculated purge volume (if applícable),
elapsed evacuation time (if applicable), total volume of water removed (if applicable), and
standard water parameter instrument readings. Sample matelia] is collected, contained, stored,
and transported to the laboratory in conformance with EP A standards. . Purgewater (if applicable)
is, likewise, collected and transported to D.K. Environmental.
Basic field infol1natiol1 is presented alongside analytical values excerpted from the laboratory
report in the cumulative table of WELL CONCENTRATIONS. The full analytical report for
the 1110st recent samples and the field data sheets are attached to this report.
At a minimum, Blaine Tech Services, Inc. field personnel are certified on completion of a forty-
hour Hazardous Materials and Emergency Response training course per 29 CFR 1910.120. Field
personnel are also enrolled in annual eight-hour refresher courses.
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Blaine Tech Services~ Inc. conducts sampling and documentation assignments of this type as an
independent third party. Our activities at this site consisted of objective data and sample
collection only. No interpretation of analytical results~ defining ofbydrological conditions or
fonnu]ation of recommendations was perfonned.
Please call if you have any questions.
y ours truly~
Francis Thie
Vice President
FT/ks
attachments: Cumulative Table of WELL CONCENTRATIONS
Certified Analytical Report
Field Data Sheets
cc: Gretchen Tagavil1a
KHM Environmental Management~ Inc.
911 S. Primrose Ave., Suite K
Monrovia, CA 91 0 16
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I· SAMPLING PROCEDURÈSOVERVIEW ,
I SAF1zTY
. . ". ·....1.., . . . :. . ',. . .,',
I· . An gr'QUndwafer,iTÍonitoring assignments pe¡formed,foi- .Equ1Vå Cómp)y with Ec¡ui,va~s såfè.ty, ,
. gufdeliI1èß, ~g CFR 1-910.,120 aDd SB-198In]uryèmd Ulness Prèventlon Program .(IIPP).. All" '
. 'Field Technidansreceive, the·ful/ 40 hour 29CFR 1910'~12o OSHA SARAHAZWOPERcourse¡
I .rt1~¡jjè:<i1 d~aråhGê and ~l:hthe4ob tråinlngþtjor tocort1mendnQ aný work on å~Y EÍ1lJlvá ~lIè",
INSPECTION AND GAÛGING ; I
I' WEills ari; rnÏ;þèctEidpriorto evacUaßònahd sampling. The cOn d iiloi1 'of ttie Wellhead is'di';Ckèd
and noted according to 'a weUhead ilis'ÇJ8ction: checklist.
I SIài1~~id measurement~ In dude the dèþth,to vial"r (DTW) and fhè tolàl ';"èll ðePlh(TD ;" ,
obtain~d with Industry stândard'electronic' sourid~rs' Which' are gradu'ated iniihcrements òf
I hundredths ota fòot., , ' ' .
The water i~'eachyje"'is ¡nspect.~dfQr'fhë.pr~sence bf Immiscibles or sheen and'when free'
I product is. $uspeçfed, It is. corifimied l.Jsirig an" electtonic interface probe -(e.g!:MMC)';· No, .
s~mípJes are cbllected froni a well containing OVer twö~hundredths of a foot (o.02') of prodUct.
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BLAINE TECH SERVICES~ ·INC. , '
METHoqs' AND PROCEDURES
FOR' THE ROl!T NE"~1-0NITORING'OF.
GROUND\lVATËR'WELLSA T EQUIVA SITES
" '. ,
B ~ine' T eC~'$ervi~esi "ib. perfórms envi¡-onm~htal sampling. and~ document?t¡Qn as :'âh'. .
independent third party. We -speoia j~e i~ groundwater rtlonitoringassighrh~nts and iritentionallY
limit the. scope of 'Out ~ervices to those'cente¡red on tlie gerier13tion of òbJective li1formé3 ti on..'
; To avoid cODflict~ of interest., Blaine Te~h Servi,ces, ,Inc. þersonnel do nòt eValu'~te;or interpret
the ihformafiqn we coflect. As' á :state licensed cQntråctor (C.,57 well drilling -'-wafer 1'""" ,746684 )
perforniJng strictly technica; serviçes, we db not make any'pr.ofessiohal recommendations anq,
. peffQrm no consulting 'of any kind. , .' " ' , . -
'. :.
I EV~CUATJON.
I' Deþt~io wate~,measu¡-ements,are collected by our periDnnef,pri6: ~ÌJ purging. andrriìnimUm, . .
purge'völumes ar~ calculated anew for each well based on the heIght of the water column and
the diameter of the well. Expected .purge volumes are riever Je~s than three cBE>è volumes and
lare set at no less'~han four case volumas In somajurlsdlctions,
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I. . PARAMETER STABILIZATION, .
Well purgJng 'corripleíio~' ~tat1datds include minimum, purge vo!úmes, but additionallY requiré·
I stabilization of spedne groundwa.ter parameters prior tcï sample ,collection. 'Typical groundwater
parameters Lisèd ,to mea~ur~ stability are electrical,çöndtictivity,,:pH, andternp'enature.· "
Instrument readings ate ,obtained at regularin'tervà!s during the evaouaUon ptQç:ess (no lE?sS
I than onos per case volume). . . .. . . .
Stabilizatior.r standards for, routine Cjuar!erly rnc;inltbring of fùel sites 'Include the following:'
Temperature'is considerèd t.o Jiavé :'stabilized when,·'successive. r.eadlrigsd6 not flûcluate' more
I than +/-1 dE?grøe Celsius. Electrical, conductivitY-is considered stable .whén sucœsslvé· .
. readings are within 1.0%. pH is considered to be stable whE?n successive .readings remain
I . constant" Dr vary no more than 0.2 of a pH unIt" . .
:DEWA TERED WELLS
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Well purging devices are ~elected .on the basis ofihe well diameter,imd the total volume to be
evacuated. Inmost-cases-.the well will be purged using an electric sUþtilersitjle pump (i.e.
'. Gtundfos) susp'ended near (bat not touéhing) the botlbm of the·we'lI. Smal! volumes of
purgewatet a~e often removed by hand bailing with a disposable bailer.
. .. ,,-
, .
Normal ev~cl,.Iatioh removes no Jess than three 'casé volumes of watêr from thê welL However,
less 'water may, be rembyed in cåses where the well ~ewptérs and dcíêS not'rechåI'Qe~ " . .
. ," . . _. . ..:1
Wells known to dewater are eVacuated as early as poss}þle during each site Visltiri Qrder tb,
, :aIiöw for the 'greátest amount of~ecöVérïrig. ,Any w~ll that does not-r.ßchargètbBD% of Its
1"orJgin8,I volume y.tilf be's!lmple~. p.rior to th:e departLire of our persoqnEiI from the $ite in order to
eliminate' the nee~ of a return VISIt. '.' '. '.. " . .: . .,,' , '. ' ' . "
I' In Jurisdietions_ where a ,certain þercentage of recovery i~ inclùded, in'the iocal completion .
standard, our pers.?nnel,follow the' regulatory expectaU~n. .'. ',' ,
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I PURGEWA TER·.CONTAI~MENT " .' " " . .
, . Allno/!-hazårdous purgêwa~et evacuated from'eaéhgroundwater:rhonitoring well Is 'captured' "~
I' andcontai!1ed in on-board storage -t~nk~. òn, thé' sa.m,' piing V ehielearid/ör special,wàt,er haÜling .
. trailers. Effluent from th~ decontaminatIon' of reusable apparatus .(soUnderš¡ electric.punipsa¡rid
. hoses,ëtc.)~' cqnsistinfJ :õf gro¡jndwat~rcomhinéd withdèicinizèdwater and non.:.phöspnëhe soàp,
lisa/so cáp,turéd and~ulT!.p~d into:effluent- tan~s. " . . , " .
. Nonhazardous purgéwater is transported und~r stE\ndard. Bill of Lading docum'éntatidli to'å '
I;'~il~;. T edi Services, Inc. facility qèfo~e being lransportedto an Equiva approved dispòsal
iAMPLE cou:'E¿i,ON DEVICES ::
(If' sa~Ples:~re collected using a ~tainle~s steel. t~fJon or disposable bailers..
'Fn"i.,~ '1',...¡.h .c::,..rv!r:¡.,.ç Tnr:,
PAO'''' ')
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SAMPLE CONTAINEFfs
Sa~ple material is deeantêd directl¥ from, the sa'r:n~lihg bailer into' sarnple,containers'provided
by the laboratory wliich wiH añaJyze 'the samples. The transfer of sample material 'from the
.'bailer to the si3niple container confomls to specificâtibns contained in the, USEPAT£.G.D., The' \ .
type of sarnple contaIner; material o(co'nstrucìian, method.of closyre and filling rèquirements
are sp~cifjc to the inìendeg ån~IYsÎs. C[l€!micpls ne~ded, to preseNè the samplë material are '
'commof!/Y placed 'inside the- sample conta.iners by the,laI;oratory or. glasswa¡-~ vendor prior to ,
'delivery öf the, bottlé to oUr'.personnel. The láboratory sets. ,the number of.replicate,èontainers.
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TRIPaLANKs
Upon reqtiest, a Trip BI¿;¡nk is carried to ,each'sile and is keptJnsid,e the,~oolèr' fçir thedurâfion of
the ÚÜllpl!ng event It is turned. O\i.er tö the laboratory for analysis with the samþle~ from that
site.
bUPUCA TES
!Jpon requêst, one DupliCé!te sample is cOllected at E?~ch sit~. It' is up.to':th~, Field, Technician tci
'çhoose the well at which the Dup!icate is collected. Tyþically, a duplicate is êollectéd from öné
of the most contaminated wells; The DupHcate sample,is labeled DUp·thus renderin£} the
" sample blind. "
'SAMPLE STORAGE·
1 All sample «?~ntainer~s are pro~ptly ,placed in f~od 'gràde ice chests ~or storag~ in t~e field ,and
,- transport (dJr:ect or via our facIlity) to the analytlcaJ'laboratory that wIll perform ,the Intended
analytical' procedures.' These.. ice ?h~sts cont~in- quantiti,es of r.estaurant grade ice as a. '
. 'refrigerant material. The sample? are,rTiaintained in :either an"ice 'chest' or a refrigerator until.
relinqµished. intqthe cus~ody of the laboratorŸ or lâbo¡-atorYC:òutier. .,'.
. .
. -.. ,
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1- DOCUMENTATION CONVENTIONS
E'athand every sample cont~ine(has a label affixed tQ it' Ih ~Qst æs'és the?elâbels are '
I: gèn'erated by -our office persohneland are partiaj/y preprinted. 'Labels Q~Ùlalso. be hand written
by our field r:iersonf'!ei: The site is identifieg with the':store numbêrärid site address, as is the '.
particular groundwater w.ell from which, the samplê is drawn (e.g. MW-1,- MW-2, S-1 ,etc.). The
I time.af:Vhjc~ the sá~pl~ w~s collected and the initials of t~~ person collectIng the sample a.re ,
,handwntten onto the label. , " . .
, .
I Chaj~ Qf ~ustÓdY records are ,created using client specific preprinted fohns' following USEPA
specIfications. . .. , " . .. .., ,. .'
ISil.' Öf Lading records are c~nÌempöraneÓus .re'Cord~' ct~~t?d in th,e fie!~ .at the.site wh~re the" .
non:-hazardous purgewater JS -generated. Field TechntCIans use' preprInted BIll of .Ladlng forms.
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')::n,,;~p "("...,.:1, .~...rvinp~ Jhr.,
'POI CTP ~
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I. . DI$SOLV¡;:Ð ciXYGÉN READINGS'
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1 'The'þrobe and reel is decontaminafed betWeen weÜls.as described above~q Thé tT)ëter is .'
calibrated 'between w$/Is as per the' instructions -.in'. the operating'mahußl. The pròbe 'arid stirrer,
l.iS']Öwered iní6.the waterct;llurrin al/Òwed'tÖ stabilize before use: '
DEcaNT AM/NATION
. .' I
'All eq uipment is brought to the site ,in éle'an and sèrviceë3ble condition and'is cleaned after use.
, in each weir and before ,subsequent use. hi .any-other well., Equipment- is decontaminated beforë·
leaving the site. "~ , , ' . ,
. , .
, , The primary decohtaminaïion device is a comrqercial steam cleaner. The steam cleane~ is de;.
tuned to functÎbn- as a hpt pressure washer which is then operated with high quaiity'dt;!kmi4ed
water which is produced at our facility and" stprr?d onboard our sampling vehidê., Cleaning is
facilitated by the usè Qf proprietary fixtu(/~s and devices inClUded in thepatentèd workstation
(U.S~: Patent 5,535,715)·thal is ihcorporatedî,,' each sampling'vehicle~ The stean'- Cleaner is
used to deoon reels, pumps arid bailers. " ", ' " '. . " '
Any, sensitive, eq uipmerit:,or pärts. (i.e. , Dissolved 'Qxyçieil se'f sör membrane,' sounder. etc.) that. :.
cannot be 'washed Lisin¡;phediot High þtèssure:watèr¡ will be ?pn3yed with a non~phbsphate', ..
soap ånd deionized ,water sdlutiQn arid ri~sèd with dêioni~èd water.
EXAMPLE: The sounder is 'çleanéd -betw~eirw~"s i.!sinil Út¡; nOIl-'phosþhate ~9ap and 'deiònized .
waterso/ution follöwed ,þy deiohited water dnses,' The sounder. is· them. washéd with the ste'åin,
cleaner between sites or as necessitated by use in a :particulárlycOi1taminateçi'-Well. ' :
.' -
AII'Di~sQlv~d Oryger'\' readings·¡;¡i-êtßker, usingÝSI.'meters (~.g. YSI'Modðl5'Bor ~CJl.Ìiv~lent YS!
meter). These -meters are' equipped·wi.th, a YSI stirring device th?lt - enables them· to collect,., .
accurate in-situ ,readings., The'probelstirring devices"are l1Jodifiêd tp allow downhole' ," .
measurements to betaken from wellsi3s.sITiali as two-inch dianìèter:' , .
I' 9XYI~ATON'REDUCT O~POTENTIAL READINGS . " ,.. .
,All readings ,are obtained with eitHer Corning or My¡:on~L meters (e.g. Coining ORP-65 or.a
I Myron-L:Ultramßter GP). The'meteris deäned he:tweeri wells as .described above. The meter
, is calibrated ,é'!tthe start ofe~ch day according to theinstructioQ ~anual.lh'usè'th~ þtpbè is
placed in a cup of freshly obtainedmonitofing well wäter,and alloWëd.to stabilize. -' 'I '
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ApPENDIX C
LABORATORY REPORT AND
CHAIN-OF-CUSTODY DOCUMENTS
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~- a/science
I:;&nvironmental
Laboratories, Inc.
June 25,2003
Nick Sudano
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Subject: Calscience Work Order No.:
Client Reference:
Dear Client:
03-06-1100
5321 Stockdale Highway, Bakersfield, CA
Enclosed is an analytical report for the above-referenced project. The samples
included in this report were received 6/20/2003 and analyzed in accordance with
the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the
guidelines established in our Quality Assurance Program Manual, applicable standard
operating procedures, and other related documentation. The original report of any
subcontracted analysis is provided herein, and follows the standard Calscience data
package. The results in this analytical report are limited to the samples tested and any
reproduction thereof must be made in its entirety.
If you have any questions regarding this report, please do not hesitate to contact
the undersigned.
Michael . Crisostomo
Quality Assurance Manager
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
.._ .....__.~. _.... ."_'_4..~.~·_.· .'~'
. __~""'_n.___. ,_ ..._._......._.__.__....... u."___&_..__.._. _ . 0" "'~'~ ".._..'~. ._. ...__. ",_ ......-. _. . .
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p--'__" _." __.'h
~- a/science
I::~nvironmental
L aborator;es~ Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
ANALYTICAL REPORT
Date Received:
Work Order No:
Preparation:
Method:
06/20/03
03-06-1100
EPA 5030B
EPA 8260B M
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 2
Date Date Date
Collected Matrix Prepared Analyzed QC Batch ID
·'!!~;·:~:·:l.;Œ~;~:;;~;~Ì:~:SÜ{t!~~ª~~~'i~~':~i~iijt~,.~~:':~::',,::,Q~~J9ªj:::'¡':t't~j)~~~L~1, :
Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units
Benzene ND 0.50 1 ug/L Tert-Butyl Alcohol (TBA) ND 10 1 ug/L
Ethylbenzene ND 1.0 1 ug/L Diisopropyl Ether (DIPE) ND 2,0 1 ug/L
Toluene NO 1.0 1 uglL Ethyl-t-Butyl Ether (ETBE) ND 2.0 1 ug/L
p/m-Xylene NO 1.0 1 uglL Tert·Amyl-Methyl Ether (TAME) NO 2,0 1 ug/L
o-Xylene NO 1.0 1 ug/L Total Purgeable Petroleum ND 50 1 ug/L
Hydrocarbons
Methyl-t-Butyt Ether (MTBE) ND 1.0 ug/L
Surrocates: REC (%) Control Qual SurrOQates: REC(%) Control Qual
Limits
1,4-0ichlorobenzene-d4- TPPH 96 70-130 1,4-0ifluorobenzene 92 70-130
1,4-0ichlorobenzene-d4 97 70-130
Parameter Result RL OF Qual Units Parameter Result RL OF Qual Units
Benzene NO 0.50 1 ug/l Tert-Butyl Alcohol (TBA) NO 10 1 ug/L
Ethylbenzene ND 1.0 1 ug/L Diisopropyl Ether (DIPE) ND 2.0 1 ug/L
Toluene NO 1.0 1 ug/l Ethyl-t-Butyl Ether (ETBE) NO 2.0 1 ug/L
p/m-Xytene ND. 1.0 1 uglL Tert-Amy -Methyl Ether (TAME) ND 2,0 1 ug/L
o-Xylene NO 1.0 1 UglL Total Purgeable Petroleum ND 50 1 ug/L
Hydrocarbons
Methyt-t-Butyl Ether (MTBE) ND 1.0 ug/L
Surroaates: REC(%) Control Qual Surroaates: REC(%) Control Qual
Limits
1,4-Dichlorobenzene-d4- TPPH 97 70-130 1,4-Difluorobenzene 99 70-130
1,4-Díchlorobenzene-d4 98 70-130
Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units
Benzene ND 0.50 1 ug/L Tert-Butyt Alcohol (TBA) NO 10 1 uglL
Ethylbenzene ND 1.0 1 ug/L Diisopropyl Ether (DIPE) ND 2.0 1 ug/L
Toluene ND 1.0 1 uglL Ethyl-t-Butyl Ether (ETBE) ND 2.0 1 ug/L
p/m-Xylene NO 1.0 1 ug/L Tert-Amyl-Methyl Ether (TAME) ND 2.0 1 uglL
o-Xylene ND 1.0 1 ug/L Total Purgeable Petroleum ND 50 1 ug/L
Hydrocarbons
Methyl-t-Butyl Ether (MTBE) NO 1,0 ug/L
Surroaates: REC(%) Control Qual Surrocates: REC(%) Control Qual
Limits
1,4-Dichlorobenzene-d4- TPPH 98 70-130 1 ,4-0if)uorobenzene 101 70-130
1,4-Dichlorobenzene-d4 98 70-130
RL - Reporting Limit. DF - Dilution Factor. Qual - Qualifiers
7440LincolnWay,GardenGrove,CA92841-1432 .. TEL:(714)895-5494 · FAX: (714)894-7501
-~~. ....-.--..-- ~._~._.. ".- ......'_..~._...._.... ......_~_.-..
.-' . .....- -..' -.. . -
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IE - a/science
I:, nvironmenta/
Laboratories;, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
ANALYTICAL REPORT
Project: 5321 Stockdale Highway, Bakersfield, CA
Date Received:
Work Order No:
Preparation:
Method:
06/20/03
03-06-1100
EPA 5030B
EP A 8260B M
Page 2 of 2
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Parameter Result RL DF Qual Units
Benzene NO 0.50 1 uglL
Ethylbenzene NO 1.0 1 uglL
Toluene NO 1.0 1 ug/L
p/m-Xylene NO 1.0 1 uglL
o-Xylene NO 1.0 1 ug/L
Methyl-t-Butyl Ether (MTBE) NO 1.0 uglL
Surrogates: REC(%) Control Qual
Limits
1,4-Dichlorobenzene-d4- TPPH 98 70-130
1,4-Dichlorobenzene-d4 99 70-130
Date
Collected
Date
Prepared
Matrix
. QC Batch 10
¡.,
Parameter Result
Tert-Butyl Alcohol (TBA) NO
Diisopropyl Ether (OIPE) NO
Ethyl·t-Butyl Ether (ETSE) NO
Tert-Amyl-Methyl Ether (TAME) ND
Total Purgeable Petroleum ND
Hydrocarbons
RL
10
2.0
2,0
2.0
50
DF Q!@!
1
1
1
1
1
Units
uglL
ug/L
ug/L
ug/L
ug/L
Surroaates:
REC (%) Control
Qual
1 ,4-Difluorobenzene
100 70-130
I
Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units
Benzene ND 0.50 1 ug/L Tert-Butyl Alcohol (TBA) ND 10 1 uglL
Ethylbenzene ND 1.0 1 ug/L Diisopropyf Ether (OIPE) ND 2.0 1 ugIL
Toluene ND 1.0 1 ug/L Ethyl-t-Butyl Ether (ETBE) ND 2.0 1 ug/L
p/m-Xylene ND 1.0 1 ug/L Tert-Amyl-Methyl Ether (TAME) ND 2.0 1 ug/L
o-Xylene ND 1,0 1 ug/L Total Purgeable Petroleum ND 50 1 ug/L
Hydrocarbons
Methyl-t-Butyl Ether (MTBE) ND 1.0 ug/L
Surrocates: REC(%) Control Qual Surrocates: REC(%) Control Q!@!
Limits
1,4-Dichlorobenzene-d4- TPPH 98 70-130 1,4-Difluorobenzene 99 70-130
1.4-Dichlorobenzene-d4 99 70-130
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1-
RL - Reporting Umil. DF - Dilution Factor, Qual - Qualifiers
l...-----'..,........ '--"'''----'' ..,-........ .-. .............--...-,....., -_.~....-,-_......_.
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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.:
~ - a/science
I::,¡g¡ nvironmental
Laboratories, Inc.
Quality Control - Spike/Spike Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
06/20/03
03-06-1100
EPA 5030B
EPA 8260B M
Project: 5321 Stockdale Hiç¡hway, Bakersfield, CA
Quality Control Sample 10
Date
Prepared
Date
Analyzed
MS/MSO Batch
Number
Matrix
Instrument
;%~1~('~:..;¡;1¿~;;~~Atj~~ici¢~,Ùlf;:;;'i~·~ii4J~~Ù;,~;,i~!;\1·~~~toj::;i'\.,.:i:;·::'03Ô~2iš01,'
Parameter MS %REC MSD %REC %REC CL BEQ RPD CL
Benzene 109 113 61-139 4 0-27
Ethylbenzene 106 110 81-123 4 0·16
Toluene 96 102 76-124 6 0-12
p/m-Xylene 113 116 85-121 3 0·15
o-Xylene 106 110 85-121 4 0-14
Methyl-t-Butyl Ether (MTBE) 102 107 73-127 4 0-18
Tert~Butyl Alcohol (TBA) 118 128 40-172 5 0-31
Diisopropyl Ether (DIPE) 99 103 73-121 4 0-14
Ethyl-t-Butyl Ether (ETBE) 99 105 77-125 6 0-15
Tert-Amyl-Methyl Ether (TAME) 96 104 74-128 8 0·16
Total Purgeable Petroleum Hydrocarbons 99 103 82-118 4 0-13
Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894·7501
_.- "'- ..,". .~_.... .._.,~..... .-. ~._... ...
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~- a/science
. I:'-.n vironmen tal Quality Control - Laboratory Control Sample
Laboratories, Inc.
Blaine Tech Services. Inc
20360 Gramercy Place
Torrance. CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
06/20/03
03-06-1100
EPA 5030B
EPA 8260B M
Project:
5321 Stockdale Highway, Bakersfield, CA
Quality Control Sample ID
LCS Batch Number
Matrix
Date Analyzed
Lab File ID
Instrument
.,: :Wci~1~~1:.: ,.
., Yo -I, )- , ,.. '! ," "M" >-"-' " ..
~ s,pe ':. " ',' ;, ~ : 06I2~lÒ3 . ;. " -:,~, 21"ÌJNOQOí" "
, , ;.;,·.,.if"~'H":"~" c.C_"~"~"" ~,,, !r1W,'
Parameter
Benzene
Ethylbenzene
Toluene
p/m-Xylene
o-Xylene
Methyl-I-Butyl Ether (MTBE)
Tert-Butyl Alcohol (TBA)
Diisopropy1 Ether (DIPE)
Ethyl-I-Butyl Ether (ETBE)
Tert-Amyl-MethyJ Ether (TAME)
Total Purgeable Petroleum
Hydrocarbons
Cone Added Cone Recovered °/, Rec 'I,Rae CL Qualifiers
50 54 107 80·122
50 54 108 87 -117
50 51 101 81-123
100 110 112 85·122
50 54 108 85-121
50 52 104 81-117
250 230 90 68-128
50 51 102 78-120
50 51 103 81-123
50 48 96 78-126
750 780 103 88-112
I
7440 Lincoln Way, Garden Grove, CA 92841-1432 ;. TEL: (714) 895-5494 · FAX: (714) 894-7501
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&.;alscience GLOSSARY OF TERMS AND QUALIFIERS
1f:1'vironmental
Laboratories, Inc.
Work Order Number: 03-06-1100
Qualifier
Definition
NO
Not detected at indicated reporting limit.
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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C:ñICl8nce
--'rlnHrm..nml
'.borIItorl... Inc.
WORK ORDER #:
03 - [Q1[fJ - [][L]~[Q]
Cooler / Of,/--
~
SAMPLE RECEIPT FORM
~
CLIENT:
TEMPERATURE - SAMPLES RECEIVED BY:
DATE:
CALSCIENCE COURIER:
Chilled, cooler with temperature blank provided
.yntlled, cooler without temperature blank,
¿ Chilled and placed in cooler with wet ice.
Ambient and placed in cooler with wet ice.
Ambient temperature,
3- DC Temperature blank.
LABORATORY (Other than Calscience Courier):
___ DC Temperature blanl<.
o C I R thermometer,
Ambient temperature,
In;';al: t$?
CUSTODY SEAL INTACT:
Sample(s):
Cooler:
No (Not Intact) :
Not Applicable (N/A):
Initial:
SAMPLE CONDITION:
Chain-Of-Custody document(s) received with samples.. .................. ~. . . ... . No . .. .. . .
Sample container label(s) consistent with custody papers.......... ,.,.. ..... ~.. .... ... ....
Sample container(s) intact and good condition.".,.,..,. .',. ",. .", '., ..,.,.. ~/,... .,. ..,.
Correct containe~s for analyses requested... ......... .,.. '. '....... ,...,..... ~.. ~ .... ... ....
Proper preservation noted on sample label(s)... .,..... ..,.. ............. =--/.... __." ....
VOAvial(s) free of heads pace. .................. .....'.......... ...... ......... V... ,... .......
Tedlarbag(s) free of condensation......................... ....,...'.. ..,.., '....__....... .......
N/A
//
¿./"
Initial: ~ 2/"
'--'
1...--
COMMENTS:
.
JIIí
IIIIÍ _ ...
LAB: ((./ St./u'Ice
..
-
Lab Idenlificalion (il necessary):
Address:
City, State, Zip:
SAMPLING COMPANY,
LOG CODE:
Blaine Tech Services, Inc.
BTST
ADDRESS
20360 Gramercy Place, Torrance, CA 90501-1511
PROJECT CONTACT (H.,.d<:opy or PDF Report to):
Nick Sudano
-
TELEPHONE: I FAX' E-MAIL:
310-782·2465 1310'0782.2958 nsudano@blalnetech.com
TURNAROUND TIME (BUSINESS DAYS):
;8:( 10 DAYS 0 5 DAYS 0 72 HOURS 0 48 HOURS 0 24 HOURS 0 LESS TIiAN 24 HOURS
o LA - RWQCB REPORT FORMAT 0 UST AGENCY:
GCIMS MTBE CONFIRMATION: HIGHEST
SPECIAL INSTRUCTIONS OR NOTES:
HIGHEST per BORING
CHECK BOX IF EDD IS !iQ! NEEDED U
ALL
:~J"
Field,Sample Identification
SAMPLING
DATE TIME
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DISTRIBUTION: While
Green 10 File. YellOW and 7nenl.
MATRIX
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Received by: (Signature)
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5321 Stockdale Highway, Bakersfield
SHELL Chain Of Custody Record
SITE ADDRESS (Street and Cltyl:
EDfDEUVEAA8LE "~RI"OIUTO(A~p.-ty.o~ :
Gretchen Tagavilla
SAMPLE-A. NAME.(S} (Pri!\l.):
ße-/I Fú."ltt.
NO. Of
CONT,
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IØSq~~E~ e~G'~EE~N~ Tony Palagyl
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FIELD NOTES:
Container/Preservative
or PIO Readings
or Laboratory Notes
TEMPERATURE ON RECEIPT C·
Time:
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Te){sco Refining
SInd l\Rar!teilng Inc
10 Universal City Plaza
Universal City CA 91608
ENV-SERVICE STATION
Dispenser Removal Report
5321 Stockdale Hwy
Bakersfield, CA
!fõJ æE (Ç; œ; II \)f œ; ~
t!! AUG 1 6 1995 MI
By= . I
August 14, 1995
---------
- --r--- - ----.----.
-~----
Mr. Howard Wines
Bakersfield City Fire Department
Office of Environmental Services
1715 Chester Avenue
Bakersfield, CA 93301
Dear Mr. Wines:
Enclosed is a copy of a Dispenser Removal Report which describes
remediation activities that were performed during the replacement
of dispensers at the subject Texaco facility.
As described in the aforesaid report generated by Pacific
Environmental Group Inc., minor soil excavation (approximately 31
tons) has enabled Texaco to collect remedial confirmation samples
that are' below Bakersfield City Fire Department action levels.
Therefore, Texaco is requesting case closure.
Should you have any questions or comments please call me at (818)
505-2739.
Sincerely,
MJ~-
ß¿
Marcel L. Bouchez
Project Coordinator
Texaco Environmental Services
MLB:mlb
w:\mlb\bako\5321disp.bfd
Enclosure
PR: .IIIEt
Building on a Tradition of Quality
-----::::' -
.,
PACIFIC
ENVIRONMENTAL
, , GRDUP.JNC.
j
"
, Mr. Lee Bòuchez
Tèxaco Environmental SerVices
.. ','. ,.
10 Universal City Plaza, 7th Floor
'Ùi1iversal City, Califomi~ 91608
.'
Re: Tránsmittal:Dispenser Removal Report ,
" /
Texaco Service Station No. 61-058-0450 .
5321 'Stû'ckdale Highway
. Bakersfield, California
, Dear Lee:'
Pacific EnviroÌ1mental Group, Inc. (PACIFIC) is pleased to transmit to you four copies of
the attached report of findings for dispen~er removal activitIes performed at the above
referenced site.' A copy of the report should beÎorwarded to the attention of Mr. Howard
Wines at the Bakersfield Fire Department, Office ofEnvirònm~nt~1 Services, '1715
, Chester Avenue,' Ba~ersfield, California 93301. .
"
PACIFIC appreciates this opportunity to be of service to Texaco.' If you have any questions
~ . . ,
regarding this report, please call either of us. '
Sincerely;'
. Pacific Environmental Group, Inc.
Jjl?~
Gary~ana '. ,',
Projèct Manager
Encl.:, ,(4) c<;>pies Dispenser Removal Report
650 Sierra Madre Villa, Suite 204, Pasadena, Californiq 91107
(818) 351~4814
FAX (818) 351-4822
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PACIFIC
ENVIRONMENTAL
"GROUP. INC~,
" -./ .
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,August 10,1995"
Projèct 740-004.1A ." "
Mr. Lee Bouchez
Texaco Environinental Services
¡ 0 Universal City Plaza, 7th Floor
Univers~l City', C~lifomia 91608
Re: Disp'enser Removal Report
Texaco Service Station No. 61~058-d450'
5321 Stockdale Highway,
Bakersfield~ California
D~ar Lee:
Pacific Environinental Group,Inc. (PACIFIC) þ.as completed observation and sampling of
'the dispenser removal oversight at the-above-referencedTexaèo sérvice station. This work
" was performed on July 6, 1995.' The purpose of this work was t~ observe dispenser
removals and to collect soil s~ples from' beneath the fuel dispensers as required by
Bakersfield FireDep~ent (BFD)., I
,BACKGROUND'
Facility D.escription. The project site is ~ operating Texaco service ~tatiOIi that provides
retail, gasoline products iIi 'the City of Bakersfield (Figure 1): The ,site' consists of a station
building, ,service bay, three fuel dispenser islands, four 'undergrovnd storage tanks (USTs),
, and ope waste oil tank (Figure '2). The site, is bordered by Stockdale Highway to the north
and New Stine Road to the 'west. /.
DISPENSERREMOV AL AND EXCAVATION
Dispellser Removal and Sampling. On July 6, 1994, the existing fu~ldispensers were
removed by K.E. ÇurtisConstruction (K.E. Curtis). Additional excavation utilizing a
backhoe, and confIrmation soil sampling was perÎormed where impacted soil waS
en~oulltered.· Prior to dispenser removal, K.E. Curtis notified the Baker:sfield Fi~e'
, DepaÎtment.·. . ' '
'.)
. "
\\gondor\projec,ts\ 740\ 7400041 ~\report\dispenser.doè '
650 Sierra Madre ViI'la, Suite 204, Pasadena, California 91107.
(818) 351-4814
FAX (818) 351-4822"
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,August 10; 1 ~95
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, ,þ Ac'IFI C 'pérsonnèl'còÍlected sóil s~ples a~ 2 and 6 fee! below e~chdispense.r ~tilizing
"hand auger equipment perBFD:requiremelits; Additional soil samples were collected after
· . over-excavation of hydrocarbon, impacted soil" was' compl~ted. ,'À. tot,!l of, thirty-on~ (31) , .
soil samþlès, were collected''frombeneath the fu~l dispensers. Initial soil samples we~e ' .
" collèète? in hand-drivenbrassslee~es, and capped with Teflon and plastic end caps, }..'. .
Confirmation soil sarÍlples' were collected from the backhoe bucket in gl~s jars with :feflon ,
, coatèd 'lids. . Initial soil ,samples: arid èonfirmatiori samples were collected at qepths ranging .
.' .' " . . I ' .
between 2 and 10,feet below ground surface (bgs)., '
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\, Over-Éxcavat~on ActivIties. Dueto elévatedleve,ls ofhydròçarbonsen~,ountéred,'in
" ..samples Dl1~I-6;,Dl1-3.,2, DI2-2-~, DI2-3,.2,and DI3-4-2, additionalexcavation'was'
performed,to remove hydro~~b,on impacted soil (Figure 2). The.areas of imp~ct were' ','
excavated to dep.ths of 4 to 6.5 feet bgs and confirmation samples Were collected at thè\
· bottom 'of th~ ,excavation (Fígm-e 2). A tbtal of approximately 20 cub,ic, yiird~ of impacted
.'spil were removéd duripg excavàtion activities. \ ' , .
. .
, . .
,Soil Disposal.: AlÍexèavated-soil frcimthedíspenser rewovals were stockpiled ~~site for,
" chàract~rizatiop. àÍ1d disposal A total of tWo (2) soil saniplè~. (Stockpile 1 0(2 an~ 2 of 2)
werecollect~d fromthestockpile'for laboràtory,analysis. , The soil stoékpiles wen~ '
· removed :from the site 'on July 1'2, ~ 995. Manifests of soil disposal ,are, iq.cluded in,
'Attachment 1. ", ' , ' . . ' " ,'. , " ,: .,','
. . .. I
\ ~, "
, Laboratory Analysis., S-<?i1 samples colleète.d during the dispenser/prodùct piping rerhoval
wen~ delivered to anonsite state-Gertified mobile analytical laboratory.' Samples were ' ,
analyzed fo~ total petroleÙ1TI 'hydròcarbons (TPH) as gasolin,e aIi,'d benzene, toluene,
. 'ethylbenzene; and total xyleÌ1es(BTEX) using US. EPA Methods 80ÌS Modified and 8020,
respectively. Selected soil sample,s ~ere also amdyzed for TPH as, diesel using U'S. EP A
, , . " .., I
Method 8015 ,Modified.· Soil samples cQllect~d from beneath the dispensers ahd from the
soil stockpilè eilibiting the high~st TPH~g àlld TPH-dconcentrati~ns were' also analyzed .
for t~tai lerid by EPA, Method 60 lÖ~ : The soil analytical results ~e sumrriariied on Table (
, " . . ~ . \ I
Cháin~of",cust~dy docuinentation is presented in Attaçhment 2:. "
, . '. - .
FINDINGS
,.
. Initial Soil Analytical Result.s. Labor':1:tory analysis of ~oil s~ples colle~ted'fiom the fuel
,'dispensër rfniova~ revealed a maxiinum tota1.petrole,umhydrocarboil (TPR-g)as gaSoline.. .
concentration of 740 mg/kg (DIl-l;.6). All remaining soil samples revealed TPH-g
, conce~tration:s r~ging fröm not detected «10 mg/kg);to 15Q mg/kg'(DI2-2-6).' Total
,', petroleum hydrocarbons as diesel (TPH-d) was detectedjn~arÍlples"DIl-3-2 (2,400 mg/kg)"
'\' " " ' ,', ':. 'I,", '.,.. .', . ,'.' " .. ' I " .
. "\\gondor\p~,ojects\740\7400041ii\réport\dispenser;doc
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, ,'Augusp 0, 1995
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DI2';3,-iq90 mg/kg), and DI3-3-~(34mg/kg). Bem:el1e ~oricentration~ in:soil s,~ples'
rangëdfrorÌ1'not detected to 0.23 mglkg{DI3~4-2) (Table 1).. . .'J
., ,
'Confirmatio~ SoilAnalytical Results~ Analysi~ of donfinnationsoll sàmples reveäledno
, 'TPH-d aboveJaboratory detec~iön limits and·a'maXimum TPH~g ~oncentratiori of 12,
'ri1glkg(DI2-2-6~5). A maxiInurrÌ,benzene concentration ofO~12 mglkgwàs detëctedin
'. sàmple DI2-2-6.'~. ' '" " "\ ' ' ,.
. Stockpilè Analytical Resúlts., Labor~torY anà1ysls of' stockpiles sàmples ~évealed.
. 'n1flXirilUm TPH;-g arid TPH-d 'con~entrations of 270mglkg {Stockpile 2} and 630 rpglkg
(Stockpile 2), respectively (Table 1). '.
" , .
-, Subsûrfaèe CondiÌions. Soils encountered dúring .excavation élÇtivities consisted prim~il)'" "
" of sands and silty s.arids to the totardeptl1 explored of 1 0 feeib~s. Groundwàter was not
. .', . encountered during' excavation or sampling.
SUMMARY
" ,
, J'
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The following:is a, summary of the res~lts of closUre' sàmpÎes collected during relI).o~al of
,the fuel dispensers:' " ' .' ' , , . ' " . '
, '
~ ,_.' ,,' ¡I
. ,OnJuly 6,.1995,- the ~~isting fuel dispensers were removed and impacted soil ,
e"xcavate~ by.K.E.Curtis Construction <K.E. Curtis). PACIFIC personnel collected,'
"0 soil sàmples from beneath the fuel dispensers pet the,BFD requirements. Additional ' \
,', " confinnati~n Saniples'wen:~ collected after oVer-excavation, of hydrocarbon impaqted
, soil was complete. Thê excavated soil was stockpiled oIÍsite, and sàmples were
" , ~ .,. collected to dete~ine the, app[opriáte disposal methqd. ' ' "
, "
, , . . TPH-g.and TP{I-d concentrations exceeding 100 rÍ1glkg were detected in fi~eofthe,' .
thirty-one sòil s~ples 'collected from beneath the fuel dispensérs.
. " " - -. . .. . \
, .
. _ Soil with TPH concèntratiònsabove 100mglkg'was ovèr-excávàt~d to depths betWeen
.4 and 65 feet bgs~ConfirmaiiOIi sàmple's indicated no TPH-g orTPH-d concentI:atio,ns ,
. I" . . " ,
above 100 mglkg (Figure 2 and Table 1). 'I" ',- . .
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Mr. Lee 'Bouchez
'AugùsU 0,--199,5 '
, . : Page 4 .' '
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Thisw6rk was perfoimed c~nsistent ~ith generally accepted enviromri.ental cònsultiJ;1g
,practices and principles. . If you have anY q~estionsregarding this report, do not hesitate to'
call. ',;' '
, -.....
. .
, S,inée~ely, ,
Environmêntal Group, Inc.
."p'Q'~".':,-',','."
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. . Sèniór Hydfogeologist
. ' GarY P: P stana'
, Project Geologist
, "
Attachmepts: Table 1'- ',Summary of Soil Analytical Results ..
F~gure '1 - Site'Location Map , ,
Figure2 - Site 'Plari .
-Attachment I - . Manifests of Disposal ' ' . .
. ' Attachment ~:- . Analytical,Report and Chain-of-Custody Documentation
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-------------------
Table 1
Summary of Soil Analytical Results
Texaco Service Station
5321 Stockdale Hwy., Bakersfield
Boring No. Date Sample Ethyl- Total Total
Sampled Depth TPH-g (1) TPH-d (2) Benzene (3) Toluene (3) benzene (3) Xylenes (3) Lead (4)
(feet) ( mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg)
DIl-1-2 6-Jul-95 2 2.9 na <0.1 <0.1 <0.1 <0.1 na
DIl-1-6 6-Jul-95 6 740 na <0.1 2.9 4.8 39 11
DIl-1-6.5 6-Jul-95 6.5 <10 na <0.1 <0.1 <0.1 <0.1 na
DI1-1-1O 6-Jul-95 10 <10 na <0.1 <0.1 <0.1 <0.1 na
DIl-2-2 6-Jul-95 2 7.0 na <0.1 <0.1 <0.1 0.28 na
DIl-2-6 6-Jul-95 6 <10 na <0.1 <0.1 <0.1 <0.1 na
DIl-3-2 6-Jul-95 2 na 2400 <0.3 <0.3 <0.3 <0.3 6.4
DIl-3-4 6-Jul-95 4 na <10 <0.1 <0.1 <0.1 <0.1 na
DIl-3-6 6-Jul-95 6 na <10 <0.1 0.12 <0.1 0.22 na
DIl-4-2 6-Jul-95 2 55 na <0.1 0.38 0.31 2.5 na
DIl-4-6' 6-Jul-95 6 21 na <0.1 0.11 <0.1 0.37 na
DI2-1-2 6-Jul-95 2 20 na <0.1 1.2 0.27 2.3 na
DI2-1-6 6-Jul-95 6 <10 na <0.1 <0.1 <0.1 <0.1 na
DI2-2-6 6-Jul-95 6 150 na <0.3 1.4 0.66 7.4 na
DI2-2-6.5 6-Jul-95 6.5 12 na 0.12 0.54 0.14 1.1 na
DI2-2-1O 6-Jul-95 10 12 na 0.16 0.36 <0.1 0.60 na
DI2-3-2 6-Jul-95 2 na 190 <0.1 <0.1 <0.1 0.10 na
DI2-3-3 6-Jul-95 3 na <10 <0.1 <0.1 <0.1 <0.1 na
DI2-3-6 6-Jul-95 6 na <10 <0.1 <0.1 <0.1 <0.1 na
DI2-4-2 6-Jul-95 2 37 na 0.10 2.0 0.43 3.6 na
DI2-4-6 6-Jul-95 6 8.2 na <0.1 <0.1 <0.1 0.15 na
DI3-1-2 6-Jul-95 2 <10 na <0.1 <0.1 <0.1 <0.1 na
DI3-1-6 6-Jul-95 6 <10 na 0.16 <0.1 <0.1 <0.1 na
DI3-2-2 6-Jul-95 2 <10 na <0.1 <0.1 <0.1 <0.1 na
DI3-2-6 6-Jul-95 6 <10 na <0.1 <0.1 <0.1 <0.1 na
DI3-3-2 6-Jul-95 2 na 34 <0.1 <0.1 <0.1 <0.1 na
DI3-3-5.5 6-Jul-95 5.5 na <10 <0.1 <0.1 <0.1 <0.1 na
DI3-3-6 6-Jul-95 6 na <10 <0.1 <0.1 <0.1 0.10 na
\\gondor\projects\ 740\ 7 400041 a\report\table l.xls Page 1 of2
-------------------
Table 1
Summary of Soil Analytical Results
Texaco Service Station
5321 Stockdale Hwy., Bakersfield
DI3-4-2 6-Jul-95 2 110 na 0.23 4.0 1.8 12 na
DI3-4-4 6-Jul-95 4 <10 na <0.1 <0.1 <0.1 <0.1 na
DI3-4-6 6-Jul-95 6 88 na <0.3 3.4 1.2 10 na
Stockpile 1 of 2 6-Jul-95 27 26 <0.3 <0.3 <0.3 <0.3 na
Stockpile 2 of 2 6-Jul-95 270 630 <1 <1 <1 12 22
REFERENCES:
(1) Analyzed by California EPA Method 8015 Modified for Gasoline reported as gasoline on Certified Analytical Reports (CARs).
(2) Analyzed by California EPA Method 8015 Modified for Diesel reported as diesel on Certified Analytical Reports (CARs).
(3) Analyzed by u.S. EPA Method 8020.
(4) Analyzed by U.S. EPA Method 6010.
NA = Not Analyzed
\ \gondor\projects\ 740\ 7400041 a\report\table I,xls
Page 2 of2
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QUADRANGLE
LOCATION
REFERENCES:
USGS 7.5 MIN. TOPOGRAPHIC MAP
TITLED: GOSFORD, CALIFORNIA
DATED: 1954 REVISED: 1973
SCALE IN FEET
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2000
I
2000
O PACIFIC
~ ENVIRONMENTAL
~ GROUP, INC.
TEXACO SERVICE STATION
5321 Stockdale Highway at New Stine Road
Bakersfield, California
FIGURE:
1
PROJECT:
740-004,1 A
SITE LOCATION MAP
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APPROACH
STOCKDALE HIGHWAY
APPROACH
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SOURCE: MAP BY TEXACO USA BLUEPRINT; DATED: 5·85
~
PACIFIC
ENVIRONMENTAL
GROUP, INC,
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WASTE
OIL TANK
1-'
PLANTER
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STATION
BUILDING
PARKING
. SOIL SAMPLE LOCATION
DI3-4'2(1101O.23) SOIL SAMPLE DESIGNATION AND DEPTH
(TPH in mglkg IBenzene in mglkg)
DI3-4-4 (NDIND)" OVER,EXCAVATION CONFIRMATION
SAMPLE DESIGNATION AND DEPTH (TPH
in mg/kg I Benzene in mglkg)
E:I
APPROXIMATE LIMIT OF EXCAVATIONS
TEXACO SERVICE STATION
5321 Stockdale Highway at New Stine Road
Bakersfield, Califomia
SITE MAP
FIGURE:
2
PROJECT:
740,004,1A
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MANIFE~TS OF DISPOSAL
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Numb", will> l'rs',
TPS Technologiès Soil Recycling
Non-Hazardous Soils
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Î _ t t _ ~ ~ 1<.....po2?ô II: Fa"iJrfll:
G'?~'WÅYtt\e Rilti'!it1f¡ i'HYfs: &. Mar~ et i ng I nc Genertl0;.rhond _ Ge11l'ralo,'s us ErA ID No.
Te)(ðCo Eov i ranllent a 1 Serv ice s ~_ ~ç r .::l 1'1' . -,-----__ '_
10 UCP "'er';~ntarß ~c.l.....
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CU8tom~'f Accounl Number with TPS;
Gen~tipn Site mtnsl'ort from); (,,¡¡me &lIddr.ssi
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Lew's
TPH
Le.'eI.
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Lewis
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Rd.lanto, California 92301
Facility I'crmil Numb"...
DJp.&d Œi.~~ ~n. tJ... ãoftttNJ
12328 Hibiacus Avenue
1:;)
~~'---
8004
.. .:! IUId Mliliog Addreó5;
25422 Trabuco Rd. *105-26~
lransporler's us EJ'A 10 Nt,.;
Sand CI
Clay Q
Ot¡;~';¡" CJ
other U
(',as a
Die"d 0
Other' 8
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Dìe~e! 0
.L_ OtJ\"r Q
~,C'!~ont'd'utll~Wl ",
,-Cl14) 8549-0109
FAXI/;
Tf¡tn.por'er·~ DOT N ),;
El Taro, CA 92630
.-.------.
Description of Soil
MoIsture Contenl
Description of Delivery
o ' 1()% c¡
1O-2(1'}1, 0
20%:· oveeO _
C-10% U
10-20% U
20% . over a
Lis. any e><oeptitm to lI.....lisl<d ~bo.c:
Sand CI
Clay 0
(.hganic IJ
OIñer U
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Generrztor's ,md/or consultunt's certifiClltim¡; I/We certify that the soil' referenced herein is taken entirely from those soils de9Cribed in the Soil Data
Sheet oompleted and certified by meíus for till! G~neratwn Sitf shown above and /Wthing has been added ar done to such soil fhClt would alter it in
any way.
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['lint "'I' 1}-pe Name'
Þ"\ 4 tl-c e. C-. L. 11 ~ ~ JI- E 2..--
Transporter's certifiUltion: //We acbwwled~e receipt of the soil described abovr. alld certify that such soil is being
condition ,as,whrn received. II We further t:vtify that this soit is being directly transported from the Generation
without off-loading, adding to, subtracting from or in any way ddaying delive t such site,
Print ur~DtM.:
~i"';-
DlsaepaJ\deo:
Goner.'",
I Siptln" .n" date: 0 , ß
. 1V1~:>,
~
-/::
=1
Li:
~
::::
~
~
Recycling F«iIity certifies the reaipt 0; the soil ;:overed try thIs /1111'1/[£5/ except
Print or 'typo Na"""
07/24/95
12:07 FAX 7148590109
BESI
I4J 004/005
I
I
" PS Technologies Soil! Re«:ycnng
. Non-Hazardous Soíls
ñanspomr'Truck II:
I
I
1nc
T~x~,co 'Envi\'onmental S~l~vicl'?~
perr:. ~ntaß~ ¿"L-.
fA II:
ç,~
Cu
Number withTPS:
10 IJC":'
UniY~rÐal 8i~y, CA 91&08
I
Consultint's Name and Billing Address:
COI(ilult~nt'~Phone II: '-,
"Z..cr
I
PersOn to Contact
FA II:
Customer Acwunt Numbet with TPS:
I
Ccnet!'tion Site (Transport from): (l1øme & address)
Sit'¡'Phone #.
BTEX
Levels
I
5" 3 J S-rOl:. k. !>t1 L. Ii:: HllÙý
~ A t£ .E It S FI (; L D (' A .
.' .
Pernon to Contact:
TPH
Levels
fAXII:
Ave.
Levels
I
Def¡(il~ t{ä~ns~g¡JI. èt$lt' tl~)
123¿B Hibiscu~-AYenue
FadIfty
Facility Pennit. Numbers
I
,.
. "
#105--269
,~. L f .
('.'
..,..J",.;.,..;__ -'r'
". 'i.
Adelanio, California ~2301
I
ãnd Mailing Addn.'5S:
Ty'abuco Hd.
Transporter's US EPA ID No,:
El Tot--n, CH
9~~6 30
Trans~r'::\.I??TNo:: ..,/
f . ·.,.t .J .
FAXIt:
Customer Acrount Number with TPS: '.
I
I
Sand Q
Clay Q
OIganic (]
Other 0
Moisture Content Contaminated by:. Approx. Qty: . ~rip1ion of Delivery
Q,,¡ Q
Diesel 0
0t1Ier 0
Gas 0
Dìesel Q
OtherQ
Gross _t Tare Weight Net WeIght
Description of SolI
I
0-]0% Q
10·2.0% 0
20% - ova- 0
O·lß% Q
10·20% Q
20% - <Wet 0
Uot any exœpfum 10 ¡!\oms lisad above:
Sand Q
O·Y Q
OrganicQ
Other Q
I
I
I
Recycling Facility certifies the receipt of the soil covered by this manifest except
Print or Type Nom",
I
'1
.
\
I
TRANSPORTFR'S r.OPY
1< .',
,I
I
I
I
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ATTACHMENT 2
,I
, .', ~NAL Y~ICALREPORT AND
, 'CHAIN-OF-CUSTODYDOCUMENTATION,
. . . '''.,
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I, '
. ¡
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"
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\\gondor\projects\ 74Ó\7 4Ó0041 a\repòrt\dispenser.d6c
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I
I
I
I
I
I
LOG NO
II ------------------------------
II ------------------------------
TPH/BTEX (8015M)
II
I
I
I
I
II ------------------------------
I
I
... ...
I ::::::
I ::111
ANALYTICAL REPORT
B C Annlytical
............................. . . . . . . . . .
801 Westem Avenue
Glendnle, C4 91201
8181247-5737
Fax: 818/247-9797
..........
. .,.
. .
LOG NO: G95-07-049
Received: 06 JUL 95
Mailed:
JUL I 3 !C]%
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
------------------------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
Date Analyzed
Dilution Factor, Times
Benzene, mg/kg
Toluene, mg/kg
Ethylbenzene, mg/kg
Total Xylene Isomers, mg/kg
Carbon Range,
TPH (Gasoline Range), mg/kg
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
Page 1
-----------------
-----------------
-----------------
07-049-1
07-049-3
07-049-2
-----------------
-----------------
-----------------
06 JUL 95
01-1-1-2
06 JUL 95
01-1-2-6
06 JUL 95
01-1-2-2
-----------------
-----------------
-----------------
07/06/95 07/06/95 07/06/95
100 100 100
<0.1 <0.1 <0.1
<0.1 <0.1 <0.1
<0.1 <0.1 <0.1
<0.1 0.28 <0.1
C6-C12 C6-C12 C6-C12
2.9 7.0 <10
----------------- ----------------- -----------------
I
I B C Analytical
I
I
I
I
I
I :~~-~~------------------------
I ______________________________
I
I
I
I
I
I ------------------------------
I
I
I ~~~~~~
I ::111
........................................ . . . . . . . .
. . . . .
801 WestemAveruæ
Glendale, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, Ste. 204
Pasadena, California 91107
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
Page 2
------------------------------
-----------------
-----------------
-----------------
07-049-5
07-049-6
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-1-4-2
06 JUL 95
01-1-4-6
-----------------
-----------------
-----------------
TPH/BTEX (8015M)
Date Analyzed
07/06/95 07/06/95
100 100
<0.1 <0.1
0.38 0.11
0.31 <0.1
2.5 0.37
C6-C12 C6-C12
55 21
Dilution Factor, Times
Benzene, mg/kg
Toluene, mg/kg
Ethylbenzene, mg/kg
Total Xylene Isomers, mg/kg
Carbon Range,
TPH (Gasoline Range), mg/kg
-----------------
-----------------
-----------------
I
I
I
I
I
I
I
I LOG NO
------------------------------
I ------------------------------
I
I
I
I
------------------------------
I
I
I
I
I ~~~,~~~
I ::111
B C Analytical
........................ . . . . . . . . . . . . . . . . . . . . . . . .
. . . . .
801 Western Averuæ
Glendale, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
Page 3
------------------------------
-----------------
-----------------
-----------------
07-049-8
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-1-3-6
-----------------
-----------------
-----------------
GRO/ORO (8015M)
Date Analyzed
07/06/95
07/06/95
1
C10-C25
Date Extracted
Dilution Factor, Times
Carbon Range, .
TPH (total), mg/kg
Other GRO/DRO (8015M)
<10
-----------------
-----------------
-----------------
II
I B C Annlytical
II
I
I
I
I
II ~~~-~~------------------------
I ------------------------------
II
II
II
I
Total Xylene Isomers, mg/kg
II --------______________________
I
II
I
I ~~~~~~
I ::11]
.......................... . . . . . . . . . . . . . . . . . . .
. . .
. . . . .
801 Westem Avelme
Glendale, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
Page 4
------------------------------
-----------------
-----------------
-----------------
07-049-8
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-1-3-6
-----------------
-----------------
-----------------
BTEX (8015M)
Date Analyzed
07/07/95
07/07/95
100
Date Extracted
Dilution Factor, Times
Benzene, mg/kg
<0.1
Toluene, mg/kg
0.12
Ethylbenzene, mg/kg
<0.1
0.22
-----------------
-----------------
-----------------
I
I B C Analytical
I
I
I
I
I
II :~~-~~------------------------
II ------------------------------
I
I
I
II
II
II ------------------------------
I
I
I ~~~~~~
I ::111
......................................... . .
. . . . .
. . . . .
801 Western Avemæ
GlentlaúJ, CA 91201
8181247-5737
Fax: 8181247-9797
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Ioc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
Page 5
------------------------------
-----------------
-----------------
-----------------
07-049-9
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-2-1-2
-----------------
-----------------
-----------------
TPH/BTEX (8015M)
Date Analyzed
07/06/95
100
Dilution Factor, Times
Benzene, mg/kg
<0.1
Toluene, mg/kg
Ethylbenzene, mg/kg
1.2
0.27
2.3
C6-Cl2
20
Total Xylene Isomers, mg/kg
Carbon Range, .
TPH (Gasoline Range), mg/kg
-----------------
-----------------
-----------------
I
I B C Analytical
I
I
I
I
I
I
I
I
I
I
I
I
II ------------------------------
I
I
I ~~~~~~
I ::111
.................................... . . . . . . . . . . . .
. . . . .
801 Westem Avenne
Glendale, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana .
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
. Page 6
------------------------------
-----------------
-----------------
-----------------
LOG NO
07-049-10
------------------------------
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-2-1-6
------------------------------
-----------------
-----------------
-----------------
TP~/BTEX (8015M)
Dilution Factor, Times
07/07/95
100
Date Analyzed
Benzene, mg/kg
<0.1
Toluene, mg/kg
<0.1
Ethylbenzene, mg/kg
<0.1
Total Xylene Isomers, mg/kg
<0.1
Carbon Range, .
C6-C12
TPH (Gasoline Range), mg/kg
<10
-----------------
-----------------
-----------------
I
I
I
I
I
I
I
I LOG NO
------------------------------
I ------------------------------
I
I
I
I
------------------------------
I
I
I
I
I ~~~~~~
.··111
B C Analyti£a1
............................................... .
. . . . .
801 Westent Averute
GknJale, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB-059B
REPORT OF ANALYTICAL RESULTS
Page 7
------------------------------
-----------------
-----------------
-----------------
07-049-11
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-2-3-2
-----------------
-----------------
-----------------
GRO/DRO (B015M)
Date Analyzed
07/06/95
07/06/95
1
C10-C25
Date Extracted
Dilution Factor, Times
Carbon Range, .
TPH (total), mg/kg
190
Other GRO/DRO (B015M)
-----------------
-----------------
-----------------
I
I B C Anolyticol
I
I
I
I
I
I LOG NO
------------------------------
II ------------------------------
I
I
I
I
Total Xylene Isomers, mg/kg
I ______________________________
I
I
I
I ~~~~~~
I ::111
............................... . . . . . . . . . .
. .
. . . . .
. . . . .
801 Western Avemœ
Glendnk, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB-059B
REPORT OF ANALYTICAL RESULTS
Page B
------------------------------
-----------------
-----------------
-----------------
07-049-11
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-2-3-2
-----------------
-----------------
-----------------
BTEX (B015M)
Date Analyzed
07/07/95
07/07/95
100
Date Extracted
Dilution Factor, Times
Benzene, mg/kg
<0.1
Toluene, mg/kg
<0.1
Ethylbenzene, mg/kg
<0.1
0.10
-----------------
-----------------
-----------------
I
I B C Analytical
I
I
I
I
I
I LOG NO
------------------------------
II ------------------------------
I
I
I
I
I
I ------------------------------
I
I
I ::::::
I ::111
............................................... .
. . . . .
801 Western Avenue
Glendnle, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
Page 9
------------------------------
-----------------
-----------------
-----------------
07-049-12
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-2-2-6
-----------------
-----------------
-----------------
TPH/BTEX (B015M)
Date Analyzed
07/06/95
250
DHution Factor, Times
Benzene, mg/kg
<0.3
Toluene, mg/kg
Ethylbenzene, mg/kg
1.4
0.66
Total Xylene Isomers, mg/kg
7.4
C6-C12
150
Carbon Range,
TPH (Gasoline Range), mg/kg
-----------------
-----------------
-----------------
I
B C Annlytkal
I .......................... · · · · · · · · · · · · · · · · · · · · · ·
801 WestemAvemæ
Glelldole, CA 91201
818/247-5737
Fax: 818/247-9797
I
I
I
I
I
. . . . .
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
------------------------------
LOG NO
II ------------------------------
DATE SAMPLED
SAMPLE DESCRIPTION
I SOIL
------------------------------
Sample Held, Not Analyzed
I ------------------------------
II
II
I
I
I
I
I
I ::::::
. .. .. .
.. .. . .
I ::111
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
Page 10
----------------- ----------------- -----------------
07 -049-13
----------------- ----------------- -----------------
06 JUL 95
01-2-2-2
----------------- ----------------- -----------------
HOLD
----------------- ----------------- -----------------
I
I B C Analytical
I
I
I
I
I
I :~~-~~------------------------
II ------------------------------
I
I Date Ext racted
Dilution Factor, Times
I Carbon Range, .
I
I
I
I
I
I ~~~~~~
I ::11
............................................... .
. . . . .
801 Westem Avenue
Glendale, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
Page 11
------------------------------
-----------------
-----------------
-----------------
07-049-14
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-2-3-6
-----------------
-----------------
-----------------
GRO/DRO (8015M)
Date Analyzed
07/06/95
07/06/95
1
C10-C25
TPH (total), mg/kg
<10
Other GRO/DRO (8015M)
------------------------------
-----------------
-----------------
-----------------
I
I
I
I
I
I
I
I LOG NO
------------------------------
I --------------________________
I
I
I
I
I
------------------------------
I
I
I
I ::::::
I ::111
B C Analytical
.................................. . . . . . . . . . . . . . .
. . . . .
801 Westem Avem.w
Glendnle, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
Page 12
------------------------------
-----------------
-----------------
-----------------
07-049-14
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
DI-2-3-6
-----------------
-----------------
-----------------
BTEX (8015M)
Date Analyzed
07/07/95
07/07/95
100
Date Extracted
Dilution Factor, Times
Benzene, mg/kg
<0.1
Toluene, mg/kg
<0.1
Ethylbenzene, mg/kg
<0.1
Total Xylene Isomers, mg/kg
<0.1
-----------------
-----------------
-----------------
I
I
I
I
I
I
I
I :~~-~~------------------------
I ______________________________
I
I
I
I
I Carbon Range,
TPH (Gasoline Range), mg/kg
I ------------------------------
I
I
I ~~~~~~
I ::111
B C Analytical
................................... . . . . . . . . . . . . .
801 Westem Avenue
Glendale, CA 91201
818/247-5737
Fax: 818/247-9797
. . . . .
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pac; fi c Env; ronmenta 1 Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
------------------------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
TPH/BTEX (8015M)
Date Analyzed
Dilution Factor, Times
Benzene, mg/kg
Toluene, mg/kg
Ethylbenzene, mg/kg
Total Xylene Isomers, mg/kg
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
Page 13
-----------------
-----------------
-----------------
07-049-15
07-049-17
07-049-16
-----------------
-----------------
-----------------
06 JUL 95
01-2-4-2
06 JUL 95
01-3-1-2
06 JUL 95
01-2-4-6
-----------------
-----------------
-----------------
07/06/95 07/07/95 07/06/95
100 100 100
0.10 <0.1 <0.1
2.0 <0.1 <0.1
0.43 <0.1 <0.1
3.6 0.15 <0.1
C6-C12 C6-Cl2 C6-C12
37 8.2 <10
----------------- ----------------- -----------------
I
I B C Analytical
I
I
I
I
I
I ~~~-~~------------------------
I ------------------------------
I
I
I
I
I
I ------------------------------
I
I
I ~~~~~~
I ::111
.......................... . . . . . . . . . . . . . . . . . . . . . .
801 Westem Avemæ
Glendnle, CA 91201
818/247-5737
Fax: 818/247-9797
. . . . .
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
------------------------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
TPH/BTEX (8015M)
Date Analyzed
Dilution Factor, Times
Benzene, mg/kg
Toluene, mg/kg
Ethylbenzene, mg/kg
Total Xylene Isomers, mg/kg
Carbon Range,
TPH (Gasoline Range), mg/kg
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
Page 14
-----------------
-----------------
-----------------
07-049-18
07-049-19
07-049-20
-----------------
-----------------
-----------------
06 JUL 95
01-3-1-6
06 JUL" 95
01-3-2-2
06 JUL 95
01-3-2-6
-----------------
-----------------
-----------------
07/06/95 07/06/95 07/06/95
100 100 100
0.16 <0.1 <0.1
<0.1 <0.1 <0.1
<0.1 <0.1 <0.1
<0.1 <0.1 <0.1
C6-C12 C6-C12 C6-C12
<10 <10 <10
----------------- ----------------- -----------------
I
B C AnnlytΣal
I
I
I
I
I
I
II :~~-~~------------------------
II ------------------------------
II
I
I
I
I
I
I
I
I ::::::
I ::111
.......................... . . . . . . . . . . . . . . . . . . . . . .
. . . . .
801 Westem Avemæ
Gkndale, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
Page 15
------------------------------
-----------------
-----------------
-----------------
07-049-21
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-3-3-2
-----------------
-----------------
-----------------
GRO/DRO (8015M)
Date Analyzed
07/06/95
07/06/95
1
C10-C25
34
Date Extracted
Dilution Factor, Times
Carbon Range, .
TPH (total), mg/kg
Other GRO/DRO (8015M)
------------------------------
-----------------
-----------------
-----------------
. . . . . .
I
I B C Analyti£al
I
I
I
I
I
I :~~-~~------------------------
I ------------------------------
I
I
I
I
Total Xylene Isomers, mg/kg
I ______________________________
I
I
I
I ~~~~~~
I :: III
.................................... . . . . . . . . . . . .
. . . . .
801 Western Avenue
Glendnle, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
Page 16
------------------------------
-----------------
-----------------
-----------------
07-049-21
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-3-3-2
-----------------
-----------------
-----------------
BTEX (8015M)
Date Analyzed
07/07/95
07/07/95
100
Date Extracted
Dilution Factor, Times
Benzene, mg/kg
<0.1
Toluene, mg/kg
<0.1
Ethylbenzene, mg/kg
<0.1
<0.1
-----------------
-----------------
-----------------
I
I
I
I
I
I
I
I LOG NO
------------------------------
II ------------------------------
I
I . Oil ut i on Factor, Times
Benzene, mg/kg
I
I
I
I ------------------------------
I
I
. . . . . .
I ::::::
1::11
B C Annlyti£a1
......................................... . . . . . . .
. . . . .
801 Western Avellue
Gkrulale, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
Page 17
------------------------------
-----------------
-----------------
-----------------
07-049-22
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
DI-3-4-2
-----------------
-----------------
-----------------
TPH/BTEX (8015M)
Date Analyzed
07/07/95
100
0.23
4.0
1.8
12
C6-C12
110
Toluene, mg/kg
Ethylbenzene, mg/kg
Total Xylene Isomers, mg/kg
Carbon Range,
TPH (Gasoline Range), mg/kg
-----------------
-----------------
-----------------
I
I B C Analytical
I
I
I
I
I
I
I
I
I
I
I
------------------------------
I
I
I
I
I ~~~~~~
I ::111
.......................... . . . . . . . . . . . . . . . . . . . . . .
. . . . .
801 Westem Averuœ
Glendale, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
Page 18
------------------------------
-----------------
-----------------
-----------------
LOG NO
07-049-23
------------------------------
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-3-3-6
------------------------------
-----------------
-----------------
-----------------
GRO/DRO (8015M)
Date Analyzed
07/06/95
07/06/95
Date Extracted
Dilution Factor, Times
1
C10-C25
Carbon Range, .
TPH (total), mg/kg
<10
Other GRO/DRO (8015M)
-----------------
-----------------
-----------------
I
I
I
I
I
I
I
II ~~:_~~------------------------
I ------------------------------
BTEX (8015M)
I
I
I
I
I ------------------------------
I
I
I
I ~~~~~~
II ::111
B C Analytical
....................... . . . . . . . . . . . . . . . . . . . . . . . . .
. . . . .
801 Westem Avemæ
Glendale, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
Page 19
------------------------------
-----------------
-----------------
-----------------
07-049-23
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-3-3-6
-----------------
-----------------
-----------------
Date Analyzed
07/07/95
07/07/95
100
Date Extracted
Dilution Factor, Times
Benzene, mg/kg
<0.1
Toluene, mg/kg
<0.1
Ethylbenzene, mg/kg
<0.1
Total Xylene Isomers, mg/kg
0.10
-----------------
-----------------
-----------------
I
I
I
I
I
I
I
I
I
I
I
I
I
I
II ------------------------------
I
I
I '~~ ~ ~ ~ ~
I ::111
B C Analyṭal
.......................... . . . . . . . . . . . . . . . . . . . . . .
. . . . .
801 Western Avenue
Gúwlale, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
Page 20
------------------------------
-----------------
-----------------
-----------------
LOG NO
07-049-24
------------------------------
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-3-4-6
------------------------------
-----------------
-----------------
-----------------
TPH/BTEX (8015M)
Date Analyzed
07/06/95
250
Dilution Factor, Times
Benzene, mg/kg
<0.3
Toluene, mg/kg
Ethylbenzene, mg/kg
3.4
1.2
10
C6-C12
88
Total Xylene Isomers, mg/kg
Carbon Range,
TPH (Gasoline Range), mg/kg
-----------------
-----------------
-----------------
I
I
I
I
I
I
I
B C Annlytͣal
........................................ . . . . . . . . . . . . .
801 Westem Avemæ
Gkndnle, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO: G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
Page 21
------------------------------
-----------------
-----------------
-----------------
LOG NO
I ------------------------------
DATE SAMPLED
SAMPLE DESCRIPTION
I SO I L
------------------------------
Lead (6010), mg/kg
I Digestion (3050), Date
I GRO/DRO (BOI5M)
Date Analyzed
07-049-7
-----------------
-----------------
-----------------
06 JUL 95
01-1-3-2
-----------------
-----------------
-----------------
6.4
07/11/95
I
I
I
I ------------------------------
I
I
I ......
.. . .. .
. . .. . .
I ::111
Dilution Factor, Times
07/06/95
07/06/95
10
CI0-C25
2400
Date Extracted
Carbon Range, .
TPH (total), mg/kg
Other GRO/DRO (8015M)
-----------------
-----------------
-----------------
. . . . . .
I
I B C Analytical
I
I
I
I
I
I
I
I
I
I
I
II _::::~_:~~:::_~::::~:~_:~~~~__
I
I
I
I ::::::
I ::111
.............................................. .
. . . . . .
801 Westem Avenue
Gkndale, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
Page 22
------------------------------
-----------------
-----------------
-----------------
LOG NO
07-049-7
------------------------------
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-1-3-2
------------------------------
-----------------
-----------------
-----------------
BTEX (8015M)
Date Analyzed
07/07/95
07/07/95
100
Date Extracted
Dilution Factor, Times
Benzene, mg/kg
<0.3
Toluene, mg/kg
<0.3
Ethylbenzene, mg/kg
<0.3
<0.3
-----------------
-----------------
-----------------
I
B C Analytical
I ................................................
801 Westem Avenue
Glendale, CA 91201
818/247-5737
Fax: 818/247-9797
. . . . .
I
I
I
I
I
LOG NO:
G95-07-049
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB-059B
REPORT OF ANALYTICAL RESULTS
Page 23
------------------------------
-----------------
----------------- -----------------
I LOG NO
------------------------------
DATE SAMPLED
SAMPLE DESCRIPTION
I SOIL
------------------------------
Lead (6010), mg/kg
I Digestion (3050), Date
07-049-4
-----------------
----------------- -----------------
06 JUL 95
01-1-1-6
-----------------
----------------- -----------------
11
07/11/95
·1 - ------ ----------- -- - --- ------
I
I
_,I
I
I
I
I ::::::
.. .. ..
. .. . . .
I ::111
-----------------
----------------- -----------------
I
I B C Analytical
I
I
I
I
I
II :~~-~~------------------------
II ______________________________
II
II
II
II
II
II ------------------------------
I
II
II ~~~~~~
I ::111
............................................... .
801 Westem Avenue
Glendale, CA 91201
818/247-5737
Fax: 818/247-9797
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, Ste. 204
Pasadena, California 91107
LOG NO:
. . . . .
Received: 06 JUL 95
G95-07-049
Project: TMLB-0598
REPORT OF ANALYTICAL RESULTS
------------------------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
-----------------
TPH/BTEX (8015M)
Date Analyzed
Dilution Factor, Times
Benzene, mg/kg
Toluene, mg/kg
Ethylbenzene, mg/kg
Total Xylene Isomers, mg/kg
Carbon Range,
TPH (Gasoline Range), mg/kg
-----------------
Site Address: 5321 Stockdale, New Stein
Bakersfield, Ca.
Texaco Contact: Mr. Lee Bouchez
Page 24
07-049-4
-----------------
-----------------
-----------------
-----------------
06 JUL 95
DI-1-1-6
-----------------
-----------------
07/06/95
100
<0.1
2.9
4.8
39
C6-Cl2
740
-----------------
-----------------
Jan
Client name T"Ë1 A GD
Address r- ,~ I IJ / _-,7 .
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B C ANALYTICAL
01085 Shary Circle, Concord, CA 94518 (510) 825-3894
.0801 Western Avenue, Glendaltil, CA 91201 (818) 247·6737
1Íif00 GM'ry w1IIìIie1m, ~5 (71iiilli113
Note: Samples are discarded 30 days after results are reported unless other arrangements are made. 'KEY; AG-Aqueous NA-Nonaqueous SL-Sludge
Hazardous samples will be returned to client or disposed of at client's expense. GW-Groundwater SO-Soil PE-Petroleum
Disposal arrangements:
,---------
.. ·~~t·· "~ ,~...........,." -.ßf1'-......~...#...........*..-'. .
,,', :.Þ ,- SCA Log Number G <1 Ç;'o 7 0 (& ~'
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CHAIN OF CUSTODY RECORD
~.,. r.""'· I
Client name TJ:"xA-W ÞroJjct or PO# (~ 4 , / Analyses reqlßPèd" j¡ /.
'-tö-(k- , V . " ,~32..1
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Sampled by ~Pn I ~ ~ \) I ~~if " k..
Lab Type' ð'- Number
Sample Date' Time See key of Q)'I y ~~09' R,'JJ{1/Jks
number sampled sampled below Sample description containers
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B C ANALYTICAL
o 1255 P~well Street, Emeryville, CA 94608 (415) 428,2300
o 801 Western Avenue, Glendale, CA 91201 (818) 247,5737
1lÍÌf00 P~venu_eim. ~05 (_,0113
Note: Samples are discarded 30 days after results are reported unless other arrangements are made,
Hazardous samples will be returned to client or disposed of at client's expense,
'KEY: AQ-Aqueous N-,\-Nonaqueous SL-Sludge,
GW-Groundwater SO-Soil OT -Other PE-Petroleum
,
Disposal arrangements:
-----
-
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o 1255 Powell Street. Emeryville. CA 94608 (415) 428,2300
o 801 Western Avenue, Glendale, CA 91201 (818) 247,5737
"00 p,.venu~im, 1IIIf5 (7..0113
Note: Samples are discarded 30 days atter results are reported unless other arrangements are made.
Hazardous samples will be returned to client or disposed of at client's expense.
'KEY: AQ-Aqueous NA-Nonaqueous SL-Sludge
GW-Groundwater SO-Soil or -':Other PE-PetroleurT1
Disposal arrangements:
--~----""--
-
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Accuracy:
Precision:
Batch:
Laboratory
Control
Standard
( LCS ) :
Matrix QC:
Method
Blank:
Batch
Number:
LC Result:
LT Result:
Percent
Recovery:
B C ANALYTICAL
ORDER QC REPORT
Definitions and Terms
The ability of a procedure to determine the "true"
concentration of an analyte.
The reproducibility of a procedure demonstrated by the
agreement between analyses performed on either dupli-
cates of the same sample or a pair of duplicate spikes.
A group of twenty samples or less, of similar matrix
type, prepped together or analyzed together if no
sample preparation is required, under the same
conditions and with the same reagents. The batch must
include a method blank, LCS and matrix QC.
A blank that is spiked with a known amount of analyte
and subjected to the same procedures as the samples.
The LCS indicates the accuracy of the analytical
method. It also serves to double-check the calibration
because it is prepared from a different source than the
standard used to calibrate the instrument.
Quality control performed on actual client samples.
The matrix spike is a client's sample spiked with a
known amount of analyte. For most analyses, the
laboratory performs matrix spikes in duplicate
(duplicate spikes).
A sample that contains no analyte. For water analysis,
organic-free or deionized water is used. For solids
analysis, analyte-free solvent is used. The method
blank serves to measure contamination associated with
laboratory storage, preparation or instrumentation.
Numeric designation for a batch of samples and the
associated QC. The batch number sequence is unique for
each determination.
Laboratory result of an LCS analysis.
Expected result, or true value, of the LCS analysis.
The percentage of analyte recovered. For LCS, the
percent recovery calculation is: LC/LT x 100.
If r. It ""/v/¡,,,,/
I
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ORDER QC REPORT
Definitions and Terms
Page 2
LCl, LC2
Results of analyzing duplicate LCS's, used to determine
precision.
Rl, R2
Result:
Results of analyzing duplicate aliquots of a sample,
with Rl indicating the first replicate and R2 the
second replicate; used to determine precision.
MS, MSD
Result:
Results of analyzing a matrix spike and a matrix spike
duplicate, used to determine precision.
Relative
% Diff
( RPD) :
Calculated using one of the following:
:LCl - LC2: x 100
( [LCl + LC2]/2 )
:Rl - R2: X 100
( [Rl + R2]/2 )
:MS - MSD: x 100
( [MS + MSD]/2 )
MS, MSD
The percentage of analyte recovered in the matrix
spikes. The percent recovery calculation is:
% :
MS %: (MS - X) x 100
(T - X)
MSD %: (MSD - X) x 100
(T - X)
where X is the sample result, listed on the analytical
report, and T is the true value, defined below.
True value:
The theoretical, or expected, result of a spiked sample
analysis.
NC Flag
Indicates that the spike recovery was not calculated
due to high sample concentration relative to the amount
of spike added.
Q Flag
Indicates that the quality control measurement is
outside the specified control limits.
Blank
Result:
Laboratory result of analysis of the method blank.
RDL
(Reporting
Detection
Limit) :
BCA-assigned limit, set at a level higher than the
method detection limit (MDL) determined using EPA
guidelines. Sample RDLs may differ from the blank RDL
if the samples were diluted.
R r. A (In/vli,,,,/
II: ORDER PLACED FOR CLIENT: Pacific Environmental Group, Inc. 9507049
: BC ANALYTICAL: GLEN LAB: 14:25:13 13 JUL 1995 - P. 1:
---------------------------------------------------------------
---------------------------------------------------------------
ILAMPLES... SAMPLE DESCRIPTION.. OETERM......... DATE...... METHOD..... EQUIP. BATCH.. 10.NO
ANALYZED
1b507049*1 01-1-1-2
~507049*2 01-1-2-2
1507049*3 01-1-2-6
507049*5 01-1-4-2
507049*6 01-1-4-6
9507049*8 01-1-3-6
!L507049*9 01-2-1-2
9507049*10 01-2-1-6
1f507049*11 01-2-3-2
~507049*12 01-2-2-6
9507049*13 01-2-2-2
1t507049*14 01-2-3-6
9507049*15 01-2-4-2
~507049*16 01-2-4-6
507049*17 01-3-1-2
507049*18 01-3-1-6
.507049*19 01-3-2-2
507049*20 01-3-2-6
507049*21 01-3-3-2
1507049*22 01-3-4-2
507049*23 01-3-3-6
1i507049*24 01-3-4-6
11507049*7 01-1-3-2
11507049*4 01-1-1-6
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
FUEL. TOT 07.06.958015M 556-11 955063 8501
GAS.BTEX 07.07.958015M 536-19 953321 8501
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
FUEL. TOT 07.06.958015M 556-11 955063 8501
GAS.BTEX 07.07.958015M 536-19 953321 8501
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
HOLD 07.10.95
FUEL. TOT 07.06.958015M 556-11 955063 8501
GAS.BTEX 07.07.958015M 536-19 953321 8501
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
FUEL.TOT 07.06.958015M 556-11 955063 8501
GAS.BTEX 07.07.958015M 536-19 953321 8501
GAS.TPH.BTEX 07.07.958015M 536-19 953321 8501
FUEL. TOT 07.06.958015M 556-11 955063 8501
GAS.BTEX 07.07.958015M 536-19 953321 8501
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
FUEL.TOT 07.06.958015M 556-11 955063 8501
GAS.BTEX 07.07.958015M 536-19 953321 8501
PB 07.12.95 6010 535-03 951008 7396
OIG,NAQ.HCL 07.11.95 3050 951008 7093
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
PB 07.12.95 6010 535-03 951008 7396
0IG,NAQ.HCL 07.11.95 3050 951008 7093
I
1**
I
I
I
I
I
Notes: Equipment = BC Analytical identification number for a
particular piece of analytical equipment.
10.NO = BC Analytical employ~e identification number of
ana lyst.
I
I
IJATE REPORTED 07/13/95
BC ANAL YTI CAL
ORDER QC REPORT FOR G9507049
Page 1
I
LABORATORY CONTROL STANDARDS
FOR eATCHES WHICH INCLUDE THIS ORDER
DATE BATCH LC
ANALYZED NUMBER RESULT
C507521*1
07.06.95 953320
07.06.95 953320
07.06.95 953320
07.06.95 953320
07.06.95 953320
07.06.95 953320
C507522*1
07.06.95 953320
07.06.95 953320
07.06.95 953320
07.06.95 953320
07.06.95 953320
07.06.95 953320
C507561*1
07.06.95 955063
07.06.95 955063
07.06.95 955063
C507615*1
07.07.95 953321 07/07/95
07.07.95 953321 1.65
07.07.95 953321 9.46
07.07.95 953321 2.12
07.07.95 953321 11.9
07.07.95 953321 112
07.12.95 951008 90.0
07.12.95 951008 87.9
IARAMETER
· TPH/BTEX
Date Analyzed
I Benzene
Toluene
Ethylbenzene
I Total Xylene Isomers
TPH (Gasoline Range)
· TPH/BTEX
Date Analyzed
I Benzene
Toluene
Ethylbenzene
_Total Xylene Isomers
TPH (Gasoline Range)
· GRO/DRO
Date Analyzed
I Date Extracted
TPH (total)
4. TPH/BTEX
I Date Analyzed
Benzene
Toluene
Ethylbenzene
I Total Xylene Isomers
TPH (Gasoline Range)
5. Lead C507846*1
II' Lead C507847*1
I
I
I
I
I
I
07/06/95
15.8
88.8
20.3
112
1120
07/06/95
17.4
95.7
20.9
119
1100
07/06/95
07/06/95
272
LT PERCENT
RESULT UNIT RECOVERY
07/06/95 Date N/A
15.2 ug/L 104
97.4 ug/L 91
20.4 ug/L 100
119 ug/L 94
1100 ug/L 102
07/06/95 Date N/A
15.2 ug/L 114
97.7 ug/L 98
20.4 ug/L 102
119 ug/L 100
1100 ug/L 100
07/06/95 Date N/A
07/06/95 Date N/A
250 mg/L 109
07/07/95 Date N/A
1.52 mg/kg 109
9.74 mg/kg 97
2.04 mg/kg 104
11.9 mg/kg 100
110 mg/kg 102
100 mg/kg 90
100 mg/kg 88
I
I
IDATE REPORTED 07/13/95
I
~ARAMETER
... TPH/BTEX
Date Analyzed
I Benzene
Ethylbenzene
Total Xylene Isomers
TPH (Gasoline Range)
f' Lead
I
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I
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I
I
SAMPLE
NUMBER
BC ANALYTICAL
ORDER QC REPORT FOR G9507049
ADDITIONAL LCS PRECISION (DUPLICATES)
BATCH QC REPORT
DATE BATCH LCl
ANALYZED NUMBER RESULT
07.06.95 953320 07/06/95
07.06.95 953320 15.8
07.06.95 953320 20.3
07.06.95 953320 112
07.06.95 953320 1120
07.12.95 951008 90.0
LC2
RESULT UNIT
07/06/95 Date
17.4 ug/L
20.9 ug/L
119 ug/L
1100 ug/L
87.9 mg/kg
RELATIVE
% DIFF
N/A
10
3
6
2
2
Page 1
- ----- ---- ----
I
I BC ANALYTICAL
ORDER QC REPORT FOR G9507049
IA TE REPORTED 07/13/95 Page 1
I MATRIX QC PRECISION (DUPLICATE SPIKES)
BATCH QC REPORT
SAMPLE DATE BATCH MS MSD RELATIVE
IARAMETER NUMBER ANALYZED NUMBER RESULT RESULT UNIT % DIFF
· GRO/DRO 9507049*14
Date Analyzed 07.06.95 955063 07/06/95 07/06/95 Date N/A
II Date Extracted 07.06.95 955063 07/06/95 07/06/95 Date N/A
TPH (total) 07.06.95 955063 284 356 mg/kg 23
· TPH/BTEX 9507049*22
Date Analyzed 07.07.95 953321 07/07/95 07/07/95 Date N/A
I Benzene 07.07.95 953321 1.93 1.74 mg/kg 10
Toluene 07.07.95 953321 11.4 11.9 mg/kg 4
Ethylbenzene 07.07.95 953321 3.32 3.51 mg/kg 6
II Total Xylene Isomers 07.07.95 953321 20.8 21.7 mg/kg 4
TPH (Gasoline Range) 07.07.95 953321 228 231 mg/kg 1
· TPH/BTEX 9507049*22
I Date Analyzed 07.07.95 953321 07/07/95 07/07/95 Date N/A
Benzene 07.07.95 953321 1.93 1.74 mg/kg 10
Toluene 07.07.95 953321 11.4 11.9 mg/kg 4
Ethylbenzene 07.07.95 953321 3.32 3.51 mg/kg 6
II Total Xylene Isomers 07.07.95 953321 20.8 21.7 mg/kg 4
TPH (Gasoline Range) 07.07.95 953321 228 231 mg/kg 1
4: Lead 9507049*4 07.12.95 951008 110 105 mg/kg 5
I
I
I
I
I
I
I
I
I
I
I
IIATE REPORTED 07/13/95
I
BC ANAL YTI CAL
ORDER QC REPORT FOR G9507049
MATRIX QC ACCURACY (SPIKES)
BATCH QC REPORT
IARAMETER
. GRO/DRO
TPH (total)
I. BTEX
Benzene
Toluene
Ethylbenzene
I Total Xylene Isomers
TPH (Gasoline Range)
3. TPH/BTEX
I Benzene
Toluene
Ethylbenzene
_Total Xylene Isomers
TPH (Gasoline Range)
. Lead 9507049*4
SAMPLE DATE BATCH
NUMBER ANALYZED NUMBER
9507049*14
07.06.95 955063 114
9507049*22
07.07.95 953321 112
07.07.95 953321 76
07.07.95 953321 75
07.07.95 953321 74
07.07.95 953321 107
9507049*22
07.07.95 953321 112
07.07.95 953321 76
07.07.95 953321 75
07.07.95 953321 74
07.07.95 953321 107
07.12.95 951008 99
I
I
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I
I
I
I
I
MS
~
o
Page 1
MSD TRUE
~ RESULT UNIT
0
142 250 mg/kg
99 1.75 mg/kg
81 13.7 mg/kg
84 3.84 mg/kg
82 23.9 mg/kg
110 220 mg/kg
99 1.75 mg/kg
81 13.7 mg/kg
84 3.84 mg/kg
82 23.9 mg/kg
110 220 mg/kg
94 111 mg/kg
I
I
~ATE REPORTED 07/13/95
BC ANAL YTI CAL
ORDER QC REPORT FOR G9507049
Page 1
I
METHOD BLANKS AND REPORTING DETECTION LIMIT (RDL)
FOR BATCHES WHICH INCLUDE THIS ORDER
DATE BATCH BLANK
ANALYZED NUMBER RESULT
B507282*1
07.06.95 953320
07.06.95 953320
07.06.95 953320
07.06.95 953320
07.06.95 953320
07.06.95 953320
B507317*1
07.06.95 955063
07.06.95 955063
07.06.95 955063
B507347*1
07.07.95 953321 07/07/95
07.07.95 953321 0
07.07.95 953321 0.029
07.07.95 953321 0
07.07.95 953321 0.028
07.07.95 953321 0
07.12.95 951008 0
IARAMETER
. TPH/BTEX
Date Analyzed
I Benzene
Toluene
Ethylbenzene
I Total Xylene Isomers
TPH (Gasoline Range)
. GRO/DRO
Date Analyzed
I Date Extracted
TPH (total)
3. TPH/BTEX
I Date Analyzed
Benzene
Toluene
Ethylbenzene
I Total Xylene Isomers
TPH (Gasoline Range)
4. Lead B507467*1
I
I
I
I
I
I
I
I
I
07/06/95
o
0.012
o
0.018
o
07/06/95
07/06/95
o
RDL UNIT METHOD
NA Date 8015M
0.005 mg/kg 8015M
0.005 mg/kg 8015M
0.005 mg/kg 8015M
0.01 mg/kg 8015M
0.05 mg/kg 8015M
NA Date 8015M
NA Date 8015M
10 mg/kg 8015M
NA Date 8015M
0.005 mg/kg 8015M
0.005 mg/kg 8015M
0.005 mg/kg 8015M
0.01 mg/kg 8015M
0.05 mg/kg 8015M
5 mg/kg 6010
I
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I ......
.... . .
"111
. .
I '
B C Anolytͣa1
..................................... .
ANALYTICAL REPORT
. . . . . . . . .
. . .
. . .
801 Westen! Avemæ
Gkndøle, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-051
Received: 06 JUL 95
Ma i 1 ed : JUL I 0 1995
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB0598
REPORT OF ANALYTICAL RESULTS
Page 1
------------------------------
-----------------
-----------------
-----------------
LOG NO
07-051-1
07-051-2
------------------------------
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-1-1-10
06 JUL 95
01-1-1-6.5
------------------------------
-----------------
-----------------
-----------------
TPH/BTEX (8015M)
Date Analyzed
07/06/95 07/06/95
100 100
<0.1 <0.1
<0.1 <0.1
<0.1 <0.1
<0.1 <0.1
C6-C12 C6-C12
<10 <10
Dilution Factor, Times
Benzene, mg/kg
Toluene, mg/kg
Ethylbenzene, mg/kg
Total Xylene Isomers, mg/kg
Carbon Range,
TPH (Gasoline Range), mg/kg
------------------------------
-----------------
-----------------
-----------------
I
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. . . .. .
. . .. ..
I ::111
B C Annlytkal
........................ . . . . . . . . . . . . . . . . . . . . . . . .
. . . . .
801 Western Avenne
Glendale, CA 91201
818/247--5737
Fax: 818/247-9797
LOG NO:
G95-07-051
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB0598
REPORT OF ANALYTICAL RESULTS
Page 2
------------------------------
-----------------
-----------------
-----------------
LOG NO
07-051-3
07-051-4
------------------------------
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-1-3-4
06 JUL 95
DI-2-3-3
------------------------------
-----------------
-----------------
-----------------
GRO/DRO (8015M)
Date Analyzed
07/06/95 07/06/95
07/06/95 07/06/95
1 1
ClO-C25 CI0-C25
<10 <10
Date Extracted
Dilution Factor, Times
Carbon Range, .
TPH (total), mg/kg
Other GRO/DRO (8015M)
------------------------------
-----------------
-----------------
-----------------
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. .. . . .
... . ..
. .. . . .
I ::111
B C Annlyti£al
........................ . . . . . . . . . . . . . . . . . . . . . . . .
. . . . .
801 Westem Avenue
Glendale, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-051
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB0598
REPORT OF ANALYTICAL RESULTS
Page 3
------------------------------
-----------------
-----------------
-----------------
LOG NO
07-051-3
07-051-4
------------------------------
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-1-3-4,
06 JUL 95
01-2-3-3
------------------------------
-----------------
-----------------
-----------------
BTEX (8015M)
Date Analyzed
07/07/95 07/07/95
07/07/95 07/07/95
100 100
<0.1 <0.1
<0.1 <0.1
<0.1 <0.1
<0.1 <0.1
Date Extracted
Dilution Factor, Times
Benzene, mg/kg·
Toluene, mg/kg
Ethylbenzene, mg/kg
Total Xylene Isomers, mg/kg
------------------------------
-----------------
-----------------
-----------------
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.. . . . .
.. . . . .
. . .. . .
··11
. .
I '
B C Analytkal
................................ . . . . . . .
801 Westem Avenue
Glendale, CA 91201
818/247-5737
Fax: 818/247-9797
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
REPORT OF ANALYTICAL RESULTS
------------------------------
-----------------
-----------------
-----------------
-----------------
LOG NO
------------------------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
. .
.......
. . . . .
LOG NO:
G95-07-051
Received: 06 JUL 95
Project: TMLB0598
Page 4
-----------------
07-051-5
07-051-6
06 JUL 95
01-2-2-10,
06 JUL 95
01-2-2-6.5
--------'----------------------
-----------------
-----------------
-----------------
TPH/BTEX (8015M)
Date Analyzed
Dilution Factor, Times
Benzene, mg/kg
Toluene, mg/kg
Ethylbenzene, mg/kg
Total Xylene Isomers, mg/kg
Carbon Range,
TPH (Gasoline Range), mg/kg
------------------------------
-----------------
-----------------
-----------------
07/06/95 07/06/95
100 100
0.16 0.12
0.36 0.54
<0.1 0.14
0.60 1.1
C6-C12 C6-Cl2
12 12
I
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I
TPH/BTEX (8015M)
I
I
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I
I
I ------------------------------
I
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I ::111
B C Analyti£a1
.............................................. . .
. . . . .
801 Western Avenue
Glendale, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-051
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB0598
REPORT OF ANALYTICAL RESULTS
Page 5
------------------------------
-----------------
-----------------
-----------------
LOG NO
07-051-7
------------------------------
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-3-4-4
------------------------------
-----------------
-----------------
-----------------
Date Analyzed
07/07/95
100
Dilution Factor, Times
Benzene, mg/kg
<0.1
Toluene, mg/kg
<0.1
Ethylbenzene, mg/kg
<0.1
Total Xylene Isomers, mg/kg
<0.1
Carbon Range,
C6-C12
TPH (Gasoline Range), mg/kg
<10
-----------------
-----------------
-----------------
. . . .. .
11; .
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GRO/ORO (8015M)
I
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I ::111
B C Analytical
.............................. . . . . . . . . . .
. .
. . . . . .
. . . . .
801 Westem Avenue
Gœndn1e, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-051
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB0598
REPORT OF ANALYTICAL RESULTS
Page 6
------------------------------
-----------------
-----------------
-----------------
LOG NO
07-051-8
------------------------------
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-3-3-5.5
------------------------------
-----------------
-----------------
-----------------
Date Analyzed
07/06/95
07/06/95
1
C10-C25
Date Extracted
Dilution Factor, Times
Carbon Range, .
TPH (total), mg/kg
<10
Other GRO/DRO (8015M)
------------------------------
-----------------
-----------------
-----------------
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Total Xylene Isomers, mg/kg
II ______________________________
I
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I ::111
B C Annlytical
.................................... . . . . . . . . . . . .
. . . . .
801 Western Avenne
Glendale, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-051
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB0598
REPORT OF ANALYTICAL RESULTS
Page 7
------------------------------
-----------------
-----------------
-----------------
LOG NO
07-051-8
------------------------------
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-3-3-5.5
------------------------------
-----------------
-----------------
-----------------
BTEX (8015M)
Date Analyzed
07/07/95
07/07/95
100
Date Extracted
Dilution Factor, Times
Benzene, mg/kg
<0.1
Toluene, mg/kg
<0.1
Ethylbenzene, mg/kg
<0.1
<0.1
-----------------
-----------------
-----------------
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I ......
· . .. ..
· . . ...
" .. ..
·'111
· .
I '
B C Annlytical
.............................. . . . . . . . . . . . . . . . . . .
. . . . .
801 Westem Avenue
Glendale, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-051
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB0598
REPORT OF ANALYTICAL RESULTS
Page 8
------------------------------
-----------------
-----------------
-----------------
LOG NO
07-051-9
07-051-10
------------------------------
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
01-3-2-4
06 JUL 95
01-3-1-4
------------------------------
-----------------
-----------------
-----------------
Sample Held, Not Analyzed
HOLD
HOLD
------------------------------
-----------------
-----------------
-----------------
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. .. . . .
... .' .
I ::111
B C Analytical
........................ . . . . . . . . . . . . . . . . . . . . . . . .
. . . . .
801 Western Avenue
Glendn1e, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-051
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB0598
REPORT OF ANALYTICAL RESULTS
Page 9
------------------------------
-----------------
-----------------
-----------------
LOG NO
07-051-11
------------------------------
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
Stockpile 1 of Z
------------------------------
-----------------
-----------------
-----------------
GRO/DRO (8015M)
Date Analyzed
07/06/95
07/06/95
1
C10-C25
26
Date Extracted
Dilution Factor, Times
Carbon Range, .
TPH (total), mg/kg
Other GRO/DRO (8015M)
------------------------------
-----------------
-----------------
-----------------
I
I
I
I
I
I
I
I
II ------------------------------
I
II
I
I
I
I ------------------------------
II
II
I ~~~~~~
I ::111
B C Annlytkal
........................ . . . . . . . . . . . . . . . . . . . . . . . .
. . . . .
801 Westem Avenue
Glendale, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-051
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB059B
REPORT OF ANALYTICAL RESULTS
Page 10
------------------------------
-----------------
-----------------
-----------------
LOG NO
07-051-11
------------------------------
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
Stockpile 1 of 2
-----------------
-----------------
-----------------
TPH/BTEX (8015M)
Date Analyzed
07/07/95
100
Dilution Factor, Times
Benzene, mg/kg
<0.3
Toluene, mg/kg
<0.3
Ethylbenzene, mg/kg
<0.3
Total Xylene Isomers, mg/kg
<0.3
Carbon Range,
C6-Cl2
27
TPH (Gasoline Range), mg/kg
-----------------
-----------------
-----------------
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B C Analytkal
........................ . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
801 Westem Avenue
Glendale, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO: G95-07-051
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB0598
REPORT OF ANALYTICAL RESULTS
Page 11
------------------------------ ----------------- ----------------- -----------------
LOG NO
07-051-12
------------------------------ ----------------- ----------------- -----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
Stockpile 2 of 2
------------------------------ ----------------- ----------------- -----------------
Lead (6010), mg/kg
Digestion (3050), Date
22
07/07/95
GRO/DRO (8015M)
Dilution Factor, Times
07/06/95
07/06/95
1
C10-C25
630
Date Analyzed
Date Extracted
Carbon Range, .
TPH (total), mg/kg
Other GRO/DRO (8015M)
------------------------------ ----------------- ----------------- -----------------
"11
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B C Analytical
........................ . . . . . . . . . . . . . . . . . . . . . . . .
. . . . .
801 Western Avenue
Gkndale, CA 91201
818/247-5737
Fax: 818/247-9797
LOG NO:
G95-07-051
Received: 06 JUL 95
Mr. Gary Pestana
Pacific Environmental Group, Inc.
650 Sierra Madre Villa Ave, SteM 204
Pasadena, California 91107
Project: TMLB0598
REPORT OF ANALYTICAL RESULTS
Page 12
------------------------------
-----------------
-----------------
-----------------
LOG NO
07-051-12
------------------------------
-----------------
-----------------
-----------------
DATE SAMPLED
SAMPLE DESCRIPTION
SOIL
06 JUL 95
Stockpile 2 of 2
------------------------------
-----------------
-----------------
-----------------
TPH/BTEX (8015M)
Date Analyzed
07/07/95
1000
Dilution Factor, Times
Benzene, mg/kg
<1
Toluene, mg/kg
<1
Ethylbenzene, mg/kg
<1
Total Xylene Isomers, mg/kg
12
C6-C12
270
Carbon Range,
TPH (Gasoline Range), mg/kg
------------------------------
-----------------
-----------------
-----------------
Site Address: 5321 Stockdale, New Stein,
Bakeksfield, Ca.
Texaco Contact: Mr. Lee Bouchez
,'-',
~\
Jan
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.¡, L~' (;.V' ~'
ram Manager
CHAIN OF CUSTODY RECORD
Client name ~~
Address )"3 2/ rkc (,- d C;(-t I~
City, State, Zip It; . ~ r I J '
~:... /:-: t-ev S tL-'€
Lab
Sample
number
Type'
See key
below
Date '
sampled
Time
sampled
/
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Relinquished by
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Relinquished by
Received by Laboratory
THrBOS- '1?
Phone #
Report attention
Sampled by
Number
of
containers
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Sample description
Analyses required
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Date
B C ANALYTICAL Note: Samples are discarded 30 days after results are reported unless other arrangements are made. 'KEY: AQ-Aqueous NA-Nonaqueous SL-Sludge
o 1255 Powell Street, EmeryviUe, CA 94608 (415) 428.2300 Hazardous samples will be returned 10 client or disposed of at client's expense. GW-Groundwater SO-Soil OT -Other PE-Petroleum
o 801 Western Avenue, Glendale, CA 91201 (818) 247.5737 Disposal arrangements:
"'00P1IIIfvenu~im,~5 (_,011~_".,,_ _ _ _ _ _ ._ _ _ _ _ _ _
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Accuracy:
Precision:
Batch:
Laboratory
Control
Standard
( LCS ) :
Matrix QC:
Method
Blank:
Batch
Number:
LC Result:
LT Result:
Percent
Recovery:
B C ANALYTICAL
ORDER QC REPORT
Definitions and Terms
The ability of a procedure to determine the "true"
concentration of an analyte.
The reproducibility of a procedure demonstrated by the
agreement between analyses performed on either dupli-
cates of the same sample or a pair of duplicate spikes.
A group of twenty samples or less, of similar matrix
type, prepped together or analyzed together if no
sample preparation is required, under the same
conditions and with the same reagents. The batch must
include a method blank, LCS and matrix QC.
A blank that is spiked with a known amount of analyte
and subjected to the same procedures as the samples.
The LCS indicates the accuracy of the analytical
method. It also serves to double-check the calibration
because it is prepared from a different source than the
standard used to calibrate the instrument.
Quality control performed on actual client samples.
The matrix spike is a client's sample spiked with a
known amount of analyte. For most analyses, the
laboratory performs matrix spikes in duplicate
(duplicate spikes).
A sample that contains no analyte. For water analysis,
organic-free or deionized water is used. For solids
analysis, analyte-free solvent is used. The method
blank serves to measure contamination associated with
laboratory storage, preparation or instrumentation.
Numeric designation for a batch of samples and the
associated QC. The batch number sequence is unique for
each determination.
Laboratory result of an LCS analysis.
Expected result, or true value, of the LCS analysis.
The percentage of analyte recovered. For LCS, the
percent recovery calculation is: LC/LT x 100.
n r. 4 n,.,/vtir,,1
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ORDER QC REPORT
Definitions and Terms
Page 2
LC1, LC2
Results of analyzing duplicate LCS's, used to determine
precision.
R1, R2
Result:
Results of analyzing duplicate aliquots of a sample,
with R1 indicating the first replicate and R2 the
second replicate; used to determine precision.
MS, MSD
Result:
Results of analyzing a matrix spike and a matrix spike
duplicate, used to determine precision.
Relative
% Diff
( RPD) :
Calculated using one of the following:
:LC1 - LC2: x 100
( [LC1 + LC2]/2 )
:R1 - R2: X 100
( [R1 + R2]/2 )
:MS - MSD: x 100
( [MS + MS D ] /2 )
MS, MSD
% :
The percentage of analyte recovered in the matrix
spikes. The percent recovery calculation is:
MS %:
(MSD - X) x 100
(T - X)
(MS - X) x 100
(T - X)
MSD %:
where X is the sample result, listed on the analytical
report, and T is the true value, defined below.
True value:
The theoretical, or expected, result of a spiked sample
analysis.
NC Flag
Indicates that the spike recovery was not calculated
due to high sample concentration relative to the amount
of spike added.
Q Flag
Indicates that the quality control measurement is
outside the specified control limits.
Blank
Result:
Laboratory result of analysis of the method blank.
RDL
(Reporting
Detection
Limit) :
BCA-assigned limit, set at a level higher than the
method detection limit (MDL) determined using EPA
guidelines. Sample RDLs may differ from the blank RDL
if the samples were diluted.
R t: 4 ""/vl;,.,,1
II: ORDER PLACED FOR CLIENT: Pacific Environmental Group, Inc. 9507051 :
: BC ANALYTICAL: GLEN LAB: 13:37:33 10 JUL 1995 - P. 1:
---------------------------------------------------------------
---------------------------------------------------------------
ILAMPLES... SAMPLE DESCRIPTION.. DETERM......... DATE...... METHOD..... EQUIP. BATCH.. ID.NO
ANALYZED
&507051*.1
1ItJ507051*2
.507051*3
'507051*4
01-1-1-10
DI-1-1-6.5
DI-1-3-4
DI-2-3-3
1507051*5 DI-2-2-10
507051*6 DI-2-2-6.5
9507051*7 01-3-4-4
1f507051*8 DI-3-3-5.5
~507051*9 DI-3-2-4
9507051*10 DI-3-1-4
1t507051*11 Stockpile 1 of 2
9507051*12 Stockpile 2 of 2
II
II
***
II
II
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Notes: Equipment
ID.NO
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
FUEL. TOT 07.06.958015M 556-11 955063 8501
GAS.BTEX 07.07.958015M 953321 8501
FUEL. TOT 07.06.958015M 556-11 955063 8501
GAS.BTEX 07.07.958015M 953321 8501
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
GAS.TPH.BTEX 07.06.958015M 516-19 953320 8501
GAS.TPH.BTEX 07.07.958015M 953321 8501
FUEL.TOT 07.06.958015M 556-11 955063 8501
GAS.BTEX 07.07.958015M 953321 8501
HOLD 07.10.95
HOLD 07.10.95
FUEL.TOT 07.06.958015M 556-11 955063 8501
GAS.TPH.BTEX 07.07.958015M 953321 8501
PB 07.07.95 6010 535-02 95980 8488
DIG,NAQ.HCL 07.07.95 3050 95980 8488
FUEL.TOT 07.06.958015M 556-11 955063 8501
GAS.TPH.BTEX 07.07.958015M 953321 8501
BC Analytical identification number for a
particular piece of analytical equipment.
BC Analytical employee identification number of
analyst.
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IÞATE REPORTED 07/10/95
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BC ANALYTICAL
ORDER QC REPORT FOR G9507051
Page 1
LABORATORY CONTROL STANDARDS
FOR BATCHES WHICH INCLUDE THIS ORDER
DATE BATCH LC LT PERCENT
IARAMETER ANALYZED NUMBER RESULT RESULT UNIT RECOVERY
· TPH/BTEX C507521*1
Date Analyzed 07.06.95 953320 07/06/95 07/06/95 Date N/A
Benzene 07.06.95 953320 15.8 15.2 ug/L 104
I Toluene 07.06.95 953320 88.8 97.4 ug/L 91
Ethylbenzene 07.06.95 953320 20.3 20.4 ug/L 100
Total Xylene Isomers 07.06.95 953320 112 119 ug/L 94
~ TPH (Gasoline Range) 07.06.95 953320 1120 1100 ug/L 102
· TPH/BTEX C507522*1
Date Analyzed 07.06.95 953320 07/06/95 07/06/95 Date N/A
I Benzene 07.06.95 953320 17.4 15.2 ug/L 114
Toluene 07.06.95 953320 95.7 97.7 ug/L 98
Ethylbenzene 07.06.95 953320 20.9 20.4 ' ug/L 102
II Total Xylene Isomers 07.06.95 953320 119 119 . ug/L 100
TPH (Gasoline Range) 07.06.95 953320 1100 1100 ug/L 100
· GRO/DRO C507561*1
Date Analyzed 07.06.95 955063 07/06/95 07/06/95 Date N/A
I Date Extracted 07.06.95 955063 07/06/95 07/06/95 Date N/A
TPH (total) 07.06.95 955063 272 250 mg/L 109
4. TPH/BTEX C507615*1
I Date Analyzed 07.07.95 953321 07/07/95 07/07/95 Date N/A
Benzene 07.07.95 953321 1.65 1.52 mg/kg 109
Toluene 07.07.95 953321 9.46 9.74 mg/kg 97
Ethylbenzene 07.07.95 953321 2.12 2.04 mg/kg 104
I Total Xyl ene Isomers 07.07.95 953321 11.9 11.9 mg/kg 100
TPH (Gasoline Range) 07.07.95 953321 112 110 mg/kg 102
5. Lead C507492*1 07.07.95 95980 98.1 100 mg/kg 98
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IJATE REPORTED 07/10/95
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IARAMETER
. TPH/BTEX
Date Analyzed
Benzene
I Ethyl benzene
Total Xylene Isomers
TPH (Gasoline Range)
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SAMPLE
NUMBER
BC ANALYTICAL
ORDER QC REPORT FOR G9507051
ADDITIONAL LCS PRECISION (DUPLICATES)
BATCH QC REPORT
DATE BATCH LCl
ANALYZED NUMBER RESULT
07.06.95 953320 07/06/95
07.06.95 953320 15.8
07.06.95 953320 20.3
07.06.95 953320 112
07.06.95 953320 1120
LC2
RESULT UNIT
07/06/95 Date
17.4 ug/L
20.9 ug/L
119 ug/L
1100 ug/L
Page 1
RELATIVE
% DIFF
N/A
10
3
6
2
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BC ANALYTICAL
ORDER QC REPORT FOR G9507051
IDATE REPORTED 07/10/95
Page 1
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MATRIX QC PRECISION (DUPLICATE SPIKES)
BATCH QC REPORT
SAMPLE DATE BATCH MS MSD RELATIVE
IPARAMETER NUMBER ANALYZED NUMBER RESULT RESULT UNIT % DIFF
1. GRO/DRO 9507049*14
Date Analyzed 07.06.95 955063 07/06/95 07/06/95 Date N/A
Ib Date Extracted 07.06.95 955063 07/06/95 07/06/95 Date N/A
TPH (tota 1) 07.06.95 955063 284 356 mg/kg 23
. TPH/BTEX 9507049*22
Date Analyzed 07.07.95 953321 07/07/95 07/07/95 Date N/A
I Benzene 07.07.95 953321 1. 93 1. 74 mg/kg 10
Toluene 07.07.95 953321 11. 4 11.9 mg/kg 4
Ethylbenzene 07.07.95 953321 3.32 3.51 mg/kg 6
It Total Xylene Isomers 07.07.95 953321 20.8 21.7 mg/kg 4
TPH (Gasoline Range) 07.07.95 953321 228 231 mg/kg 1
. TPH/BTEX 9507049*22
Date Analyzed 07.07.95 953321 07/07/95 07/07/95 Date N/A
I Benzene 07.07.95 953321 1. 93 1. 74 mg/kg 10
Toluene 07.07.95 953321 11. 4 11.9 mg/kg 4
Ethylbenzene 07.07.95 953321 3.32 3.51 mg/kg 6
I Total Xylene Isomers 07.07.95 953321 20.8 21.7 mg/kg 4
TPH (Gasoline Range) 07.07.95 953321 228 231 mg/kg 1
4. Lead 9507084*1 07.07.95 95980 129 126 mg/kg 2
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BC ANALYTICAL
ORDER QC REPORT FOR G9507051
~ATE REPORTED 07/10/95
Page 1
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MATRIX QC ACCURACY (SPIKES)
BATCH QC REPORT
SAMPLE DATE BATCH MS MSD TRUE
IARAMETER NUMBER ANALYZED NUMBER 9-< 9-< RESULT UNIT
0 0
. GRO/DRO 9507049*14
TPH (total) 07.06.95 955063 114 142 250 mg/kg
(' 'BTEX 9507049*22
Benzene 07.07.95 953321 112 99 1. 75 mg/kg
Toluene 07.07.95 953321 76 81 13.7 mg/kg
Ethylbenzene 07.07.95 953321 75 84 3.84 mg/kg
I Total Xylene Isomers 07.07.95 953321 74 82 23.9 mg/kg
TPH (Gasoline Range) 07.07.95 953321 107 110 220 mg/kg
3. TPH/BTEX 9507049*22
I Benzene 07.07.95 953321 112 99 1. 75 mg/kg
Toluene 07.07.95 953321 76 81 13.7 mg/kg
Ethylbenzene 07.07.95 953321 75 84 3.84 mg/kg
II Total Xylene Isomers 07.07.95 953321 74 82 23.9 mg/kg
TPH (Gasoline Range) 07.07.95 953321 107 110 220 mg/kg
. Lead 9507084*1 07.07.95 95980 101 98 128 mg/kg
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lATE REPORTED 07/10/95
BC ANALYTICAL
ORDER QC REPORT FOR G9507051
Page 1
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METHOD BLANKS AND REPORTING DETECTION LIMIT (RDL)
FOR BATCHES WHICH INCLUDE THIS ORDER
IARAMETER
· TPH/BTEX
Date Analyzed
I Benzene
Toluene
Ethylbenzene
Total Xylene Isomers
I TPH (Gasoline Range)
· GRO/DRO
Date Analyzed
~ Date Extracted
TPH (total)
· TPH/BTEX
I Date Analyzed
8enzene
Toluene
Ethylbenzene
I Total Xylene Isomers
TPH (Gasoline Range)
4. Lead 8507270*1
DATE 8ATCH
ANALYZED NUMBER
8507282*1
07.06.95 953320
07.06.95 953320
07.06.95 953320
07.06.95 953320
07.06.95 953320
07.06.95 953320
8507317*1
07.06.95 955063
07.06.95 955063
07.06.95 955063
B507347*1
07.07.95 953321
07.07.95 953321
07.07.95 953321
07.07.95 953321
07.07.95 953321
07.07.95 953321
07.07.95 95980
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BLANK
RESULT RDL
07/06/95 NA
0 0.005
0.012 0.005
0 0.005
0.018 0.01
0 0.05
07/06/95 NA
07/06/95 NA
0 10
07/07/95 NA
0 0.005
0.029 0.005
0 0.005
0.028 0.01
0 0.05
3.1 5
UNIT METHOD
Date 8015M
mg/kg 8015M
mg/kg 8015M
mg/kg 8015M
mg/kg 8015M
mg/kg 8015M
Date 8015M
Date 8015M
mg/kg 8015M
Date 8015M
mg/kg 8015M
mg/kg 8015M
mg/kg 8015M
mg/kg 8015M
mg/kg 8015M
mg/kg 6010
,.,
{."
a
California Regional Water Quality Control Board
Central Valley Region
Terry Tamminen
Secretmy for
Environmental
Protection
Fresno Branch Office
Internet Address: http://www.swrcb.ca.gov/-rwqcb5
1685 E Street, Fresno, California 93706-2020
Phone (559) 445-5116' FAX (559) 445-5910
Arnold Schwarzenegger
Governor
7 June 2004
Regional Board Case No. 5T15000886
Mr. Tony Palagyi
Shell Oil Products U.S.
2555 13th Avenue SW
c 'SêatÜe,~wãshingÚ:)!i 981'34
-- - --
UNDERGROUND TANK RELEASE, SHELL SERVICE STATION, 5321 STOCKDALE
HIGHWAY, BAKERSFIELD, KERN COUNTY
You submitted First Quarter 2004 Groundwater Monitoring Report (Monitoring Report) dated
3 May 2004 and prepared by Delta Environmental Consultants, Inc., Monrovia (Delta). The Monitoring
Report documents a groundwater monitoring event at the above-referenced site on 24 February 2004. In
a letter dated 17 June 2003, the Bakersfield Fire Department referred thé subject case to our agency for
regulatory oversight. It also provided us with information indicating that gasoline range petroleum
hydrocarbons and the fuel oxygenates methyl tertiary butyl ether (MTBE) and tertiary butyl alcohol
(TBA) leaked at the subject site degrading soil and may threaten groundwater quality. The January 2004
site assessment was conducted lateral to the underground storage tank (UST) cluster rather than beneath
the cluster. You have indicated that Shell Oil Products, U.S. (Shell) expects to remove the UST system
in the near future and that soil sampling will be conducted during this work in compliance with City of
Bakersfield Fire Department (BFD) requirements. Therefore, we do not request additional site
investigation at present. We will determine site closure requirements based upon our review of site
assessment data collected during thè UST system removal. Detectable gasoline or diesel range
__ _ R~trol~um constituents have not been detected during six groundwater monitoring events. Groundwater
monitoring fr~quericy ~ay be reduced to årÏnual. The ñ'ext monitoring eýèrìt slÌòúÌd be conåudëd during
the first quarter 2005. Analysis for "full scan" EP A Method 8260 analytes, lead scavengers, dissolved
lead, general minerals, nitrate, and total Kjeldahl nitrogen may be discontinued. A summary of the
Monitoring and Site Assessment Reports and our comments follow.
Monitorin2 Report Summary
Blaine Tech Services, Inc., San Jose (Blaine Tech) collected groundwater samples from the monitoring
wells on 24 February 2004. Depth to groundwater was measured from 127.48 and 128.74 feet below
ground surface (bgs). Delta determined groundwater flow to be toward the southeast with a water table
slope of 0.015 feet per foot, consistent with previous monitoring events.
Samples collected from MW -1 through MW -4 were analyzed for total petroleum hydrocarbons as
gasoline and diesel (TPH-g and TPH-d) by EPA Method 8015M, volatile organic compounds by "full
CaliforniaEnvironmental Protection Agency
""
~<:1 Recycled Paper
"
Mr. Tony Palagyi
- 2 -
7 June 2004
i
'r;
scan" EP A Method 8260B analysis, including benzene, toluene, ethylbenzene, and xylenes (BTEX),
MTBE, TBA, di-isopropyl ether (DIPE), ethyl tertiary butyl ether (ETBE), tertiary amyl methyl ether
(TAME), 1,2-dichloroethane (1,2-DCA), and 1,2-dibromoethane (EDB). The samples were also
analyzed for dissolved lead by EPA Method 6010B. Analytes were not detected in the samples.
Samples collected from MW-1 through MW-3 were analyzed for general minerals (various methods),
nitrate by EP A Method 300.0, and total Kjeldah1 nitrogen (TKN) by EP A Method 351.3. Total
dissolved solids (TDS) ranged from 160 to 200 milligrams per liter (mg/L), while specific conductance
(Ee) ranged from 270 to 310 µmhos/centimeter. Total hardness ranged from 74 to 96 mg/L. Alkalinity
ranged from 82 to 100, resulting from bicarbonate. Carbonate was not detected. Iron ranged from 0.109
to 0.215 mg/L. Chloride ranged from 18 to 110 mg/L. Nitrate was detected at concentrations up to 1.3
mg/L. TKN and dissolved lead were not detected.
Comments
~- -~~'----:'"
.~~
~--
KHM-Environmental Management, Inc., Monrovia (now Delta) conducted a voluntary groundwater
assessment program (GRASP) investigation on behalf of Shell Oil Products U.S. (Shell) on-site.
KHM's GRASP Site Assessment Report (Site Assessment Report) dated 25 April 2003 describes that
investigation. KHM discovered low concentrations ofTPH-g, MTBE and TJ3..A in subsurface soils to a
depth of 35 feet bgs in a position lateral to the UST cluster. This data suggested that higher
concentrations ofthese analytes might be present beneath the UST system and could threaten
groundwater quality. Impacted soils were not encountered in boring B-1, drilled in another position
lateral to the UST cluster. Although B-1 did not investigate soils beneath the UST cluster, the analytical
data does not indicate a major release with lateral spreading. The constituents previously detected in
sòils may have resulted from a minor vapor release. Gasoline and diesel range petroleum constituents
have not been detected in groundwater during five monitoring events.
You have indicated that Shell expects to remove the UST system in the near future and conduct
associated soil sampling under the supervision of the BFD. We do not request that you conduct
additional site investigation at present. We will review the results of the UST system removal
assessment prior to detennining site'closure requirements. Please contact us by 26 July 2004 with an
update concerning the UST removals.
~~
Due to the absence of detectable analytes during groundwater monitoring, we request that you reduce
monitoring frequency to annual beginning with the first quarter 2004. The next monitoring report
should be conducted during the first quarter 2005. Please submit the first quarter 2005 monitoring report
by 3 May 2005.
By our letter dated 25 July 2003, we requested that you expand the current groundwater sample analysis
program to confinn constituents of concern (COCs). Samples were to be analyzed for the analytes
usually reported in a full EP A 8260 analysis, the lead scavengers 1,2-DCA, and EDB, and dissolved
lead. You conducted these analyses during the third and fourth quarters of 2003. Since these analytes
were not detected, analysis by "full scan" EP A Method 8260B, the lead scavengers, and dissolved lead
may be discontinued.
V:\UG1ìProjectsVDW _files\2004 Con-espondence\City of Bakersfield Cases\Shell Stn Stockdale Hwy GW 5-04.doc
,.¿:-,
~"
'õ'
Mr. Tony Pa1agyi
- 3 -
7 June 2004
You conducted general minerals, nitrate, and TKN analyses during the third quarter 2003 and the first
quarter 2004 monitoring events. Since you have adequately characterized groundwater quality, you may
discontinue these analyses.
Please contact this office at least five days prior to fieldwork. If you have any questions regarding this
correspondence, please contact me at (559) 445-5504.
~IT: (¡)~ '
Engineering Geologist
R.G. No. 5951
...-~--
c:
Ms. Barbara Rempel, SWRCB, UST Cleanup Fund, Sacramen~
Mr. Howard H. Wines III, Bakersfield Fire Department, BakersfieÌèN'
Mr. Bradley Clark, Delta Environmental Consultants, Inc., Monrovia
Ms. Kathryn Ewing, Delta Environmental Cons.!Jltants, Inc., Monrovia
File: UST/Kern/Shell Service Station, 5321 Stockdale Highway, Bakersfield/5Tl5000886
V:\UG1ìProjectsVDW _files\2004 Correspondence\City of Bakersfield Cases\Shel1 Stn Stockdale Hwy GW 5-04,doc
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·Â Delta
Environmental
~... Consultants, ine.
Solving en~ronment-reIated business problems worldwide
www.deItaenv.com
911 South Primrose Avenue · Suite K
Monrovia, California 91016 USA
626,256.6662 800.477.7411
Fax 626.256.6263
May 3, 2004
Project No. PA5321S-1
Mr. John D. Whiting
California Regional Water Quality Control Board
Central Valley Region
1685 E. Street
Fresno, California 93706-2020
"
Re: FIRST QUARTER 2004GROUNDW ATER MONITORING REPORT
Texaco Service Station
5321 Stockdale Highway
Bakersfield, California
Dear Mr. Whiting:
On behalf of Equilon Enterprises LLC dba Shell Oil Products (SHELL), Delta Enviromnental Consultants, Inc.
(DELTA) has prepared this First Quarter 2004 Groundwater Monitoring Report for the above-referenced site.
This quarterly report represent DELTA's professional opiriions based upon the currently available information and
are arrived at in accordance with currently acceptable professional standards. This report is based upon a specific
scope ofwork"requested by the client. The Contract between DELTA and its client outlines thè scope of work, and
only those tasks specifically authòrized by that contract or outlined in this report were performed. This report is
iniendedonly for the use of DELTA's Client and anyone else specifically listed on this report. . DELTA will not
, and cannot be liable for µnauthorized reliance by any other third party. Other than as contained in this paragraph,
DELTA makes rio express or implied warranty as to the contents of this report.
If you have any questions regardIDg this site, please contact Mr. Brad clark (DELTA) at (626) 256-6662 or .
Mr. Tony Palagyi (SHELL)(425) 377-8530.
Sincerely,
Delta Environmental Consultants, Inc.
~.
Bradley E. Clark, P.E. C55425
SemorPr0ectEngineer
. Attachment: First Quarter 2004 Groundwater Momtoring Report
cc: Tony Palagyi, Shell Oil Products US
Howard H. Wines ill, City of Bakersfield Fire Department
A member of
X Ino g ~!!:entalAmanCe
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May 3, 2004
SHELL QUARTERLY STATUS REPORT
5321 Stockdale Highway
PA532lS-l
Tony Palagýil( 425) 377-8530
Kathryn Ewing/( 626) 256-6662
CVRWQCB/ John Whiting
City of Bakersfield Fire Department! Howard H. Wines
III
WORK PERFORMED THIS QUARTER (FIRsT - 2004):
1. Quarterly groundwater monitoring and sampling. Submitted quarterly report.
2. Submitted additional site investigation report dated February 12, 2004.
3. Received agency letter dated March 26,2004 reducing sampling to annual monitoring and
discontinuing "full scan" EP A Method 8260 and dissolved lead.
Station Address:
DELTA Project No.:
SHELL Environmental. Engin.lPhone No.:
DELTA Site ManagerlPhone No.:
Primary AgencylRegwatory ill No_:
Other Agencies to Receive Copies:
WORK PROPOSED FOR NEXT QUARTER (SECOND- 2004):
1. No activities, per agency letter dated March 26,2004.
Current Phase of Project: Groundwater monitoring only
Frequency of Sampling: Annual
Frequency of Monitoring: Annual
Is Separate Phase Hydrocarbon Present On-site (Well #'s):
Cumulative SPH Recovered to Date: NA
SPH Recovered This Quarter: None
Sensitive Receptor(s) and Respective
Direction(s):
DYes ~No
Nearest field verified well is Well CBI<, 06-01 (State
Well No. 30S/27E-03B02 M) ofllie City of Bakersfield
approximately 825 feet South of the site.
Current Remediation Techniques:
Permits for Discharge:
Approxlinate Depth to Groundwater:
Groundwater Gradient .
Current Agency Correspondence:
~~-:~O/
Kathryn Ewing
Site Manager (DELTA)
None
None
127.48' to 128.74'
Southeast @ approxlinately 0.015 ftIft
Central Valley RWQCB letters datèd March 26,2004.
. None
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ATTACHED:
· Table 1 - Groundwater Gauging and Analytical Results
· Table 2 - Additional Chemicals of Concern
· Figure 1 -Site Location Map
· Figure 2 - Groundwater Elevation Contour Map
· Figure 3 - Hydrocarbon Distribution in Groundwater Map
· Figure 4 - TPH-G Concentrations in Groundwater Map
· Figure 5 - Benzene Concentrations in Groundwater Map
· Figure 6 - MTBE Concentrations in Groundwater Map
· Appendix A - Field Data Sheets
· Appendix B - Field Procedures
· Appendix C - Laboratory Report and Chain-of-Custody Documents
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TABLES
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TABLE 1 I I
HISTORICAL GROUNDWATER GAUGING AND ANALYTICAL DATA
TEXACO SERVICE STATION I
5321 Stockdale Highway, Bakersfield, California
I I
: < :ÒAT'E<:::: : )i!:P-TH::::::::: SpiI:::::::: :GWÜi!:V;:::::: :t.p.iicj):: :tpiIcG: BEhjZItNË ::rOLU'ENE
: :/<:::::::i>/g~f:::':·T:j~~t;::}r:~~~tW:::::~~~~;::: :iú;;¡¿i:: ::::~~~il{:: ::::i~~it;;::::
I I
~p of casinl!; elevation (ft): 386.61
129.17 0.00 257.44
129,38 0.00 257.23
130.76 0,00 255.85
132,68 0.00 253,93
132,11 0.00 254,50
MW-l
3!l7/2003
3/25/2003
6/19/2003
9/3/2003
ll/2l/2003
ll/21/2003
2/24/2004
128,74
0,00
257.87
MW~ _,Top of casinl!; elevation (ft): 386.06
3!l7/2003 128,64 0.00 257.42
3/25/2003 128.84 0,00 257.22
6/19/2003 130.27 0.00 255.79
9/3/2003 131.79 '0.00 254,27
11/21/2003 131.45 0.00 254.61
11/21/2003
2/24/2004 127.91 0.00 258.15
MW-3
371m003
3/25/2003
6/19/2003
9/3/2003
11/21/2003
11/21/2003
2/24/2004
MW-4
3/17/2003
3/25/2003
6!l9/2003
9/3/2003
11/21/2003
2/24/2004
Top of casinl! elevation (ft): 386.34
128,30 0.00 258.04
128.45 0.00 257,89
129.82 0.00 256.52
131.44 0.00 254.90
131.14 0.00 255.20
127.71
0.00
258.63
ND<IOOO
ND<IOOO
ND<IOOO
ND<\ 000
ND<IOOO
ND<IOOO
ND<lOOO
ND<lOOO
ND<lOOO
ND<IOOO
ND<lOOO
ND<lOOO
ND<IOOO
ND<IOOO
ND<1000
ND<IOOO
ND<IOOO
ND<IOOO
ND<1000
ND<50
ND<50
ND<50
ND<50
ND<50
ND<50
ND<50
ND<50
ND<50
ND<50
ND<50
ND<50
ND<50
ND<50
ND<50
ND<50
ND<50
ND<50
ND<50
ND<50
ND<50
ND<50
ND<50
ND<0.50
ND<0.50
ND<0.50
ND<0.50
ND<0.50
ND<0.50
ND<0.50
ND<0.50
ND<0.50
ND<0.50
ND<O,50
ND<0.50
ND<0.50
ND<0.50
ND<0.50
ND<0.50
ND<0.50
ND<0.50
ND<0.50
ND<0.50
ND<0.50
ND<0.50
ND<0.50
ND<I.O
ND<I.O
ND<I.O
ND<I.O
ND<I.O
ND<I.O
ND<I.O
ND<I.O
ND<I.O
ND<\.O
ND<I.O
ND<I.O
ND<I.O
ND<I.O
ND<I.O
ND<I.O
ND<I.O
ND<I.O
ND<I.O
ND<I.O
ND<I.O
ND<I.O
ND<I.O
~'-I--
Notes:
GW - Groundwater
SPH - Separate'phase hydrocarbons
MSL - Mean sea level I
ND -.Not detected I
~!\!!:..:.parts Eer billion I
TPH-D - Total petroleum hydrocarbons as diesel
TPH-G - Total petroleum hydrocarbons as gasoline using either EPA Method 8015M or the DHS LUFT Method
MTBE - Methyl-tert butyl ether
TB~ - Tert,butyl alcohol I
DIPE - Di-isopropyl ether
ETBE - Ethyl-tert butyl ether
TAME· Tert-amyl methyl ether
I
Top of casing elevation (ft): 386.57
128.17 0.00 258.40
128.25 0.00 258.32
129,59 0.00 256.98
131.26 0.00 255.31
130,90 0.00 255,67
127.48 0.00 259.09
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-
::tíijYj;.::: :::1'mAL:>
BENZENE; :XYLENES:
: :::(~~iL)::: :: ::iú¡¡iLV:
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Page \ of \
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ND<2.0
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--.-.-
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-
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:.:.: 'DAn:·:·:· :Cl1mRIDE:' :rjl:rRn:E':' :NIJ'RATt·:·: SlJ.U';nE:·:,: ·:rI<I(·:·: ·ALKi\.L(Nrry.:· :alCi\.ROOIII~TE·:· :C.AJ!JlONi\:rE:· :I1YOROxmE:· ': L£>\O':':' :C>\~CIVM:"·'· /ROO':':' :M>\<;IjES:WJlf·: ·POTi\S5IVJlf·:· SODIUNI: : MANGANESE'" .'. :sYEClf.IC·····,:·:' :r.0.Ti\":·:,·,·,·, PH:·:·: 'TDS:"
:::..:.:.:..:.......:.: ·;~eiL;:::.::: j~~æ~:::::: :~~;::::.: '(~ln.~.':::: ¡~~¿::::: !~~~~t~:.:::: !~i~:i~~~::' ': :~S;~:~~3.~::.. :~~~(;:~~~:. : :iiBWtj::::::: ¡Þ¡~i::::::. (~~.:.:.:.: .i~~~;.:.:.:.::'. (~i¡i:::::.·. (Jri~L\'::::.: .i~iiLi:.:::: ~~~~t~~~~~~ :i~j~~Zi~~:·: ~~~;i~;:::::: (~~¡j:;::
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--91312003J'--2¡¡- ND<O.IO 1.60 27 ND<Ò-:5õ 100 100 ND<1.0 ND<1.0 ND<O,OI 30.8 ND<Õ}"~:¡S- 2.06 40,3 ND<O,00500 ---3S¡¡--C---¡-¡Ò-- 6,31 220
,l!~:i, --.?O__~!'IA 1.30 23 ND<050 100 --I----Too--ND<1.0 ND<1.0 ND<O.OI 29.5 0.129 5j~--=-=:,'2.32-:::: 29,8 ND<O,00500 310 96~.--!.§.Q..~
------
MW-3
~~9~12_0.Q.L -~ ND<O,IO -¡-:w-I---27"' ND<O,50 100 100 ND<I.O ND<1.0 ND<O,OI 32,6 ND<O.I 5.94'2,34--34 ND<O,00500 350- 100 6.36 --22Õ'-
,~<IQºO'±', 20 NA 1.20 23 ND<O,50 94 94 ND<I.O ND<1.0 ND<O.OI 28.0 0.109 5.66 ___, 2.33 29,8 ND<0.00500 310 92 6.85 __,.2.QQ....
"__n_____'____."
--~---
MW,4
_._,--~--"-_..- ~
.,. ?.Q!~-º-~.. ~1~ ND<O,IO 1.50 , 26 ND<0.50 80 80 ND<I.O ND<I.O
2/24/2004 18 NA 0.75 21 ND<0.50 82 82 ND<I.O ND<I.O
,~~~~~~~.., ==----
II5J':1,:.Iotal Kjeldaþl Ni1!<2g~_,
TDS - Total Dissolved Solids
!'JA· Not.aE.alyzed
~-==~,':=+-
Note: AddJt!9~,al Chemicals of Concern Anal~sis are only for the first and third Quarters for wells MW,2, MW-3, and MW-4,
---- -'--
ND<O.OI
ND<O,OI
30.5
22,[
ND<O, ( 5.48 .__~ 41
0.2\.5_ __ ~~_,_,~ 28.3
--1-'.
~,-~--
ND<O,00500
----º'º.o~
350
270
96 _+__~~_ 220
74 6.89 180
---..
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FIGURES
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,
 DELTA
ENVIRONMENTAL
~~ CONSULTANTS INC,
SHELL OIL PRODUCTS US
TEXACO SERVICE STATION
BAKERSFIELD, CALIFORNIA
FIGURE 1 ,
SITE LOCA TIOt'-~ MAP
5321 STOCKDALE HIGHWAY
BAKERSFIELD, CALIFORNIA
-
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STOCKDALE HIGHWAY
CANOPY
(TYP)
---
I
DISPENSER
ISLAND
(TYP)
/
UST
(TYP)
/ í l
/ I I
r~MW-4 I I
(259,09) ~
, r 1 r) ~ +~B'1 ~ :
I........,. I II II I : I
I II II II I I
1/ I II II II I I I
1~ JlJlJlJ: :
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~MW-3 cr-
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---
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~
IIServerlkhm_dataIClientsl..Shelll..Shell SIte51515321 Stockdalel2004'04,)OUQ04 Monitoring ReportlFIGURE 2(5321LGROUNDWATER ELEVATION CONTOUR MAP,dwg, Model, 4/12/2004 3:23:05 PM
-
-
-
LEGEND
-
-
-
-
N
W<>E
S
MW-1-$- GROUNDWATER MONITORING
WELL LOCATION AND
DESIGNA TION
(255,67) GROUNDWATER ELEVATION
IN FEET ABOVE MEAN SEA
LEVEL (Ft!MSL)
256.20- - GROUNDWATER CONTOUR
IN FEET ABOVE MEAN SEA
LEVEL (Ft/MSL)
CONTOUR INTERVAL~O.25 FEET
. I. APPROXIMATE GROUNDWATER
FLOW DIRECTION
o
20
40
~--
SCALE IN FEET
 Delta
ENVIRONMENTAL
~~ CONSULTANTS INC.
SHELL OIL PRODUCTS US
TEXACO SERVICE STATION
BAKERSFIELD, CALIFORNIA
FIGURE 2
GROUNDWATER ELEVATION
CON TOUR fA AP
02/24/04
S321 STOCKDALE HIGHWAY
BAKERSFIELD, CALIFORNIA
-
-
'-
-
-
-
UST
(TYP)
-,-
f 1 f 1 r
I II II
I II II
I II II
\ J \ J l
I M:':3___~
: / ~ \
\ }
\ I
\ I
'--____-1
-
-
-
CANOPY
(TYP)
STOCKDALE HIGHWAY
DISPENSER
ISLAND
(TYP)
) f
II
II
II I
J l J
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L___--J,
BUILDING
I.
I/MW-2
t
--
Date
MW-l
TPH-g BENZENE
(µoIL) (µoIL)
ND<50 NO<O,50
ND<50 NO<0.50
ND<50 ND<O,50
ND<50 ND<0.50
ND<50 ND<O,50
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Date (:/0 BENZENE MTBE
(µoIL) (µgIL)
03/25/03 ND<50 ND<O,50 ND<1,O
06/19/03 NO<50 NO<0.50 ND<LO
09/03/03 ND<50 ND<0.50 NO<LO
11/21/03 NO<50 ND<O,50 NO<1,O
02/24/04 ND<50 ND<O,50 ND<LO
MW 3
Dote TPH-g BENZENE MTBE
(µoIL) (µoIL) (µg/L)
03/25/03 ND<50 ND<0.50 ND<I.0
06/19/03 ND<50 ND<0.50 ND<LO
09/03/03 ND<50 ND<0.50 ND<LO
11/21/03 ND<50 NO<0.50 NO<LO
02/24/04 ND<50 NO<O,50 ND<LO
0
<t:
0
D:::
W
z
F=
(f)
3
w
Z
MW-2
Date (:ÏL"J BENZENE MTBE
(µoIL) (µoIL)
03/25/03 ND<50 ND<O,5D ND<1.0
06/19/03 ND<50 ND<0.50 ND<1.0
09/03 03 ND <50 ND<O,50 ND<1'.O
11/21/03 ND<50 ND<O,50 ND<1.0
02 24/04 ND<50 ND<O,50 ND<1.0
03/25/03
06/19/03
09/03/03
11/21/03
02/24/04
IIServerlkhm)1ata\Clients\..Shell\..Shell Sites\S\S321 Stockdale12004'04'XX_IQ04 Monitoring ReportlF1GURE 3(S32ILHYDROCARBON DISTRIBUTION IN GW MAP,dwg, Model, 4/12/2004 3:23:S1 PM
>-
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MTBE
(µoIL)
ND<1.0
ND<1.0
ND<l,O
ND<I,O
ND<1.0
-
WASTE
OIL
TANK
I
-
-
-
-
-
N
W<>E
S
LEGEND
MW-l~ GROUNDWATER MONITORING
WELL LOCATION AND
DESIGNA TION
TPH-g
TOTAL PETROLEUM
HYDROCARBONS
AS GASOLINE
MTBE
METHYL TERT -BUTYL
ETHER
.L9/L
MICROGRAMS PER LITER
NO
NOT DETECTED
o
20
40
~
SCALE IN FEET
JøÅ
Delta
ENVIRONMENTAL
CONSULTANTS INC.
SHELL OIL PRODUCTS US
TEXACO SERVICE STATION
BAK,ERSFIELD, CALIFORNIA
FIGURE 3
HYDROCARBON DISTRIBUTIONIN
GROUNDWATER MAP
5321 STOCKDALE HIGHWAY
BAKERSFIELD, CALIFORNIA
-
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-
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-
STOCKDALE HIGHWAY
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(TYP)
-
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I\5eTVerli<hm_data\Clients\.Shell\.5hell 5Ite'\5\5321 5toci<dale\2004'04'X)UQ04 Monitoring Report\FIGURE 4(5321LTPH-gCONCEN1AATIONMAP.dwg, Model, 4/12/2004 3:24:09 PM
UST
(TYP)
CANOPY
(TYP)
/
/
r~MW-4
ND~~1 f 1 r ì f
I II II II
I II II II
I I II II II
I MW-3 l J l J l J l
IND::____
If 1- \
I I \
\ }
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~ ~ ~~;5'O
----
-
-
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I I
I I
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I I WASTE
I I~ I OIL
I I ~ TANK
l - J
---
~MW-1
ND<50
BUILDING
-.-----
-
-,-
-
--
-
-
N
W<>E
S
LEGEND
MW-1 ~ GROUNDWATER MONITORING
WELL LOCATION AND
DESIGNATION
ND<50 TPH-g CONCENTRATIONS
IN MICROGRAMS PER LITER
().Jg/L)
TPH-g TOTAL PETROLEUM
HYDROCARBONS
AS GASOLINE
J.J9/l MICROGRAMS PER LITER
ND NOT DETECTED
o
20
40
r---__
SCALE IN FEET
 Delta
~ ENVIRONMENTAL
W"J.. CONSULTANTS INC.
SHELL OIL PRODUCTS US
TEXACO SER\,1CE ST A nON
8 AKERStlElO , CALIFORNIA
FIGURE 4
TPH-g CONCENTRATIONS IN
GROUNDWA TER MAP
02/24/04
5321 STOCKDALE HIGHWAY
BAKERSFIELD, CALIFORNIA
-
-
-
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(f]
N
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-
-
-
-
CANOPY
(TYP)
-
STOCKDALE HIGHWAY
DISPENSER
ISLAND
(TYP)
/
/
r~MW-4
ND<O.50
I
fir 1 f ì f 1 I
I II II II I I
I I II II II I :
I II II II I I
I MW-3 l J l Jl J l J I
INO<O.5 L
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1\------/
BUILDING
---
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---
~MW-1
ND<O.50
f- ~~;~50 _ _ _ __
-,
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WASTE
OIL
TANK
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IIServerlkhm_datalClients\..Shell\..Shell Slte'I5\5321 Stockdalel2004,04,)(JUQ04 Monitoring ReportlFIGURE S(S321LBENZENE CONCENTRATlONMAP,dwg, Model, 4/12/2004 3:24:24 PM
-
-J
-
-
-
-
...
-
N
W<>E
S
LEGEND
MW-1 ~ GROUNDWATER MONITORING
WELL LOCAllON AND
DESIGNATION
ND<O.50 BENZENE CONCENTRATIONS
IN MICROGRAMS PER LITER
(JJg/L)
JJg/L MICROGRAMS PER LITER
ND NOT DETECTED
o
20
40
r----_
SCALE IN FEET
 Delta
ENVIRONMENTAL
~Â CONSULTANTS INC.
SHELL OIL PRODUCTS US
TEXACO SERVICE STATION
BAKERSFIELD, CALIFORNIA
FIGURE 5
BENZENE CONCENTRATIONS IN
GROUNDWATER MAP
02/24/04
5321 STOCKDALE HIGHWAY
BAKERSFIELD. CALIFORNIA
-
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-
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-
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\\5erverlkhm_datalClients\..5hell\..5hell 5ite51515321 5tockdalel2004,04,XJUQ04 Monitoring ReportlFIGURE 6(5321LMTBECONCENTRATIONMAP,dwg, Model, 4/12/2004 3:24:40 PM
CANOPY
(TYP)
/
/
r~MW-4
ND~ ~~ r 1 r 1 i
I II II II
I II II II
I I II I I I I I
I MW-3 l J l J l J l J
IND:~~__~
II ~ \
I I \
( }
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l___--J
~MW-1
ND<1.0
BUILDING
-------
,-
WASTE
OIL
I TANK
I
I
-
-
-
-
-
-
-
N
w-r>E
S
LEGEND
MW-l ~ GROUNDWATER MONITORING
WELL LOCATION AND
DESIGNA TION
.lliì.0.J) MTBE CONCENTRATIONS
IN MICROGRAMS PER LITER
(µg/L)
J.Jg/L MICROGRAMS PER LITER
ND NOT DETECTED
MTBE METHYL TERT-BUTYL
ETHER
o
40
20
r---: _
SCALE IN FEET
 . Delta
ENVIRONMENTAL
I. CONSULTANTS INC.
SI-IELL OIL PRODUCTS US
TEXACO SER~CE STATION
BAKERSFIELD, CALIFORNIA
FIGURE B
MTBE CONCENTRATIONS IN
GROUNDWA TER MAP
02/24/04
5321 STOCKDALE HIGHWAY
. BAKERSFIELD, CAliFORNIA
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ÀPPENDIXA
FIELD DATA SHEETS
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Client ~\
Site Address _ ?3> 2-\
Job Number ~O2..2-~--:-
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NOTES:
WELLHEAQ INSPECTION CHECKLIST
pagelorL
Waler Bailed WeJlbox Other Action
From Components Cap Lock Taken
Replaced Replaced (e (plaln
WeUbo ( Cleaned below)
Well Not
Inspected
(e)(plaln
below)
RepaIr Order
SubmlUed
..
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llLAINE TECH SERVICES, INC.
SAN OIEGO
SAN JOSE
www.blalnelech.com
SACRAMENTO
LOS ANGELES
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·
·
·
,
sit~3 ;zj
WelllD
Sheen I
Odor
Depth to
Immiscible
Liquid (ft.)
WELL GAUGING DATA
Date
Thickness
of
Immiscible
Liquid (ft.)
Volume of
Immiscibles
Removed
(rnl)
C:lieI1t~
Depth to water Depth to wen
(ft.)
·
,
,
·
·
..
·
Project # <Y\~\
~~CÀ\e \\"1 ~~~\~ ~.
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, :
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Blaine Tech Services, Inc. 1680 Rogers Ave., San ~ose, CA 95112 (408) 573·0555
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Sampler:
SHELL WELL MONITORING DATA SHEET
Site: <=1.1
Date: 42J
Well Diameter: 2 3 @ 6 8
Depth to Water (DTW): 1.28..1
Thiel mess of Free Product (feet):
D.O. Meter (ifreq'd): YSI
BTS#:
Depth to Free Product:
Referenced to:
Grade
HACH
DTW with 80% Recharge [(Height of Water Column x 0.20) + DTW]:
Purg~od: Bailer Waterra Samp1ing Method: Baiter
. .. _.~ . osable Bailer Peristaltic (Disposable Eia~
Positi iT Displacement Extraction Pump Extraction Port
Electric Subm 'ble Other Dedicated Tubing
. \ œ~
Screened Interval:~ If well is listed as a no-purge, confinn that water level is below the top
f Oth·th 11 b d
o screen. erwlse, e we must e purge .
Well Dinmeter Multiplier Well Diameter Multiolier
I" 0.04 4" 0.65
(Gals.) X = Gals. 2" 0.16 6" 1.47
1 Case Volume Specified Volumes Calculated Volume 3" 0.37 Other radius2 · 0.163
Condo Turbidity,
Time Temp (OF) pH (mS or (.íS~ (NTUs) Gals. Removed Observations
\2l\S ~,~ 7t~ 2.'1 \2-6 ---.
"
Baller lowered "? I below
DTW .to obtnln sample
Did well dewater? Yes No Gallons actually evacuated:
Sampling Date:z.b_'1 . ð\ Sampling Time: lZ- L\S Depth to Water: JZ~ ·1Y
\ \
Sample I.D.: N\\t~-. \ Laboratory: ~ce Columbia Other
Analyzed for: @ @x' MTBE ~ O~ates (5) Other;
EB I.D. (if applicable): @ Duplicate I.D. (if applicable):
Tint.
Analyzed for: TPH-G BTEX MTBE TPH-D Oxygenates (5) Other:
D.O. (ifreq'd): Pre-purge: mg/L Post-purge: mC/L
O.R.P. (ifreq'd): Pre-purge: mV Post-purge: mV
Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (800) 545~7558
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SHELL WELL MONITORING DATA SHEET
BTS#:
Site:
3 ~ 6 8
Sampler:
Well I.D.:
Total Well Depth (TD): \
Date:
Well Diameter: 2
.2-6
Depth to Water (DTW):
Depth to Free Product: Thiclmess of Free Product (feet):
Referenced to: v Grade D.O. Meter (ifreq'd): ysr HACH
. DTW with 80% Recharge [(Height of Water Column x 0.20) + DTW]:
Bailer
'sposable Bailer
Pas! . e Air Displacement
Electric mersible
Waterra
Peristaltic
Extraction Pump
Other
Sampling Method:
. Bailer
~ab e Bai1el)
Extraction Port
Dedicated Tubmg
, ' \:
Screened Interval: ø - \l\~
Other:
Ifwell is listed as a no-purge, confirm that water level is below the top
th 11 b d
of screen. OtherwIse, e we must e DUfQ:e ,
WeIJ Dinmeter Multiplier Well Dinmcter Multiplier
I" 0.04 4" 0.65
(Gals.) X == Gals. 2" 0.16 6" 1.47
1 Case Volume Snecified Volumes Calculated Volume 3" 0.37 Other rodius2 · 0,163
Condo Turbidity
Time Temp tF) pH (mS or ® (NTUs) Gals. Removed Observations
\24V:J bb~ 7.. '78, t ~~~ L~
Baller lowered 3. I below
DTW to obtain snmple
Did well dewater? Yes No Gallons actually evacuated:
Sampling Date: 'Z/V1 Joy Sampling Time: 12.15 Depth to Water: } L7~ q ,
Sample I.D.:\'J\~ -, 2- Laboratory: Qce Columbia Other
~ MTBE ~ - Sm;- ~oW
. Analyzed for: ~ O~genàtð.j> (5) Other:
EB I.D.(ifapplicable): @ Duplicate I.D. (if applicable):
Time
Analyzed for: TPH-G BTEX MTBE TPH-D Oxygenates (5) Other:
D.O, (ifreq'd): Pre-purge: mg/L Post-purge: ' mg/L
O.R.P, (ifreq'd): Pre-purge: mV Post-purge: mV
Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (800) 545-7558
. .--_.....~....---...._~-~..,.,.
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SHEL:L WELL MONITORING DAT~SHEET
BTS#:
\
Site:
Sampler:
Total Well Depth (TD): Vt5"ll
Well Diameter: 2 3 (Ð' 6 8
Depth to Watèr (DTW): \2.1,'11
Depth to Freè Product: Thiclœess of Free Product (feet):
Referenced to: PV Grade D.O. Meter (ifreq'd): YSI HACH
TW with 80% Recharge [(Height of Water Column x 0.20) + DTW]:
Bailer Waterra
Disposable Bailer Peristaltic
Po . 've Air Displacement Extraction Pump
Electric ~mersible Other
Other:
Screened InterVal: \~ - \~ Ifwell is listed as a no-purge, confinn that water level is below the top
f Oth th 11 b d
Sampling Method:
Bailer
~osable Bai)~
Extraction Port
Dedicated Tubing
o screen. erwlse, ewe must e uurge .
Well Diameter Multinlier Well Dinmeter Multinlier
1" 0.04 4" 0.65
(Gals.) X = Gals. 2" 0.16 6" 1.47
I Case Volume Specified Volumes Calculated Volume 3" 0.37 Other rndius2 · 0.163
, Condo Turbidity
Time Temp (oF) pH (mS or(@) (NTUs) Gals. Removed Observations
\\'30 b5..5 b.:s '3>'10 88
Ballcr lowcred '3 I below
DTW to obtaIn sample
Did well dewater? Yes No Gallons actually evacuated:
Sampling Date: -:zj 2..tflo~ Sampling Time: H3D· Depth to Water: 12r·71
Sample I.D.: N\~- 3> Laboratory: ~Cl~, Columbia Other
Analyzed for: \[P~ @ MTBE @:J) (ºxygenãfe~(5) OtherC: ~ 5()\ l\
. ,..::::f? (/~
EB I.D. (if applicable): @ Duplicate I.D. (if applicable):
Tim.
Analyzed for: TPH-G BTEX MTBE TPH-D Oxygenates (5) Other:
.
D.O. (ifreq'd): Pre-purge: mg/L Post-purge: mg/L
O.R.P. (ifreq'd): Pre-purge: mV Post-purge: mV
Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (800) 545-7558
.'-_"'_. n~~' ..
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SHELL WELL MONITORINGDATÁ-iSHEET
\
Date:
Total Wen Depth (TD): \
Well Diameter: 2 3 @) '. 6 8
. Depth to Water (DTW): l2J!lß
Depth to Free Product: Thic1mess of Free Product (feet): '
Referenced to: Grade ' D.O. Meter (ifreq'd): YSI fIACH
DTW with 80% Recharge [(Height of Water Column x 0.20) + DTW]:
Bailer
í~osable Bailer
Positì ir Displacement
E1ectric Sub ¡ble
Waterra
Peristaltic
Extraction Pump
Other
Sampling Method: Bailer
~posa:le B~
xuac on Po
Dedicated Tubing
Screened lnterval\2D' .. \45'
Otl1er:
If well is listed as a no-purge, confinn tl1at water level is below the top
of screen. Otherwise, the well must be ur ed.
Well Diametcr MuHì )]jer Well Diameter
I" 0.04 4"
2" 0.16
3" 0.37
(Gals.) X
] Case VoIwm: S ecified Volumes
Gals.
Calculated Volume
6"
Multiplier
0.65
\.47
radius' * O. ] 63
Other
Time
Condo
pH (mS or~
of' l~o 3\
Turbidity
(N1Us)
t~
Gals. Removed
ObsefýatioDs
Bullcr lowcred · below
DTW to obtalo sample
Did well dewater?
Yes
No
Gallons actually evacuated:
Sampling Date:-
: Sample LD.:
Sampling Time: to
Laboratory:
Columbia Other
Analyzed for: ~<!TEJY MTBE
EB I.D. (if applicable): @
Analyzed for: TPH-G BTEX MTBE
D.O. (ifreq'd): Pre-purge:
O.R.P. (ifreq'd): Pre-purge:
IZl . yß
Time Duplicate I.D. (ifapplicable):
TPH-D Oxygenates (5) Other:
mg/L Post-purge: mg/L
mV Post-purge: mV
Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (800) 545-7558
......._.. ...·..,·_·v...
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. ÁPPENDIX B
FIELD PROCEDURES
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BLAINE 1680 ROGERS AVENUE
TECH SERVICES,,, SANJOSE,CA95112-1105
(408) 573-7771 FAX
(408) 573-0555 PHONE
CONTRACTOR'S LICENSE #746684
www.blainetech.com
April 1, 2004
Tony Pa1agyi
Shell Oil Products US
P.O. Box 7869
Burbank, CA 91510-7869
First Quarter 2004 Groundwater Monitoring at
Shell-branded Service Station
5321 Stockdale Highway
Bakersfield, CA
Monitoring performed on February 24, 2004
Groundwater Monitoring Report 040224-CD-l
This report covers the routine monitoring of groundwater wells at this Shell-branded facility. hI
accordance with standard procedures that confoIln to Regional Water Quality Control Board
requirements, routine field data collection includes depth to water, total well depth, thiclmess of
ally separate immiscible layer, water column volume, calculated purge volume (if applicable),
elapsed evacuation time (if applicable); total volume of water removed (if applicable), and
standard water parameter instnunent readings. Sample material is collected, contained, stored,
and transported to the laboratory in conformance with EP A standards. Purgewater (if applicable)
is, likewise, collected and transported to D.K. Environmental.
Basi~ field information is presented alongside analytical values excerpted ftom the laboratory
report in the cumulative table of WELL CONCENTRATIONS. The full analytical report for
the most recent samples and the field data sheets are attached to this report.
At a mÎni1mml, Blaine Tech Services, Inc. field personnel are certified on completion of a forty-
hour Ha2;ardous Materia~~ and Emergency Response traÌI1Î11g courseper ~9C:FJ:{ 191 0~12.0. Field
personnel are also enrolled in annual eight-hour refì-esher courses. '
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Blaine Tech Services, Inc. conducts sampling and documentation assigrnnents ofthis type as an
independent third party. Our activities at t1ús site consisted of objective data and sample
collection only. No interpretation of analytical results, defining ofhydrological conditions or
fonnulation of recommendations was performed.
Please call if you have any questions.
Yours truly,
Francis True
Vice President
FT /ks
attachments: Cumulative Table of WELL CONCENTRATIONS
Certified Analytical Report
Field Data Sheets
cc: Kathryn Ewing
, Delta Environmental Consultants, Inc.
911 S. Primrose Ave., Suite K
Monrovia, CA 910 16
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. .
BLAINE TECH SERVICES, INC.
METHÖDSANDPROCEDURES
FOR THE ROUTINE MONITORING OF
GROUNDWATER WELLS AT SHELL SITES
Blaine Tech Services, Inc. performs environmental sampling and documentation as an
independent third party. We specialize in groundwater monitoring assignments and intentionally
limit the scope of our services to those èentered on the generation of objective information.
To avoid conflicts of interest, 81aine Tech Services, Inc. personnel do not evaluate or interpret
the information we collect. As a state licensed contractor (C":S7 well drilling -water - 746684 )
performing strictly technical services, we do not make any professional recommendations and
perform no consulting of any kind.
SAMPLING PROCEDURES OVERVIEW,
SAFETY
All groundwater monitoring assignments performed for Shell comply wit~ Shell's safety
guidelines,29 CFR 1910.120 and S8-198 Injury arid Illness Prevention Þrogram (IIPP). All
Field Technicians receive the full 40-hour 29CFR 1910.120 OSHA SARA HAZWOPER course,
, medical clearance and on-the-job training prior to commencing any work on any Shell site.
. .
INSPECTION AND GAUGING
Wells are inspected prior to evacuation and sampling. The condition of the wellhead is checked
and noted according to a wellhead i~spection checklist.
Standard ¡measurements include the depth to water (OTW) and the total well depth (TO)
obtained with industry standard electronic water level indicators that are graduated in
inCrements of hundredths of a foot. ^
The water in each well is inspected for the presence of immiscibles. When free product is
suspected, its presence is confirmed ùsing an electronic interface probe (e.g. MMC). No
samples are collected from a well containing over two-hundredths 'of a foot (0.02') of product.
EVACUATION
, .
Dí3pth to water measurements are collected by our personnel prior to purging and minimum
.,.. þUrge volumes are calculated anew for each well based onthe height of the watercolumn and.
the diameter oHheiNell.· Expected purge volumes àrè never less than three case volumes and,
are set at no less than four case volumes in some jurisdictions.
BlÎiiiie Tech Services, Inc.
.. -. .~-
Standard
Shell Oil Products US
'", ···ì,-_.'·....._';':y .
- - ---.----."..,."
'"_'n
.' "-'-;..~.,,~. -.,
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Well purging. devices are selected on the basis of the well diameterand the total. volume to be
evacuated. 'In most cases the well will be purged using an electric submersible pump (i.e.
, GJundfos) suspended near (but not touching) the bottom of the well.
PARAMETER STABILIZATION
Well purging completion standards include minimum purge volumes, but additionally require
stabilization of spècific groundwater parCimeters prior to sample collection. Typical groundwater
parameters used to measure stability are electrical conductivity, pH, and temperature.
Instrument readings are obtained at regular intervals during the evacuation process (no less
than once per case volume).
Stabilization standards for routine quarterly monitoring of fuel sites include the following:
Temperature is considered to have stabilized when successive readings do hot fluctuate more
than +/- 1 degree Celsius. Electrical conductivity is considered stable when sucéessive
readings are within 10%. pH is considered to be stable when successive readings remain
constant or vary no more than 0.2 of a pH unit.
DEWATERED WELLS
Normal evacuation removes no less than three case volumes of water from the well. However,
less water may be removed.in cases where the well dewaters and does not immediately
recharge.
MEASURING RECHARGE:
Upon completion öf well purging, a depth to water measurement is collected and notated to
ensure that the well has recharged to within 80% of its static, pre-purge level prior to sampling.
W~lIs that do not immediately show 80% recharge or dewatered wells will be allowed a
minimum of 2 hours to re'charge prior to sampling. The water level at time of sampling will be
noted.
PURGEWATER CONTAINMENT
All non-hazardous purgewater evacuated from each groundwater monitoring well is captured
and contained in on-board storage tanks on the Sampling Vehicle and/or special Water hauling
trailers. Effluent from the decontamination of reusable apparatus (sounders, electric pUmps and
hoses etc.), consisting of groundwater combined with deionized water and non-phosphate soap,
is also captured and pumped into effluent tanks.
Non-hazardous purgewater is transported under standard Bill of Lading documentation to a, .
Blaine Tech Services, Inc. facility before being transported to a Shell approved disposalf8ëiliti
..
".' .".::.<:':;':
":'.':.,'" .
Standard Methods &: Procedures
Shell Oil Products US
Page 2. : .
Services, Inc.
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1;'>;,\L:é,.
-
." .->.'
SAMPLE COLLECTION DEVICES
All samples are collected using a stainless steel, Teflon or disposable baile~s.
SAMPLE CONTAINERS
Sample material is decanted directly from the sampling bailer into sample containers provided
by the laboratory that will analyze the samples. The transfer of sample material from the bailer
to the sample container cònforms to specifications contained in the USEPA T.E.G.D. The type
of sample container, material of construction, method of closure and fiJling requirements are'
specific to the intended analysis. Chemicals needed to preserve the sample material are
commonly placed inside the sample containers by the laboratory or glassware vendor prior to
delivery of the bottle to our personnel. The laboratory sets the humber of replicate containers.
TRIP BLANKS
Trip Blanks, if requested, are taken to the site and kept inside the sample cooler for the duration·
of the event. They are turned over to the laboratory for analysis with the samples from that site.
DUPLICATES
Duplicates, if requested, may be collected at a site. The Field Technician uses their discretion
in choosing the well at which the Duplicate is collected, typically one suspected of containing
measurable contaminants. The Duplicate sample is labeled "DUP" and the time of collectinn is
omitted from the COC, thus rendering the sample blind.
SAMPLE STORAGE
All sample containers are promptly placed in food grade ice chests for storage in the field and
transport (direct or via our facility) to the designated analytical laboratory. These ice chests'
contain quantities of restaurant grade ice as a refrigerant material. The samples are maintained
in either an ice chest or a refrigerator until relinquished into the custody of the laboratory òr
laboratory courier.
DOCUMENTATION CONVENTIONS
A label must be affixed to all sample containers. In most cases these labels are generated by
our office personnel and qre partially preprinted. Labels can also be hand written by our field
. personnel. The site is identified with the store number and site address, as is the particular
groundwater well from which the sample is drawn (e.g. MW-1, MW-2, S-1 etc.). The time and
date of sample collection along with the initials of the person who collects the sample are
handwritten onto the label. ' " '
, .. .. ...' \ . .., " ,.,.. ,. ...."..,. .
Chain of Custody records are created using client specific preprinted forms following USEPA
specifications.
Blaine Tech Services,JIl"c,:
Standard M~thods· &. P~o¿edi.lres
Shell Oil Products US ,.
'".,'(,"
..
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".. .,-
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Bill of Lading records are contemporaneous records created in the field at the site whe're the
non-hazar~ous purgewater is gènerated. Field Technicians use preprinted Bill of Lading forms.
DECaNT AMINA TION
All equipment is brought to the site in clean and serviceable condition and is cleaned after use
in each well and before subsequent use in any other well. Equipment is decontaminated before
leaving the site. '
The primary decontamination device is a commercial steam cleaner. The steam cleaner is de-
tuned to function as a hot pressure washer that is then operated with high quality deionized
water that is produced at our facility and stored onboard our sampling vehicle. Cleaning is
facilitated by the use of proprietary fixtures and devices included in the patented workstation
(U.S. Patent 5,535,775) that is incorporated in each sampling vehicle. The steam Cleaner is
used to decon 'ree!s, pumps and bailers.
Any sensitive equipment or parts (i.e. Dissolved Oxygen sensor membrane, water level
indicator, etc.) that cannot bewashed using the high pressure water, will be $prayed with a non-
. phosphate soap and deionized water solution and rinsed with deionized wateL
DISSOLVED OXYGEN READINGS
Dissolved Oxygen readings are taken pre- and/or post-purge using YSI meters (e.g. YSI Model
54, 58 or 95) or HACHfield test kits.
The YSI meters are equipped with a stirring device that enables them to collect accurate in-situ
readings. The probe/stirring devices are modified to allow downhole measurements to be taken
from wells with diameters as small as two inches. The probe and reel is decontaminated
between wells as described above. The meter is calibrated between wells as per the
instructions in the operating manual. The probe and stirrer is lowered into the water column.
. The reading is alJowed to stabilize prior to collection.
OXYIDA TON REDUCTION POTENTIAL READINGS
All readings are obtained with either Corning or Myron-L meters (e.g. Corning ORP.;.65 or a
Myron.;.L Ultrameter GP). . The meter is cleaned between wells as described above. The meter
is caHbrated at the start of each day according to the instruction manual.
FERROUS IRON MEASUREMENTS
All field measurements are collected at time of sampling with a HACH test kit.
. ....
,_ B\8:p:è. Tech Services, Inc.
. . 'Stand~d Methods & Procedures
..,-- ".- .~-.--".__._,
. ¥'.' .-
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ApPENDIX C
LABORATORY REpORT AND
CHAJN-OF-CUSTODY DOCUMENTS '
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-- .
§ -a/science
'=ªn vironmen tal
Laboratories, Inc.
March 08, 2004
Nick Sudano
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Subject: Calscience Work Order No.:
Client Reference:
04-02-1425
5321 Stockdale Highway, Bakersfield, CA
Dear Client:
Enclosed is an analytical report for the above-referenced project. The samples
included in this report were received 2/24/2004 and analyzed in accordance with
the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the
guidelines established in our Quality Assurance Program Manual, applicable standard
operating procedures, and other related documentation. The original report of any
subcontracted analysis is provided herein, and follows the standard Calscience data
package. The results in this analytical report are limited to the samples tested and any
reproduction thereof must be made in its entirety. .
If you have any questions regarding this report, please do not hesitate to contact
. the undersigned.
~
Michael J. nsostomo
Quality Assurance Manager
7440 Lincoln Way, Garden Grove, CA 92841-1427 . TEL: (714) 895-5494 · FAX: (714) 894-7501
~____ ___.....~~_._ ._h~ .~__.
-~"'-'-""----
-----~---_.._------
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L- a/science
1::,1'vironmental
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place'
Torrance, CA 90501-1511
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Analytical Report
Project: 5321 Stockdale Highway, Bakersfield, CA
Date Received:
Work Order No:
Preparation:
Method:
02/24/04
04-02-1425
N/A
EPA 120.1
Client Sample Number
Page 1 of 1
I
" .;
«....
'1)4-'02-1425-2 '62124104 "Aé¡uEiOus .' 'N/A
Matrix
MW-2:.: '
I
Parameter
Result RL
310 1,0
Result RL
310 1.0
Specific Conductance
I
.,MW-3
Parameter
I
Specific Conductance
;~~~",...
04-02-1425-4 '02l24l04,:,>Aquec:ius N/A' ·02l24Ìo,l 4D224SCD1
I
Parameter
Result
RL
1.0
Specific Conductance
270
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Lab Sample
Number
DF
Date
Collected
Date
Prepared
Date
Analyzed
O~24I04
QC Batch ID
40224SCD1
. ~ .
04-02-1425-3· ,', .(212411)4: ;: :~µ~Q~,'i J, .:~IA, ·,'02124104 ' 40224SCD1
DF
DF
RL, Reporting Limit, ,DF . Dilution Factor, Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
Qual
Units
umhos/cm
Qual
Units
umhos/cm
Qual
Units
umhos/cm
..--...--..--__~ .._.__....·_..·.4._....·___,.._ ______....____.~...__..... ._______.._w.___..._._______._.
._____._...,.~N. .__...
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(..= a/science
I::ªn vironmen tal
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received:
Work Order No:
Preparation:
Method:
02/24/04
04-02-1425
N/A
EPA 130.2
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
Client Sample Number
Lab Sample Date
Number Collected Matrix
. . O4-o2~1425-2 .. . 02124104···' .... Aqueous
.: ,
Result RL DF Qual Units
96 2 mg/L
Date Date
Prepared Analyzed QC Batch ID
N/A 02127/04 40227HARB2
Parameter
Hardness, Total
Parameter
. :O+02~1425i3 . 02!2i1(Q4; ..;.Ä9u~oµs N/A 02127/04 . .' .40227HARB2
Result RL DF Qual Units
92 2 mg/L
.. '0#24104 '."". 40227HARB2
04-02-142504- .. Aqueous . NJA 02127/04 . .
Result RL DF Qual Units
74 2 mg/L
;Ò99-o5"o70-1 ;491: .··NIA . Aqueous . . 02127/04 .40227HARB2
.. N/A
Result RL DF Qual Units
ND 2.0 mg/L
Hardness, Total
è¥W,04-
Parameter
Hardness, Total
I MëtÌî(j~t~I~Ni:'. .... "
Parameter
I Hardness, Total
I'
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1,-"",.,_.-
RL - Reporting Limit, OF - Dilution Factor, Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
,_~_",_._______,,,,,_P~w_..,_.~_.____....._,_~_______..___"_'
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1..,-,..,-
~- a/science
'= nvironmental
Laboratories, Inc.
Blaine.Tech Services, Inc
20360 Gramercy' Place
Torrance, CA 90501-1511
Analytical Report
Date Received:
Work Order No:
Preparation:
Method:
02/24/04
04-02-1425
N/A
EPA 150.1
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
Client Sample Number
Lab Sample
Number
Date Date
Prepared Analyzed QC Batch 10
Date
Collected
Matrix
"·s
. .. ,"'~.
:-.,...:.... ·:,.fi.."
~fA.;.~>~24f04. 40224PHD1
)0i:ö2~142~~; , ,O~4IÒ4. ,~uëó\J~
.MV«:;~ }.<¡,,;
,";,.'
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Parameter
Result
Qual
Units
DF
RL
0.01
pH units
pH
6.75
Q~~#~~425-:t;';':;0;1Ï2'i2410..A(¡uèous ·'··';;Nlli.:'·' 02/24104 ··.40224PHD1
Parameter
Qual
Units
Result
B1
DF
pH
6.85
pH units
0.01
.',: ':':. . :·:····:.04:(j2·~1425~: ,", .:':.Q~~04 :·.....;.>~U80~S..~..
::. ::. ).~..,. ,'.
Nlllki:,' ·,·02124104
40224PHD1
Parameter
Result
RL
0.01
pH units
OF
Qual
Units
pH
6.89
RL - Reporting Limit, OF - Dilution Factor, Qual -Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
.~....". .n.' .. ___..
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~ a/science
I::.ªn vironmen tal
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance. CA 90501-1511
Analytical Report
Date Received: .
Work Order No:
Preparation:
Method:
02/24/04
04-02-1425
N/A
EPA 160.1
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
Lab Sample
Number
Date Date
Prepared Analyzed QC Batch ID
NIA . . 02125104 4022STDSD1
Date
Collected
Matrix
. 0f02~1425-2 '. . 02124104 ..' ',' Attu~åLiS
Parameter Result RL DF Qual Units
Solids, Total Dissolved 160 1.0 mglL
"",
0+02~1 2~' ·,··02124104 Aqueous NIA ..,,' 02125104 .. . 4O~,5TDSD1
Parameter Result RL DF Qual Units
Solids, Total Dissolved 200 1.0 mg/L
I~W-4;::" ".': ;;':Oiti~04 '. I
.,,, :.D4.,oH4~ 02124104", ··~AqLieOus. . . ·.·",:·NiA"-. 40225TDSD1
.,....".
Parameter Result RL DF Qual Units
Solids, Total Dissolved 180 1.0 mg/L
RL - Reporting Limit, DF . Dilution Factor, Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
1.- _.._-~---------,-----
_.._._._.~.___ _ _ri_~_'
..---.,,-.
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~ a/science
I:~nvironmenta/
Laboratories, Inc.
/
Analytical Report
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project: 5321 Stockdale Highway, Bakersfield, CA
Date Received:
Work Order No:
Preparation:
Method:
02/24/04
04-02-1425
N/A
EPA 300.0
Client Sample Number
Page 1 of 1
Lab Sample
Number
()+O~:~~25-;1,
Parameter
Nitrate (as N)
Result
0.61
......,...
..
RL DF Qual Units
0.10 1 mg/L
Date
Collected
Date
Prepared
Matrix
02l241Ó4';~';~µ~U!:/ " "N1À
. . '" .
,,;.~,i~gf1,~,~2~ '~~~04Aqueous' ,NiA'
, ;"
Date
Analyzed QC Batch ID
02124104 . 040224L01
RL
1
0.1
DF Qual Units
1 E mg/L
1 mg/L
Parameter
Sulfate
Result
27
02124104' 040224L01
RL OF Qual Units
1 1 E mg/L
,02124104 040224L01
RL
10
DF Qual Units
10 D mg/l
Parameter
Chloride
Nitrate (as N)
Result
97
1.3
'0+02~1425-2
RL
10
DF Qual Units
10 0 mg/l
02l241Ô4 ; Ag~eous' NiA
Parameter
Sulfate
Result
23
, ,
02124/04" 040224L01
Rl DF Qual Units
1 1 E mg/l
02124104 Ó40224L01'
Rl DF Qual Units
10 10 D mg/l
02124104 040224L01
RL OF Qual Units
1 1 E mg/l
I"'W-3'
. ,";,
MW4
Parameter
Chloride
Result
18
. ,
;¡:(t¡4~2""42~-3. ,"02i24104:AqÜÍlOLU¡.. '.N/A '
Rl
1
0.1
DF Qual Units
1 E mg/l
1 mg/l
Parameter
Sulfate
Result
26
~2~14254 " 02Ì24i04 ,l\queC)us N/A 02124104 " 040224L01
RL DF Qual Units Parameter Result Rl OF Qual Units
10 10 0 mg/l Sulfate 21 10 10 D mg/l
099~5~118-2;O98 NJA Aqueous NJA 02/24104 040224L01
RL DF Qual Units Parameter Result RL DF Qual Units
1,0 1 mg/L Sulfate ND 1.0 1 mg/L
0,10 1 mg/L
DF - Dilution Factor
'. ',. . . . . .
. ().4..,()2-;.1~~~h 02124104 . " AquÍlÖus'N/À "
RL
10
DF Qual Units
10 D mg/L
MW..2',
~2~14254
RL
1
0.10
DF Qual Units
1 E mg/L
1 mg/L
Parameter
Sulfate
Result
23
Parameter
Chloride
Result
20
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I
1",.._
MW-3.
. : ·..·,'.:t<::'{:;'...¿~.·:·:··· ,"
Qual - Qualifiers
02124104
. ... . .
. Aqueous' ,; "N/A,
RL· Reporting Limit
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 ·
FAX: (714) 894-7501
Parameter
Sulfate
Result
23
Parameter
Chloride
Nitrate (as N)
Result
110
1,2
.._------_._..~---- ..._._----,--~------._----~._~.._--_. -------..--------.-.-' .---..--,'. -.--.. -_.
'. ",)"
Parameter
Chloride
Result
20
Parameter
Chloride
Nitrate (as N)
Result
69
0.75
Method Blank
Parameter
Chloride
Nitrate (as N)
Result
ND
NO
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1
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1
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~ a/science
I:: nvironmental
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received:
Work Order No:
Preparation:
Method:
02/24/04
04-02-1425
N/A
EPA 351.3
Project: 5321, Stockdale Highway, Bakersfield, CA
Page 1 of 1
Lab Sample
Number
Date
Matrix Prepared
. AqUeOl.ls>; 'N/A
Date
Analyzed QC Batch ID
03/01/04'. 40301TKNB1
Date
Collected
.. .~2"14~~"2,.,:;·()~2jì()4
Parameter Result RL DF Qual Units
Total Kjeldahl Nitrogen ND 0,50 mg/L
'\;~2~1425,3 . ·,·..·02l241Ö4 AqU8Qµ5 N/A ()3/01/04 40301TKNB1
Parameter Result RL DF Qual Units
Total Kjeldahl Nitrogen ND 0,50 mglL
. ,Q4.;OM425-4,02l~~ ;:'::~~ûs;N1Â:
03101104 40301TKNB1
Parameter Result RL DF Qual Units
Total Kjeldahl Nitrogen ND 0.50 mglL
. Mê~9d BI~,,~~~, . '~76-1'2f15 . ... . . . ".~ . N/A . 40301TKNB1
NrA " AqùeouS.·· 03/01/04
Parameter Result RL DF Qual Units
Total Kjeldahl Nitrogen ND 0.50 mglL
RL . Reporting Limit. OF . Dilution Factor, Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 . TEL: (714) 895-5494 . FAX: (714) 894-7501
. ....-.......--.-----.- .._~._.__._-_.._--_..- ...-. ..---.-.------.-,.-..--.--.--....-----.. ~ -_._.__.__.._~_._----~ .__._---~.__..-...- - ....-........ "--"--'"
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1,_..,___,
~ - al§cience
I:~nvironmental
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received:
Work Order No:
Preparation:
Method:
02/24/04
04-02-1425
N/A
SM 2320B
Project: 5321 Stockdale Highway, Bakersfield. CA
Page 1 of 1
Lab Sample
Number
Date Date
Prepared Analyzed QC Batch 10
Date
Collected
Matrix
, ,
:<~~142~2 02lZ4I04;:~IJ~tis: .N/A ":03l03l0440303ALKD1
Parameter
Result \
Units
RL
OF
Qual
Hydroxide (as CaC03)
NO
1.0
mglL
. :, .: ~.. '
Aq~~~ø.:/
·03lG4/Ø4 :40303A1.KD1
'~¥~'142~',· ,'02124104'
NfA
Parameter
RL
Units
Result
OF
Qual
Hydroxide (as CaC03)
NO
1.0 mg/L
MW,4 '" :::'.~<:':/:
t;~;,~2-1425-4,<,';·Ô~~:'!(:ACj~~'·." NfA
'þ3(Q3I04;. '40303ALKD1
Parameter
Result
RL
1.0
OF
Ql@!
Units
mg/L
Hydroxide (as CaC03)
NO
...
Rl - Reportin9 Limit. DF - Dilution Factor, Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
_..-,----.- --,_._--
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La/science
I!:. nvironmental
. Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received:
Work Order No:
Preparation:
Method:
02/24/04
04-02-1425
N/A
8M 2320B
Project: 5321 Stockdale Highway, Bakersfield. CA
Page 1 of 1/
Client Sample Number
Lab Sample
Number
04':(12:.:i42$-2 .
Date
Prepared
QC Batch ID
40303AlKD1
Date
Analyzed
.... 0310~/04
Date
Collected
Matrix
"".' :. ". ...,':..;".....,-.
·~·~W~~/:~·~)?? .:~;.~)';".~ .~.;.~.,.
02l2~04.;,;~Ç Li~9,~~/ . .N/A
Parameter
Result
RL
1.0
DF
Qual
Units
Carbonate (as CaC03)
ND
mglL
. MW~.::g~)r:J;)i'i: "
:;.;L'';A:è,:;:;,,;,,¡-;,;;;:<::;,,-b+o2.1~~!·''"d2i2..y04 .. ÄqLiGOUS-., . ··N/A .
:o3/o~/04' '. 40303AlKD1'
Parameter
Result
Units
RL
OF
Qual
Carbonate (as CaC03)
ND
1.0 mglL
. ," . .- ", . .... .
. '()4.:.(J2~142~~;;,..9,2124i04 :1uiûe9µ~, /';'OJUA;03l(l3lM '40303ALKD1
Parameter
Result
DF
QYID
Units
RL
Carbonate (as CaC03)
ND
1.0
mglL
RL - Reporting Limit, DF - Dilution Factor, Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
._.___,,_..__ h.__.
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~= a/science
I:.Environmental
L aboratories!I Inc.
Blaine Tech Services, Inc'
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received:
Work Order No:
Preparation:
Method:
02/24/04
04-02-1425
N/A
SM 2320B
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
Client Sample Number
MW·2
Lab Sample
Number
Date
Prepared
QC Batch ID
40303ALKD1
Date
Analyzed
O.3/03Ì04
Date
Collected
Matrix
Aijµ~I,IS.
;toIl",; .
. "'04-02~1425-2g:; '02124104 '.
Parameter
Result
RL
5,0
Qual
Units
DF
Bicarbonate (as CaC03)
100
mg/L
MW,.3. . .
;. 0.4~-'~~~'" '02l24JI>4;Aqu6~US<':,tN/A .'
03103/04.· '. 4()303~KD1
. .
Parameter
Qual
Units
Result
RL
DF
Bicarbonate (as CaC03)
mg/L
94
1.0
MW-4
o+P~d1~~4. ,'. J>2I24i04>ÅqlJttQ~ .... '.' , ·NIÄ. '. . . 03103104 . . o10303ALKD1 .'
......,..,:.;.,...,
,"" :
Parameter
Qual
Units
Result
RL
1.0
DF
Bicarbonate (as CaC03)
mg/L
82
RL - Reporting Limit, DF . Dilution Factor, Qual· Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
1.........."...,---------.,'-,-----...--'-----.--,..,,---.-.. .---..--..--,-,-----.----.-..-,.........." ...,.. ----.
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~ a/science
I:ªn vironmen tal
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance,'CA 90501-1511
Analytical Report
Date Received:
Work Order No:
Preparation:
Method:
02/24/04
04-02-1425
N/A
SM 2320B
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
Client Sample Number
~Vi;.2
Lab Sample
Number
Date Date
Prepared Analyzed QC Batch ID
N/A. .' 03103/04 .' 40303ALKD1
Date
Collected
Matrix
. .04"92.1"25~2:H';;~,:o2t24104 ·.::;AqueÔU5 .
Parameter
Result
Units
Qual
RL
5.0
DF
Alkalinity, Total (as CaC03)
100
mg/L
MW.;J.
0.4042.-1425-3 . 0,2/2~D4' AqUêÔUS.· ,'. N/A.· . . ,OJ¡03I~.· 40303ALKD1
Parameter
Result
RL
DF
Qual
Units
Alkalinity, Total (as CaC03)
94
1.0 mg/L
. . ,,~
... .
.'·M,W4:··.::···
... .,...
03103/04' ,40303ALKD1
:., :~2~142S-4;\:/>:ô2ì241Q4;AqueoUS ',:...:' ..:.~/A
Parameter
Result
RL
1.0
DF
Qual
Units
Alkalinity, Total (as CaC03)
82
mglL
RL - Reporting Limit, DF . Dilution Factor
Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
-.-.-.....-..... .--."~._,.
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L- a/science
I:jlvironmental
Laboratories, Inc.
Analytical Report
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
02124/04
04-02-1425
EPA 3005A Filt.
EPA 601 OB
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 2
Client Sample Number
Lab Sample
Number
Date
Collected
QC Batch ID
Date Date
Prepared Analyzed
Matrix
!J4:02~~~2$.1·'Q~:4íþ4· .·Aquåous '02125104/ :,02126104
040225L05F
Parameter
Lead
Result
ND
RL OF Qual Units
0,0100 1 mg/L
'."'~ .~.
0<HI2~142S::f . .'~~#.Ö'H"::~~eO~!i"~21~~iJ4:> '02l2W~040225L05F
'MW~2',···· .
':,:",',...,,"
Parameter
Lead
Result
NO
RL DF Qual Units
0.0100 1 mg/L
I MW"3'·
, ;~J.t;::.~:.\.~:><.'..
04'( 2·142S~3
02,l24í64 ):AQueous-' ':02l2Sl04 'i)2126iÖ4 ,. 040225LOSF
Parameter
Lead
Result
ND
RL DF Qual Units
0.0100 1 mg/L
04:02~14254;{ ... ~~~Q¡t,"<;~:AQijèóuš '>'Ò2Î2S/04: ·,/'02126104 040225L05F
Parameter
Lead
Rl OF Qual Units
0.0100 1 mg/l
Result
ND
:M~~~od Bla.,k .
040225L05F
Ac¡Ù8clUS .' :. ..Ò2I25/04,;:···.:02l25!04
..: O~7'( 1 ;.o03~~¡~ ... ./~~Å;
Parameter
lead
Magnesium
RL
0.0100
0.100
Parameter
Iron
Manganese
Result Rl
ND 0.100
ND 0.00500
OF Qual Units
1 mg/L
1 mg/l
OF Qual Units
1 mg/L
1 mglL
Result
ND
ND
Rl- Reporting Limit, DF - Dilution Factor, Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
.n . __.._.....u.___
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~ a/science
I:: nvironmenta/
Laboratories, Inc.
Analytical Report
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
02/24/04 .
04-02-1425
EPA 3010A Total
EPA 6010B
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 2 of 2
Client Sample .Number
Lab Sample Date
.Number Collected Matrix
... ..
()4.:( 2~1425-2 '. 02124104 ' . Aquéot.is
Result RL DF Qual Units Parameter
.ND 0.00500 mg/L Calcium
2.32 0.50 nig/L Iron
29.8 0.5 mg/L Magnesium
RL DF Qual Units
0,1 1 mg/L
0.100 1 mg/L
0.10 1 mg/L
02126104' . ,.040225L6
RL DF ili@! Units
0.1 1 mg/L
0.100 1 mg/L
0.10 1 mg/L
Date Date
Prepared Analyzed QC Batch ID
02125/04) .' .02126/04 '. 040225L6
Parameter
Manganese
Potassium
Sodium
Result
29.5
0.129
5.76
I MW-3·
", . .' .
" Ó2{~4lO4 .', Aque()u$ . '
',. .:
><: /'()4io2-1425-3
02125/04
, .
Parameter
Manganese
Potassium
Sodium
Result
.ND
2.33
29,8
RL DF
0.00500
0.50
0,5
Qual Units
mg/L
mg/L
mg/L
Parameter
Calcium
Iron
Magnesium
Result
28.0
0,109
5.66
i~~·t'
Parameter
Manganese
Potassium
Sodium
,. ~2"142s-4 . . 02124/04' . ,Aqueous· 02l25ii)4" ;' 02l2~~' : 040225L6
\'<":' - - '. . .,":::::"
Result RL DF Qual Units Parameter Result RL DF Qual Units
0,00702 0,00500 mg/L Calcium 22.1 0.1 ,1 mg/L
2,16 0.50 mg/L Iron 0.215 0.100 1 mg/L
28.3 0.5 mg/L Magnesium 4,43 0.10 1 mg/L
097'()1'()031,63~,N!~ ···~u~ús .02125104< ",'02l2,13i04.' 040225L6
Parameter
Lead
Calcium
Iron
Magnesium
Result RL DF ili@! Units Parameter Result RL DF Qual Units
.NO 0.0100 1 mg/L Manganese .ND 0.00500 mg/L
.NO 0.100 1 mg/L Potassium .ND 0.500 mg/L
ND 0.100 1 mg/L Sodium ND 0.500 mg/L
ND 0.100 1 mg/L
RL - Reporting Umit, DF - Dilution Factor" Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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----_._----~~---. -----.-.
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La/science
I:§nv;ronmental
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received:
Work Order No:
Preparation:
Method:
02/24/04
04-02-1425
EPA 5030B
DHS LUFT
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 2
Client Sample Number
'\MVi-1
Lab Sample
Number
Date
Collected
Date Date
Prepared Analyzed QC Batch ID
NiÂY'''','L-02l26104 '.... '040226801
Matrix
O4.oi.142S;;1;' '02l24J04.~~~ous .
Parameter
Result
DF
Qual
Units
RL
50
ug/L
TPH as Gasoline
ND
Surrooates:
REC(%}
1,4-Bromofluorobenzene
92
Control
Limits
49-133
Qual
. .
.. . . ......
Q+02-1425-2 . 02124104 . Aqueoüii
NfÅ(:(':'02l26Îò4 040226801
Parameter Result RL DF Qual Units
TPH as Gasoline ND 50 ug/L
Surrooates: REC(%} Control' Qual
Limits
1,4-Bromofluorobenzene 91 49-133
MW~3 .. ..
..~2~1~S-3·> tI~4I94 Aqueous' NfA ' 02126/04 040226801
Parameter Result RL DF Qual Units
TPH as Gasoline ND 50 ug/L
Surrooates: REC(%} Control ~
Limits
1,4-Bromofluorobenzene 71 49-133
.Mw~~L<'{;·i.. ~2-1425-4%::::I)~:4fó4·· Aquei?us . . NfA .; Ô~6lØ4 040226801
Parameter Result RL DF Qual Units
TPH as Gasoline ND 50 ug/L
SurrOQates: REC(%) Control Qual
Limits
1,4-Bromofluorobenzene 95 49-133
RL - Reporting Limit, DF - Dilution' Factor, Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I ."-' ,"...'..'-.....---...-----,--,.-------------.----..--.--
-......-, -.-........---.-.
I
I
e-- a/science
I:=nvironmental
L aboratories7 Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
I
I
I
Project: 5321 Stockdale Highway, Bakersfield, CA
Date Received:
Work Order No:
Preparation:
Method:
. 02/24/04
04-02-1425
EPA '5030B
DHS LUFT
I
Client Sample Number
MethodS'M,,~;,· ;.'
Lab Sample
Number
Page 2 of 2
," ,·f'·'
Date
Collected
Matrix
. . .. ,.
};;~>Ò,9.8-o3'-OD6~923 <N/A . . ,'Aqueous
Date Date
Prepared Analyzed
NJA<:., 92/26/04
Result RL DF Qual Units
ND 50 ug/L
REC(%) Control Qual
Limits
92 49-133
I
I:
Parameter
TPH as Gasoline
Surroqates:
1,4-Bromofluorobenzene
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RL - Reportin9 Limit. DF - Dilution Factor, Qual - Qualifiers
QC Batch 10
040226S01
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
~
,
.. .._-._-_._-~----
.-------------.-..
~_._~... -..",'. - ....-.-.
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~ alscience
'=/,Vironmental
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received:
Work Order No:
Preparation:
Method:
02/24/04
04-02-1425
EPA 3510C
DHS LUFT
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 2
Client Sample Number
Lab Sample
Number
Date Date
Prepared Analyzed QC Batch ID
02125104 ;Ô~6t04'o40225807
Date
Collected
Matrix
. -'AquéOus
..
~2-1425-;1' ,;" '. 02124104
"
Parameter
Result
Qual
Units
RL
1000
DF
TPH as Diesel
ND
uglL
SUIToaates:
REC(%)
Decachlorobiphenyl
80
Control
limits
51-141
Qual
,'MW-2"
..
'04.:02-1425'-202124104" Aqueous ,02125104
02tt1f04' ',' 040225807
Parameter
Result
Qual
Units
RL
1000
DF
TPH as Diesel
ND
uglL
SUITOQates:
REC(%)
Oecachlorobiphenyl
85
Control
limits
51-141
Qual
, '.
02124104
..
. " " ., ~:
Aqueous
, 0~~q4;;, 02126104 . 040225807
04.:02~1425-3
-.' .
: .." ,"," ,..
Parameter
Result RL DF Qual Units
NO 1000 uglL
REC(%) Control Qual
limits
81 51-141
04.:02-1425-4,' '02l2!'1104 .' Aqueous " .;. 0'2125/04, ,02i26104 040225807
Result RL OF Qual Units
NO ·1000 uglL
REC(%) Control Qual
limits
81 51-141
TPH as Diesel
- SUIToaates:
Decachlorobiphenyl
Parameter
TPH as Diesel
SurrOQates:
Decachlorobiphenyl
RL - Reporting Limit, DF - Dilution Factor, Qual - QualifIers
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
,_. M _.__.__~______..___.h.._.._.__.___
_ _.____~___._._.V_M__.__M.______.._..._..._~____ ______....._____.__
I
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I
I
c.; a/science
I:: nvironmental
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received:
Work Order No:
Preparation:
Method:
I
Project: 5321 Stockdale Highway, Bakersfield, CA
02/24/04
04-02-1425
EPA 3510C
DHS LUFT
I
Lab Sample Date
Number Collected
Matrix
Page 2 of 2
Client Sample Number
:, ..' "; ^. ~
, MethOd ~Iår\k "..
09s:.o3;'()03-2,01J.~/A::'::"l\qü~~~~:;,02l25104:
Date
Prepared
..
I
Parameter
Result RL DF Qual Units
ND 1000 ug/L
REC(%) Control Q!g¡
Limits
113 51-141
TPH as Diesel
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Surroaates:
Decachlorobiphenyl
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RL - Reporting Limit. OF - Dilution Factor. Qual - Qualifiers
Date
Analyzed' QC Batch ID
02l2~04 040225807
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
--------- - ------ ------- --- - ------------
I
I ~- a/science
I:, nvironmental
I ' Laboratories, Inc. Analytical Report
Blaine Tech Services, Inc Date Received: 02124/04
I 20360 Gramercy Placè Work Order No: 04-02-1425
Torrance, CA 90501-1511 Preparation: EPA 5030B
Method: EPA 8260B
I Project: 5321 Stockdale Highway, Bakersfield, CA Page 1 of 5
I Lab Sample Oate Oate Oate
Client Sample Number Number Collected Matrix Prepared Analyzed QC Batch 10
MW~1;;>~:", ,,' 04-02-,1425-1 02.l24IM H , Aqueous " ' "'A ' , 02l26ì04.
" <,':.Nl, ,'.' 040225L03
I Parameter Result RL OF Qual Units Parameter Result RL OF Qual Units
Acetone NO 10 1 ug/L 1,1-0ichloropropene NO 1.0 1 ug/L
Benzene NO 0,50 1 ug/L c-1,3-0ichloropropene NO 0.50 1 ug/L
Bromobenzene NO 1,0 1 ug/L t-1,3-0ichloropropene NO 0.50 1 ug/L
I Bromochloromethane NO 1.0 1 ug/L Ethylbenzene NO 1,0 1 ug/L
Bromodichloromethane NO 1.0 1 uglL 2-Hexanone NO 10 1 ug/L
Bromoform NO 1.0 1 uglL Isopropylbenzene NO 1.0 1 ug/L
Bromomethane NO 10 1 ug/L p-Isopropyltoluene NO 1.0 1 ug/L
2-Butanone NO 10 1 ug/L Methylene Chloride NO 10 1 ug/L
I n·Butylbenzene NO 1.0 1 ug/L 4·Methyl-2-Pentanone ND 10 1 ug/L
sec-Butylbenzene ND 1.0 1 ug/L Naphthalene ND 10 1 ug/L
tert-Butylbenzene ND 1.0 1 ug/L n-Propylbenzene ND 1.0 1 ug/L
Carbon Disulfide NO 10 1 ug/L Styrene ND 1.0 1 ug/L
I Carbon Tetrachloride NO 0.50 1 ug/L 1,1,1,2-Tetrachloroethane ND 1.0 1 ug/L
Chlorobenzene NO 1.0 1 uglL 1,1,2,2-Tetrachloroethane NO 1.0 1 ug/L
Chloroethane ND 1.0 1 ug/L T etrachloroethene ND 1,0 1 ug/L
Chloroform NO 1.0 1 ug/L Toluene ND 1,0 1 ug/L
I Chloromethane ND 10 1 ug/L 1,2,3-Trichlorobenzene NO 1,0 1 ug/L
2-Chlorotoluene ND 1.0 1 ug/L 1,2.4"Trichlorobenzene ND 1.0 1 ug/L
4-Chlorotoluene NO 1.0 1 ug/L 1,1,1-Trichloroethane NO 1.0 1 ug/L
Oibromochloromethane NO 1.0 '1 ug/L 1,1,2- Trichloroethane NO 1.0 1 ug/L
1,2-0ibromo-3-Chloropropane NO 5.0 1 ugll Trichloroethene NO 1.0 1 uglL
I 1,2-Dibromoethane ND 1,0 1 ug/L T richlorofluoromethane NO 10 1 ug/L
Oibromomethane NO 1.0 1 ug/L 1,2,3- Trichloropropane NO 5.0 1 ug/L
1,2-0ichlorobenzene NO 1.0 1 ug/L 1,2,4-Trimethylbenzene NO 1.0 1 ug/L
1,3-0ichlorobenzene NO 1.0 1 ug/L 1 ,3,S- Trimethylbenzene NO 1.0 1 ug/L
I 1,4-0ichlorobenzene NO 1.0 1 ug/L Vinyl Acetate NO 10 1 ug/L
Oichlorodifluoromethane NO 1.0 1 ug/L Vinyl Chloride NO 0.50 1 ug/L
1,1-0ichloroethane NO 1.0 1 uglL p/m-Xylene .. NO 1.0 1 ug/L
1.2-0ichloroethane NO 0.50 1 ug/L o-Xylene NO 1.0 1 ug/L
1,1·0ichloroethene NO 1.0 1 ug/L Methyl-t-Butyl Ether (MTBE) NO 1.0 1 ug/L
I c-1,2-0ichloroethene NO 1.0 1 ug/L Tert-Butyl Alcohol (TBA) NO 10 1 uglL
t-1,2-0ichloroethene NO 1.0 1 ug/L' Diisopropyl Ether (OIPE) NO 2.0 1 ug/L
1,2-0lchloropropane NO 1.0 1 ug/L Ethyl-t-Butyl Ether (ETBE) NO 2.0 1 ug/L
1,3-0ichloropropane NO 1.0 1 ug/L Tert-Amyl-Methyl Ether (TAME) NO 2.0 1 uglL
I 2,2-0ichloropropane NO 1.0 1 ug/L Ethanol NO 100 1 ug/L
SurroQates: REC(%) Control Qual Surroaates: REC(%) Control Qual
Limits
Oibromofiuoromethane 96 57-157 Toluene-dB 96 75-123
I 1,4-Bromofluorobenzene 93 76-113
I
I RL - Reporting Limit DF . Dilution Factor Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 TEL: (714) 895-5494 FAX: (714) 894-7501
.
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0
c..... -a/science
I:;~pvironmental Analytical Report
Laboratories, Inc.
Blaine Tech Services, Inc Date Received: 02/24/04
20360 Gramercy Place Work Order No: 04-02-1425
Torrance, CA 90501-1511 Preparation: EPA 5030B
Method: EPA 8260B
Project: 5321 Stockdale Highway, Bakersfield, CA Page 2 of 5
Lab Sample Date Date Date
Client Sample Number Number Collected Matrix Prepared Analyzed QC Batch ID
::NI~~~·:,,\)·::lt,: " .'::':.,!>4' )2-1425-~, ...." :>~~04 " ~. 02126104
AquåQJ š. . N/A ,040225L03 ,
Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units
Acetone ND 10 1 uglL 1,1-Dichloropropene ND 1.0 1 ug/L
Benzene ND 0.50 1 ugfL c-1,3-Dichloropropene ND 0.50 1 ug/L
Bromobenzene ND 1.0 1 ug/L t-1,3-Dichloropropene ND 0.50 1 ug/L
Bromochloromethane ND 1.0 1 ug/L Ethylbenzene NO 1.0 1 ug/L
Bromodichloromethane ND 1,0 1 ugfL 2-Hexanone ND 10 1 ug/L
Bromoform ND 1.0 1 uglL Isopropylbenzene ND 1.0 1 ug/L
Bromomethane NO 10 1 uglL p-Isopropyltoluene ND 1.0 1 ug/L
2-Butanone ND 10 1 uglL Methylene Chloride ND 10 1 ug/L
n-Butylbenzene ND 1.0 1 ugfL 4-Methyl-2-Pentanone ND 10 1 ug/L
sec-Butylbenzene ND 1.0 1 ugfL Naphthalene NO 10 1 ugfL
tert-Butylbenzene ND 1,0 1 ugfL n-Propylbenzene ND 1.0 1 ugfL
Carbon Disulfide ND 10 1 ug/L Styrene ND 1.0 1 ug/L
Carbon Tetrachloride ND 0.50 1 ugfL 1,1,1,2-Tetrachloroethane ND 1.0 1 ugfL
Chlorobenzene ND 1.0 1 ug/L 1,1,2,2- Tetrachloroethane NO 1.0 1 ug/L
Chloroethane ND 1.0 1 ugfL T etrachloroethene ND 1.0 1 ugfL
Chloroform ND 1.0 1 ugfL Toluene NO 1.0 1 ugfL
Chloromethane ND 10 1 ug/L 1,2,3- T richlorobenzene ND 1.0 1 ug/L
2-Chlorotoluene NO 1.0 1 uglL 1,2,4- Trichlorobenzene ND 1.0 1 ug/L
4-Chlorotoluene ND 1.0 1 ug/L 1,1,1- Trichloroethane ND 1.0 1 ug/L
Dibromochloromethane ND 1.0 1 ugfL 1,1,2-Trichloroethane ND 1.0 1 ugfL
1,2-Dibromo-3-Chloropropane NO 5.0 1 uglL Trichloroethene ND 1.0 1 ugfL
1,2-Dibromoethane NO 1.0 1 uglL T richlorofluoromethane NO 10 1 ug/L
Oibromomethane NO 1.0 1 ug/L 1,2,3- Trichloropropane ND 5.0 1 ugfL
1,2-DiclÌlorobenzene ND 1.0 1 ugfL 1,2,4- Trimethylbenzene NO 1,0 1 ugfL
1,3·Dichlorobenzene ND 1.0 1 ugfL 1,3,5- Trimethylbenzene ND 1.0 1 ugfL
1,4-Dichlorobenzene ND 1.0 1 ug/L Vinyl Acetate ND 10 1 ugfL
Dichlorodifluoromethane ND 1.0 1 ug/L Vinyl Chloride ND 0,50 1 ug/L
1,1-Dichloroethane ND 1.0 1 ugfL pfm-Xylene ND 1.0 1 ugfL
1,2-0ichloroethane· ND 0,50 1 ugfL o-Xylene ND 1.0 1 ugfL
1,1-Dichloroethene ND 1.0 1 ugfL Methyl+Butyl Ether (MTBE) ND 1.0 1 ugfL
c·1,2-Dichloroethene NO 1.0 1 ugfL Tert-Butyl Alcohol (TBA) NO 10 1 ugfL
t-1,2-Dichloroethene ND 1.0 1 ugfL Diisopropyl Ether (DIPE) ND 2.0 1 ugfL
1,2-0ichloropropane ND 1.0 1 ugfL Eihyl-t-Sutyl Ether (ETSE) ND 2.0 1 ugfL
1,3·0ichloropropane ND 1.0 1 uglL Tert-Amyl-Methyl Ether (TAM~) ND 2,0 1 ugfL
2,2-Dich loropropane ND 1.0 1 ugfL Ethanol ND 100 1 ugfL
SurroGates: RECI%) Control Qual Surrooates: RECI%) Control Qual
Limits
Oibromofluoromethane 90 57-157 Toluene-d8 96 75-123
1,4-Bromofluorobenzene 94 76-113
RL - Reporting Limil ,
OF - Dilution Factor, Qual - Qualifiers
· TEL: (714) 895-5494 ·
FAX: (714) 894-7501
7440 Lincoln Way, Garden Grove, CA 92841-1427
..-. - .--- ,,--.----....------.- _..._-~_._------
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I
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I/:;¡1vironmental
Laboratories, Inc.
. Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
I
I
I
Project: 5321 Stockdale Highway, Bakersfield, CA
I
Client Sample Number
':,'MW43:·(·;· ;','
I
Parameter
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Oibromochloromethane
1,2-0ibromo-3-Chloropropane
1,2-0ibromoethane
Oibromomethane
1,2-0ichlorobenzene
1,3-0ichlorobenzene
1,4-0ichlorobenzene
Oichlorodifluoromethane
1,1-0ichloroethane
1,2-0ichloroethane
1,1-0ichloroethene
c-1,2-0ichloroethene
t-1,2-0ichloroethene
1,2·0ichloropropane
1,3·0ichloropropane
2,2-0ichloropropane
Result
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
I
I
I
I
I
I
I
I
Surroaates:
REC(%)
I
Oibromofluoromethane
1,4-Bromofluorobenzene
98
95
I
I
RL
10
0.50
1.0
1.0
1.0
1.0
10
10
1.0
1.0
1.0
10
0,50
1.0
1,0
1.0
10
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
0.50
1.0
1,0
1.0
1.0
1,0
1,0
Control
Limits
57-157
76-113
RL - Reporting Limit OF . Dilution Factor
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 ·
FAX: (714) 894-7501
I "H
.,....-.--.----.--.-------
OF
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Lab Sample
Number
04-Ò2~1425-3 .
Qual Units
ug/L
uglL
uglL
ug/L
uglL
uglL
ug/L
U9/L
ug/L
ug/L
ug/L
ug/L
uglL
uglL
uglL
ug/L
ug/L
ug/L
ug/L
uglL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
uglL
ug/L
ug/L
ug/L
ug/L
ug/L
uglL
ug/L
Qual
Qual - Qualifiers
Analytical Report
Date Received:
Work Order No:
Preparation:
Method:
Oate
Collected
Matrix
Date Date
Prepared Analyzed
02124104 ~u~usN/A' <0~6/04
Parameter
1,1-0ichloropropene
c-1,3-0ichloropropene
t-1,3·0ichloropropene
Ethylbenzene
2-Hexanone
Isopropyl benzene
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-Pentanone
Naphthalene
n-Propylbenzene
Styrene
1.1,1.2- Tetrachloroethane
1,1,2,2- Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3- Trichlorobenzene
1,2,4- Trichlorobenzene
1,1,1- Trichloroethane
1,1,2- Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3- Trichloropropane
1,2,4·Trimethylbenzene
1,3,5- rrimethylbenzene
Vinyl Acetate
Vinyl Chloride
p/m-Xylene
o-Xylene
Methyl-t-Butyl Ether (MTBE)
Tert-Butyl Alcohol (TBA)
Oiisopropyl Ether (OIPE)
Ethyl-t-Butyl Ether (ETBE)
Tert-Amyl-Methyi Ether (TAME)
Ethanol
Surrooates:
Toluene-dB
Result
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
REC(%)
96
RL
1.0
0,50
0,50
1.0
10
1.0
1.0
10
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1,0
1.0
1,0
1.0
1.0
10
5.0
1.0
1.0
10
0.50
1.0
1.0
1.0
10
2,0
2.0
2,0
100
Control
75-123
OF Qual
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
02/24/04
04-02-1425
EPA 5030B
EPA 8260B
Page 3 of 5
QC Batch 10
040225L03 .
Units
ug/L
ug/L
ug/L
uglL
ug/L
ug/L
uglL
ug/L
ug/L
ug/L
ug/L
ug/L
uglL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
uglL
ug/L
ug/L
~
..,..-.-...'-._-_..~....-...__.._..__.
I
I ~- a/science
If:. nvironrÍ1enta/
Analytical Report
I I- aboratories, Inc.
Blainé Tech Services, Inc Date Received: 02/24/04
I 20360 Gramercy Place Work Order No: 04-02-1425
Torrance, CA 90501-1511 Preparation: EPA 5030B
Method: EPA 8260B
I Project: 5321 Stockdale Highway, Bakersfield, CA Page 4 of 5
I Lab Sample Date Date Date
Client Sample Number Number Collected Matrix Prepared Analyzed QC Batch ID
MW4,;,q~;:g1' ';,-" ,:.. ,~2.~4254, 'L;,/()2t2~04 .', ~u~us '.' 02/26104 '. 040225L03
I Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units
Acetone ND 10 1 ug/L 1,1-Dichloropropene ND 1.0 1 ug/L
Benzene ND 0.50 1 ug/!- c·1,3-Dichloropropene ND 0.50 1 ug/L
Bromobenzene ND 1.0 1 ug/L t-1,3-Dichloropropene ND 0.50 1 ug/L
I Bromochloromethane ND 1.0 1 ugfL Ethylbenzene ND 1,0 1 ug/L
Bromodichloromethane ND 1.0 1 ug/L 2-Hexanone ND 10 1 ug/L
Bromoform ND 1.0 1 ugfL Isopropylbenzene ND 1.0 1 ug/L
Bromomethane ND 10 ,1 ug/L p-Isopropyltoluene ND 1.0 1 ug/L
2-Butanone ND 10 1 ug/L Methylene Chloride ND 10 1 ug/L
I n-Butylbenzene ND 1.0 1 ug/L 4-Methyl-2-Pentanone ND 10 1 ug/L
sec-Butylbenzene ND 1.0 1 ug/L Naphthalene ND 10 1 ug/L
tert-Butylbenzene ND 1.0 1 ug/L n-Propylbenzene NO 1.0 1 ug/L
Carbon Disulfide ND 10 1 ug/L Styrene ND 1.0 1 ug/L
I Carbon Tetrachloride ND 0.50 1 uglL 1,1; 1,2- Tetrachloroethane ND 1.0 1 uglL
Chlorobenzene ND 1.0 1 .ug/L 1,1,2,2· Tetrachloroethane ND 1.0 1 ug/L
Chloroethane NO 1.0 1 ug/L T etrachloroethene NO 1.0 1 ug/L
Chloroform NO 1.0 1 ug/L Toluene NO 1.0 1 uglL
I Chloromethane NO 10 1 ugfL 1,2,3-Trichlorobenzene NO 1.0 1 ug/L
2-Chlorotoluene ND 1.0 1 ugfL 1,2,4-Trichlorobenzene NO 1.0 1 ug/L
4-Chlorotoluene NO 1.0 1 ug/L 1,1,1-Trichloroethane NO 1,0 1 ug/L
Oibromochloromethane NO 1.0 1 ug/L 1.1.2-Trichloroethane NO 1.0 1 ug/L
1,2-0ibromo-3-Chloropropane NO 5.0 1 ugfL Trichloroethene NO 1,0 1 ug/L
I 1,2-0ibromoettiane NO 1.0 1 ugfL Trichlorofluoromethane NO 10 1 ug/L
Oibromomethane NO 1.0 1 uglL 1,2,3-Trichloropropane NO 5,0 1 ug/L
1,2-0ichlorobenzene NO 1.0 , uglL 1,2,4-Trimethylbenzene NO 1.0 1 ug/L
1,3-Dichlorobenzene NO 1.0 1 ug/L 1,3,5- Trimethylbenzene NO 1.0 1 ug/L
I 1,4-0ichlorobenzene NO 1.0 1 ug/L Vinyl Acetate NO 10 1 ug/L
Oichlorodifluoromethane NO 1,0 1 uglL Vinyl Chloride NO 0.50 1 ug/L
1,1-0ichloroethane ND 1.0 1 ug/L p/m-Xylene NO 1.0 1 ugIL
1,2-0ichloroethane ND 0.50 1 ug/l o-Xylene NO 1.0 1 ug/l
1,1-0ichloroethene NO 1.0 1 ug/l Methyl-t-Butyl Ether (MTSE) NO 1.0 1 ug/L
I c-1,2-0ichloroethene NO 1,0 1 ug/l T ert-Butyl Alcohol (TBA) NO 10 1 ug/L
t-1,2-0ichloroethene NO 1.0 1 ug/l Oiisopropyl Ether (OIPE) NO 2.0 1 ug/l
1,2-0ichloropropane NO 1.0 1 ug/L Ethyl-t-Butyl Ether (ETSE) NO 2.0 1 ug/l
1,3·0ichloropropane NO 1.0 1 ug/L Tert-Amyl-Methyl Ether (TAME) NO 2,0 1 . ug/L
I 2,2-0ichloropropane NO 1.0 1 ug/l Ethanol NO 100 1 ug/L
Surroaates: REC (%) Control Qual Surroaates: REC(%) Control Qual
Limits
Oibromofluoromethane 93 57-157 Toluene-dB 95 75-123
I 1 ,4-Bromofluorobenzene 96 76-113
I
I RL - Reporting Urni! DF . Dilution Factor Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 . TEL: (714) 895-5494 . FAX: (714) 894-7501
I .. ..... -----------.-..-- _._._. _._------_._~-- ,".---.-'. ._---~. .......--...-....-.
- ----~--~~- -- --~~----~------ ----------------- ---- - ------~------ --------- - -----~----
I
I ~ = a/science
I::, nvironmental
I Laboratories, Inc. Analytical Report
Blaine Tech Services, Inc Date Received: 02/24/04
I 20360 Gramercy Place Work Order No: 04-02-1425
Torrance, CA 90501-1511 Preparation: EPA 50308
Method: EPA 8260B
I Project: 5321 Stockdale Highway, Bakersfield, CA Page 5 of 5
I Lab Sample Date Date Date
Client Sample Number Number Collected Matrix Prepared Analyzed ac Batch ID
::I..M,,~âJfJfani( ...... ·j);J~::;'~;5(;'':'099'1 Q-D06-1\1i9'i i ·N1AX>/·:L:Þòciueous . 'NfA ß~61Ø4 :'. .040225L03.
, .. ."':".
I Parameter Result RL OF Qual Units Parameter Result RL OF Qual Units
Acetone ND 10 1 ug/L 1,1-0ichloropropene NO 1.0 1 ug/L
Benzene NO 0.50 1 ug/L c-1,3-0ichloropropene ND 0.50 1 ug/L
Bromobenzene NO 1.0 1 ug/L t-1,3-0ichloropropene NO 0.50 1 ug/L
I Bromochloromethane NO 1.0 1 ug/L Ethylbenzene NO 1.0 1 ug/L
Bromodichloromethane NO 1.0 1 ug/L 2,Hexanone ND 10 1 ug/L
Bromoform ND 1.0 1 ug/L Isopropyl benzene ND 1.0 1 ug/L
Bromomethane ND 10 1 ug/L p·lsopropyltoluene ND 1.0 1 ug/L
2·Butanone NO 10 1 ug/L Methylene Chloride ND 10 1 ug/L
I n·Butylbenzene NO 1.0 1 ug/L 4-Methyl-2-Pentanone NO 10 1 ug/L
sec-Butylbenzene ND 1.0 1 ug/L Naphthalene NO 10 1 ug/L
tert-Butylbenzene ND 1.0 1 ug/L n-Propylbenzene NO 1.0 1 ug/L
Carbon Disulfide ND 10 1 ug/L Styrene ND 1.0 1 ug/L
I Carbon Tetrachloride ND 0.50 1 ug/L 1,1 ,1,2- Tetrachloroethane NO 1.0 1 ug/L
Chlorobenzene ND 1.0 1 ug/L 1,1,2;2- Tetrachloroethane ND 1.0 1 ug/L
Chloroethane ND 1.0 1 ug/L T etrachloroethene NO 1.0 1 ug/L
Chloroform ND 1.0 1 ug/L Toluene ND 1.0 1 ug/L
Chloromethane ND 10 1 ug/L 1,2,3- Trichlorobenzene NO 1.0 1 ug/L
I 2-Chlorotoluene ND 1.0 1 ug/L 1,2,4- Trichlorobenzene ND 1.0 1 ug/L
4-Chlorotoluene ND 1.0 1 ug/L 1,1,1-Trichloroethane ND 1.0 1 ug/L
Dibromochloromethane NO 1.0 1 ug/L 1,1,2- Trichloroethane ND 1.0 1 ug/L
1,2·Dibromo-3-Chloropropane ND 5.0 1 ug/L Trichloroethene ND 1.0 1 ug/L
I 1,2-0ibromoethane ND 1.0 1 ug/L Trichlorofluoromethane ND 10 1 ug/L
Oibromomethane NO 1.0 1 ug/L 1,2.3-Trichloropropane ND 5.0 1 ug/L
1,2-Dlchlorobenzene NO 1,0 1 uglL 1.2,4- Trimethylbenzene ND 1,0 1 ug/L
1,3-Dichlorobenzene NO 1.0 1 ug/L 1.3,5- Trimethylbenzene ND 1.0 1 ug/L
I 1 A-Dichlorobenzene ND 1.0 1 ug/L Vinyl Acetate NO 10 1 ug/L
Oichlorodifluoromethane NO 1.0 1 ug/L Vinyl Chloride NO 0.50 1 ug/L
1,1-Dichloroethane ND 1.0 1 ug/L p/m-Xylene ND 1.0 1 ug/L
1,2-0ichloroethane ND 0.50 1 ug/L o·Xylene ND 1.0 1 ug/L
1,1-Dichloroethene ND 1.0 1 ug/L Methyl-t-Butyl Ether (MTBE) NO 1.0 1 ug/L
I c-1,2-Dichloroethene ND 1.0 1 ug/L Tert·Butyl Alcohol (TBA) NO 10 1 ug/L
t-1,2-0ichloroethene NO 1.0 1 ug/L Diisopropyl Ether (OIPE) ND 2.0 1 ug/L
1.2·0ichloropropane NO 1.0 1 ug/L Ethyl,t-Butyl Ether (ETBE) NO 2.0 1 ug/L
1,3-Dichloropropane ND 1.0 1 ug/L Tert-Amyl-Methyl Ether (TAME) ND 2.0 1 ug/L
I 2,2-Dichloropropane NO 1.0 1 ug/L Ethanol ND 100 1 ug/L
Surrooates: REC(%) Control Qual Surroaates: REC(%) Control Qual
Limits
Dibromofluoromethane 89 57-157 Toluene-d8 96 75-123
I 1,4-Bromofluorobenzene 94 76-113
I
I RL . Reporting Limit DF - Dilution Factor Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 . TEL: (714) 895-5494 . FAX: (714) 894-7501
I
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La/science
I:ªn vironmen tal
L -aboratories~ Inc.
I
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I
Quality Control - Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project:
5321 Stockdale Highway, Bakersfield, CA
Date Received:
Work Order No:
Preparation:
Method:
02/24/04
04-02-1425
N/A
EPA 120.1
I
Quality Control Sample ID
I
I
.. ", .... "
.., . ."
·04;0~~1~?Z~;t·, ,,': ii'
Parameter
Specific Conductance
I
I
I
I
I
I
I
I
I
I
I
Matrix
. ......,..:,.. :
Acjuèous
SamDle Cone
1400
Instrument
Date
Prepared:
Date
Analyzed:
Duplicate Batch
Nùmber
;.40224SCD1
Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
',.{",': ".,
..,$C1-.
.". .
N1A . '},O~4104
.~------_._------------~-~-_._-_._- _.__.~-.-.. ---------.-.-.. --_._-~._---._.__.. -.
DUP Conc
1400
RPD RPD Cl
o 0-25
I
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I
I
I
I
I
I
I
I
I
I
I
I
I
I
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!l - alscience
I:; nvironmental
Laboratories, Inc.
Quality Control- Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
02/24/04
04-02-1425
N/A
EPA 130.2
Project:
5321 Stockdale Highway, Bakersfield, CA
Quality Control Sample ID
!~~,&1,¡tu·1
Date
Prepared:
Date
Analyzed:
Duplicate Batch
Number
Matrix
Instrument
. ,. ...... ._...
;;:'~~?p.,:\i¡;>(0',~,>,~f~:: ." .....,
40227HARD2
. .N/A i·.···· "02127104 .
". '~}.'..:.
.~~ ;
Parameter
RPD CL
0-25
Qualifiers
Sample Cone
DUP Cone
RPD
o
Hardness, Total
120
120
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAA: (714) 894-7501
'-"--,,,_~__,,__________.__v_____.____._. ____..._.____....______ _..
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~alscience
I::, nvironmental
Laboratories, Inc.
Quality Control - Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project:
5321 Stockdale Highway, Bakersfield, CA
Date Received:
Work Order No:
Preparation:
Method:
02/24/04
04-02-1425
N/A
EPA 150.1
Quality Control Sample ID
:ôBIiq1377-1 . "H' .
"'-"
Parameter
pH
Matrix
" ".
~.' ".
. '~I.iëÖIJS;
Instrument
Date
Prepared:
'., N/A. ...... .
Date
Analyzed:
02l241ö4" .
RPD CL
0-25
Duplicate Batch
Number
40224PHD1
Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
.,.~. ____...__~._-_P-- _."____ _._._"__._~_._.. ______.,_." ___.___.._._ ___._~.___________ ---.-.-.-......-.--
Sample Cone
7.71
HPH1 . ..' '
DUP Cone
RPD
o
7.74
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t.....- a/science
I:ªnvironmental
Laboratories, Inc.
I
I
I
Quality Control - Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project:
Date Received:
Work Order No:
Preparation:
Method:
5321 Stockdale Highway, Bakersfield, CA
02/24/04
04-02-1425
N/A
EPA 160.1
I
I
I
I
I
I
Quality Control Sample ID
.,. DtQ2-1~;f,:,,~;,'i/:: '" . .'..
Parameter
Solids, Total Dissolved
I
I
I
1
I
I
I
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714)895-5494 · FAX: (714) 894-7501
Matrix
Date
Prepared:
Instrument
. . . ,: "\:·<:·\:~,:,?i~k~:~~~~$
.. ',,".,
,". .':.' ,,: . ','. :......., ~':' .-
,,/'WA ',:>,;>:,;c/l!/~\'
Sample Cone
DUP Cone RPD
3600
3700 3
I".. '___...·________'_._____....______________'.._,___.....nm__ ,...,'U'___ --. .,
Date
Analyzed:
. . 'O~5/94:"
RPD CL
0-25
Duplicate Batch
Number
.' ·.40225TDSD1
Qualifiers
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
t....- a/science
I:, nvironmenta/
Laboratories, Inc.
Quality Control - Spike/Spike Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
Project: 5321 Stockdale Hiç¡hway, Bakersfield, CA
Quality Control Sample 10
Instrument
Date
Prepared
Matrix
, ..
Jë:2'·t(( .
··''''NlA·,, ,
Parameter MS %REC MSD %REC %REC Cl
Chloride 91 91 50-150
Nitrate (as N) 96 95 50-150
Sulfate 95 96 50-150
Date
Analyzed
02124104
RPO
RPD Cl
02/24/04
04-02'-1425
N/A
EPA 300.0
MS/MSO Batch
Number
040224s01
Qualifiers
7440 Uncoln Way, Garden Grove, CA 92841-1427 ~. TEL: (714) 895-5494 · FAX: (714) 894-7501
-._." '-"~_.'--'-----"'-.~"-'-'--' -.-_.---.._,_._._--~_._'_.' - ------
o 0-25
1 0-25
1 0-25
I
I
I
I
I
I
I
I
I
I
I
I
I
I"
I
I
I
I
I
~- alscience
1:1'vironmental Quality Control - LCS/LCS Duplicate
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
N/A
04-02-1425
N/A
EPA 300.0
Project: 5321 Stockdale Highway, Bakersfield, CA
LCS/LCSD Batch
Number
, ~~~Ó1 ' '
RPD CL Qualifiers
0-25
0-25
0-25
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
. . ,...__...-.__ ,.,~.~~,.v.._._~..____". .~..___ ___~_ _~,____._ ~'__'_"..u.m'_' ....__.....__. __._._______.._,__._~.__ . .__".', .__..___.____.._____.... ____..________._..._.. ''''..._
Quality Control Sample 10
099'()5-;11'S-2,098 ".
Date Date
Prepared Analyzed
'Nil(' " ';,;"Q2J24104
Matrix Instrument
'.,."+;":::~~eo~$,,>:": " · " IC 2 "
Parameter
LCS %REC LCSD %REC %REC CL RPD
90 91 80-120 '1
97 97 80-120 0
98 97 80-120 1
Chloride
Nitrate (as N)
Sulfate
1
I
1
I
I
I,
I
I
I
I
I
1
I
1
I
I
1
I
I,..... ...__.."_,___.._'___.__,_____,'
L- a/science
I:, nvironmenta/
Laboratories, Inc.
Quality Control - Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project:
5321 Stockdale Highway, Bakersfield, CA
Date Received:
Work Order No:
Preparation:
Method:
02/24/04
04-02-1425
N/A
EPA 351.3
Quality Control Sample ID
MW-4
::::~:r::"~:~'~'; .
. "";,'
", ,
...
.. ,.,....
, .
. .
Parameter
Total Kjeldahl Nitrogen
Matrix
. ·····..ei>''':;!';'~!¡:;Aqu~~$.~-.
Samole Cone
ND
Instrument
Date
Prepared:
Date
Analyzed:
"03/01/04
RPD CL
0-25
Duplicate Batch
Number
40301T1<ND1
Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
tùA
N/A .'
DUP Cone
RPD
NA
ND
,-.
--_._--.-.~-.
I
I
fL a/science
,I:~nvironmental
Laboratories, Inc.
I
I
Quality Control - Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
I
I
I
I
Project:
5321 Stockdale Highway, Bakersfield, CA
Date Received:
Work Order No:
Preparation:
Method:
02/24/04
04-02": 1425
N/A
SM 2320B
Quality Control Sample ID
, b:4"92~f626-'1
Parameter
Alkalinity, Total (as CaC03)
Bicarbonate (as CaC03)
I
I
Carbonate (as CaC03)
Hydroxide (as CaC03)
I
I
I
I
I
I
I
I
I
Matrix
;;,~~~
.. ".' ~ '~.' i:. :. .
:; :,::~,,:~-':~-'.:':":,
Instrument
Date Date Duplicate Batch
Prepared: Analyzed: Number
.... , N/A, ' 03/03104 ,.,. 403Q3ALKD1,
. ......".."..
RPD RPD CL ~
0-25
2 0·25
NA 0-25
NA 0-25
Samole Cone DUP Cone
410 420
410 420
ND ND
ND ND
~Pìi1
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
.. ..- ..---.-
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
¡";alscience
I:jI vironmen tal
Laboratories, Inc.
Quality Control· Spike/Spike Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
02/24/04
04-02-1425,
EPA 301 OA Total
EPA 6010B
Project: 5321 Stockdale Hiqhway, Bakersfield, CA
Quality Control Sample ID
Date
Prepared
Date
Analyzed
MS/MSD Batch
Number
Matrix
Instrument
~;..JCP 3300 ,'.,. ' ";"'O~;~:;' '02J2SJi)4
,".,. .'
;-.. -\.,; .,~%;.,;;>...~,",
040225805
Parameter
MS %REC
MSD %REC
%REC CL
RPD
RPD CL
Qualifiers
Lead
0-20
80-120
4
104
100
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
. n_". ~ _....~___.___~.__..._.'w__._.
~-....,~_._-,_.
.... -~ ,.--.,
I
I
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I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
~ a/science
I:§n vironmen tal
Laboratories, Inc.
Quality Control - Spike/Spike Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
, 02/24/04
04-02-1425
EPA 3010A Total
EPA 6010B
Project: 5321 Stockdale Hiohwav, Bakersfield, CA
Quality Control Sample 10
··~Jö~~1\~~~~?'
Date
Prepared
Date
Analyzed
MS/MSD Batch
Number
Matrix
Instrument
.I,.,.~ .
... '. ... . .
, .... ," . ".. .
02J25tó4>:':\;~:~:02l26104;'" . ., 040225806
·.ICP 3300
'>~;::"~:(~;: ~~.'.
Parameter
MSD %REC
Qualifiers
%REC CL
RPD
RPD CL
MS %REC
Lead
97
80-120
97
0-20
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 . FAX: (714) 894-7501
'--"..-. _._---~.. ....-......-.
",-.,..-.. -..-...---------,.- .._---_.~--~------_._----_._._----._--_._..._-- ......__..._..~_.
---- ._._...~ _. _.._-
I
I
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I
I
I
I
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I
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I
I
I
I,
I
I
I
I
I
~ a/science
I:: nvironmental Quality Control - Laboratory Control Sample
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
N/A
04-02-1425
EPA 3005A Filt.
EPA 6010B
Project: 5321 Stockdale Highway, Bakersfield, CA
Quality Control Sample ID
Matrix
Lab File ID
LCS Batch Number
Instrument
Dale Analyzed
:~Q91~~,~Ò3-3,63~·..;.
>, ,"'o4o~~~5< .:
',;ÅQ4~OÚS >, .
,··.·ICP3300., .,
. 02/~5I04
·040225L05F
."."
. .
Parameter
Cone Added Conc Recovered %Rec ·/.Rec CL Qualifiers
1.00 1,02 102 80:.120
1,00 1.00 100 80-120
1.00 1.03 103 80-120
1.00 1.06 106 80-120
Lead
Iron
Magnesium
Manganese
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
'.-.~_.. -..--.....----..-..-..-----..--.-,.-.----.... .--
.._______R____.__··.. ."
-----_._~
I
I
I
I
t....- a/science
I:, nvironmental Quality Control· LCS/LCS Duplicate
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project: 5321 Stockdale Highway, Bakersfield, CA
Date Received:
Work Order No:
Preparation:
Method:
I
N/A
04-02-1425
EPA 301 OA Total
EPA 6010B
I
I
I
I
I
Date'
Matrix Instrument Prepared
~~~Lls:~/>,ICP 33ÓO)¡~:~;;if~;ip~~/04 '
Date
Analyzed
..·'O2l2~04.
Quality Control Sample 10
'. 097iõ~'<¥ÖÔ3.3.63t
.. .,""".','''''',' . ..
Parameter
LCS %REC LCSD %REC %REC CL RPD
102 104 80-120 1
99 98 80-120 2
102 105 80-120 2
102 103 80-120 2
102 102 80-120 0
99 97 80-120 2
110 113 80-120 3
Lead
Calcium
Iron
Magnesium
Manganese
Potassium
Sodium
I
I
I
I
I
I
I
I
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
- - --" -.-.,.- .--------.-----.--.----.
LCS/LCSD Batch
Number
'040225L6
RPD CL Qualifiers
0-20
0-20
0-20
0-20
0-20
0-20
0-20
- ---.-,.-..-..........-.--..
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
l...= a/science
'=$nVironmenta/
Laboratories, Inc.
Quality Control - Spike/Spike Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
02/24/04
04-02-1425
EPA 5030B
DHS LUFT
Project: 5321 Stockdale Hiqhway, Bakersfield, CA
Quality Control Sample ID
;2~~,iä8~1
Date
Prepared
Date
Analyzed
MS/MSD Batch
Number
Matrix Instrument
. . . .
AU$OUS' ;G(;28.,·
'c....··<NJA '.
02126104 ;. ". '·'040226S01
/'<:',
Parameter
RPD
RPD CL
Qualifiers
MS %REC
MSD %REC
%REC CL
TPH as Gasoline
70-112
3
0-17
81
83
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
. .. ...--.---.----- ...--
,- '.--.....-. -. .-.....---.
,--..-... "--.--.-.--' .-.....--.-.--.-..-.. ..- ,---~._----¥_- ..-.._-_._--~-,...__._-~--_..
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
~- alscience
~nVironmental Quality Control - LCS/LCS Duplicate
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
Project: 5321 Stockdale Highway, Bakersfield, CA
N/A
04-02-1425
EPA 5030B
DHS LUFT
Quality Control Sample 10
09S003-OÓ64i923 '.,
Date' Date
Prepared Analyzed
'NIA " 02126/04'
Matrix
'\ "(;Y'!~f;9~~~u~,'
Instrument
··õGC2S.
Parameter
LCS %REC
%REC CL
LCSD %REC
TPH as Gasoline
89
72-114
85
LCS/LCSD Batch
Number
. ,
···'ó40226B01
RPO
5
RPD CL Qualifiers
0-10
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
- -.. p-".----.---..-.-- .....
- ..-. .---- --~-- .... ..-- -.---... ..------.--"----..-------.---..
-..__.._.__.._~~....-.__..
I
I
I
I
I
I
I
I
I
I'
I
I
I
I
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I
I
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1"...,.'..-.'-,----------..-.----------.-:...-----------,-,---.
~ a/science
I:: nvironmenfa/ Quality Control - LCS/LCS Duplicate
L aborafories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance. CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
N/A
04-02-1425
EPA 351 OC
DHS LUFT
Project:
5321 Stockdale Highway, Bakersfield, CA
Quality Control Sample ID
. ,ô!l8-ðii>9i~iqif
Date Date
Prepared Analyzed
"q~$!()4H.. ···'..02126/04
Matrix
Instrument
LCS/LCSD Batch
Number '
040225.BÖi.
.. :''';'"
..;, "; ,,;~9;~~;~JrL;:',..Gq~\.
Parameter
LCS %REC
LCSD %REC
%REC CL
RPD
RPD CL
0-11
. Qualifiers
TPH as Diesel
88
85
60·132
2
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 .. FAX: (714) 894-7501
_u._._._.. n.'_
I
I
I
"- a/science
I:; nvironmenta/
Laboratories, Inc.
Quality Control - Spike/Spike Duplicate
I
I
I
Blaine Tech Services, Inè:
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
Project: 5321 Stockdale Hiqhway, Bakersfield, CA
Quality Control Sample ID
Date Date
Matrix Instrument Prepared Analyzed
, H~~O~~ " " , H
GC1M!fFF ' H' :,/,',)'¡./;N/A ;.'....:~':<~,'" >.:;":. 02126104
MS %REC MSD %REC %REC CL RPD RPD CL
98 97 85-121 1 0-11
106 105 70-142 1 0-16
95 95 84-120 0 0-10
93 92 84-120 1 0-10
93 96 78-138 3 0-16
96 99 86-122 4 0-11
100 101 85-121 1 0-12
82 84 71-131 3 0-19
89 90 68-128 1 0-16
90 98 25-157 8 0-35
89 86 76-124 4 0·12
94 91 75-123 4 0-13
92 93 72-120 1 0-12
88 94 51-135 7 0-30
I
I
".. """:,':;F<:;:;;,::>:~';;'<'",: ',.
, MW.~1:6~:';,:',),,;,<·:',;::_.
." ~ .
-',I·
Parameter
I
I
Benzene
Carbon Tetrachloride
Chlorobenzene
1,2-Dichlorobenzene
1,1·Dichloroethene
Toluene
Trichloroethene
Vinyl Chloride
Methyl-t-Butyl Ether (MTBE)
Tert-Butyl Alcohol (TBA)
Diisopropyl Ether (DIPE)
Ethyl-t-Butyl Ether (ETBE)
Tert-Amyl-Methyl Ether (TAME)
Ethanol
I
I
I
I
I
I
I
I
I
02/24/04
04-02-1425
EPA 50308
EPA 82608
MS/MSD Batch
Number
040225502 I
Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501 .
_.__u., ..__.,.._ .
I
I
~ a/science
I::g¡gnvironmental Quality Control - Laboratory Control Sample
Laboratories, Inc.
I
I
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
I
Project:
5321 Stockdale Highway, Bakersfield, CA
N/A
04-02-1425
EPA 5030B
EPA 8260B
Quality Control Sample 10
Matrix
Instrument Date Analyzed Lab File ID lCS Balch Number
'. ~ ',' i-:.,. . .';, ... .. ... .. ,
.. . ".~ 'J'.gC!,.,~:: FF J)2I26J04 . .. 2~FÊBÓ31" . 040225L03
" . ,~. ~.~ .. ". ..
Conc Added Cone Recovered %Rec ~ Qualifiers
50 48 96 91.-115
50 50 101 77-143
50 47 94 88-118
50 47 93 88-118
50 45 91 85-133
50 49 97 83-125
50 48 96 85-121
50 40 80 76-130
50 44 87 83-119
250 230 91 47-149
50 44 88 82-118
50 46 92 86-116
50 48 95 81-117
500 450 91 60-132
I
~'()99~~~~ÔÖ~1'O;~~9":'~;'i}Š~;Jl1f~j,7!~~~~~'" .
I
Parameter
Benzene
Carbon Tetrachloride
Chlorobenzene
1,2-0ichlorobenzene
1,1-0ichloroethene
Toluene
Trichloroethene
Vinyl Chloride
Methyl-t-Butyl Ether (MTBE)
Tert·Butyl Alcohol (TBA)
Oiisopropyl Ether (OIPE)
Ethyl-t-Butyl Ether (ETBE)
Tert-Amyl-Methyl Ether (TAME)
Ethanol
I
I
I
I
I
I
I
I
I
I
I
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
.."-.. ._------_.~-
,_______w_~_..._..__,_...._
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
1--
~ -al.$Cience
I::, nvironmental
Laboratories, Inc.
Glossary of Terms and Qualifiers
Work Order Number: 04-02-1425
Qualifier
Definition
NO
No! detected at indicated reporting limit.
7440 Lincoln Way, Garden Grove, CA 92841-1427 · TEl: (714) 895-5494 . FAX: (714) 894-7501
I
I
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C.'lfCi.fJç.
~VlrOfJm.øtgl
IIbor8torlBB. 'nc..
WORK ORDER #:
04 -[Q]~ -Q[i]~@
Cooler
of
I
(
SAMPLE RECEIPT FORM
CUSTODY SEAL INTACT:
Sample(s):
Cooler:
CLIENT:
B ~ f
. I.
DATE:
TEMPERATURE - SAMPLES RECEIVED BY:
CALSCIENCE COURIER:
Chilled, cooler with temperature blank provided.
---:--7"Chilled, cooler without temperature blank.
---'L- Chilled and placed in cooler with wet ice.
Ambient and placed in cooler with wet ice.
Ambient temperature.
+ 0 C Temperature blank.
LABORATORY (Other than Calscience Courier):
o C Temperature blank.
o C IR thermometer.
Ambient temperature.
Initial:
T Þ't--
No (Not Intact) :
Not Applicable (N/A): ,V
Initial: --r v1- .
SAMPLE CONDITION:
Chain-Of-Custody document(s) received with samples.........................
Sample container label(s) consistent with custody papers................ .....
Sample container(s) intact and good condition.... ... ... '" .,. .'. ... ... ... ... ....
Correct containers for analyses requested.............................. ...........
Proper preservation noted on sample label(s)................. '...................
VOA ,,¡al(s) free of headspace. ... ... '" ... ... ... ... ... .,. ... ... ..... ... ... ... ..... ...
Tedlar bag(s) free of condensation... ......,..... ............... ... ..,...... '.' .._..
Yes
1/
(/
l/'
t/
v
t/
'No
N/A
t/
-a;.,
Initial:
COMMENTS:
.. ,- - -
LAB(èàcr~~^CQ.
-
-
..
-
Lab Identificalion (if necessary):
Address:
Ci\y I S\a\e. Zip:
SAMPLING COt.4PAtlY:
LOG CODE:
-
-
-
-
..
-
SHELL Chain Of Custody Record
-
:::'::[N,$IP,~:NT NUMêÈR,.~~~~'R,t.l4'0;:'"
9 7 4 6 ~2 2
:;¡'~i~r,~,t~~MT NUM~S~~~~"::
Blaine Tech Services, Inc.
BTST
SrrE ADDRESs ISIr..t and Cityl:
Shell Project Manager to be invoiced:
10:~&~~¿~~~ti(>iME~it!N~ Tony Palagyi
IO#CH~ê4L~R0çÉ$ :)
!n~RMii1óUST.CJN:':':·: ·1
5321 Stockdale Highway, Bakersfield
EtFceU\lERM.EJ. ~Rff'OR1TO R'IØ"'I~PIlty«D.sigl'1Hl PHQNENO.:
AOOREss:
20360 Gramercy Place, Torrance, CA 90501-1511
f'fIO.eCT CONTACT H.arå:opy 01 PDF Report 10):
NIck Sudano
TEl...fPHONE:
E-MAIL:
Brltney Gunderson
SAMPLER NAME(S (Prlrt :
I FAA'
310-Y82.2465 1310-782.2958 nsudano@blalnetach.com
!f-NAROUND TIME (BUSINESS DAYS):
~ 10 DAYS 0 S DAYS 0 72 HOURS 0 48 HOURS 0 24 HOURS 0 lESS THAN 24 HOURS
o LA· RWQCB REPORT FORMAT 0 UST AGENCY:
GCIMS MTBE CONFIRMATION: HIGHEST
HIGHEST per BORING
ALL
~
<>
~
..
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..
"
'"
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.... CD
.. '"
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SPECIAL INSTRUCTIONS OR NOTES: CHECK BOX IF EOD IS NOT NEEDED, '0'
HNO:, poly's were field filtered prior to presarvlltlon
<Must state whether bicarbonate Is reported as either calcium carbonate
(CaCO:,), or bicarbonate (HCq)
,
: ,:....
-';'" ::':
~
it
Field Sample Identification
SAMPLING MATRIX HO.Of X m
DATE TIME CONT, ' !: III
~ II()~ ~~ W fb 'x. \
'I ~~ ^ .'"
1tÿ1 ^ f.-
ori.... IO~~ W ~ .x)l
M\,) ~
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California Regional Water Quality Control Board
Central Valley Region
Terry Tamminen
Secretary for
Environmental
Protection
Fresno Branch Office
Internet Address: http://www.swrcb.ca.gov/-rwqcb5
1685 E Street, Fresno, California 93706-2020
Phone (559) 445-5116' FAX (559) 445·5910
Arnold Schwarzenegger
Governor
26 March 2004
Regional Board Case No. 5T15000886
Mr. Tony Palagyi
Shell Oil Products U.S.
2255 13th Avenue SW
"Sèatffi:Wâ:šhington 98134'
UNDERGROUND TANK RELEASE, SHELL SERVICE STATION, 5321 STOCKDALE
HIGHWAY, BAKERSFIELD, KERN COUNTY
You submitted Fourth Quarter 2003 Groundwater Monitoring Report (Monitoring Report) dated
2 February 2004 and Site Assessment Report (Assessment Report) dated 12 February 2004. Delta
Environmental Consultants, Inc., Monrovia (Delta) prepared the Monitoring and Assessment reports.
The Monitoring Report documents a groundwater monitoring event at the above-referenced site on
21 November 2003. The Assessment Report summarizes an investigation at the above-referenced site
conducted on 13 January 2004. In a letter dated 17 June 2003, the Bakersfield Fire Department referred
the subject case to our agency for regulatory oversight. It also provided us with information indicating
that gasoline range petroleum hydrocarbons and the fuel oxygenates methyl tertiary butyl ether (MTBE)
and tertiary butyl alcohol (TBA) leaked at the subject site degrading soil and may threaten groundwater
quality. The January 2004 site assessment was conducted lateral to the underground storage tank (UST)
cluster rather than beneath the cluster. You have indicated that Shell Oil Products, U.S. (Shell) expects
to remove the UST system in the near future and that soil sampling will be conducted during this work in
compliance with City of Bakersfield Fire Department (BFD) requirements. Therefore, we do not request
additional site i~ve~tigation at present. We will determine site closure requirements based_ up<:m our
review of šite assëssment data collected during the UST system removal. Detectable gasoline or diesel
range petroleum constituents have not been detected during five groundwater monitoring events.
Groundwater monitoring frequency may be reduced to annual. Analysis by the "full scan" EP A Method
8260 analysis and analysis for dissolved lead may be discontinued. A summary of the Monitoring and
Site Assessment Reports and our comments follow.
Monitoring Report Summary
Blaine Tech Services, Inc., San Jose (Blaine Tech) collected groundwater samples from the monitoring
wells on 21 November 2003. Depth to groundwater was measured from 130.90 to 132.11 feet below
ground surface (bgs). Delta determined groundwater flow to be toward the southeast with a water table
slope of 0.014 feet per foot, consistent with previous monitoring events.
Samples were collected prior to and after purging monitoring wells MW -1 through MW -3. A pre-purge
sample was collected from MW-4. The samples were analyzed for total petroleum hydrocarbons as
California Environmental Protection Agency
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Mr. Tony Palagyi
- 2 -
26 March 2004
gasoline and diesel (TPH-g and TPH-d) by EP A Method 80I5M, volatile organic compounds detected in
a "full scan" EP A Method 8260B analysis, including benzene, toluene, ethylbenzene, and xylenes
(BTEX), MTBE, TBA, di-isopropyl ether (DIPE), ethyl tertiary butyl ether (ETBE), tertiary amyl methyl
ether (TAME), 1,2-dichloroethane (1,2~DCA), and 1,2-dibromoethane (EDB). The samples were also
analyzed for dissolved lead by EPA Method 6010B. Analytes were not detected in the pre-purge or post-
purge samples.
Site Assessment Summary
Delta drilled boring B-I to a depth of 130 feet bgs on 13 January 2004 using hollow stem auger
tech1)ology. Soil samples were collected at five-foot intervals to the total depth of the boring. Delta
summarizes soils encountered as primarily well-graded sands with lenses of silt and clay. Field evidence
of volatile organic compounds was not discovered. Groundwater was encountered at 126 feet bgs.
B-1 was proposed as a slant boring to access soils beneath the UST cluster, but was drilled adjacent to
the UST cluster as a vertical boring due to access restrictions.
Soil samples collected at twenty-foot intervals and at 130 feet bgs were analyzed in the laboratory for
TPH-g and TPH-d by EPA Method 80l5M, BTEX, MTBE, TBA, DIPE, ETBE, TAME, and ethanol by
EP A Method 8260B. Analytes were not detected in the samples.
Comments
KHM Environmental Management, Inc., Monrovia (now Delta) conducted a voluntary groundwater
assessment program (GRASP) investigation on behalf of Shell Oil Products U.S. (Shell) on-site.
KHM's GRASP Site Assessment Report (Site Assessment Report) dated 25 April 2003 describes that
investigation. KHM discovered low concentrations of TPH -g, MTBE and TBA in subsurface soils to a
depth of 35 feet bgs in a position lateral to the UST cluster. This data suggested that higher
concentrations of these analytes might be present beneath the UST system and could threaten
groundwater quality. Impacted soils were not encountered in boring B-1, drilled in another position
lateral to the UST cluster. Although B-1 did not investigate soils beneath the UST cluster, the analytical
data does not indicate a major release with lateral spreading. The constituents previously detected in
=--soÜs-maThàYe~reBulted-fr"Om-nfìirrör-vapöne'kas-e:-6'ITsöltm::-éll1-cr-dte-se'l ran-ge p'etro leum c'öñstìtüentS--=- ---,-
have not been detected in groundwater during five monitoring events.
You have indicated that Shell expects to remove the UST system in the near future and conduct
associated soil sampling under the supervision of the BFD. We do not request that you conduct
additional site investigation at present. We will review the results of the UST system removal
assessment prior to determining site closure requirements. Please contact us by 28 June 2004 with an
update concerning the UST removals.
Due to the absence of detectable analytes during groundwater monitoring, we request that you reduce
monitoring frequency to annual beginning with the first quarter 2004. The next monitoring report
should be conducted during the first quarter 2005. Please submit the first quarter 2004 monitoring report
by 3 May 2004.
By our letter dated 25 July 2003, we requested that you expand the current groundwater sample analysis
program to confirm constituents of concern (COCs). Samples were to be analyzed for the analytes
V:\UGlìProjectsVDW _fi1es\2004 Correspondence\City of Bakersfield Cases\Shell Stn Stockdale Hwy GW-SA 3-04,doc
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Mr. Tony Palagyi
- 3 -
26 March 2004
usually reported in a full EPA 8260 analysis, the lead scavengers 1,2-DCA, and EDB, and dissolved
lead. You conducted these analyses during the third and fourth quarters of2003. Since these ana1ytes
were not detected, analysis by "full scan" EP A Method 8260B and dissolved lead may be discontinued.
As of the date ofthis letter, electronic data deliverab1es for your site have not been submitted. Electronic
submittals uploaded to Geotracker should include soil or groundwater sample analytical data (various
file names), wellhead horizontal and vertical positioning data (GEO_XY and GEO_Z files), depth-to-
water measurements (GEO_ WELL files), and site maps (GEO_MAP files).
Please contact this office at least five days prior to fieldwork. If you have any questions regarding this
correspondence, please contact me at (559) 445-5504.
~-)f. úJ~'
JOHN D. WHITING
Engineering Geologist
R.G. No. 5951
c:
Ms. Barbara Rempel, SWRCB, UST Cleanup Fund, Sacramen~
Mr. Howard H. Wines III, Bakersfield Fire Department, Bakersfield"
Mr. Bradley Clark, Delta Environmental Consultants, Inc., Monrovia
Ms. Kathryn Ewing, Delta Environmental Consultants, Inc., Monrovia
File: UST/Kern/Shell Service Station, 5321 Stockdale Highway, Bakersfield/5Tl5000886
V:\UG1ìProjects\JDW _files\2004 Correspondence\City of Bakersfield Cases\Shell Stn Stockdale Hwy GW-SA 3-04,doc
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Solving environment~related business problems worldwide
911 South Primrose Avenue .- Suite K'
Monrovia, California 91016 USA
626.256.6662 800.477.7411
Fax 626.256.6263
www.deItaenv.com
February 2, 2004
Project No. PA5321S-1
Mr. John D. 'Whiting
California Regional Water Quality Control Board
Central Valley Region
1685 E. Street
Fresno, California 93706-2020
Re: FOURTH QUARTER 2003 GROUNDWATER MONITORING REPORT
Texaco Service Station
5321 Stockdale Highway
Bakersfi~ld, California
Dear Mr. Whiting:
On behalf of Equilon Enterprises LLC dba Shell Oil Products (SHELL), Delta Environmental Consultants, Inc.
(DELTA) has prepared this Fourth Quarter 2003 Groundwater Monitoring Report for the above-referenced sIte.
This quarterly report represent DELTA's' professional opinions based upon the currently available information and
are ai:rived at in accordance with currently acceptable professional standards. This report is based upon a specific
scope of work requested by the client. The Contract between DELTA and its client outlines the scope of work:, and
only those tasks specifically authorized by that contract or outlined in this report were performed. This report is
intended oIily for the use of DELTA's Client and anyone else specifically listed on this report. DELTA will not
and cannot be liable for unauthorized reliance by any other third party. Other than as contained in tbis paragraph,
DELTA makes no express or implied warranty as to the contents of this report.
If you havè any questions regarding this site, please contact Mr. Brad Clark (DELTA) at (626) 256-6662 or
Mr. Tony Palagyi (SHELL) (425) 377-8530.
Bradley E. Clark, P.E.
Senior Project Engineer
. Sincerely, .
Delta Environmental Consultants, Inc.
gG-
Attaclunent: Fourth Ql!arter 2003 Groundwater Monitoring Report
cc: Tony Palagyi, Shell Oil Products US
Howard H. Wines ill, City of Bakersfield Fire Department
A member of
Xlnogçn:entalAUiance·
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February 2, 2004
SHELL QUARTERLY STATUS REPORT
Station Address:
DELTA Project Nos.:
SHELL Environmental Engin./Phone No.:
DELTA Site Manager/Phone No.:
Primary Agency/Regulatory ill No.:
Other Agencies to Receive Copies:
5321 Stockdale Highway
PA5321S-l
Tony Palagyil( 425) 377-8530
Kathryn Ewing/(626) 256-6662
CVRWQCB/ John Whiting
City of Bakersfield Fire Department/ Howard H. Wines
III
WORK PERFORMED THIS QUARTER (FOURTH - 2003):
1. Quarterly groundwater monitoring and sampling. Submitted quarterly report.
2. Implemented additional site investigation per work plan dated October 6,2003.
3. Implemented no-purge sampling as approved in a CVRWQCBletter dated October 10, 2003.
WORK PROPOSED FOR NEXT QUARTER (FIRST- 2004):
1., Quarterly groundwater monitoring and sampling. Submit quarterly report.
2. Submit Additional Site Investigation Report.
\
Current Phase of Project: Groundwater monitoring
Frequency of Sampling: Quarterly
Frequency of Monitoring: Quarterly
Is Separate Phase Hydrocarbon Pr~sent On-site (Well #'s):
Cumulative SPH Recovered to Date: NA
SPH Recovered This Quarter: None
Sensitive Receptor(s) and Respective·
Direction(s):
DYes rg¡ No
Nearest field verified well is WellCBK 06-01 (State
Well No; 30S/27E-03B02 M) of the City of Bakersfield
àpproximately 825 feet South of the site.
Current Remediation Techniques:
Permits for Discharge:
Approximate Depth to Groundwater:'
Groundwater Gradient'
Current Agency Correspondence:
Summary of Unusual Activity:
None
None
130.90 to 132.11'
Southeast @J approximately 0.014 ft/ft
Central Valley RWQCB letters dated December 30,2003.
None
~~,
/
Kathryn Ewing
Site Manager (DELTA)
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ATTACHED:
· Table 1 - Groundwater Gauging and Analytical Results
· Table 2 - Additional Chemicals of Concern
· Figure 1 - Site Location Map
· Figure 2 - Groundwater Elevation Contour Map
· FigUre 3 - Hydrocarbon Distribution in Groundwater Map ,
· Figure 4 - TPH-G Concentrations in Groundwater Map
· Figure 5 - Benzene Concentrations in Groundwater Map
· Figure 6 - MTBE Concentrations in Groundwater Map
· Appendix A - Field Data Sheets
· Appendix B - Field Procedures
· 'AppendixC - Waste Disposal Documents
· Appendix D - Laboratory Report and Chain-of-Custody Documents
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HISTORICAL GROUNDWATER GAUGING AND ANALYTICAL DATA
SHEL SERVICE STATION
5321 Stockdale Hil!.hway, Bakersfield, California
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~_!1_~:!..... _~p of c~g elevation (ft): 386;61
3/17/2003 129,17 0.00, 257.44
..lQ~~QQi.. ~~ 0.00 257,23
6/19/2003 130.76 0,00 255.85
9/3/2003 132.68 0.00 253.93
11/21/2003 132,11 0.00 254.50
.11/21/2003
_,!1:.~ __.!!'J~~~a~g elevation (ft): 386.06
3/17/2003 128.64 0.00 257.42
3/25/2003 128.84 0,00 257.22
---
6/19/2003 130.27 0.00 255.79
9/3/2003 131.79 0:00 254.27
11/21/2003 131.45 0.00 254,61
11/21/2003
---
--------- --
_M~-3 _~p of casing elevation (ft): 386.34
3/17/2003 128.30 0.00 258.04
3/25/2003 128.45 0,00 257,89
-----~
6/19/2003 129.82 0,00 256,52
9/3/2003 131.44 0,00 254.90
11/21/2003 131.14 0,00 255,20
11/21/2003
--.!'::!.~~~!!. of ca.!!'!.g elevation (ft): 386.57
3/17/2003 128,17 0.00 258.40
--
3/25/2003 128,25 0,00 258.32
6/19/2003 129.59 0.00 256.98
--
9/3/2003 131.26 0,00 255.31
,
11/21/2003 130.90 0.00 255.67
-----
Notes:
----
GW - Groundwater
SPH - Separate, phase hydrocarbons
MSL - Mean sea level I
ND ' Not detected I
ugIL - parts per billion I
TPH,D - ToÙ;1 p~troleum hydrocarbons as diesel
TPH·G - Total petroleum hydrocarbons as gasoline
MTBE .: Met~~,tert butyl ether
TBA - Tert-butyl alcoholJ
DlPE . Di,isopropyl eth~~-
ErnE - Ethyl-tert bu!)il ether
TAME - Tert-amyl methyl ether
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ADDITIONAL CHEMICALS OF CONCERN
TEXACO SERVICE STATION
5321 Stockîale H!~~ay, Bakersfield, California
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........ .(;,,¡¡n;j.:::... ¡,;,wÙ.: :.. :i¡';iiI.i;i" :::::¡I;i;,/i,¡:...: ..:.... ¡.;.;ir.ii....:: :":·.i¡';0Li.·:·" ... .i¡i¡è/i;i:·:·.: >¡-¡i¡iü[;( ·.·.·.i¡;..¡i;i.·.·.: ·:::ift¡iJLI:...· ·.iß¡;üÜ· ·.·.i;"iJL¡·.·.· .... i.¡i¡i¡.;r.,¡i¡......... .iiilO¡Ú...
---
MW-I -¡; A'
--.-.--
9/3/2003 NA NA NA NA NA NA NA NA ND<O,OI NA NA NA NA NA NA NA NA NA NA
--- ~- --
MW-2
9/3/2003 26 ND<O,10 1.60 27 ND<0.50 100 100 ND<1.0 ND<1.0 ND<O.OI 30,8 ND<O,I 5.45 2,06 40.3 ND<0.005 350 -~ 6,31 220
MW-3 ,- --
------'-=-- '
9/3/2003 26 ND<0.10 1.60 27 ND<0.50 100 100 ND<1.0 ND<1.0 ND<O.OI 32.6 ND<O,I 5.94 2,34 34 ND<O,005 350 100 6,36 220
MW-4 - -,-
9/3/2003 26 ND<O.IO 1.50 26 ND<O,50 80 80 ND<1.0 ND<1.0 ND<O.OI 30.5 ND<O.1 5.48 2.01 41 ND<0.005 350 96 6.43 220
,
---
Notes: f----
---- ----
TKN ,Total Kj~~l Nitrogen -- f---- 1- -
TDS ' Total Dissolved Solidi
;A-~~~~~F=-E .
Note: Additional Chemicals of Concern Analvsis are only for the first and third Quarters,
,-
.-.---
Page I.of I
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I Â DELTA SHELL OIL PRODUCTS US
ENVIRONMENTAL TEXACO SERVICE STATION
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I FIGURE 1
SITE LOCATION MAP
5321 STOCKDALE HIGHWAY
I BAKERSFIELD, CALIFORNIA
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IIServerlkhm_dataIClients'-Shell'-Shell SiteslSIS321 Stockdalel2004,02,02_ 4Q03 Monitoring ReportlFIGURE 2(S32ILGROUNDWATER ELEVATION CONTOUR MAP,dwg, Model, 1/28/2004 1:11:21 PM
/
-
DISPENSER
ISLAND
(TYP)
-
-
-
-
-
-
-
N
W<>E
S
LEGEND
MW-1 ~ GROUNDWATER MONITORING
. . WELL LOCATION AND
DESIGNATION
(255.67) GROUNDWATER ELEVATION
IN FEET ABOVE MEAN SEA
LEVEL (Ft/MSL)
256.20- - GROUNDWATER CONTOUR
IN FEET ABOVE MEAN SEA
LEVEL (Ft/MSL)
CONTOUR INTERVAL=O,50 FEET
... APPROXIMATE GROUNDWATER
FLOW DIRECTION .
o
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.----
SCALE IN FEET
 Delta
ENVIRONMENTAL
I... CONSULTANTS INC.
SHELL OIL PRODUCTS US
TEXACO SERVICE STATION
BAKERSFIELD, CALIFORNIA
FIGURE 2
GRDUNDWA TER ELÈVA llON
CONTOUR. MAP
11/21/03
5321 STOCKDALE HIGHWAY
BAKERSFIELD, CALIFORNIA
-
-
-
-
-
-
-
-
-
-
-
CANOPY
(TYP)
STOCKDALE HIGHWAY
DISPENSER
ISLAND
(TYP)
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Date
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(µg/l) (µg/l) (µg/l)
03/25/03 ND<50 NO<O,50 ND<1.0
D6/19/03 ND<50 ND<O,50 ND<1.0
09/03/03 NO <50 NO<O,50 NO<I.0
11/21/03 ND<50 ND<O,50 NO<1.0
MW-3
Dote TPH-~ BENZENE MTBE
(µg/l (µg/L) (µg/l)
03/25/03 NO<50 NO<0.50 NO<1.0
06/19/03 NO<50 ND<0.50 ND<1.0
09/03/03 NO<50 ND<0.50 ND<1.0
11/21/03 NO<50' NO<0.50 NO<1.0
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Date ~/l) BENZENE MTBE
(µg/l) (µg/l)
03/25/03 NO<50 NO<O,50 NO<1.0
OB/19/03 ND<50 ND<O,50 NO<1.0
09 03 03 NO <50 ND<0.50 NO<1.0
11/21/03 NO<50 NO<0.50 NO<1.0.
03/25/03
06/19/03
09 03/03
11/21/03
I\5erverlkhm_datalCllents\.5hell\.5hell 51te51515321 5tockdalel2003'X,XX_ 4Q03 Monitoring ReportlFIGURE 3(5321LHYDROCARBON DISTRIBUTION IN GW MAP,dwg, Model, 1/19/2004 11:41:38 AM
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ND<1.0
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WASTE
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-
-
-
N
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S'
LEGEND
MW-1 ~ GROUNDWATER MONITORING
WELL, LOCA TION AND
DESIGNATION
TPH-g TOTAL PETROLEUM
HYDROCARBONS
AS GASOLINE
MTBE METHYL TERT-BUTYL
ETHER
¡..g/L MICROGRAMS PER LITER
NO NOT DETECTED
o
20
40
~--
SCALE IN FEET
Â.
Delta
ENVIRONMENTAL
CONSULTANTS INC.
SHELL OIL PRODUCTS US
TEXACO SERVICE ST A nON
BAKERSFIELD, CALIFORNIA
FIGURE 3
HYDROCARBON DISTRIBUTlONIN
GROUNDWA TER MAP
5321 STOCKDALE HIGHWAY
BAKERSFIELD, CALIFORNIA
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\\5erverlkhm_datalCllentsL5hellL5hell 51tesl515321 5tockdalel2003,X,XJC 4Q03 Monitoring ReportlFlGURE 4(5321LT1'H-gCONCENTRATJONMAP,dwg, Model, I/IQ/2004 11:45:00 AM
-
-
-
-
-
-
-
N
w-Q-E
S
LEGEND
MW-l-$- GROUNDWATER MONITORING
WELL LOCATION AND
DESIGNATION
ND<50 TPH-g CONCENTRATIONS
IN MICROGRAMS PER LITER
(µg/L)
TPH-g TOTAL PETROLEUM
HYDROCARBONS
AS GASOLINE
¡..g/L MICROGRAMS PER LITER
ND NOT DETECTED
o
20
40
~---
SCALE IN FEET
 Delta
ENVIRONMENTAL
~Â CONSULTANTS INC.
SHELL OIL PRODUCTS US
TEXACO SERVICE ST A T10N
BAKERSFIELD, CALIFORNIA
FIGURE 4
TPH-g CONCENTRATIONS IN
GROUNDWATER MAP
11/21/03
5321 STOCKDALE HIGHWAY
BAKERSFIELD, CALI,FORNIA
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IIServerlkhm_datalClients\.Shell\.Shell SiteslSIS321 Stockdalel2003'X,XX_ 4Q03 Monitoring ReportlFlGURE S(532ILBENZENE CONCENTRATION MAP,dwg, Model, 1/19/2004 11:47:03 AM
/
/
r~MW-4
ND<O.50
. r 1 f 1 r 1 r 1
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(TYP)
r
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~ :~;o250 __ _ _ _ _ __
~
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-
-
N
W~E
S
LEGEND
MW-1 ~ GROUNDWATER MONITORING
WELL LOCATION AND
DESIGNATION
ND<O.50 BENZENE CONCENTRATIONS
IN MICROGRAMS PER LITER
(µg/L)
µg/L MICROGRAMS PER LITER
ND NOT DETECTED
o
20
40
. --
SCALE IN FEET
 Delta
ENVIRONMENTAL
~.Â. CONSULTANTS INC.
SHELL OIL PRODUCTS ,US
TEXACO SERVICE ST A 110N
BAKERSFIELD, CALIFORNIA
FIGURE 5
BENZENE CONCENTRATIONS IN
GROUNDWA TER MAP
11/21/03
5321 STOCKDALE HIGHWAY
BAKERSFIELD, CALIFORNIA
-
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115ervèrlkhm_datalClients\.5hell\.5hell 5ite51515321 5tockdalel2003'X,)O,- 4Q03 Monitorin9 ReportlFIGURE 6(532ILMTBECONCENTRAllONMAP,dwg, Model, 1/19/200411:48:28 AM
-
-
STOCKDALE HIGHWAY
UST
(TYP)
DISPENSER
ISLAND
(TYP)
CANOPY
(TYP)
/
/
r~ND<1'O
, "W~411_1111 I
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I MW-3 l j l J l l
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ND<1.0
~:~;,20 __ _ __ _ __
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TANK
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-
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-
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W~E
S
LEGEND
MW-1 ~ GROUNDWATER MONITORING
WELL LOCATION AND
DESIGNA TION
~ MTBE CONCENTRATIONS
IN MICROGRAMS PER LITER
(µg/L)
µg/L MICROGRAMS PER LITER
NO NOT DETECTED
MTBE METHYL' TERT-BUTYL
ETHER
o
20
40
,- ->
SCALE' IN FEET
 Delta
. . ENVIRONMENTAL
I.. CONSULTANTS INC.
SHELL OIL PROOUCTS US
TEXACO SERVICE STATION
BAKERSFIELD, CALIFORNIA
FIGURE 6
MTBE CONCENTRA T10NS IN
GROUNDWATER MAP
11/21/03
5321 STOCKDALE HIGHWAY
BAKERSFIELD, CALIFORNIA
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ApPENDIX A
FIELD DATA SHEETS
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WELLH.EAD INSPECTION CHECKLIST
Client L) ~ell
Site Address S3Z1 ~-6G{0a (e
Job Number ()"5 II 2./-0(2;1
page-.L- of-L
Date f11211o~
y.wtr~ 8r::tters.f'lefcl
Technician ,();,v:=.~. ¡vi; /LG. P. ~{C(G. U.
Well Inspected -
No CorrecUve
Well 10 Action Required
MlA/- \ /
Mw-2- /
Mw-3 /
MW-Y V
, .
NOTES:
Water Balled Wellbox Other Action
. From Components Cap Lock Taken
Replaced Replaced (explain
Wellbox Cleaned below)
..
WeU Nòt
Inspected
(explaIn
below)
Repair Order
SubmItted
\'
BlAINE TECH SERVICes, INC.
SAN JOSE
LOS ANGELES
SAN DIEGO
SACRAMENTO
wwwblalnalech.mm
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WELL GAUGING DATA
I
Project # 0311 Z.J- De, I
Date ll/ZJ!Cß
Client' -5 W J
.
I
Site 11 ~ZI ~f< del Ie Mw&(
&k-ef3ftW
I
Thickness V olurne of
Well Depth to of Immiscibles Survey
\
Size Sheen I Inuniscible Immiscible Removed Depth to water 1;>epth to well Point: TOB
Wen ID (in.) Odor Liquid (ft.) Liquid (ft.) (DÙ) (ft.) bottom (ft.) or TOe
I,
I
MW- 11 13Z.I/ 1'17. G5 TOe
M\,\)- z. l,f 131.1.1; 1t.f5, I;
¡V1 w-3 Lf 13/.1l.f IL LfI'Ó~
Mw~Lf L.1 13Q·CfO 1£14·63
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Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (408) 573~0555
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! .
SHELL WELL MONITORING DATA SHEET
BTS#: 03112.1- 001 Site: q 7'1 G 7 z.Z.Z-
.
Sampler: ,...,p Date: \ l . 2. \ . O~
Well I.D.: ¡t.'Iw-/ Well Diameter: 2 3 @ 6 8
Total Well Depth (TD): \"'\ ï:53 Depth to Water (DTW): \'~z. "
Depth to Free Product: Thiclrness of Free Product (feet):
Referenced to: aID Grade D.O. Meter (ifreq'd): YSI BACH
DTW with 80% Recharge [(Height of Water Column x 0.20) + DTW]:
Purge Method: ner
Dispo e Bailer
Positive Air . acement
Electric Submersible
Sampling Method:
Bailer
(1SfsPi>sã~
Extraction Port
Dedicated Tubing
Waterra
Peristaltic
Extraction
Other
Screened Interval: I l.2.' . \'-\1 .
Other:
If well is listed as a no-purge, confinn that water level is below the top
f Oth th 11 b d
o screen., erwlse, ewe must e Dume .
Well Dinmcter Multiplier ' Well Dinmeler Multiplier
1" 0.04 4" 0.65
(Gals.) X = Gals. 2" 0.16 6" 1.47
1 Case Volume Suecified Volumes Calculated Volume 3" 0.37 Olher mdius1 · 0.163
Condo Turbidity
Time Temp (OF) pH (mS or ~ (NTUs) Gals. Removed Observations
~S- PRE PIJ~\7E-,
\ p-\ c. Iø '2 .'13" (c·3 Z- C''\l,,,, . ì c::..\c..:>~ u
Baller lowered .3 (" ' below
DTW to obtaIn snmple
Did well dewater? Yes No Gallons actually evacllated:
Sampling Date: 1\' Z.i .o)¡. Sampling Tune: \\'-1.0 Depth to Water:
Sample I.D.: ~",",\Ñ - \ Laboratory: (éaISci~ Columbia Other
Analyzed for: ~~G Oxyr@ates (5) \. 1.. i:> C.A 6 t.~ ~ P '-\ ~l.\.O'
B1@X MTBE ~-D Other: :t:"\:>\\ ~_~ \)\....~\,,"'_..) \ð_~
EB J.D. (if applicable): @ Duplicate I.D. (if applicable):
Time
Analyzed for: TPH-G BTEX MTBE TPH-D Oxygenates (5) Other:
D.O. (ifreq'd): Pre-purge: mg/L Post-purge: mg/L
O.R.P. (ifreq'd): Pre-purge: mV Post-purge: mV
Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (800) ,545..7558
-'-"~"--"'''''~''.'''''''-'''''
. ...,..,........
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s:ÐJil.,£ WELL MONITORING DATA SHEET
BTS #: D~ it J-(-O
Sampler: WI
Well I.D.: "" ..../
Total Well Depth (TD): 1c.f1.~3
Site:
Date:
Well Diameter: 2 3 (j) 6 8
Depth to Water (DTW): Is z.. I(
Depth to Free Product: 'Thic1mess of Free Product (feet):
Referenced to: .yC Grode D.O. Meter (ifreq'd): YSI BACH
DTW with 80% Recharge [(Height ofWateifloTumn x 0.20) + DTW]: i 3.J-: t 1
Purge Method: Bai1er Waterra Sampling Method: ~
Disposable Bailer Peristaltic Disposable Bailer ..
Positive Air Displacement Extraction Pump Extraction P-ort
'Z-bb I ~~mer~ì1bje.-::> Other Dedicated Tubing
Other:
Sc;reened Interval: )...-O ·-1 t. \' If welJ is listed as a no-purge, confirm that water level is below the top
f Oth· th 11 t b d
o screen. eI"Wlse, ewe rous e DUrge .
Well Dinmeter Multinlier Well Dinmeler MulLiDlier
/0. C> 3 3D. D I" 0.04 4" 0.65
(Gals,) X ,- Gals. 2" 0.16 6" 1.47
] Case Volume SDecified VolumeS: Calculated Volume. 3" 0,37 Other IUdius2 ... 0.163
Condo Turbidity
Time Temp tF) pH (mS or ~ (NTUs) Gals. Removed Observations
{1.10 ~S·~ 1,3 27~ ~j ID
/21-'3, 6:;11 7,L '2.11 tòS- 2D
'("2 '}... ~ , 7.0 7" '2-70 .~ 30 ."
..
Buller lowercd ,5 I below
- DTW to obtulo Jumple ..-
Did well dewater? Yes W Gallofls.actually evacuated: JO
Sampling Date: {I / 1- il~J ~ . '- " 'L3(
Såmpling Time: { , Depth to Water: 132.·,b
I ','
Sample I.D.: t4 IN -[ Laboratory: ~afScie~ Columbia Other
Analyzed for: ~~. ' . -=- ~~ )T2td s'l-OP è
MTBE (TPH-g) Other:
EB I.D. (if applicable): @ Duplicate LD. (if applicable):
Time
Analyzed for: TPH-G BTEX MTBE TPH-D.,., , Oxygenate,~ (5) Other:
D.O. (ifreq'd): <\~"t: mS/L Post-purge: mgl
Pre-purge: .L
O.R.P. (ifreq'd): Pre-purge: ·'f.:rgV Post-purge: mV
~'. .
Blaine Tech Services, Inc. 1680 R~gers Ave., San Jose, CA 95112 (800) 545-1558
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SHELL WELL MONITORING DATÆ'SHEET
BTS#: 03112.' - OBI Site: Cf 7'i~7Z2-7.-
Sampler: ~() Date: \l·z.\·c3>
I'
Well I.D.: þr1w- Z Well Diameter: 2 3 @ 6 8
Total Well Depth (TD): I~Ç.IS Depth to Water (DTW): l~ \'4S"
Depth to Free Product: Thiclmess of Free Product (feet):
Referenced to: (P~ Gmde D.O. Meter (ifreq'd): YSJ HACH
DTW with 80% Recharge [(Height of Water Column x 0.20) + DTW]:
PurgeM~' Bailer
. osable Bailer
Posi Air Displacement
Electric Su ~rsjble
Sampling Method:
Bailer
Œsposable B~
Extraction Port
Dedicated Tubing
Screened Interval: 1"2. \ I. l'-\lD '
Other:
If well is listed as a no-purge, corrfinn that water level is below the top
f Oth h 11 b d
o screen. erwlse, t e we must e DurQ:e .
Well Diameter Multiplier Wen Diameter Multiplier
, I" 0.04 4" , 0.65
(Gals.) X = Gals. 2" 0.16 6" \.47
1 Case Volume Specified Volumes Calculated Volume 3" 0.37 Other I11dius2 · 0.163
Condo Turbidity
Time Temp (Op) pH (mS or µS) (NTUs) Gals. Removed Observations
PR E f'vRIJt::.
\'l.o Q \0'"2.·7 fø·C; ~~\. '-0 8' c::..lè-.Ioc,d"
Baller lowcrcd ~ç~ 'bclow
DTW to obtain samplc
Did well dewater? Yes No Gallons actually evacuated:
Sampling Date: \\.-z.\.t',~ Sampling Time: /7-00 Depth to Water:
Sample I.D.: i"n ~ - z... Laboratory: Cal@ce Columbia Other
Analyzed for: TPtW' B@ TPij)D Ox~ates (5) \ . z. 1'>c:..... 11. \::b'b .b\ "ò¿c.:.(3'
MTBE Other: t:.. \ I c:...."'..... 1'-..",-... \....~;) \... c:>.j,
@ .
EB I.D. (if applièable): Duplicate I.D. (if applicable):
Tunc
Analyzed for: TPH-G BTEX MTBE TPH-D Oxygenates (5) Other:
D.O. (ifreq'd): Pre-purge: mg/L Post-purge: m&/L
O.R.P. (ifreq'd): Pre-purge: mV Post-purge: mV
Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (800) 545-7558
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SHELL WELL MONITORING DATA 'SHEET
BTS#: o ~ l . Site:
Sampler: Mh Date:
Well J.D.: /vttv-L Well Diameter: 2 6 8
Total Well Depth (TD): It-f~-.IS- Depth to Water (DTW): I~"C¡J
Depth to Free Product: Thiclmess of Free Product (feet):
Referenced to: PV Grade D.O. Meter (ifreq'd): ysr HACH
DTW with 80% Recharge [(Height of Water ColJcin x 0:20) + DTW]: I $0/./ ~
Purge Method; Bailer
Disposable Bailer
Positive Air Displacement .
dJe"ë1TiE"Su5merstbJS
Screened Interval: J..I -1'H,t
Waterra
Peristaltic
Extraction Pump
Other
Sampling Method:
Bailer
~ableBai~
Extraction Port
Dedicated Tubing
Other:
Ifwel] is listed as a no-purge, confinn that water level is below the top
f Dh' th 11 b d
o screen. t eIWJse, e we must e purl!e .
. Well Diameter MultiDlier Well Diameter Mullin1ier
ß·C1 S 7.6. 7 1" 0.04 4" 0.65
(Gals.) X = Gals. 2" 0.16 6" 1.47
1 Case Volume Specified Volumes Calculated Volume J" 0.31 Other rndlus1·0.163
CO~ Turbidity
Time Temp (lip) pH (mS 0 µS (NTUs) Gals. Removed Observations
I:) oj be· q '{ ~ '3 s)L{ 3sS- '1
l3 D,b by·( í..1 3~3 2- 2-r lrf
I ~ () .~ b8·/ -11 '3 t.-( .3> ,'Ç" ( 'J-7
Baller lowered :i 'below
DTW to obtoln sn¡nple
Did well dewater? Yes (NO) Gallons actually evacuated: ?-7
II ( z.,tl'O 3' ......., '.
Sampling Date: Sampling Time: J3J'-f Depth to Water: f3 ~. J-7
Sample J.D.: l\lLw /.%- Laboratory: (CáIScien~ Columbia Other
Analyzed for: ~TÈ~ MTBE~ ~enatesW Other: See )S.c..:JPE
EB I.D. (if applicable): @ Duplicate J.D. (if applicable):
Time
Analyzed for: TPH!Ò BTEX MTBE TPH-D Oxygenates (5) Other:
D.O. (ifreq'd): Pre-purge: mg/L Post-purge: mS/L
O.R.P. (ifreq'd): Pre-purge: mV Post-purge: mV
Blaine Tech Services, Inc. 1680 Rogers Ave., 5an Jose, CA 95112 (800) 545-7558
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Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (800) 545-7558
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SHELL WELL MONITORING DATA SHEET
Sampler:
Site:
'1 ï'-tG 7ZZ-L
/1/2-I/D3
BTS#:
Date:
Well J.D.:
}.Altv- 3
Well Diameter: 2
3
8
Total Well Depth (TD):
{i v· r
Depth to Water (DTW):
Depth to Free Product: Thiclmess of Free Product (feet): '
Referenced to: Gf~de' , D.O. Meter (ifreq1d): YSI
DTW with 80% Recharge [(Height of Water Column x 0.20) + DTWJ:
Purge Method: Bail~"""-/ , .------waterra Sampling Method: Bailer
. ysposable Bailer;' ",:, ~ _ ~erista.ltic~ C u;posable'~ .
~ Positive Air DispÜic~Úient Extrac~Peiiñ'P'" xtrnctlOn ort
~ Electric SUÈJJ1eŒ¡¡;¡;- O~ ~ Dedicated Tubing
---- Other:
I ¡. 11 .- 14 r I If well is listed as a no-purge, confirm that water level is below the top
f Oth· th 11 t b d'
HACH
o screen. el"Wlse, ewe mus e Dume .
Well Dinmeter Multiplier Well Diameter Multiplier
I" 0.04 4" 0.65
(Gals.) X = Gals. 2" 0.16 ( 6" 1.47
1 Case Volume Suecified Volumes Calculated Volume 3" OJ7 Other radius2 · 0.163
Condo Turbidity
Time Temp (OF) pH (mS or-{š)) (NTUs) Gals. Removed ' ¡: Oþservations
/lY D bt¿ :.:~ .' l''"-' ,
',' j () l.{ ¡ " 70 c:---
7. ( .p":':a. -'þ ¡r(¡ð
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- Boller lowered ~ 'below
, DTW to obtnln snmple
Did well qe\vater? Yes No . '<.', Gallons actually evacuated:" ,
~ ..~ r. .
\lfL.-l/\) 5 . .
Sampling'Date: Sampling Time: IIYO. Depth to Water: . ",
I ~~
Sample ¡.D.: M.w-3 Laboratory: Columbia Other
- ,c;,.,. r - ____ . !!.;;¿~ J'!1
Analyzed for: (TPH:cy~" . M~BE (fPH:9J ~ygenate3 ~ Other: 5e.e Sœ> ue
.", '@ Duplicatè J.D. (if applicable): ¡
EB J.D. (if applicable): " Tim.
"-
Analyzed for: TPH-G BTEX MTBE TPH-D. O~ygenates (5) Other:
mg/t .. mg/t
D.O. (ifreq'd): Pre-purge: ~ost-purge:
O.R.P. (ifreq'd): Pre-purge: mV Post-purge: mV
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SHELL WELL MONITORING DATA SHEET
BTS #: D
Sampler:
Well J.D.:
Total Well Depth (TD): 1 ~ '-f.-cfS-
Site:
Date:
Well Diameter: 2
6 8
Depth to Water (DTW):
Depth to Free Product: Thiclmess of Free Product (feet):
Referenced to: vc Grade D.O. Meter (ifreq'd): YSI HACH
r~7l . /1,
DTW with 80% Recharge [(Height of Water Column x 0.20) + DTW]: ./ 3 '
Purge Method:
Waterra
Peristaltic
Extraction Pump
Other
Samp1ing Method:
Bailer
':m5pg¡l1hl~~
Extraction Port
Dedicated Tubing
Screened Interval: 1'2.- () - i',(..s-'
Otber:
If well is listed as a no-purge, confinn that water level is .below the top
f Otb· th 11 t b d
o screen. erwlse, ewe mus e OUfl!e .
Well Dinmeter MultiDlier' Well Diameter MultiDlÎer
~(Gals.)X 3 Z-b. 7 Gals. I" 0.04 4" 0.65
= 2" 0.16 6" 1.47
) Case Volume Specified Volumes Calculated Volume 3" 0.37 Other mdiu~ + 0.163
COts» Turbidity
Time Temp (ap) . pH (mS 0 µS) (NTUs) Gals. Removed Observations
~.( 7/L .....- S'1(
1 3 't,Ï- ~77 c¡
131-r 61- ¡ -¡, I 2JL 110 1 }t
}32--f ~-o '1. I ?-ff3 íl ?-7
-
Bllller lowered j 'below
~ DTW ta obtllln slImple
Did well dewater? Yes No) Gallons actually evacuated: ~7
fJ/2./lu3 -
Sampling Date: Sampling Time: ) 3 ~ Æ Depth to Water: lJ (, I L./
Sample I.D.: M IV~ 3 I':~ Laboratory: {Caméiencv Columbia Other
'I ~
Analyzed for: ~ MTBE (fPH-E-J (dXÿgena~ Other: Sæ- Swpe
EB I.D. (if applicable): @ Duplicate J.D. (if applicable):
Time
Analyzed for: TPH-G BTEX MTBE TPH-D Oxygenates (5) Other;
D.O. (ifreq'd): Pre-purge: mS/L Post-purge: m¡¡/L
O.R.P. (ifreq'd): . Pre-purge: mY Post-purge: mY
Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (800) 545-7558
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SHELL WELL MONITORING DATA SHEET
BTS#: 0 Site: b' 222-
Sampler: Date: 11/2110 ~
WellI.D.: Well Diameter: 2 3 6 8
Total Well Depth (TD): \ l.f L{.. b ? Depth to Water (DTW): 13o.t(~
Depth to Free Product: Thic1mess of Free Product (feet):
Referenced to: ~ . Grade D.O. Meter (ifreq'd): YSI BACH
DTW with 80% Recharge [(Height of Water Column xO.20) + DTW]:
Purge Method: iler
nis osable Bailer
Positi Air Displacement
Electric bmersible
" Waterra
~erista]tic
Extracti ÒÌT-~mp
Otller
Sampling Method: Bailer
~õšãb1ëB~,
Extraction Port
Dedicated Tubing
. 1 I I
Screened lnterval: J...ð - ..., \
Other:
If well is listed as a no-purge, confinn that water level is below the top
f Oth th II tb d
. 0 screen. efWlse, ewe mus e DUrge .
NO prJ~ Well Diameler Multiplier Well Diameter Multiplier
I" 0.04 4" 0.65
(Oals.) X = Gals. 2" 0.16 6" 1.47
1 Case Volume SDecified Volumes Calculated Volume 3" 0.37 Other mdius1 · 0.163
Condo Turbidity
Time . Temp (OF) pH (mS or µS) (NTUs) Gals. Removed Observations
It CjQ GO.L 7. I sf7 \~ - ~le. () II VV{"L ~
\ J
.,.
..
Baller lowered , 'below
, DTW to obtain sample
Did well dewater? ¥es-Nu- Gallons actually evacuated: .-
Sampling Date: {I!Z/!O ~ Sampling Time: ilISO Depth to Water: - ",.
Laboratory: é&lScienc~ Columbia .,
Sample J.D.:, ¡v¡ vJ-Lf Other ,/
Analyzed for: (TP~~ MTBE ~ (Ûxyg~nates (5)) Other: ,~/~ ~
@ ,
EB J.D. (if applicable): TIm. Duplicate J.D. (if applicable):
Analyzed for: TPH-G BTEX MTBE TPH-D Oxygenates (5) Other:
D.O. (ifreq'd): Pre-purge: maIL Post-purge: mg/L
O.R.P. .(ifreq'd): Pre-purge: mV Post-purge: mV
Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (800) 545..7558
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ApPENDIX B
FIELD PROCEDURES
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BLAINE 1680 ROGERS AVENUE
TECH SERVICES"" SAN JOSE, CA 95112-1105
(408) 573-7771 FAX
(408) 573-0555 PHONE
CONTRACTOR'S LICENSE #746684
www.blainetech.com
December 5, 2003
, Tony Palagyi
Shell Oil Products US
P.O. Box 7869
Burbank, CA 91510-7869
Fourth Quarter 2003 Groundwater Monitoring at
Shell-branded Service Station
5321 Stockdale Highway
Bakersfield, CA
Monitoring perfonned on November 21, 2003
Groundwater Monitoring Report 031121-DB~1
This report covers the routine monitoring of groundwater wells at this Shell-branded facility. In
accordance with standard procedures that confonn to Regional Water Quality Control Board
requirements, routine field data collection includes depth to water, total well depth, thiclmess of
any separate immiscible layer, water column volume, calculated purge volume (if applicable),
elapsed evacuation time (if applicable), total volume of water removed (if applicable), and
standard water parameter instrument readings. Sample material is collected, contained, stored,
and transported to the laboratory in confonnance with EP A standards. Purgewater (if applicable)
is, likewise, collected and transported to D.K. Environmental.
Basic field infonnation is presented alongside analytical values excerpted from the laboratory
report in the cumulative table of WELL CONCENTRATIONS. The full analytical report for
the mo~t recent samples and the field data sheets are attached to this report.
At a minimum, Blaine Tech Services, Inc. field personnel are certified on completion of a forty-
hour Hazardous Materials and Emergency Response training course per 29 CFR 1910.120. Field
personnel are also enrolled in arumal eight-hour refresher courses.
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Blaine Tech Services, Inc. conducts sampling and documentation assignments ofthis type as an
independent third paI1y. Our activities at this site consisted of objective data and sample
collecti,on only. No interpretation of analytical results, defining of hydrological conditions or
fonnulation of recommendations was perfonned.
Please call if you have any questions.
Yours truly,
Francis Thie
Vice President
FT /ks
attachments: Cumulative Table of WELL CONCENTRATIONS
Certified Analytical Report
Field Data Sheets
cc: Kathryn Ewing
Delta Environmental Consu1tànts, Inc.
911 S. Primrose Ave., Suite K
Monrovia, CA 910 16
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BLAINE TECH SERVICES, INC.
METHODS AND PROCEDURES
FOR THE ROUTINE MONITORING OF
GROUND'vVATER WELLS AT SHELL SITES
Blaine Jech Services, Inc. performs environmental sampling and documentatiOn as an
independent third party. We specialize in groundwater monitoring assignments and inte'ntionally
limit the scope of our services to those êentered on the generation of objective information. , .
Tò avoid conflicts of intðrest, Blaine Tech Services, Inc. personnel do not evaluate or interpret
the information we collect. . As a state licensed contractor (C":57 Well drilling -Water- 746684 )
performing strictly technical services, we do not make any professional recommendations and
, perform no cònsultiilg.;ofany kind.
SAMPLING PROCEDURES OVERVIEW
SAFETY
AU groundWater'monitorÎng assignments pel'foffned fOr Shell comply with Shell's sàfety
. .' . ' f. .
'guidelines, 29 CFR 1910.120 and S8-198 Injury arid Illness Prevention Program (IIPP), All
Fiëld Tecihnicians receive the full 40-hour 29CFR 1910.120 OSHA SARA HAZWOPER course,
, medical clearance and on-the-job training prior to commencing ariy work on any Shell site.
. .
INSPECTION ANO GAUGING
Wells are iryspected prior to evacuation and sampling. The conditIon of the wellhead is checked
and noted according to a wellhead i~spection checklist. '
, '.
Standard 'measurements include the depth to water (OTW) and the totai well depth (TO)
obtained with industry standard electronic water level indicators that are graduated in
, incremerits Of hundredths of a foot. '
Thè water in each well is inspected for the presencè of immíscibles. When free product is
suspeèted, its presence is confirmed ùsing an electronic intérface probe (e.g. MMC). No
. samples are cOllecte,d fròm a well containing over twb-hundredths'of a foot (().02') of product.
EVACUATION
';:\Dépth to watermeasurêm,é'nfs are collécted by oúrp¡3'rsönriel prior to purgihg'and minImum'
;·purge volumes are calcLÍrated anew fOr each well ba,$ed on the height of the water column and
,":the diameter of the' welL· Expectedpurgevolumesäh:~ never less than three 'Case volumes and
àre sefat no less than fOur case volumes in some jurisdictions;
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Blaine Tech Sery-îces, Ir:-9:.· .
Standard Methods & Procedures '
Page 1
Sbell Oil Pròducts US
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Well purging, devices are selected on the basis of the well diameter,and the total volume to be
evacuated. ''In most cas'es the well will be purged using an electric submersible pump (i.e.
. Grundfos) suspended near (but not touching) the bottom of the well.
PARAMETER STABILIZATION
Well purging completion standards include minimum purge volumes, but additionally require
stabilization of specific groundwater parameters prior to sample collection. Typit;al'groundwater
parameters used to measure stabiiity àre electrical cónductivity¡pH, and temperature.
Instrument readings are obtained at regUlar intervals during the evacuation process (no less
than once per case volume). '
Stabilization standards for routine quarterly monitoring of fuel sites include thèfollowing:
. Temperature is considered to have stabilized when successive readings do not fluctuate more
, thàn +/- 1 degree Celsius. Electrical conductivity is considered stable When sucéessive , .
, readings are within 10%. pH is considered to be stable when successl'oJe readings remain
constant or vary n'o more than 0.2 of a pH unit.
DEWA TERED WELLS
Normal eVÇ3cuation removes no less than three case volumes of water from the well. However,
less water may be removed'.in cases where the well dewaters and does not immediately
recharge; . .
MEASURING RECHARGE
/
Upon completion of well purging, a depth to water measurement is collected and notated to
ensure that the well has recharged to within 80% of i!s static, pre-purge level prior to, sampling.
Wells that do not immediately show 80% recharge or dewatered wells will be allowed a '
minimum of 2 hours to recharge prior to sampling. The water level at time of sampling will be
noted.
PURGEWATER CONTAINMENT
All non-hazardous þurgewater evacuated from each groundwater monitoring well is captured
and contained in òn-board storage tanks on the Sampling Vehicle and/or special vváter hauling
trailers. Effluentfrom the decontaminatioJiofrèusàble apparatus (sounders, electric pumps and
hoses etc.), consisting of groundwater combined with deionized watèt and non~phosphate soap,
is also captured ánd pumped into effluent tanks. .
'"
. ,
NOh-hazardous purgewater'is transported Under stàndard Bill of Ladingdocumentationtoa ,,"
,~Iaine Tech Service~, Inc.: facility before bei,~~~,tranSPQrted toa Shell~Rproved dispåsalfacility'. ",-
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Blaine Tech Se~f~es, Inc.
Standard Methods &. Procedures
Shell oil Products US
Page 2
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SAMPLE COLLECTION DEVICES
, .
All samples are collected using a stainless steel, Teflon or disposable baile(s.
SAMPLE CONTAINERS
Sample material is decanted directly from the sampling bailer into sample containers provided
by the laboratory that will analyze the samples. The transfer of sample material from the bailer
to the sample container conforms to specifications contained in the US,EPA T.E.G.D. The type
of sample container, material of construction; method of closure and filling requirenients are'
. specific to the intended analysis. Chemicals needed to preserve the sample material are
commonly placed inside the sample containers by the laboratory or glassware vendor prior to
delivery of the bottle to our personnel. the laboratory sets the humber of replicate containers.
TRIP BLANKS
Trip Blanks" if requested, are taken to the site and kept inside the sample cooler for the duration '
of the event They are turned over to the laboratory for analysis with the samples from that site.
DUPLICATES
Duplicates¡' if requested, ,may be collected at a site. The Field Technician uses their discretion
in choosing the well at which the Duplicate is ,collectèd, typicãlly one suspected of containing
measurable contaminants, . The Duplicate sample is labeled "DUP" and the time of collectron is
o.i11ittèd from the COC, thus rendering the sample blind.
SAMPLE STORAGE
AÎI sample containers ani promptly placed in food gradè ice chests for storage ih the field and.
transport (direct or via bur facility) to the designated analytical laboratory. These iêe chests'
contain quantities of restaurant grade ice ás a refrigerant material. The samples are maintained
in either an ice chest or a refrigerator until relinquished ilito the custody of the laboratorY or
laboratory courier. . ,
DOCUMÈNTATION CONVENTIONS
, , ,
A label must be. affixed to all sample containers. In most cases these labels are generated by
our office persohhel and are partially preprinted. Labels c8h 'also be hand written by OUr field
. personnel. The site is ide'ntified with the store number and site àddress, as is the particular
grOl~ndwater well from which the sample is drawn (e.g. MW-1, MW,2¡ 8'-1 etc.). The time and
. date Òf samplecollettiÓn alohg with the ,initials of the person who.colleCts thesamþle are
handwrittenonfo _ the label. ' . . ':,:.,:~,; . . .
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Chain ~f C~~t~dY re~~rds are crêated Using client specific prepr{gt~d for~sföllowing USEPA
specifications.
.. "
B.l~:iIie T.~2~t?ervlèes, Inc.
Shell Oil Piòduds 'uS
Page3
Standard Methocls &: Procedures
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Bill of Lading records are contemporaneous records created in the field at the site where the
non.,hazardous purgewater is gènerated. Field Technicians ,use preprinted Bill of Lading forms.
DECONTAMINATION
All equipment is brought to the site in clean and serviceable condition and is cleaned after use
in eâch well and before subsequent use in any other we". Equipment is decontaminated before
leaving the site. '
The primary decontamination device is a commercial steam cleaner. The steam cleaner is de-
tuned to function as a hot pressure washer that is then operated with high quality deionized
water that is produced at our facility and stored onboard our sampfíng vehicle. Cleàning is
facilitated by the use of proprietary fixtures and devices included in the patented workstation
(U.S. Patent 5,535,775) that is incorporated in each sampling vehicle; The steam cleaner is
used to decon'reels, pumps and bailers.
Any'sensitive equipment or parts (I.e. Dissolved Oxygen sehsor membrari'e, water level'
,indicator, etc.) that cannot be washed using the high prèssure water, will be sprayed with a nOh-
'phosþhate soap arid dêionized water solution and rinsed with deionized water: ' ' .
DISSOLVED OXYGEN READINGS
. .. .
Dissolved Oxygen readings are taken pre- and/or post-purge using YS¡ meters (e.g. YS( Model
54, 58 or 95) or HACH field test kit~, '
The YSI meters are equipped with a stirring deVice that enables them to collect accUrate in-situ
readings. The probe/stirring devices are modified tó allow downhol.8 measurements to be taken
ftom wells with diameters as srl!a'" as two inches. The probe and reel is decontaminated
between wells as descdbed åböve. The meter is calibrated' between wells as per the
instructions in thé operating manual. The probe and stirrer is lowered i¡;¡to thë water column.
, The reading is allOwed to stabilize prior to collection.
ÒXYIDA TON REDUCTION POTENTIAL READINGS
All readings areDbt~¡~ed with either Corning or Myron-L meters (e.g. Corning ÒRp.:.65 or a
Myron'-!,. Ultrameter GP). : The meter is cleaned between wells as described above. The meter
is calibrated at the start of each dayaccordJng to the instruction manual.
FERROUS IRON MEASUREMENTS
All field m$asl.Jrements are collected at time of sampling with a HACH t$st kit.
...
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Blajne Tech Setvices,Iric.
'. . Standard Methods & Procedures .
Shell Oil Products US. " Page 4
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ApPENDIX C
WASTE DISPOSAL DOCUMENTS .
I
NAME
NO. '636503
NON-HAZARDOUS WASTE DATA FORM
GENERATING SITE:
wrc# 5321 S1ø~kk- :0.
fÞt 11,«5~'eb{ CA NO.
ni'
, ,-
c¡(
I
SHELL OIL PRODUqs US
,P.O. BOX 7869
ADDRESS
BURBANK, CA 91.5:LQ-7B69.
CITY, STATE, ZJP AITN: "ìOlllr fl:.t Iq~f)'
CONTAINERS: ND. VOLUME.~.5.~J~(.p./
'!.-,/ TANK 0 DUMP 0 0 0
ðt TRUCK TRUCK ' DRUMS CARTONS' OTHER
NON-HAZARDOUS GROUNDWATER
PHONE NO.
WEIGHT
TYPE:·
WASTE DESCRIPTION
COMF~MWASTE
PPM
99-1~OO/ø
GENERATING PROCESS
COM§1ÄWlI OF WASTE
PPM
'11>'
1
I
,
PURGED GROUNDWATER
1.
5.
2.
&,
INCIDENT#' 0( 7'f 6 7.lZX../
j r
¡
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TPH
<1%
3,
7.
BESI :fI:
4.
PROPERTIES:
7 :La XX B."·
pH _ 0 SOLID 0 LIQUlO 0 SLUpGE 0 ",SlURRY 0 OTHER
24-HOUR EMERGENCY PHONE (BOO) 424-9300
HANOLING INSTRUCTIONS:
NIETO AND SONS TRUCKl:N'G, INC.
of SOP US) J-""Z
, IZlc{.l./
THE GENERATOR CERTIFIES THAT THE
WASTE AS DESCRIBED IS 100%
NON·HAZARDOUS.
12B1 BREA CANYON ROAD
FIRST TRANSPORTER
AODRESS
, í
BRB\. CALIFORNIA 92821
.
20360 Gramercy Ptr.ce
(310) 782·2-485
PICK P DATE
CITY, STATE, ZIP
(114) 990-6855
PHONE NO.
EPA
1.0.
NO,
OATE
TRUCK UNIT, I.D. NO.
DIK ENVIRONMENTAL
3650 E. 261H STREET
TYPED OR PRINTED FULL NAME & SIGNATURE
ADDRESS
,DISPOSAL METHOD
o !-ANDFllL 0 OTHER
!
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I
LOS ANGELES, CA. 90023
CITY, STATE, ZIP .
(323) 268-5056
PHONE NO.
TYPÈD OR PRINTED FULL NAME & SII3NATURE
OATE
OLD/NEW L A TONS
S 8
RT/CD HWOF
NONE
\'
DISCREPANCY
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ApPENDIX D
LABORATORY REPORT AND
CHAIN-OF-CUSTODY DOCUMENTS
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I.:alscience
I::, nvironmental
Laboratories, Inc.
December 02, 2003
Nick Sudano
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Subject: Calscience Work Order No.:
Client Reference:
03-11-1386
5321 Stockdale Highway, Bakersfield, CA
Dear Client:
Enclosed is an analytical report for the above·referenced project. The samples
included in this report were received 11/21/2003 and analyzed in accordance with
the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the
guidelines established in our Quality Assurance Program Manual, applicable standard
operating procedures, and other related documentation. The original report of any
subcontracted analysis is provided herein, and follows the standard Calscience data
package. The results in this analytical report are limited to the samples tested and any
reproduction thereof must be made in its entirety.
If you have any questions regarding this report, please do not hesitate to contact
the undersigned.
Michael . Crisostomo
Quality A surance Manager
7440 Lincoln Way, Garden Grove, CA 92841-1432 . TEL: (714) 895-5494 . FAX: (714) 894-7501
_......,.~..~..... ..... ........,-.....
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I_...~____.__...._________~_.._...____,_______..___________......__,___._...,...._,......, ...,·.·".u. ,....... .
(:alscience
I::ffEp vironmen tal
Laboratories, Inc.
December 02, 2003
Nick Sudano
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Subject: Calscience Work Order No.:
Client Reference:
03-11-1385
5321 Stockdale Highway, Bakersfield, CA
Dear Client:
Enclosed is an analytical report for the above-referenced project. The samples
included in this report were received 11/21/2003 and analyzed in accordance with
the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the
guidelines established .in our Quality Assurance Program Manual, applicable standard
operating procedures, and other related documentation. The original rl¡!port of any
subcontracted analysis is provided herein, and follows the standard Calscience data
package. The results in this analytical report are limited to the samples tested and any
reproduction thereof must be made in its entirety,.
If you have any questions regarding this report, please do not hesitate to contact
the undersigned.
. risostomo
ssurance Manager
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
. . .. ".. ...
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1...= a/science
I::~nvironmenta/
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
I
Date Received:
Work Order No:
Preparation:
Method:
11/21/03
03-11-1385
EPA 3005A Filt.
EPA 60108
I
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
I
Lab Sample Date Date Date
Number Collected Matrix Prepared Analyzed QC Batch ID
I
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Parameter Result RL DF Q!lID Units
Lead NO 0.0100 mglL
~í~~~tjf~~Li¡?(,~~
Parameter BäY!! B.b DF Qual Units
Lead ND 0.0100 mg/L
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Parameter Result B!. OF Qual Units
Lead ND 0.0100 mg/L
1~~j~~~p(,:'t'-'{
Parameter Result RL DF Qual Units
Lead ND 0.0100 mg/L
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Parameter
Result
ND
RL
0.0100
DF
Q!lID
Units
I
Lead
mgIL
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I
RL - Reporting Limit, OF - Dilution Factor, Qual· Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894·7501
1..--,-'_______'.______.__.___... ,...,__,.____,______..____., ......_.._._____,_" .__._.______.."...._,_.w... ....... .. .
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L ã/~cience
I:. nvironmental
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received:
Work Order No:
Preparation:
Method:
11/21/03
03-11-1385
EPA 50308
DHS LUFT
,Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 2
Lab Sample
Date
Analyzed QC Batch ID
Parameter Result RL DF ~ Units
TPH as Gasoline ND 50 uglL
Surroaates: ~ Control QyID
Limits
1,4-Bromofluorobenzene 55 49-133
Parameter Result ill. DF QYSI UDit§
TPH as. Gasoline ND 50 ug/L
Surroaates: ~ ~ gym
b!mi!§
1,4-Bromofluorobenzene 72 49-133
,,: ~. .,t~~~~~Jf.11~_~:1A;·~~;~;~i~ii;~~'
Parameter 8m!!! ill: Q.E Qual J.!r!.I!§
TPH as Gasoline ND 50 ug/L
Surroaates: ~ Control Qual
Limits
1,4-Bromofluorobenzene 70 49~133
Parameter Result RL Q.E QYSI UDit§
TPH as Gasoline ND 50 ug/L
Surroaates' ~ .!Æ!!rQL Qual
Limits
1,4-Bromotluorobenzene 69 49-133
RL - Reporting Limit, DF - Dilution Faclor, Qual - Qualifiers
7440 Lincoln Way, Gardén Grove, CA 92841·1432 · TEL: (714) 895·5494 · FAX: (714) 894·7501
I,
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(.;a/science
1:,1'vironmental
Laboratories, Inc.
Analytical Report
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance. CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
11/21/03
03-11-1385
EPA 5030B
DHS LUFT
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 2 of 2
Client Sample Number
Lab Sample
Number
Date
Prepared
·QC Batch ID
Date
Analyzed
Date
Collected
Matrix
Parameter
Result
Qual
Units
RL
DF
TPH as Gasoline
ND
50
uglL
Surroaates:
Qual
REC(%)
Control
~
49-133
1,4-Bromofluorobenzene
89
RL - Reporting Umit ,
OF . Dilution Factor ,
Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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&;alscience
'=l'vironmental
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytic~1 Report
Date Received:
Work Order No:
Preparation:
Method:
11/21/03
03-11-1385
EPA 3510C
DHS LUFT
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 2
Lab Sample
Number
Óate
Prepared
, ac Batch ID
Date
Collected
Matrix
Parameter Result RL OF .Q!m! J.!!:!!§
TPH as Diesel ND 1000 ug/L
Surrooates: REC(%) Control Qual
Limits
Decachloroblphenyl 84 51-141
Parameter B§yll Bb OF Q!.!š!! Units
TPH as Diesel ND 1000 ug/L
Surrocates: REC(%) Control .Q!m!
limits
Decachlorobiphenyl 87 51-141
:,~~':','ï91~~!~i~~~1;;:1~~{j~!~
Parameter Result RL OF g¡gJ ~
TPH as Diesel ND 1000 ug/L
Surrocates: REC (%) Control ~
.b!.Inim
Decachloroblphenyl 74 51-141
Parameter Result RL .QE g¡gJ Jlni!§
TPH as Diesel ND 1000 ug/L
Surrooates: ~ Control Qual
Limits
Oecachlorobiphenyl 78 51-141
Rl - Reporting limit
DF . Dilution Factor, Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894·7501
1.._,.,-,,-,_.....,......,. .'
. .........,.....- ." ...'....._..,....-~,-........._.....-...._-..,............,_....,,_.. ....... '.-~.....,......__.~~_.~-..,......._....--.. ...-..............-. . .... . -,.." .
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(,.ãlscience
1!/:,1'vironmental
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received:
Work Order No:
Preparation:
Method:
11/21/03
03-11-1385
EPA3510C
DHS LUFT
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 2 of 2
Client Sample Number
Lab Sample
Number
Date Date
Prepared Analyzed QC Batch ID
Date
Collected
Matrix
Parameter
Result RL DF Qual Units
ND 1000 ug/L
REC(%) Control Q!!ID
.I.!IIIlliì
93 51-141
TPH as Diesel
Surroaates:
Decachloroblphenyl
RL - Reporting Limit ,
DF· Dilution Factor ,
Qual· Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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~=alscience
I:!;l'vironmental Analytical Report
I. aboratories, Inc.
Blaine Tech Services, Inc Date Received: 11/21/03
20360 Gramercy Place Work Order No: 03-11-1385
Torrance, CA 90501-1511 Preparation: EPA 5030B
Method: EPA 8260B
Project: 5321 Stockdale Highway, Bakersfield, CA Page 1 of 5
Date
Client Sample Number
Parameter Result fib DF Qual Units Parameter Result RL DF Q!mI !Jnl!§
Acetone ND 10 1 ug/L 1,1.Dlchloropropene ND . 1.0 1 uglL
Benzene ND 0.50 1 ug/L c-1,3·Dichloropropene ND 0.50 1 uglL
Bromobenzene ND 1.0 1 uglL t·1,3-Dichloropropene ND 0.50 1 uglL
Bromochloromethane ND 1.0 1 ug/L Ethylbenzene NO 1.0 1 ug/L
Bromodichloromethane ND 1.0 1 uglL 2-Hexanone ND 10 1 ug/L
Bromoform ND 1.0 1 uglL Isopropylbenzene ND 1.0 1 uglL
Bromomethane NO 10 1 uglL p-Isopropyltoluene ND 1.0 1 ug/L
2·Butanone ND 10 1 uglL Methylene Chloride NO 10 1 uglL
n"Butylbenzene ND 1.0 1 ug/L 4-Methyt-2-Pentanone NO 10 1 ugIL
sec-Butylbenzene NO 1.0 1 ug/L Naphthalene ND 10 1 uglL
tert-Butytbenzene ND 1.0 1 uglL n-Propytbenzene ND 1.0 1 uglL
Carbon Disulfide ND 10 1 ug/L Styrene NO 1.0 1 uglL
Carbon Tetrachloride ND 0.50 1 uglL 1,1,1,2- Tetrachloroethane ND 1.0 1 uglL
Chlorobenzene NO 1.0 1 uglL 1,1,2,2-Tetrachloroethane ND 1.0 1 ug/L
Chloroethane ND 1.0 1 uglL T etrachloroethene NO 1.0 1 uglL
Chloroform NO 1.0 1 uglL Toluene NO 1.0 1 ug/L
Chloromethane ND 10 1 ug/L 1,2,3-Trichlorobenzene ND 1.0 1 uglL
2-Chlorotoluene ND 1.0 1 ug/L 1,2,4- Trichlorobenzene ND 1.0 1 ug/L
4-Chlorotoluene NO 1.0 1 ug/L 1,1,1· Trichloroethane ND 1.0 1 ug/L
Dibromochloromethane NO 1.0 1 ug/L 1 ,,1 ,2-Trichloroethane NO 1.0 1 ug/L
1,2-0ibromo-3-Chloropropane NO 5.0 1 ug/L Trlchloroethene ND 1,0 1 uglL
1,2-0ibromoethane NO 1.0 1 ug/L Trichlorofluoromethane ND 10 1 uglL
Oibromomethane NO 1.0 1 ug/L 1,2,3- T ric:h1oropropane NO 5.0 1 ug/L
1,2-Dichlorobenzene ND 1.0 1 ug/L 1,2,4- Trlmethytbenzene ND 1.0 1 ug/L
1,3-0ichlorobenzene ND 1.0 1 ug/L 1,3,5- Trimethylbenzene ND 1.0 1 ug/L
1,4-0ichlorobenzene ND 1.0 1 ug/L Vinyl Acetate ND 10 1 ug/L
Oichlorodifluoromethane NO 1.0 1 ug/L Vinyl Chloride NO 0.50 1 ug/L
1,1-0lchloroethane NO 1.0 1 ug/L p/m-Xytene NO 1.0 1 ug/L
1,2-0ichloroethane NO 0.50 1 ug/L o-Xylene ND 1.0 1 ug/L
1,1-0ichloroethene NO 1.0 1 ug/L Methyl-t-Butyl Ether (MTBE) NO 1.0 1 ug/L
c-1,2-0ichloroethene NO 1.0 1 ug/L Tert-Butyt Alcohol (TBA) NO 10 1 uglL
t-1,2-0Ichloroethene ND 1.0 1 uglL Oiisopropyl Ether (OIPE) NO 2.0 1 ug/L
1,2-0ichloropropane NO 1.0 1 ug/L Ethyl-t-Butyl Ether (ETBE) ND 2.0 1 uglL
1,3-0ichloropropane NO 1.0 1 ug/L Tert-Amyl-Methyl Ether (TAME) ND 2.0 1 uglL
2,2-0ichloropropane NO 1.0 1 uglL
Surrocates: !illLOO Control º"'ª' Surroaates: REC(%) Control Qual
Limits
Oibromoßuoromethane 116 84-120 Toluene-d8 101 . 91-109
1,4-Bromoßuorobenzene 95 84-1 08
RL - Reporting Limit, DF - Dilution Factor. Qual· Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
1.,...,_,.____.....'_..___...,.,.. ,
.... .~~. 4......_..~.·~... ..' .. '._ M_. _...__ ._.",._..~__............._.. __.M...__.~._........... ...~... '~'_""_ø""._.~·."_'" ._.... ._. "R" .,,_........._.ø_... ..MO........ . .. . . ........
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1....)/science
I::, nvironmental
Laboratories, Inc.
Analytical Report
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Pr~paration:
Method:
11/21/03
03-11-1385
EPA 50308
EPA 82608
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 2 of 5
Parameter Result RL DF ~ Units Parameter Bmill B!, ill: Qual Units
Acetone NO 10 1 ug/L 1,1-0lchloropropene NO 1.0 1 uglL
Benzene ND 0.50 1 ug/L c-1,3-0ichloropropene NO 0,50 1 ug/L
Bromobenzene NO 1.0 1 ug/L t-1,3-0Ichloropropene NO 0.50 1 ug/L
Bromochloromethane NO 1.0 1 ug/L Ethylbenzene NO 1.0 1 uglL
Bromodichloromethane NO 1.0 1 ug/L 2-Hexanone NO 10 1 ug/L
Bromoform NO 1.0 1 ug/L Isopropylbenzene NO 1.0 1 ugIL
Bromomethane ND 10 1 uglL p-Isopropyltoluene NO 1.0 1 ug/L
2-Butanone NO 10 1 ug/L Methylene Chloride ND 10 1 uglL
n-Butylbenzene NO 1.0 1 uglL 4-Methyl-2-Pentanone NO 10 1 uglL
sec-Butylbenzene NO 1.0 1 ugIL Naphthalene ND 10 1 ugIL
tert-Butylbenzene NO 1.0 1 ugIL n-Propylbenzene NO 1.0 1 uglL
Carbon Disulfide NO 10 1 uglL Styrene ND 1.0 1 uglL
Carbon Tetrachloride NO 0.50 1 uglL 1,1,1,2-Tetrachloroethane NO 1.0 1 ug/L
Chlorobenzene ND 1.0 1 ug/L 1,1,2,2-Tetrachloroethane NO 1.0 1 ug/L
Chloroethane ND 1.0 1 ug/L Tetrachloroethene ND 1.0 1 ug/L
Chloroform NO 1.0 1 ug/L Toluene NO 1.0 1 ug/L
Chloromethane NO 10 1 ug/L 1,2,3- Trichlorobenzene NO 1.0 1 ug/L
2-Chlorotoluene ND 1.0 1 ug/L 1,2.4- Trichlorobenzene ND 1.0 1 uglL
4-Chlorotoluene NO 1.0 1 ug/L 1,1,1- Trichloroethane NO 1.0 1 uglL
Oibromochloromethane NO 1.0 1 uglL 1,1,2- Trichloroethane , NO .1.0 1 uglL
1,2-0ibromo-3-Chloropropane NO 5.0 1 ug/L Trlchloroethene NO 1.0 1 ug/L
1,2-0ibromoethane NO 1,0 1 ug/L Trichlorofluoromethane NO 10 1 ug/L
Oibromomethane NO 1.0 1 ug/L 1,2,3- Trichloropropane NO 5.0 1 uglL
1,2-0ichlorobenzene NO 1.0 1 uglL 1,2,4- Trimethylbenzene ND 1.0 1 uglL
1,3·DichlorObenzene NO 1.0 1 uglL 1,3,5-Trimethylbenzene NO 1.0 1 uglL
1,4-0ichlorobenzene NO 1.0 1 uglL Vinyl Acetate ND 10 1 ugll
Oichlorodifluoromethane NO 1.0 1 ug/L Vinyl Chloride NO 0.50 1 uglL
1,1-0lchloroethane ND 1.0 1 uglL p/m-Xylene ND 1.0 1 uglL
1,2-Dlchloroethane ND 0.50 1 ug/L o-Xylene ND 1.0 1 uglL
1,1·Dichloroethene ND 1.0 1 ug/L Methyl-t·Butyf Ether (MTBE) ND 1.0 1 uglL
c-1,2-Dlchloroethene ND 1.0 1 ug/L Tert-Butyf Alcohol (TBA) ND 10 1 ug/L
t-1,2-Dichloroethene ND 1.0 1 ug/L Oilsopropyl Ether (OIPE) NO 2.0 1 ug/L
1,2-Dichloropropane ND 1.0 1 ug/L Ethyl-t-Butyf Ether (ETBE) NO 2.0 1 ug/L
1,3-Dlchloropropane ND 1.0 1 uglL Tert-Amyl-Methyl Ether (TAME) ND 2.0 1 ug/L
2,2-Dichloropropane ND 1.0 1 ug/l
Surrooates: ,RECC%) Qm!rQL Qual Surrooates: REC f%) Control .Qlli!!
Limits
Dlbromofluoromethane 113 84-120 Toluene-d8 106 91-109
1,4-Bromofluorobenzene 97 84-108
RL - Reporting Limit ,
DF . Dilution Factor, Qual- Qualifiers
7440 Lincoln Way, Garden Grove, CA92841-1432
. TEL: (714) 895-5494 ·
FAX: (714) 894-7501
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I c...=aISCience
I:J'Vironmental
I Analytical Report
'- aboratories, Inc.
Blaine Tech Services, Inc Date Received: ~ 1/21/03
I 20360 Gramercy Place Work Order No: 03-11-1385
Torrance, CA 90501-1511 Preparation: EPA 5030B
Method: EPA 8260B
I
Project: 5321 Stockdale Highway, Bakersfield, CA Page 3 of 5
I
I Parameter Result RL OF Qual Units. Parameter Result RL OF Qual Units
Acetone NO 10 1 uglL 1,1-0ichloropropene NO 1.0 1 ug/L
Benzene ND 0.50 1 uglL c-1,3-Dichloropropene NO 0.50 1 ug/L
Bromobenzene NO 1.0 1 uglL t-1,3-0ichloropropene NO 0.50 1 uglL
I Bromochloromethane ND 1.0 1 ug/L Ethylbenzene NO 1.0 1 ug/L
Bromodlchloromethane NO 1.0 1 uglL 2-Hexanone NO 10 1 ug/L
Bromoform NO 1.0 1 uglL Isopropyfbenzene NO 1.0 1 ug/L
Bromomethane ND 10 1 uglL p-lsopropyltoluene ND 1.0 1 uglL
2-Butanone NO 10 1 ug/L Methylene Chloride ND 10 1 uglL
I n-Butylbenzene NO 1.0 1 ug/L 4-Methyf-2-Pentanone NO 10 1 uglL
sec-Butylbenzene NO 1.0 1 uglL Naphthalene NO 10 1 uglL
tert-Butylbenzene NO 1.0 1 uglL n-Propyfbenzene NO 1,0 1 uglL
Carbon Disulfide NO 10 1 uglL Styrene NO 1.0 1 ug/L
I Carbon Tetrachloride NO 0.50 1 uglL 1,1,1,2- Tetrachloroethane NO 1.0 1 uglL
Chlorobenzene NO 1.0 1 uglL 1,1,2,2-Tetrachloroethane NO 1.0 1 uglL
Chloroethane NO 1.0 1 uglL Tetrachloroethene NO 1.0 1 uglL
Chloroform ND 1.0 1 uglL Toluene ND 1.0 1 uglL
Chloromethane NO 10 1 ug/L 1,2,3- Trlchlorobenzene NO 1.0 1 ug/L
I 2-Chlorotoluene NO 1.0 1 uglL 1,2,4- Trichlorobenzene ND 1.0 1 uglL
4-Chlorotoluene ND 1.0 1 uglL 1,1,1-Trichloroethane ND 1.0 1 uglL
Dibromochloromethane NO 1.0 1 uglL 1.1,2' Trichloroethane NO 1.0 1 uglL
1,2-0Ibromo-3-Chtoropropane NO 5.0 1 ug/L Trlchloroethene ND 1.0 1 ug/L
I 1.2-0ibromoethane NO 1.0 1 uglL Trichlorofluoromethane NO 10 1 ug/L
Oibromomethane NO 1'.0 1 ug/L 1,2,3- Trlchloropropane NO 5.0 1 uglL
1.2-0ichlorobenzene NO 1.0 1 ug/L 1,2,4- Trlmethyfbenzene NO 1.0 1 ug/L
1,3-0ichlorobenzene NO 1.0 1 ug/L 1,3,5- Trimethyfbenzene NO 1.0 1 ug/L
1,4-0ichlorobenzene NO 1.0 1 ug/L Vlnyf Acetate ND 10 1 ug/L
I Olchlorodifluoromethane NO 1.0 1 uglL Vinyl Chloride NO 0.50 1 uglL
1 ,1-0Ichloroethane NO 1.0 1 uglL p/m-Xylene ND 1.0 1 ug/L
1,2-0ichloroethane NO 0.50 1 uglL o-Xylene NO' 1.0 1 ugJL
1,1-0lchloroethene NO 1.0 1 ugJL Methyl·t·Butyl Ether (MTBE) NO 1.0 1 ugJL
I c-1,2-0ichloroethene NO 1.0 1 ug/L Tert-Butyl Alcohol (TBA) NO 10 1 uglL
t-1,2.0Ichloroethene NO 1.0 1 uglL Oiisopropyl Ether (OIPE) NO 2.0 1 uglL
1,2-Dichloropropane NO 1.0 1 ug/L Ethyl-t-Butyl Ether (ETSE) NO 2.0 1 ug/L
1,3-0ichloropropane NO 1.0 1 ug/L Tert-Amyl·Methyl Ether (TAME) ND 2.0 1 ug/L
I 2,2-0ic!ìloropropane NO 1.0 1 uglL
Surroaates: REC(%} Control Qual Surrocates: REC(%) Control ~
Limits
Olbromofluoromethane 111 64-120 Toluene-d8 105 91-109
I 1,4-Bromofluorobenzene 95 64-108
I
I RL . Reporting Limit '. OF . Dilution Factor Qual· Qualifiers
7440 Lincoln Way, Garden Grove. CA 92841-1432 . TEL: (714) 895-5494 . FAX: (714)894-7501
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I.,;alscience
I::, nvironmental
ª Analytical Report
I.. aboratories, Inc.
Blaine Tech Services, Inc Date Received: 11/21/03
20360 Gramercy Place Work Order No: 03-11-1385
Torrance, CA 90501-1511 Preparation: EPA 5030B
Method: EPA 82608
Project: 5321 Stockdale Highway, Bakersfield, CA Page 4 of 5
Date
Prepared ac Batch 10
;j~'~;;:;:i:;¡~,~:~~;~~i~~(li~fii~~~~I~~'
Parameter BMY!! ßb QE Qual Units Parameter Result RL QE ili@l ~
Acetone ND 10 1 uglL 1,1-Dichloropropene NO 1.0 1 ugIL
Benzene ND 0.50 1 ug/L c-1,3-0Ichloropropene NO 0.50 1 uglL
Bromobenzene NO 1.0 1 uglL t-1,3-0íchloropropene NO 0.50' 1 ug/L
Bromochloromethane NO 1.0 1 ug/L Ethylbenzene ND 1.0 1 ug/L
Bromodlchloromethane NO 1.0 1 ug/L 2-Hexanone NO 10 1 ug/L
Bromoform NO 1.0 1 uglL lsopropylbenzene NO 1.0 1 ug/L
Bromomethane NO 10 1 uglL p-Isopropyltoluene NO 1.0 1 ug/L
2·Butanone NO 10 1 uglL Methylene Chloride ND 10 1 uglL
n-Butylbenzene NO 1.0 1 uglL 4-Methyl-2-Pentanooe NO 10 1 uglL
sec-Butylbenzene NO 1.0 1 ug/L Naphthalene NO 10 1 uglL
tert-Butylbenzene ND 1.0 1 ugIL n·Propylbenzene NO 1.0 1 ug/L
Carbon Disulfide ND 10 1 uglL Styrene NO 1.0 1 uglL
Carbon Tetrachloride NO 0.50 1 uglL 1,1,1,2- Tetrachloroethane' ND 1.0 1 uglL
Chlorobenzene ND 1.0 1 uglL 1.1,2,2-Tetrachloroethane ND 1,0 1 uglL
Chloroethane ND 1.0 1 uglL T etrachloroethene ND 1.0 1 uglL
Chloroform ND 1.0 1 uglL Totuene ND 1.0 1 ugIL
Chloromethane ND 10 1 ug/L 1,2,3- Trichlorobenzene ND 1.0 1 uglL
2-Chlorololuene ND 1.0 1 ug/L 1,2,4- Tricl1lorobenzene NO 1.0 1 uglL
4-Chlorotoluene NO 1.0 1 ug/L 1,1,1- Trichloroethane NO 1.0 1 ugIL
Olbromochloromethane NO 1.0 1 uglL 1,1,2-Trichloroethane NO 1.0 1 ug/L
1,2-Dlbromo-3-Chloropropane NO 5.0 1 uglL Trlchloroethene NO 1.0 1 ug/L
1,2-0ibromoethane NO 1.0 1 ug/L Trichlorofluoromethane NO 10 1 ug/L
Dibromomethane NO 1.0 1 uglL 1,2,3-Trichloropropane NO 5.0 1 uglL
1,2-Dichlorobenzene NO 1.0 1 uglL 1.2,4- Trimethytbenzene NO 1.0 1 uglL
1,3-0lchlorobenzene NO 1.0 1 uglL 1.3,5- Trimethytbenzene NO 1.0 1 uglL
1,4-Dichlorobenzene NO 1.0 1 uglL, Vinyl Acetate NO 10 1 uglL
Dichlorodjfluoromethane NO 1.0 1 uglL Vinyl Chloride ND 0,50 1 uglL
1.1-Dlchloroethane ND 1.0 1 ug/L p/m-Xylene NO 1.0 1 ug/L
1,2-Dichloroethane NO 0.50 1 ug/L o-Xylene NO 1.0 1 ug/L
1,1-0ichloroethene NO 1.0 1 uglL Methyl-I-Butyl Ether (MTBE) ND 1.0 1 uglL
c-1,2-Dlchloroethene NO 1.0 1 ug/L Tert·Butyl Alcohol (TBA) NO 10 1 uglL
t-1,2-0ichloroethene ND 1.0 1 ug/L Diisopropyl Ether (DIPE) NO 2.0 1 ug/L
1,2-0ichloropropane ND 1.0 1 uglL Ethyl·t-Butyl Ether (ETBE) ND 2.0 1 ug/L
1,3-0lchloropropane NO 1.0 1 uglL Tert-Amyl·Methyl Ether (TAME) NO 2,0 1 ug/L
2,2-0ichloropropane NO 1.0 1 ug/L
Surroaates: REClO/O} Control Qual Surrooales: ~ Control Qual
Limits
Oibromofluoromethane 108 84-120 Toluene-d8 105 91-109
1,4-Bromofluorobenzene 97 84-108
.
RL - Reporting limn, DF . Dilution Factor, Qual· Qualifiers
7440 Lincoln Way, Garden Grove, CA 92641-1432 · TEL: (714) 695-5494 · FAX: (714) 894-7501
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~- a/science
'1, I:j'vironmental Analytical Report
Laboratories, Inc.
I Blaine Tech Services. Inc Date Received: 11/21/03
20360 Gramercy Place Work Order No: 03-11-1385
Torrance, CA 90501-1511 Preparation: EPA 5030B
Method: EPA 82608
I
Project: 5321 Stockdale Highway, Bakersfield, CA Page 5 of 5
I Lab Sample Date Date
ac Batch ID
I Parameter Result RL OF Qual Units Parameter Result RL Q.E QyID Units
Acetone NO 10 1 ug/L Ethanol NO 100 1 ug/L
1,1-Dlchloropropene NO 1.0 1 uglL Benzene NO 0.50 1 ug/L
c-1.3-0Ichloropropene ND 0.50 1 ug/L Bromobenzene NO 1.0 1 ug/L
-I t-1.3-0ichloropropene ND 0.50 1 ug/L BromochJoromethane ND 1.0 1 ug/L
Ethylbenzene ND 1.0 1 ug/L Bromodlchloromethane ND 1.0 1 ug/L
2-Hexanone ND 10 1 ug/L Bromoform ND 1.0 1 ug/L
Isopropylbenzene NO 1.0 1 ug/L Bromomethane ND 10' 1 ug/L
p-Isopropyltoluene NO 1.0 1 ug/L 2-Butanone NO 10 1 uglL
I Methylene Chloride ND 10 1 uglL n-Butylbenzene NO 1.0 1 ug/L
4-Methyl-2-Pentanone ND 10 1 ug/L sec-Butylbenzene ND 1.0 1 ug/L
Naphthalene NO 10 1 uglL tert-Butylbenzene ND 1.0 1 uglL
n-Propylbenzene ND 1.0 1 ug/L Carbon Disulfide ND 10 1 ug/L
I Styrene ND 1.0 1 ug/L Carbon Tetrachloride ND 0.50 1 ug/L
1,1,1,2- Tetrachloroethane ND 1.0 1 uglL Chlorobenzene NO 1,0 1 ug/L
1,1,2,2- Tetrachloroethane ND 1.0 1 uglL Chloroethane ND 1,0 1 ug/L
T etrachloroethene NO 1.0 1 ug/L Chloroform NO 1,0 1 ug/L
Toluene ND 1.0 1 uglL Chloromethane ND 10 1 ug/L
I 1,2.3- Trichlorobenzene NO 1.0 1 uglL 2-Chlorotoluene NO 1.0 1 uglL
1,2,4-Trlchlorobenzene NO 1.0 1 ug/L 4-Chlorotoluene NO 1.0 1 uglL
1,1,1- Trichloroethane NO 1.0 1 uglL Oibromochloromethane NO 1.0 1 uglL
1,1,2- Trichloroethane NO 1.0 1 uglL 1,2-0ibromo-3-Chloropropane NO 5.0 1 ùglL
I' Trlchloroelhene NO 1.0 1 ug/L 1.2-0ibromoethane ND 1.0 1 ug/L
Trichlorofluoromethane ND 10 1 ug/L Oibromomelhane ND 1.0 1 uglL
1,2,3- Trichloropropane ND 5.0 1 uglL 1,2-0lchlorobenzene NO 1.0 1 uglL
1,2,4- Trlmethylbenzene ND 1.0 1 ug/L 1,3-Dlchlorobenzene NO 1.0 1 ug/L
I 1,3,5- Trimethylbenzene ND 1.0 1 ug/L 1,4-0Ichlorobenzene NO 1.0 1 ugIL
Vinyl Acetate ND 10 1 ug/L Ðlchlorodifluoromethane ND 1.0 1 ugIL
Vinyl Chloride ND 0.50 1 ug/L '1,1-0ichloroelhane ND 1.0 1 ug/L
p/m-Xylene ND 1.0 1 ug/L 1,2-Dichloroethane NO 0.50 1 ug/L
o-Xylene ND 1.0 1 ug/L 1,1-Dichloroethene ND 1.0 1 ug/L
I Methyl·t-Butyl Ether (MTBE) ND 1.0 1 ug/L c·1,2-0ichloroethene NO 1.0 1 ug/L
Tert·Butyl Alcohol (TBA) ND 10 1 uglL t-1,2-Dichloroethene ND 1.0 1 uglL
Diisopropyl Ether (DIPE) ND 2.0 1 ug/L 1.2-0Ichloropropane NO 1.0 1 ug/L
Ethyl-t-Butyl Ether (ETBE) ND 2.0 1 uglL 1,3-Dlchloropropane ND 1.0 1 ug/L
I Tert·Amyl·Methyl Ether (TAME) ND 2.0 1 uglL 2,2-0ichloropropane NO 1.0 1 uglL
Surroaates: RECIo¡.,} Control Qual Surroaates: RECio/.} Control Qual
Limits
Dibromofluoromethane 110 84-120 Toluene.cJ8 107 91·109
I 1,4-Bromofluorobenzene 97 84-108
I
I RL . Reporting Limit OF . Dilution Factor Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 . TEL: (714) 895-5494 . FAX: (714) 894-7501
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~=alscience
I!:~nvironmental
Laboratories, Inc. '
Quality Control - Spike/Spike Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
. Preparation:
Method:
11/21/03
03-11-1385
EPA 3005A Filt.
EPA 6010B
Project: 5321 Stockdale Hiqhwav. Bakersfield, CA
Quality Control Sample ID
Date
Prepared
Date
Analyzed
MS/MSD Balch
Number
Matrix
Instrument
Parameter
MS %REC
RPD
Qualifiers
MSD %REC
%REC CL
RPD CL
Lead
80-120
0-20
4
114
109
7440 Lincoln Way, Garden Grove, CA 92841·1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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~=alscience
I:.==n vironmen tal
. Laboratories, Inc.
Quality Control . LCS/LCS Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
11/21103
03-11-1385
EPA 3005A Filt.
. EPA 60108
Project:
5321 Stockdale Highway, Bakersfield. CA
Date
Date
Parameter
LCS %REC
Qualifiers
LCSD %REC
°/oREC CL
RPD
RPD CL
Lead
108
111
80-120
2
0-20
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7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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&.;a,!cience
l:,11vironmental
Laboratories, Inc.
Quality Control - Spike/Spike Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
11/21/03
03-11-1385
EPA 5030B
DHS LUFT
Project:
5321 Stockdale HiQhwav. Bakersfield. CA
Quality Control Sample ID
Date
Prepared
Date
Analyzed
MS/MSD Batch
Number .
Matrix
Instrument
Parameter
MS %REC
MSD %REC
Qualifiers
%REC CL
RPO
RPO CL
TPH as Gasoline
70-112
'0-17
87
87
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7440 Lincoln Way, Garden Grove. CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894·7501
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t..= a/science
I:: nvironmenta/
,. aboratories, Inc.
Quality Control· LCS/LCS Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
11/21/03
03-11-1385
EPA 5030B
DHS LUFT
Project:
5321 Stockdale Highway, Bakersfield, CA
Date
LCS/LCSD Batch
Number
Parameter
LCS %REC
97
BEQ.Ç!,
0-10
Qualifiers
LCSD %REC
95
TPH as Gasoline
%REC CL
72-114
RPD
7440 Lincoln Way, Garden Grove. CA 92841·1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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Quality Control- LCS/LCS Duplicate
Blaine Tech ~ervices, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
11/21/03
03-11-1385
EPA 3510C
DHS LUFT
Project:
5321 Stockdale Highway, Bakersfield, CA
Date
Parameter
LCS %REC
100
LCSD %REC
111
RPD CL
0-11
Qualifiers
%REC CL
60-132
RPD
10
TPH as Diesel
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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Quality Control· Spike/Spike Duplicate
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BlaineTech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
Project: 5321 Stockdale HiQhwav. Bakersfield. CA
Instrument
Date
Prepared
Date
Analyzed
Quality Control Sample ID
Matrix
11/21/03
03-11-1385
EPA 5030B
EPA 8260B
MS/MSD Batch
Number
I
Parameter MS %REC MSD %REC %REC CL RPD BfQ...Qb , Qualifiers
Benzene 100 101 84·120 2 0-13
Carbon Tetrachloride 110 111 72-132 1. 0-15
Chlorobenzene 99 101 87.Jl1 2 0-12
1.2·Dlchlorobenzene 96 97 66-116 1 0-13
1.1-Dlchloroethene 106 108 ' 77-137 0 0-15
Toluene 94 95 85-121 1 0-15
Trichloroethene 100 101 66-120 1 0-13
Vinyl Chloride 117 123 66-140 4 0-16
Methyl-t-Butyl Ether (MTBE) 90 93 66-128 4 0-18
Tert-Butyl Alcohol (TBA) 59 65 30-156 10 0-26
Diisopropyt Ether (DIPE) 101 105 75-123 3 0-14
Ethyl·t-Butyl Ether (ETBE) 93 97 66-132 5 0-33
Tert·Amyl-Methyl Ether (TAME) 88 93 59-131 5 0-47
Ethanol 62 87 20-176 6 0-42
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Quality Control· LCS/LCS Duplicate
RPD
3
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2
1
1
4
1
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1
14
1
1
3
2
, Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
Project: 5321 Stockdale Highway, Bakersfield, CA
11/21/03
03-11-1385
EPA 50308
EPA 8260B
Date
LCSILCSD Batch
Number
Parameter
LCS %REC
%REC CL
RPD CL
Qualifiers
LCSD %REC
Benzene
Carbon Tetrachloride
Chlorobenzene
1,2-Dichlorobenzene
1.1-Dlchloroethene
Toluene
Trichloroethene
Vlnyt Chloride
Methyl-t-Butyl Ether (MTBE)
Tert-Butyl Alcohol (TBA)
Diisopropyl Ether (DIPE)
Ethyl-t-Butyl Ether (ETBE)
Tert·Amyl-Methyl Ether (TAME)
Ethanol
102
106
101
98
109
101
99
117
94
77
104
96
97
92
99
106
99
99
110
97
100
117
92
67
103
97
94
93
87-117
77-137
89-113
90-114
81-129
88-118
67-121
71-131
65-125
38-140
77-119
73-121
71-119
54-132
0-5
0-9
0-5
0-8
0-15
0-71
0-21
0-34
0-49
0-98
0-53
0-31
0-33
0-55
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7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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S ~!~cience
I:.=nvironmental
Laboratories, Inc.
Glossary of Terms and Qualifiers
Work Order Number: 03-11-1385
Qualifier
Definition
NO
Not detected at indicated reporting limit.
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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C. 'fJl:;¡.ncø
.e-lV,,.onmflntsl
aboratorføs. Inc.
WORK ORDER #:
03 . [][] . []]~[I][5j
Cooler L of
SAMPLE RECEIPT FORM
CLIENT: 1:L4-t J € -' , -6df--
TEMPERATURE - SAMPLES RECEIVED BY:
CALSCIENCE COURIER:
Chilled, cooler with temperature blank provided.
Chilled, cooler without temperature blank.
\....-""" Chilled and placed in cooler with wet ice.
Ambient and placed in cooler with wet ice.
Ambient temperature.
DATE: \\ -2\,-03
LABORATORY (Other than Calscience Courier):
DC Temperature blank.
o C IRthermometer.
Ambient temperature.
..3:. 0 C Temperature blank.
Initi!'il: y\::,/)
CUSTODY SEAL INTACT:
Sample(s):
Not Applicable (N/A): \/
Initial: VL.z{)
Cooler:
No (Not Intact) :
SAMPLE CONDITION:
Yes
N/A
No
Chain-Of-Custody document(s) received with samples...... .......... ,........
Sample container label(s) consistent with custody papers.......... ...... .....
Sample container( s) intact and good condition.... ... ... ... ... ... ... ... ... ... ... .
Correct containers for analyses requested.............................. .... .......
Proper preservation noted on sample label( s)..... ... ... ... ... ... ... ... ... ... ... ..
VOA vial(s) free of headspace. ...... ... ..:............... ... ... .............. "... ...
Tedlar bag(s) free of condensation................................................ ...
~ .......
¡..-- .. . .. ..
..................
-.----...... .
........-" ... ....
-
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... .........
Initial:
COMMENTS:
-
- --
LAB: ~SC;~
-
-
-
-
-------
SHELL Chain Of Custody Record
-
-
-
-
Lab Identnlcallon (n necessary): Shell Project Manager to be invoiced: 1¡~j~:!~~.~il~:~~~~f.\~~~J¡~IfI~i!!lm
Address: 1·0:~6ii~¿*:~E~~);~ -
City. Slate. Zip: Tony Palagyi DATE: I I Zot/O '"3>
l':O:f~êAi:~Sf~~::<::1 I (
1¡j,tPXi:~ŠiÞN:··.:··':··:·:1 PAGE: of
Slt.MPLNG COMPANY: LOG CODE: SITE ADDRESS {s..... and Cltyt: Gil.OØI\LDNO..;
BlalneTech Servlces,lnc. BT5T 5321 Stockdale Highway, Bakersfield Pending
AIJORESS: 8F~1. ~REPOATTO{R~F"aI\'«OdIar-~ PHONE NO.: ~, --
20360 Gramercy Place, Torrance, CA 90501-1511 031ill-OßI
PRO..ECT CONTACT (~..d::apr« PŒ R~ tD): Britney Gunderson 626·256-6662 bgunderson@deltaenv.com BTS"
Nick Sudano .....P\.ER ......E(S (!'!WI:
TEUPHONE I/~ E~AL: p
310.782·2465 310-782-2958 nsudano@blainetech.com CÞve ß. .N1 ;. ke.. ,vIr.L" .AA
TURNAROUND TIME (BUSINESS DAYS):
¡( 10 DAYS 0 S DAYS 0 n HOURS 0 48 HOURS 0 24 HOURS 0 lESS THAN 24 HOURS REQUESTED ANALYSIS
0 LA - RWQCB REPORT FORMAT 0 usr AGENCY: General Minerals
GClMS M'rne CONFIRMATION: HIGHEST Ê
HIGHEST per BORING ALL '" S Ê ~ FIELD NOTES:
Ê ..
.. '" u
SPECIAL INSTRUCTIONS OR NOTES: CKECK BOX IF EDD IS.!':!Q! NEEDED 0 on e- c if 111 u
... íã Ii ~ 0 ¿ II Contalnw/Preservlltlve
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!!!. 0 '" :ã .. E 3 or PID Readings
HNO;I poly's were field filtered prior to preservation <D Õ u 0 'R c E
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:¡; e- m .. i '" " or Laboratory Notes
~ ~ c ii ..
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"Must state whether bicarbonate Is reported as either calcium carbonate " ... c Ii ~ ti :z; :E ~ Õ
e> Œ '" ... .. w 0 c ~ Ë UI
(Caeo,), or bicarbonate (Hcq) '" ãì ãì .. 0 ~ tJ " II
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SAMPLING ~ ~- 1: ! " TEMPERATURE ON RECEIPT CO
Field Sample Identification NO.OF :z: ~ .. .. III .. Z :z: :ã ü 0 é í ;; ~
MATRIX CONT. ~ >C :5 .. 0 .¡: ~ :; ~ ¡¡; :ë II :z: c1!
DATE TIME III 0 W Õ ... w z ... ¡¡ 0 0 :z; Q. l-
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DISTRIBUTION. 'M\I1e wilt¡ tlnal r~art. GrMI'I to File, Yellow and Pink 10 Chenl
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I.:alscience
I::vironmental
Laborator;es~ Inc.
December 02, 2003
Nick Sudano
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Subject: Calscience Work Order No.:
Client Reference:
03-11-1386
5321 Stockdale Highway, Bakersfield, CA
Dear Client:
Enclosed is an analytical report for the above-referenced project. The samples
included in this report were received 11/21/2003 and analyzed in accordance with
the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the
guidelines established in our Quality Assurance Program Manual, applicable standard
operating procedures, and other related documentation. The original report of any
subcontracted analysis is provided herein, and follows the standard Calscience data
package. The results in this analytical report are limited to the samples tested and any
reproduction thereof must be made in its entirety.
If you have any questions regarding this report, please do not hesitate to contact
the undersigned.
Michael . Crisostomo
Quality A surance Manager
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895·5494 . FAX: (714) 894·7501
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L=a~~cience
I:=nvironmental
Laboratories, Inc.
Blaine Tech Services. Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received:
Work Order No:
Preparation:
Method:
11/21/03
03-11-1386
EPA 3005A Filt.
EPA 601 OB
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
Client Sample,Number
Lab Sample
Number
Date Date
Prepared Analyzed ac Batch ID
';::~~9.'P;!;~';)~·l:¡
Date
Collected
Matrix
Parameter
Result
º"'ª'
Units
mglL
Lead
ND
RL
0.0100
Q.E
Parameter ~ RL DF Q!.@ Units
Lead ND 0.0100 mg/L
":~~~i~~~ªPtMi·*¡~
Parameter B.!lIDill fib DF Q!.@ Units
Lead NO 0.0100 mg/L
Parameter
RL
0.0100
Q!.!ê!
Units
Result
DF
Lead
ND
mglL
RL - Reporting Limit, OF - Dilution Factor, Qual· Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
1'---__..___.._,.........'_... ....".. .,___,. ........,____.." '''''''''_'''_ ____._.__.__.____.,..___.,__.____...,.._....._..:....__.. .-_,__._" ............. ......,.. ,..-:.... ." ..,." , .., , .
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(.;alscience
I:~nvironmental
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received:
Work Order No:
Preparation:
Method:
11/21/03
03-11-1386
EPA 5030B
DHS LUFT
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
Client Sample Number
Lab Sample
Number
Date
Prepared
QC Batch ID
Matrix
Parameter
~ RL DF ~ Units
ND 50 ugIL
RECI%} Control ~
Limits
83 49-133
TPH as Gasoline
Surrooates:
1,4-Bromofluorobenzene
Parameter Result fib QE ~ !.!n!m .
TPH as Gasoline ND 50 uglL
SurrOQates: ~ ~ Qual
!.lr!:!i!§
1,4-Bromofluorobenzene 80 49-133
Parameter Result RL DF Qual Units
TPH as Gasoline ND 50 ug/L
Surroaates: ~ ~ Q!m!
Limits
1,4-Bromo!1uorobenzene 84 49-133
Parametèr Result RL DF Qual ~
TPH as Gasoline ND 50 ug/L
SUITOQates: REC("!o\ Control Qual
Limits
1,4-Bromofluorobenzene 89 49-133
RL . Reporting Limit. DF . Dilution Factor, Quat - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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L=alscience
I:=nvironmental
LaboratOries, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Analytical Report
Date Received:
Work Order No:
Preparation:
Method:
11/21/03
03-11-1386
EPA 3510C
DHS LUFT
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
Client Sample Number
Lab Sample
Number
Date
Prepared
QC Batch 10
Date
Collected
Matrix
Parameter
Decachlorobiphenyl
Result RL DF
ND 1000
REC(%I Control
Limits
71 51-141
º"'ª' Units
ug/L
Qual
TPH as Diesel
SUITooates:
Parameter Result . RL DF Qual !hill!¡
TPH as Diesel ND 1000 ug/L
Surroaates: ~ Control Qual
Ÿ!!!i!§
Decachlorobiphenyl 73 51-141
Parameter Result RL OF º"'ª' Units
TPH as DIesel ND 1000 ug/L
SUIToaates: REC(%I Control Qual
Limits
Decachlorobiphenyl 79 51-141
Parameter Result RL OF º"'ª' Units
TPH as Diesel ND 1000 uglL
SUIToaates: ~ Control Qual
Limits
Decachlorobiphenyl 93 51-141
RL . Reporting Limit. OF .. Dilution Factor, Qual· Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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c..=alscience
.I:~nvironmental Analytical Report
Laboratories, Inc.
Blaine Tech Services, Inc Date Received: 11/21/03
20360 Gramercy Place Work Order No: 03-11-1386
Torrance. CA 90501-1511 Preparation: EPA 5030B
Method: EPA 82608
Project: 5321 Stockdale Highway, Bakersfield, CA Page 1 of 4
Lab Sample Date Date
Client Sample Number Number Collected Matrix Prepared QC Batch 10
". . .~,.~~¡~~"t!.:i~:;~~~[i~~
Parameter &§!!lI RL OF ~ Units Parameter Result RL OF QYãl . !J!!im
Acetone NO 10 1 uglL 1,1-0ichloropropene NO 1.0 1 ug/L
Benzene NO 0,50 1 uglL o-1,3-0ichloropropene NO 0.50 1 ug/L
Bromobenzene NO 1.0 1 uglL t-1,3-0Ichloropropene NO 0.50 1 ug/L
Bromochloromethane NO 1.0 1 uglL Ethylbenzene NO 1.0 1 ug/L
Bromodichloromethane NO 1.0 1 ug/L 2-Hexanone NO 10 1 ug/L
Bromoform NO 1.0 1 uglL Isopropyl benzene ND 1.0 1 ug/L
Bromomethane NO 10 1 uglL p-Isopropyltoluene NO 1.0 1 ug/L
!2-Butanone NO 10 1 ug/L Methylene Chloride NO 10 1 ug/L
n-Butylbenzene NO 1.0 1 uglL 4-Methyl-2-Pentanone NO 10 1 uglL
seo-Butylbenzene NO 1.0 1 uglL Naphthalene NO 10 1 uglL
tert-Butylbenzene NO 1.0 1 uglL n-Propylbenzene ND 1.0 1 ug/L
Carbon Disulfide NO 10 1 ugll Styrene NO 1.0 1 uglL
Carbon Tetrachloride NO 0.50 1 uglL 1,1,1,2- Tetrachloroethane ' NO 1.0 1 uglL
Chlorobenzene NO 1,0 1 uglL 1,1,2,2-Tetrachloroethane ND 1.0 1 uglL
Chloroethane NO 1.0 1 ug/L Tetrachloroethane NO 1.0 1 uglL
Chloroform NO 1.0 1 ug/L Toluene NO 1.0 1 ug/L
Chloromethane NO 10 1 uglL 1,2,3- Trichlorobenzene NO 1.0 1 ug/L
2-Chlorotoluene NO 1.0 1 ug/L 1,2,4- Trlchlorobenzene NO 1,0 1 uglL
4-Chlorotoluene NO 1.0 1 ug/L 1,1,1- Trichloroethane NO 1.0 1 uglL
Oibromochloromethane NO 1.0 1 ug/L 1,1,2-Trichloroethane NO 1.0 1 ug/L
1,2-0Ibromo-3-Chloropropane ND 5.0 1 ug/L Trichloroethene NO 1.0 1 ug/L
1,2-0ibromoethane NO 1.0 1 ugfL Trichlorofluoromethane NO 10 1 ug/L
Olbromomethane NO 1.0 1 uglL 1,2,3- Trlchloropropane NO 5.0 1 ug/L
1,2-0ichlorobenzene NO 1.0 1 ug/L 1,2,4- Trimethylbenzene NO 1.0 1 ug/L
1,3-Dlchlorobenzene NO 1.0 1 uglL 1,3,5- Trimethylbenzene ND 1.0 1 ug/L
1,4-0ichlorobenzene NO 1.0 1 ug/L Vinyl Acetate NO 10 1 ug/L
Olchlorodifluoromethane NO 1.0 1 ug/L Vinyl Chloride NO 0.50 1 ugfL
1,1-0ichloroethane NO 1.0 1 ug/L p/m-Xylene NO 1.0 1 uglL
1,2-0ichloroethane ND 0.50 1 ug/L o-Xylene NO 1.0 1 uglL
1,1-0ichloroethene NO 1.0 1 ugfL Methyl-t-Butyl Ether (MTSE) ND 1.0 1 ug/L
c-1,2-Dichloroethene NO 1.0 1 ugfL Tert-Butyl Ncohol (TBA) ND 10 1 ug/L
t-1,2-0Ichloroethene NO 1.0 1 uglL Diisopropyl Ether (OIPE) NO 2.0 1 ugfL
1,2-Dichloropropane ND 1.0 1 uglL Ethyl-t-Butyl Ether (ETBE) NO 2.0 1 uglL
1,3-Dichloropropane NO 1.0 1 uglL Tert-Amyl-Methyl Ether (TAME) NO 2.0 1 uglL
2,2-Dlchloropropane NO 1.0 1 uglL
Surroaates: REC(%) Control QYãl Surroaates: REC(%) Control Qual
Limits
Oibromofluoromethane 112 84-120 ToIuene-d8 100 91-109
1,4·Bromofluorobenzene 97 84-108
RL - Reporting Limit, DF - Dilution Factor. Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895·5494 · FAX: (714) 894·7501
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L=alscience
=--
~=nvironmental Analytical Report
==
I.. aboratories, Inc.
Blaine Tech Services, Inc Date Received: 11/21/03
20360 Gramercy Place Work Order No: 03-11-1386
Torrance, CA 90501-1511 Preparation: EPA 5030B
Method: EPA 8260B
Project: 5321 Stockdale Highway, Bakersfield, CA Page 2 of 4
Matrix QC Batch 10
Parameter Result B!. OF Qual .!1ni!§ Parameter Result RL OF QY2I .!1ni!§
Acetone NO 10 1 uglL 1,1-0ichloropropene NO 1.0 1 ug/L
Benzene ND 0.50 1 uglL c-1,3-0ichloropropene NO 0.50 1 ug/L,
Bromobenzene ND 1.0 1 ug/L t-1,3-0ichloropropene NO 0.50 1 ug/L
Bromochloromethane ND 1.0 1 uglL Ethy1benzene NO 1.0 1 ug/L
Bromodichloromethane NO 1.0 1 ug/L 2-Hexanone ND 10 1 uglL
Bromoform NO 1.0 1 uglL Isopropylbenzene NO 1.0 1 uglL
Bromomethane NO 10 1 uglL p-Isopropyltoluene NO 1.0 1 uglL
2-Butanone NO 10 1 uglL Methylene Chloride NO 10 1 ug/L
n-Butylbenzene NO 1.0 1 uglL 4-MethyI-2-Pentanone NO 10 1 uglL
sec-Butylbenzene NO 1.0 1 uglL Naphthalene NO 10 1 uglL
tert-Butylbenzene NO 1.0 1 ug/L n-Propylbenzene NO 1.0 ' 1 ug/L
Carbon Disulfide NO 10 1 uglL Styrene NO 1.0 1 ug/L
Carbon Tetrachloride NO 0.50 1 ug/L 1,1.1,2-Tetrachloroethane NO 1.0 1 uglL
Chlorobenzene NO 1.0 1 uglL 1,1.2,2-Telrachloroethane NO 1.0 1 uglL
Chloroethane NO 1.0 1 ug/L Tetrachloroethene NO 1.0 1 ug/L
Chloroform NO 1.0 1 uglL Toluene NO 1,0 1 ug/L
Chloromethane NO 10 1 uglL 1,2,3- Trlchlorobenzene NO 1.0 1 uglL
2-Chlorotoluene NO 1.0 1 uglL 1,2,4- Trlchlorobenzene NO 1.0 1 'uglL
4-Chlorotoluene NO 1.0 1 ug/L 1,1.1- Trichloroethane ND 1.0 1 ug/L
Olbromochloromethane NO 1.0 1 ug/L 1,1,2- Trichloroethane ND 1.0 1 ug/L
1,2-Dibromo-3-Chloropropane NO 5.0 1 uglL Trichloroethene NO 1.0 1 uglL
1,2-0ibromoethane NO 1.0 1 ug/L Trlchlorofluoromethane NO 10 1 uglL
Dibromomethane ND 1.0 1 uglL 1,2,3- Trichloropropane NO 5.0 1 ug/L
1,2-0ichlorobenzene NO 1.0 1 uglL 1,2,4- Trimethyfbenzene NO 1,0 1 uglL
1,3-0ichlorobenzene NO 1.0 1 ug/L 1,3,5- Trimethylbenzene NO 1.0 1 uglL
1,4-0ichlorobenzene NO 1.0 1 ugIL Vinyf Acetate NO 10 1 uglL
Oichlorodifluoromethane NO 1.0 1 ug/L Vinyl Chloride NO 0.50 1 ug/L
1,1-0ichloroethane NO 1.0 1 uglL plm-Xylene NO 1.0 1 uglL
1,2-0ichloroethane NO 0.50 1 uglL o-Xylene NO 1,0 1 uglL
1,1-0lchloroethene NO 1.0 1 uglL Methyl-t-Butyl Ether (MTBE) ND 1,0 1 uglL
. c-1,2-0Ichloroethene NO 1.0 1 ug/L Tert-Butyl Alcohol (TBA) ND 10 1 uglL
t-1,2-0ichloroethene NO 1.0 1 uglL Dlisopropyl Ether (OIPE) ND 2.0 1 ug/L
1,2-0ichloropropane NO 1.0 1 ug/L Ethyl-t-Butyl Ether (ETSE) NO 2.0 1 ug/L
1,3-0lchloropropane NO 1.0 1 uglL Tert-Amyl-Methyl Ether (TAME) NO 2.0 1 uglL
2,2-0ichloropropane NO 1.0 1 ug/L
Surroaates: REC/%) Control Qual Surroaates: REC/O/O) Control Qual
Limits
Oibromofluoromethane 111 84-120 Toluene-dB 105 91-109
1,4-Bromof1uorobenzene 97 84-1 06
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RL - Reporting Limit .
OF . Dilution Factor, Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 ·
FAX: (714) 894-7501
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I
I ~-a~cience
=--
I 6:=nvironmental Analytical Report
Laboratories, Inc.
I: Blaine Tech Services, Inc Date Received: 11/21/03
20360 Gramercy Place Work Order No: 03-11-1386
Torrance, CA 90501-1511 Preparation: EPA 5030B
Method: EPA 8260B
I
Project: 5321 Stockdale Highway, Bakersfield, CA Page 3 of 4
I Date
I Parameter Result RL QE Qual Units Parameter Result RL Q.E Qual Units
Acetone NO 10 1 ug/L 1.1-0ichloropropene NO 1.0 1 uglL
Benzene NO 0.50 1 uglL c-1,3-0ichloropropene NO 0.50 1 uglL
Bromobenzene NO 1.0 1 uglL t-1,3-Dichloropropene NO 0.50 1 uglL
I, Bromochloromethane NO 1.0 1 ug/L Ethylbenzene NO 1.0 1 ug/L
Bromodlchloromethane NO 1.0 1 uglL 2-Hexanone NO 10 1 uglL
Bromoform NO 1.0 1 uglL Isopropylbenzene NO 1.0 1 uglL
Bromomethane NO 10 1 uglL p--Isopropyltoluene NO 1.0 1 uglL
2-Butanone NO 10 1 uglL Methylene Chloride ND 10 1 ug/L
1- n-Butylbenzene NO 1.0 1 ug/L 4-Methyl-2-Pentanone ND 10 1 u¡j/L
sec-Butylbenzene NO 1.0 1 uglL Naphthalene ND 10 1 ug/L
tert-Butylbenzene NO 1.0 1 uglL n-Propylbenzene NO 1.0 1 ug/L
Carbon Disulfide ND 10 1 uglL Styrene ND 1.0 1 ug/L
I Carbon Tetrachloride NO 0.50 1 uglL 1,1,1,2- Tetrachloroethane NO 1.0 1 uglL
Chlorobenzene NO 1.0 1 uglL 1,1,2.2- Tetrachloroethane NO 1.0 1 ug/L
Chloroethane NO 1.0 1 uglL T etrachloroethene NO 1,0 1 uglL
Chloroform NO' 1.0 1 uglL Toluene ND 1,0 1 ug/L
Chloromethane ND 10 1 uglL 1,2,3- Trichlorobenzene ND 1.0 1 ug/L
I 2-Chlorotoluene NO 1.0 1 ug/L 1,2.4- Trlchlorobenzene NO 1.0 1 uglL
4-Chlorotoluene NO 1.0 1 uglL 1,1,1- Trichloroethane NO 1.0 1 uglL
Oibromochloromethane NO 1.0 1 uglL 1,1,2- Trichloroethane NO 1.0 1 uglL
1,2-Dibromo-3-Chloropropane NO 5.0 1 uglL Trichloroethene NO 1.0 1 ug/L
I~ 1,2-0ibromoethane NO 1.0 1 uglL Trichlorofluoromethane NO 10 1 ug/L
Oibromomethane NO 1.0 1 ug/L 1,2,3- Trichloropropane NO 5.0 1 ug/L
1,2-0ichlorobenzene NO 1.0 1 ug/L 1,2,4- Trlmethylbenzene NO 1.0 1 ug/L
1,3-Dlchlorobenzene NO 1.0 1 uglL 1,3,5- Trlmethylbenzene NO 1.0 1 uglL
1,4-Dichlorobenzene NO 1.0 1 uglL Vinyl Acetate NO 10 1 uglL
I' Olchlorodifluoromethane NO 1.0 1 ug/L Vinyl Chloride NO 0.50 1 . ug/L
1.1-Dichloroethane NO 1.0 1 uglL p/m-Xylene ND 1.0 1 ug/L
1,2-Dichloroethane ND 0.50 1 uglL o-Xy1ene NO 1.0 1 ug/L
1,1·Dichloroethene NO 1.0 1 uglL Methyl-t-Butyf Ether (MTBE) NO 1.0 1 ug/L
I c-1,2-0ichloroethene NO 1.0 1 ug/L Tert-Butyl Alcohol (TBA) NO 10 1 ug/L
t-1,2-Dichloroethene NO '1.0 1 uglL Diisopropyl Ether (OIPE) NO 2.0 1 ug/L
1.2-0ichloropropane NO 1.0 1 uglL Ethyl-t-Butyl Ether (ETBE) ND 2.0 1 uglL
1,3-Dichloropropane ND 1.0 1 ug/L Tert-Amyf-Methyl Ether (TAME) NO 2.0 1 ug/L
I 2,2-Dichloropropane ND 1.0 1 uglL
Surroaates: B5Q..OO Control Qual Surroaates: REC(%} Control Qual
Limits
Oibromofluoromethane 111 84-120 Toluene-dB 105 91-109
I 1,4-Bromofluorobenzene 9B 84·108
II
I RL - Reporting Limit DF - Dilution Factor , Qual· Qualifiers
7440 Lincoln Way, Garden Grove. CA 92841-1432 . TEL: (714) 895-5494 . FAX: (714) 894-7501
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I '=¡»vironmèntal Analytical Report
Laboratories, Inc.
I Blaine Tech Services, Inc Date Received: 11/21/03
20360 Gramercy Place Work Order No: 03-11-1386
Torrance, CA 90501-1511 Preparation: EPA 5030B
I Method: EPA 82608
Project: 5321 Stockdale Highway, Bakersfield, CA Page 4 of 4
I Date Date
Matrix ac Batch ID
I Parameter Result RL DF .QyID Units Parameter Result RL OF Q!!i! Units
Acetone NO 10 1 ug/L Ethanol NO 100 1 ug/L
1,1-Dichloropropene NO 1.0 1 ug/L Benzene NO 0.50 . 1 ug/L
c-1,3-Dichloropropene ND 0.50 1 ug/L Bromobenzene NO 1.0 1 uglL
I t-1,3-0ichloropropene NO 0.50 1 ug/L Bromochloromethane NO 1.0 1 uglL
Ethylbenzene NO 1.0 1 ug/L Bromodichloromethane ND 1.0 1 ug/L
2-Hexanone ND 10 1 uglL Bromoform ND 1.0 1 ug/L
Isopropyl benzene ND 1.0 1 ug/L Bromomethane ND 10 1 ug/L
I p-Isopropyltoluene ND 1.0 1 uglL 2-Butanone ND 10 1 ug/L
Methylene Chloride NO 10 1 uglL n-Butylbenzene ND 1.0 1 uglL
4-Methyl-2-Pentanone ND 10 1 uglL sec-Butylbenzene ND 1.0 1 uglL
Naphthalene NO 10 1 uglL tert-Butylbenzene ND 1.0 1 uglL
n-Propylbenzene ND 1.0 1 ug/L Carbon Disulfide . ND 10 1 uglL
I Styrene NO 1.0 1 uglL . Carbon Tetrachloride ND 0.50 1 uglL
1,1,1,2- Tetrachloroethane ND 1.0 1 ug/L Chlorobenzene ND 1.0 1 uglL
1,1,2,2-Tetrachloroethane NO 1.0 1 ugIL Chloroethane ND 1.0 1 ug/L
Tetrachloroethene ND 1.0 1 ug/L Chloroform ND 1.0 1 uglL
I Toluene ND 1.0 1 ug/L Chloromethane ND 10 1 uglL
1.2.3-Trichlorobenzene NO 1.0 1 uglL 2.chlorotoluene ND 1.0 1 uglL
1,2,4-Trlchlorobenzene ND 1.0 1 ug/L 4.chlorotoluene ND 1.0 1 uglL
1.1.1-Trlchloroethane NO 1.0 1 uglL Dibromochloromethane NO 1.0 1 ug/L
1,1,2- Trichloroethane NO 1.0 1 ug/L 1,2-Dibromo-3-Chloropropane ND 5.0 1 uglL
I Trlchloroethene NO 1.0 1 uglL 1,2-Dibromoethane , NO 1.0 1 ug/L
Trlchlorofluoromethane NO 10 1 uglL Oibromomethane ND 1.0 1 uglL
1,2.3-Trichloropropane NO 5.0 1 ug/L 1,2-Dichlorobenzene ND 1.0 1 ÜglL
1,2,4-Trlmethylbenzene NO 1.0 1 uglL 1,3-Dlchlorobenzene ND 1.0 1 uglL
I 1,3,5- Trlmethylbenzene NO 1.0 1 uglL 1,4-0lchlorobenzene ND 1.0 1 uglL
Vinyl Acetate NO 10 1 ugIL Dlchlorodifluoromethane ND 1.0 1 ug/L
Vinyl Chloride NO 0.50 1 ugIL 1,1-0lchloroethane NO 1.0 1 ug/L
p/m-Xylene NO 1.0 1 ug/L 1,2-Dichloroethane ND 0.50 1 uglL
o-Xylene NO 1.0 1 uglL 1.1-0Ichloroethene NO 1.0 1 ug/L
I Methyl-t-Butyl Ether (MTBE) NO 1.0 1 uglL c-1,2-Dlchloroethene ND 1.0 1 ug/L
Tert-Butyl Alcohol (TBA) ND 10 1 uglL t-1,2-Dichloroethene NO 1.0 1 ug/L
Dilsopropyl Ether (DIPE) NO 2.0 1 uglL 1,2-Dlchloropropane NO 1.0 1 ug/L
Ethyl-t-Butyl Ether (ETBE) NO 2.0 1 ug/L 1,3-Dichloropropane NO 1.0 1 , ug/L
I Tert-Amyl-Methyl Ether (TAME) NO 2.0 1 uglL 2,2-Dichloropropane ND 1.0 1 ug/L
Surrocates: RECIO/O) Control .QyID Surrocates: ~ ~ Qual
Limits
Dibromoftuoromethane 108 84-120 Toluene-d8 105 91-109
I 1,4-Bromofluorobenzene 101 84-108
I
I RL . Reporting Limit DF . Dilution Factor Qual - Qualifiers
7440 Lincoln Way. Garden Grove, CA 92841-1432 . TEL: (714) 895-5494 . FAX: (714) 894-7501
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Quality Control - Spike/Spike Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No: .
Preparation:
Method:
11/21/03
03-11-1386
EPA 3005A FiJt.
EPA 60108
Project:
5321 Stockdale Hiç¡hwav. Bakersfield, CA
Quality Control Sample 10
Date
Prepared
Date
Analyzed
MS/MSD Batch
Number
Matrix
Instrument
Parameter
MS %REC
%REC CL
RPD
RPD CL
MSD %REC
Qualifiers
Lead
80-120
0-20
4
114
109
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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Laboratories, Inc.
Quality Control· LCS/LCS Duplicate
Blaine Tech Services. Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparátion:
Method:
11/21/03
03-11-1386
EPA 3005A Filt.
EPA 6010B
Project:
5321 Stockdale Highway, Bakersfield, CA
Date
Parameter
LCS %REC
108
Quàlifiers
LCSD %REC
111
%REC CL
80-120
BEQ
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7440LincolnWay,GardenGrove,CA92841-1432 · TEL:(714)895-5494 · FAX: (714)894-7501
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Quality Control· Spike/Spike Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
11/21/03
03-11-1386
EPA 5030B
DHS LUFT
Project:
5321 Stockdale HiQhway. Bakersfield. CA
Quality Control Sample ID
Date
Prepared
Date
Analyzed
MS/MSD Batch
Number
Matrix
Instrument
Parameter
MS %REC
RPD CL
Qualifiers
MSD %REC
%REC CL
RPD
TPH as Gasoline
o
0-17
87
87
70-112
7440 Lincoln Way. Garden Grove. CA 92641-1432 · TEL: (714) 895-5494 · FAX: (714) 694-7501
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I:~nvironmental
Laboratories, Inc.
Quality Control - LCS/LCS Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
11/21/03
03-11-1386
EPA 50308
DHS LUFT
Project: 5321 Stockdale Highway, Bakersfield, CA
Date
LCS/LCSD Batch
Parameter
TPH as Gasoline
LCS %REC
97
LCSD %REC
95
.BeQ
BfQ...Çb Qualifiers
0-10
%REC CL
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7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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I/:,¡¡gnvironmental
'- aboratories, Inc.
Quality Control· LCS/LCS Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
11/21/03
03-11-1386
EPA 351 OC
DHS LUFT
Project:
5321 Stockdale Highway, Bakersfield, CA
LCS/LCSD Balch
Number
Parameter
LCS %REC
100
%REC CL
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Qualifiers
RPD
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RPD CL
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LCSD %REC
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7440LincolnWay,GardenGrove,CA92841-1432 · TEL:(714)895-5494 · FAX: (714)894-7501
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Laboratories, Inc.
Quality Control - Spike/Spike Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
Project: 5321 Stockdale Hiç¡hwav. Bakersfield, CA
Matrix
Instrument
Date
Prepared
Date
Analyzed
Quality Control Sample ID
11/21/03
, 03-11-1386
,EPA 5030B
EPA 8260B
MS/MSD Batch
Number
Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers
Benzene 101 99 84-120 1 0-13
Carbon Tetrachloride 112 108 72-132 4 0·15
Chlorobenzene 100 101 87-117 0 0-12
1,2-Dlchlorobenzene 96 97 86-116 1 0-13
1,1-Dichloroethene 110 103 77·137 7 0-15
Toluene 97 97 85-121 0 0-15
Trichloroethene 103 100 66-120 3 0-13
Vinyl Chloride 120 118 68-140 1 0-16
Methyl·t·Butyl Ether (MTBE) 96 92 68-128 4 0-18
Tert·Butyl Alcohol (TBA) 67 68 30-156 3 0-26
Diisopropyl Ether (DIPE) 102 100 75-123 2 0-14
Ethyl-t-Butyl Ether (ETBE) 98 96 66-132 2 0-33
Tert·Amyl-Methyl Ether (TAME) 97 96 59-131 1 0·47
Ethanol 89 93 20-176 4 0-42
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Laboratories, Inc.
Quality Control . LCS/LCS Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:'
Work Order No:
Preparation:
Method:
11/21/03
03-11-1386
EPA 50308
EPA 8260B
Project: 5321 Stockdale Highway, Bakersfield, CA
Date Dale
Parameler LCS %REC LCSD %REC %REC CL BfQ RPD CL Qualifiers
Benzene 100 98 87-117 1 0-5
Carbon Tetrachloride 114 108 77-137 6 O·g
Chlorobenzene 100 101 89-113 1 0-5
1,2-Dlchlorobenzene 96 96 90-114 0 0-8
1,1-Dichloroethene 108 106 81-129 2 0-15
Toluene 96 97 88-118 1 0-71
Trichloroethene 101 98 67-121 3 0-21
Vinyl Chloride 124 120 71-131 4 0-34
Methyl-I·Butyl Elher (MTBE) 96 92 65-125 4 0-49
Tert-Butyl Alcohol (TBA) 68 68 38-140 0 0·98
Diisopropyl Ether (DIPE) 103 99 77-119 4 0-53
Ethy1-I·Butyl Ether (ETBE) 100 95 73-121 6 0-31
Tert-Amyl-Methy1 Ether (TAME) 96 94 71-119 3 0-33
Ethanol 87 87 54-132 0 0-55
7440 Lincoln Way, Garden Grove, CA 92841·1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501
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Glossary of Terms and Qualifiers
Work Order Number: 03-11-1386
Qualifier
Definition
NO
Not detected at indicated reporting limit.
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 89t:¡-5494 · FAX: (714) 894-7501
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WORK ORDER #:
03 .[][] - rn~[I[(;]
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SAMPLE RECEIPT FORM
CLIENT: "tLA-I AJ € -' \ .a:.:H-
TEMPERATURE - SAMPLES RECEIVED BY:
CALSCIENCE COURIER:
Chilled, cooler with temperature blank provided.
Chilled, cooler without temperature blank.
~ Chilled and placed in cooler with wet ice.
Ambient and placed in cooler with wet ice.
Ambient temperature.
DATE: \ \ - 2- \ - 0 ·5
LABORATORY (Other than Calscience Courier):
o C Temperature blank.
o C IR thermometer.
Ambient temperature.
...::3. 0 C Temperature blank.
Initi~l: y\::,/)
CUSTODY SEAL INTACT:
Sample(s):
Not Applicable (N/A): \ /
Initial: 'Y'1z()
Cooler:
No (Not Intact) :
SAMPLE CONDITION:
Yes
No
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Chain-at-Custody document(s) received with samples... ..... ....... ...... ....
Sample container label(s) consistent with custody papers...........,........,
Sample container(s) intact and good condition...................... ... ..........
Correct containers for analyses requested......... ... ... ...... ...... ..............
Proper preservation noted on sample label(s).......,..........................,..
VOA vial(s) free of headspace. ................................. ..... .................
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Central Valley Region
Terry Tamminen
Secretw)'.tiJr
Envirrmmenlal
Protectíon
Fresno Branch Office
Internet Address: http://www.swrcb.ca.gov/-rwgcb5
1685 E Street, Fresno, California 93706,2020
Phone (559) 445-5'[ 16· FAX (559) 445-5910
Arnold Schwarzenegger
Governor
16 December 2003
Regional Board Case No. 5T15000886
Mr. Tony Palagyi
Shell Oil Products U.S.
tb
___25.5513,,_Av:enue-SW _ _ _d'
Seattle, Washington 98134
-- ..
EXTENSION REQUEST - UNDERGROUND TANK RELEASE, SHELL SERVICE STATION,
5321 STOCKDALE HIGHWAY, BAKERSFIELD, KERN COUNTY
You submitted Extension Request: Site Assessment Report (Letter) dated 11 December 2003 and
prepared by Delta Environmental Consultants, Inc., Monrovia (Delta). The Letter requests an extension
for submittal of a site assessment report. We approved the scope of work proposed in Delta's Response
to Agency Requestfor Site J¡1vestigation (Wor-~laÍ1}dated 6 October 2003 by our letter dated
21 October 2"003. vie requested that a site assessment report be submitted by 21 January 2004.
L' ....-
~--~-_.-
Assessment fieldwork will be delayed due to a:v:a:itaÞil-it,y of the limited-access drill rig necessary for the
fieldwork. Delta -vJ;ill conduct the fieldwork dltfin~1anuary 2004 and submit a site assessment report by
21 February 2004. _
We grant your reqdest. The site àssessmept reI20rt is ñow due by 21 February 2004. Please contact this
office at least five days prior to fieldwork.~' If you have any questions regarding this correspondence,
.- .- - . -.--..
please contact me at (559) 445-5504.
-- ---- - -- -~ -
~$:ú)~'
JOHN D. WHITIN6 .
Engineering Geologist
R.G. No. 5951
-.~=----_._.
c:
Ms. Barbar~ Rempel, SWRCB, UST Cleanup Fund, Sacramen~
Mr. Howarcl H. Wines ill, Bakersfiem:PlreDepartment, Bakersfie~
Ms. Kathryn Ewing, Delta Environmental Consult·ants, Inc., Monrovia
File: UST/Kern/Texaco Service Station, 2401 N, Oak St., Bakersfield/5T15000885
California Environmental Protection Agency
~
~¢1 Recycled Paper
~
....,
''f' .
a
CalifQrnia Regional Water Quality Control Board
Central Valley Region
Terry Tamminen
Secretaryfi}r
Environmental
Protection
Fresno Branch Office
Internet Address: http://www.swrcb.ca.gov/-rwqcb5
1685 E Street, Fresno, California 93706-2020
Phone (559) 445-5116· FAx (559) 445-591O
Arnold Schwarzenegger
Governor
30 December 2003
Regional Board Case No. 5T15000886
Mr. I?r:ry P~lagyi
Shell Oil Products U.S.
2255 13th Avenue SW
Seattle, Washington 98134
UNDERGROUND TANK RELEASE, SHELL SERVICE STATION, 5321 STOCKDALE
HIGHWAY, BAKERSFIELD, KERN COUNTY
You submitted Third Quarter 2003 Groundwater Monitoring Report (Monitoring Report) dated
3 November 2003 and prepared by Delta Environmental Consultants, Inc., Monrovia (Delta). The
Monitoring Report documents a groundwater monitoring event at the above-referenced site on
3 September 2003. In a letter dated 17 June 2003, the Bakersfield Fire Department referred the subject
case to our agency for regulatory oversight. It also provided us with information indicating that gasoline
range petroleum hydrocarbons and the fuel oxygenates methyl tertiary butyl ether (MTBE) and tertiary
butyl alcohol (TBA) leaked at the subject site degrading soil and may threaten groundwater quality. We
requested that you submit a work plan to identify the source of leakage, abate the leakage, and determine
the extent of impacted soil by our 3 July 2003 letter. We also requested that you conduct quarterly
groundwater monitoring for two quarters. Groundwater monitoring should continue on a quarterly
schedule, Provided that you conduct a "full scan" EPA Method 8260 analysis and analysis for dissolved
lead during the fourth quarter 2003, we anticipate that these analyses may be subsequently discontinued.
Provided that you conduct general mineralS, nitrate, and tãtarKjeldahl nitrogen analyses during the
fourth quarter 2003, these analyses may be subsequently discontinued. A summary of the monitoring
report and our comments follow.
Monitorim! Report Summary
Blaine Tech Services, Inc., San Jose (Blaine Tech) collected groundwater samples from the monitoring
wells on 3 September 2003. Blaine Tech measured depth to groundwater at 131.26 to 132.68 feet below
ground surface (bgs). KHM determined groundwater flow to be toward the southeast.
The samples were analyzed for total petroleum hydrocarbons as gasoline (TPH-g), and benzene, toluene,
ethylbenzene, and xylenes (BTEX), MTBE, TBA, di-isopropyl ether (DIPE), ethyl tertiary butyl ether
(ETBE), tertiåry amyl methyl ether (TAME), 1,2-dichloroethane (l,2-DCA), and 1,2-dibromoethane
(EDB) and other volatile organic compounds detected in a "full scan" EP A Method 8260B analysis. The
California Environmental Protection Agency
~
"'-" Recycled Paper
/
~tt:l
;
(
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Mr. Tony Palagyi
- 3 -
30 December 2003
Please contact this office at least five days prior to fieldwork. If you have any questions regarding thi~
correspondence, please contact me at (559) 445-5504.
~ hZ. {¿/~'
JOHN D. WHITING
Engineering Geologist
R.G. No. 5951
Enclosure:
Required Electronic Deliverable Format for Laboratory and Site Data Submittals...
c: Ms. BarbaraRempel, SWRCR:UST Cleanûp Fund, Sacramento, w/o enclosure
Mr.Howard H. Wines III, Bakerstìeld Fire Department, Bakersfield, w/o enclosure
Ms. Kathryn Ewing, Delta Environmental Consultants, Inc., Monrovia, w/enclosure
File: UST/Kern/Shell Service Station, 532] Stockdale Highway, BakerstïeId/5TlS000886
V:\UGT\Projects\JDW _files\2003 Correspondence\City of Bakersfield Cases\Shell Stn Stockdale Hwy GW 12,03.doc
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A. g~J~~
Solving e:nvironme:nt~reIated business problems worldwide
911 South Primrose Avenue · Suite K
Monrovia, California 91016 USA
626.256.6662 800.477.7411
Fax 626.256.6263
www.deItaenv.com
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November 1, 2003
Delta Project PA53-21S-1
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Mr. John D. W1riting
California Regional Water Quality Control Board
Central Valley Region
1685E.Street .----...'
Fresno, California 93706-2020
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Re:. N otke of Consultant Name Change
Texaco Service Station
5321 Stockdale Highway
Bakersfield, California
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Dear Mr. John D. Whiting:
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Pleasê consider this letter notification that KHM Environmental Management, Inc. (KHM) has merged with Delta
Environmental Consultants, Inc. (DELTA).' Please address any future correspondence for the above reference site to:
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. Delta Environmental Consultants, Inc.
911 S. Primrose Avenue
Suite K
Monrovia, CA 91016
Attn: Mr. Bradley E. èIark
Phone: (626) 256-6662
Fax: (626) 256-6263
Email: bcIark@deltaenv.com
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Jfyou have any questions, please contact Mr. Bradley E. Clark (DELTA) at (626) 256-6662 or Mr. Tony Paiaygi (SHELL) at
(425) 377-8530.
,
Sincerely,
Delta Environmental Çonsultants, Inc.
~~
I Bradley E. Clark, PE
Senior Project Engineer
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cc: .
Mr. Tony Palaygi, Shell Oil Products US ..
Mr. Howard H. Wines ill, City of Bakersfield Fie Department
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A member' of:
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X Ino g~!1:entaIA¡¡;ance
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ÂIÀ g~~~c.
Solving environment-related business problems worldwide
911 South Primrose Avenue · Suite K
Monrovia, California 91016 USA
626.256.6662 800.477.7411
Fax 626.256,6263
www.deltaenv.com
November 03, 2003
Delta Project No. PA5321S~1
Mr. John D. Whiting
CalifoÍnia Regional Water Quality Control Board
Central Valley Region
1685 E. Street
Fresno, California 93706-2020
Re: THIRD QUARTER 2003 GROUNDW ATERMONITORING REPORT
Texaco Service Station
5321 Stockdale HighViray
Bak~rsfield, California
Dear:Mr. Whiting:
On behalf of Equilon Enterprises LLC dba Shell Oil Products (SHELL), Delta Environmental Consultants, Inc.
(Delta) has prepared this Third Quarter 2003 Groundwater Monitoring Report for the above-referenced site.
If you have any questions regarding this site, please contact Brad Clark at (626) 256-6662 or Tony Palagyi
(425) 377-8530. .
Bradley E. Clark, J:>.E.
SemorPr~ectEngmeer
Sincerely,
Delta Environmental Consultants, Inc.~, /
l ~/l/-
Attachment: Third Quarter 2003 Groundwater Momtoring Report
cc: Tony Palagyi; Shell Oil Products US
Howard H. Wines ill, City of Bakersfield Fire Depal1:~ent
'W . A member of
Xlno g~aLen;'IAllianCe
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November 03, 2003
SHELL QUARTERLY STATUS REPORT
Station Address:
Delta Project Nos.:
SHELL Environmental Engin.IPhone No.:
Delta Site ManagerIPhone No.:
Primary AgencylRegulatory ill No.:
Other Agencies to Receive Copies:
5321 Stockdale Highway
PA532IS-I
Tony Palagyil(425) 377-8530
Kathryn Ewing/(626) 256-6662
CVRWQCBI John Whiting
City of Bakersfield Fire Department! Howard H. Wines
ill
WORK PERFORMED TillS QUARTER (THIRD- 2003):
1. Quarterly groundwater monitoring and sampling. Submitted quarterly report.
2. Prepared and submitted Response to Agency Request for Site Investigation dated October 6, 2003,
WORK PROPOSED FOR NEXT QUARTER (FOURTH- 2003):
1. Quarterly groundwater monitoring and samþling. Submit quarterly report.
2. Implement additional site investigation per wo!k plan dated October 6, 2003.
Current Phase of Project: Groundwater monitoring
Frequency of Sampling: Quarterly
Frequency of Monitoring: Quarterly
Is Separate Phase Hydrocarbon Present On-site (Well #'s):
Cumulative SPH Recovered to Date: NA
SPH Recovered This Quarter: None
Sensitive Receptor(s) and Respective
Direction( s):
Current Remediation Techniques:
Permits for Discharge:
Approximate Depth to Groundwater:
Groundwater Gradient
Current Agency Correspondence:
Summary of Unusual Activity:
~~ ='
I, .~
Kathryn Ewing
Site Manager (Delta)
DYes ~No
Nearest field verified well is Well CBK 06-01 (State
Well No. 30S/27E-03B02 M) of the City of Bakersfield
approximately 825 feet South of the site.
None
None
131.26' to 132.68'
South-southeast @], approximately 0.018 ft/ft
Central Valley RWQCB letters dated July 3 and July 25, 2003.
None
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ATTACHED:
· Table 1 - Groundwater Gauging and Analytical Results
· Table 2 - Additional Chemicals of Concern
· Figure 1 - Site Location Map
· Figure 2 - Groundwater Elevation Contour Map
· Figure 3 - Hydrocarbon Distribution in Groundwater Map
· Figure 4 - TPH-G Concentrations in Groundwater Map
· Figure 5 - Benzene Concentrations in Groundwater Map
· Figure 6 - MTBE Concentrations in Groundwater Map
· Appendix A - Field Data Sheets
· Appendix B - Field Procedures
· Appendix C - Waste Disposal Documents
· Appendix D - Laboratory Report and Chain-of-Custody Documents
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TABLES
TABLE 11
HISTORICAL GROUNDWATER GAUGING AND ANALYTICAL DATA
TEXACO SERVICE STATION
5321 Stockdale Highway, Bakersfield, California
I'
::'. :"))ÀT~::' -::: :D~r¡'a: -::::::: :a~a::::::::: :Ç:W:lj;:ç~y;:::::: :TNH>:::::::: :Tf.f)';Q:::::: :ß~:l'i~),:N1<;:
.' 'TO:Gw·:-'i:'incKN.' (feet¡'clative:···<: .,':. .':", : ' ,:'.':,:.....::'..
. ,. .: ." :-:::-:¡iÚÜ:::-:':ifeeÙ . to MSÜ ' ' . : :¡;¡¡¡¡Ü:- .. " :¡,¡ÌiÌÜ-:' . ::::í.;¡;'ïÙ:::
I I
Top of casing elevation (It): 386.61
129.17 0.00 257.44
129.38 0,00 257.23
130,76 0,00 255.85
132,68 0.00 253,93
-
. .
MW-l
3/17/2003
3/25/2003
6/19/2003
9/3/2003
MW-2
3/17/2003
3/25/2003
6/19/2003
9/3/2003
MW-3
3/17/2003
3/25/2003
6/19/2003
9/3/2003
MW-4
3/17/2003
3/25/2003
6/19/2003
9/3/2003
-
-
-
Top of casin!! elevation (It): 386.06
128.64 0.00 257.42
128,84 0,00 257.22
130.27 0,00 255.79
131.79 0,00 254,27
Top of casing elevation (ft): 386.34
128.30 0.00 258,04
128.45 0,00 257,89
129.82 0.00 256.52
13 1.44 0,00 254.90
Top of casing elevation (ft): 386.57
128,17 0,00 258.40
128.25 0,00 258.32
129.59 0.00 256,98
131.26 0,00 255.31
Notes:
GW - Groundwater
SPH - Separate-phase hvdrocarbons
MSL - Mean sea level
ND, Not detected
ug/L - parts per billion
TPH,D - Total petroleum hydrocarbons as diesel
TPH,G - Total petroleum hydrocarbons as gasoline
MTBE - Methyl,tert butyl ether
TBA ' Tert-butyl alcohol I
DIPE - Di-isopropyl ether I
ETBE - Ethyl_tert butyl ether
TAME - Tert,amyl methyl ether
KHM Environmental Management, Inc.
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-
-
-
-
-
-
-
-
-
-
-
.'-
J:O~~~~::::: :~ray:µ;:::::::: :T:(}:I'Ai:::::::::: :~¡nl!;: :::::::: :1:8.'\; ::::::::::: Jn~~:::::::::: ~:r~~::::::: :::rÀ~£::: :::: :~T:~~~L::::: ::::: ::: (:~~M.&~t~:::: :::::::-
. .. ..,.... BENZENE. . ,XYLENES. . . , . 826() . . . .826.0, . . . ,_ .826(1. . ' ,. 8260."...8260···...8015..,....". '.'..... .'..,.....,'. , . . . . .
::: ::i~¡;¡Ü:::::::::::: :¡;;~iÙ:::: :::::::: :i~~IÖ<:::::: ::: ::i-';¡;7L1: ::::::: :1;;~iÙ::-:::-: <¡,¡-"¡-Ö::::::::: ::i~¡':fÜ::::::::: :i~~IÜ:::::::::::: (';~IX:::::::: <::- ::: :-::::::::::::::: <:::::::::::::::
ND<IOOO
ND<2,O
ND<2.0
ND<2,O
ND<100
ND<2,O
ND<2.0
ND<2.0
ND<50
ND<50
ND<50
ND<O,50
ND<O,50
ND<O,50
ND<1.0
ND<1.0
ND<1.0
ND<1.0
ND<1.0
ND<1.0
ND<1.0
ND<1.0
ND<1.0
ND<1.0
ND<1.0
ND<1.0
ND<10
ND<lO
ND<10
ND<2,O
ND<2,O
ND<2.0
ND<I00
ND<IOOO
ND<1000 ND<50 ND<O,50 ND<1.0 ND<1.0 ND<1.0 ND<1.0 ND<IO ND<2,O ND<2,O ND<2,O ND<IOO
ND<50 ND<0.50 ND<1.0 ND<I,O ND<I.0 ND<1.0 ND<10 ND<2.0 ND<2,O ND<2.0
ND<IOOO ND<50 ND<0.50 ND<l.O ND<l.O ND<l.O ND<1.0 ND<10 ND<2,O ND<2.0 ND<2,O ND<lOO
ND<lOOO ND<50 ND<O .50 ND<l.O ND<l.O ND<l.O ND<1.0 ND<lO ND<2.0 ND<2.0 ND<2,O ND<100
ND<50 ND<0.50 ND<l.O ND<l.O ND<l.O ND<1.0 ND<lO ND<2,O ND<2.0 ND<2,O
ND<lOOO ND<50 ND<O,50 ND<l.O ND<l.O ND<l.O ND<l.O ND<lO ND<2,O ND<2,O ND<2.0 ND<lOO
ND<lOOO ND<50 ND<0.50 ND<l.O ND<l.O ND<l.O ND<l.O ND<lO ND<2.0 ND<2.0 ND<2,O ND<lOO
ND<50 ND<0.50 ND<l.O ND<l.O ND<l.O ND<l.O ND<lO ND<2,O ND<2,O ND<2,O
ND<lOOO ND<50 ND<0.50 ND<l.O ND<1.0 ND<l.O ND<l.O ND<lO ND<2.0 ND<2.0 ND<2,O ND<lOO
Page 10fl
No purge sample
No purge sample
No purge sample
No purge sample
-.-
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TABLE 2 I I
ADDITIONAL CHEMICALS OF CONCERN
TEXACO SERVICE STATION I
5321 Stockdale Highway, Bakersfield, California
I I .
':- )i\¡~:::-: ç~()I1.I )¡¡:·:·mWT¡¡·:· :~~~:?~~~~: ·:-:r¡p;j':·: ~~I1'i1n ': ·)l ÇAI\J!QIiA:n: :-~OIi"'T'¡¡:' . ]ro!~QXU>~:' u,w.·:- I;Al;Qv\\( . ':')\l.Q~:' : :~Q!&&1V\\(':' J'P:T~lJ1J'l.·:· &QQIV\l(':' J\W'ìGA:J'i};S¡¡:.:.:.: ·~1¡¡ÇlAÇ,:,:,:·:·: ·rO¡~:·:· ::-::11'1:::::: ::'¡I>:>:-
. , . . . , . . . :::(a~¡i¡}:::: : (i¡S:é;~i:;Q3j:::::: :i'µ ç~é;<N¡: : (~~ :ç~ÇO~): : :: :(a~ ¢~¢Ø3)::: . . , . , . . . . ·:::::::i:;QNiicçiÄ.Jil¢i;:;iWU)m:~:
(mgi'¡:.¡::: .' ::(mgfIo): :. ('Ii1~ì::: ',:' :(irlgiL):': :::(in~)::: . (m~ì:'::: ' . '-:(ingiL¡:::: ::(itigi'¡:.} :::-:'(ni.liti;j:::: . ·t'l',~):- ::(ntg¡'l;r· ::(R;¡i¡i;j: ::(mg¡Lj:::::: :::::(itigi'¡:.)::: . (1I\g{L}':::: -::(!>iliti;j ..... :(MlhQ"I~m): .:.' .(mg{L):.:. .' (Unitsj:,'· :.(ugiL):
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MW-l .
9/3/2003 NA NA NA NA NA NA NA NA NA ND<O.OI NA NA NA NA NA NA NA NA NA NA
MW-2 .
9/312003 26 ND<O.IO 1.60 27 ND<0.50 100 100 ND<1.0 ND<1.0 ND<O.OI 30,8 ND<O,I 5.45 . 2.06 40.3 ND<O,005 350 110 6,31 220
MW-3
9/312003 26 ND<O,IO 1.60 27 ND<O,50 100 100 ND<1.0 ND<1.0 ND<O,Ol 32.6 ND<O,l 5.94 2,34 34 ND<0.005 350 100 6.36 220
MW-4
9/312003 26 ND<O.lO 1.50 26 ND<0.50 80 80 ND<1.0 ND<1.0 ND<O.Ol 30.5 ND<O.l 5,48 2,01 41 ND<0.005 350 96 6.43 220
Notes:
TKN ' Total Kjeldahl Nitrogen
IDS - Total Dissolved Solids
NA ' Not analyzed
Page I of 1
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FIGURES
I 119°05'00" W 119°04'00" W 119°03'00" W WGS84 119°02'00" W
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119°05'00" W 119°04'00" W 119°03'00" W WGS84 119°02'00" W
TN~N 9 l'o!Ilf
I 14" ~oo:!rm9 !OJ ...JIIOO MUms
Printed ftom TOPO! 'e2001 National Geographic Holdil'lgs (www.topo.com)
SHELL OIL PRODUCTS US
I TEXACO SERVICE STATION
Environmental BAKERSFIELD, CALIFORNIA
Sb Oonsultant Int:.
I SIT N FIGURE 1
E
SIT :: LOCATION MAP
I 5321 STOCKDALE HIGHWAY.
BAKERSFIELD, CALIFORNIA
- - - _. - - - - -, - - '- - - '- - - ..- -
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(f)
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(TYP)
/
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(255.31 )
r 1 r~1 (}("1
. I Iy n II I
yll II II I
I/"I II II II I
1~-3 l J l J l J l J
(254.90
-$-
/
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STOCKDALE HIGHWAY
DISPENSER
ISLAND
(TYP)
1--
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---
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/ (253.93)
-$- MW-}
(254.27)
/
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W~E
S
- - --¡-
LEGEND
MW-l-$- GROUNDWATER MONITORING
WELL LOCATION AND
DESIGNA TION
(255.85) GROUNDWATER ELEVATION
IN FEET ABOVE MEAN SEA
LEVEL (Ft/MSL)
256.20- - GROUNDWATER CONTOUR
IN FEET ABOVE MEAN SEA
LEVEL (Ft/MSL)
CONTOUR INTERVAL=O,50 FEET
.... APPROXIMATE GROUNDWATER
FLOW DIRECTION
~
WASTE
OIL
TANK
o
20
40
--~
~---
SCALE IN FEET
RAil.. SHELL OIL PRODUCTS US
WIIILd TEXACO SERVICE STATION
~ BAKERSFIELD, CALIFORNIA
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FIGURE 2
GROUNDWATER ELEVATION
CONTOUR MAP
09/03/03
5321 STOCKDALE HIGHWAY
BAKERSFIELD. CALIFORNIA
-
-
-
-
-
I
(f)
N
I"'J
L()
-<
a.
f-
U
~
0
""
"-
MW-4
>- Dote TPH ~ BENZENE MTBE
'" (µg/L (µg/L) (µgIL)
0
w 03/25/03 NO<50 NO<0.50 NO<1.0
>
0 06/19/03 NO<50 ND<O,50
"" ND<l,O
"-
"- 09/03/03 ND<50 ND<0.50 ND<1.0
<C
>-
'"
0 MW-3
w
0<:
u Dote TPH-~ BENZENE MTBE
w (µg/L , (µg/L) (µg/L)
J:
u 03/25/03
ND<50 ND<0.50 ND<1,O
06/19/03 ND<50 ND<O,50 ND<l,O
a 09 03/03 ND<50 ND<0.50 ND<l,O
~
~~
z 0
~ «
o~ 0
œ:
w
z
-
(f)
3:
w
Z
MW-2
Dote TPH ~ BENZENE MTBE
(µg/L (µg/L) (µg/L)
03/25/03 ND<50 ND<O,50 ND<l,O
06/19/03 ND<50 ND<O,50 ND<1.0
09/03/03 ND<50 ND<O,50 NO<1.0
-
-
-
-
-
-
-
-
-
STOCKDALE HIGHWAY
CANOPY DISPENSER
ISLAND
(TYP) (TYP)
I I
1 r 1 r 1 r 1 I I
I I I I I I I I I
I I I I I I I I I WASTE
I II II II I I [g::mc[J I OIL
l J l J l J l J I I ~ TANK
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l _J
MW-3
,----,
II ~ \
I I \
I )
\ I
\ I
L.____...J
MW-2
BUILDING
Dote
03/25/03
06/19/03
09/03/03
~
MW-1
1PH-Q BENZENE
(µg/L) (µgIL)
ND<50 ND<0.50
ND<50 ND<O,50
ND<50 ND<O,50
MTBE
(µg/L)
ND<1.0
ND<1.0
ND<1.0
-'-
I
-
-
-
N
W<>E
S
illJJ:ill.
MW-l-$- GROUNDWATER MONITORING
WELL LOCATION AND
DESIGN A TION
TPH-g TOTAL PETROLEUM
HYDROCARBONS
AS GASOLINE
MTBE METHYL TERT-BUTYL
ETHER
µg/L MICROGRAMS PER LITER
ND NOT DETECTED
o 20
r--_-_
SCALE IN FEET
40
"AIM SHELL OIL PRODUCTS US
~IIIII TEXACO SERVICE STATION
~ BAKERSFIELD. CALIFORNIA
FIGURE 3
HYDROCARBON DISTRIBUTION
IN GROUNDWATER MAP
5321 STOCKDALE HIGHWAY
BAKERSFIELD. CALIFORNIA
-
-
-
I
(f)
N
."1
l/)
...:
D..
85
.,<D
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5:
w
z
-.-
UST
(TYP)
-
CANOPY
(TYP)
_. -
-
-
-
STOCKDALE HIGHWAY
/
/
r-$-MW-4
ND<50
I
. r 1 r 1 r 1 r 1 1
I II ,I 1 1 I 1 1
I I II 1 I 1 I I I
I II II II I I
I
I MW-3 l J l J l J l J I
ND<50 L
~
,-----,
II ~ \
I I \
I I
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-$- MW-2
ND<50
I
I
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J
BUILDING
-$- MW-1
ND<50
DISPENSER
ISLAND
(TYP)
--'-
-- ---¡
~
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-~
I
I
I
WASTE
OIL
TANK
I
I
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-
-
-.-
-
N
wiQ-E
S
LEGEND
MW-1 ~ GROUNDWATER MONITORING
WELL LOCATION AND
DESIGNA TION
ND<50 TPH-g CONCENTRATIONS
IN MICROGRAMS PER LITER
(µg/L)
TPH-g TOTAL PETROLEUM
HYDROCARBONS
AS GASOLINE
JJ9/L MICROGRAMS PER LITER
ND NOT DETECTED
o 20
,....----
SCALE IN FEET
40
ft."","" SHEll Oil PRODUCTS US
IllUUIIII TEXACO SERVICE STATION
~ BAKERSFIELD. CALIFORNIA
FIGURE 4
TPH'9 CONCENTRATIONS IN
GROUNDWATER MAP
09/03/03
5321 STOCKDALE HIGHWAY
BAKERSFIELD, CALIFORNIA
-
-
-
í
U)
N
r<)
t[)
<{
(L
t¡
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0
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W
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z
-
-
-
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(TYP)
CANOPY
(TYP)
-
-
-
---
/'
/'
i-$-MW_4
ND<O.50
r I r I r I f I
I II I I I I I
I I II II \ I I
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ND<O.5
-$-
r----'
II I \
I I \
( I
\ I
\ I
L____...J
-$- MW-2
ND<O.50
STOCKDALE HIGHWAY
DISPENSER
ISLAND
(TYP)
-
-
-
-,-
-
-
-'
N
W~E
S
/- ~
I I MW-1-$- GROUNDWATER MONITORING
I I WELL LOCATION AND
DESIGNATION
I I
I I ND<O.50 BENZENE CONCENTRATIONS
I I WASTE IN MICROGRAMS PER LITER
I Qþm::[J I OIL (µg/L)
~ TANK
I I µg/L MICROGRAMS PER LITER
L _J
NO NOT DETECTED
-$- MW-1
ND<O.50
BUILDING
-~
I
I
I
o 20
40
~---
SCALE IN FEET
fl\,,¡,1\tar. SHELL OIL PRODUCTS US
&Mia. TEXACO SERVICE STATION
~ BAKERSFIELD, CALIFORNIA
FIGURE 5
BENZENE CONCENTRATIONS IN
GROUNDWATER MAP
09/03/03
5321 STOCKDALE HIGHWAY
BAKERSFIELD, CALIFORNIA
-
-
-
í
(f]
N
I")
l{)
«
a.
~eJ
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æ::.
Q.Z
6
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w
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-
-
-
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(TYP)
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(TYP)
/
/
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'I"" ND<1.0
r 1 r 1 r 1 r 1
I II II \ I I
I I I I I I I I
I I II I I I I I
I MW-3 l J l J l J l J
ND<1.0
-$-
,----,
II ¡ \
I I \
( !
\ I
\ I
L____..J
-$- MW-2
ND<1.0
-
-
-
-.'-
-
STOCKDALE HIGHWÁ Y
DISPENSER
ISLAND
(TYP)
--I
I I
I I
I I
I I WASTE
I [g:::¡m:::QJ I OIL
I I
I I ~ TANK
l_ -- __J
BUILDING
-$- MW-1
ND<1.0
--~
-
-
-
-
LEGEND
-
-
-
N
W<>-E
S
MW-1-$- GROUNDWATER MONITORING
WELL LOCATION AND
DESIGNA TION
~ MTBE CONCENTRATIONS
IN MICROGRAMS PER LITER
(µg/L)
.u;¡/L MICROGRAMS PER LITER
NO NOT DETECTED
MTBE METHYL TERT-BUTYL
ETHER
o
20
40
,...----
SCALE IN FEET
~ SHELL OIL PRODUCTS US
~. 'TEXACO SERVICE S'TA'T\ON
~ BAKERSFIELD, CALIFORNIA
FIGURE 6
MTBE CONCENTRATIONS IN
GROUNDWATER MAP
09/03/03
5321 STOCKDALE HIGHWAY'
BAKERSFIELD. CALIFORNIA
I
I
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....
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APPENDIX A
FIELD DATA SHEETS
I
I
I
Client S k-e \ {
I Site Address
I Job Number
I Well 10
f"\b.t.~,
I ~ \d- 't.
I -3
1M w . c.f
I
I
I
WELLHEAD INSPECTION CHECKLIST
Page ~ of.c..-L
Date 'í" '3 . ~ 0 C>::s
53.::Lt
5+«, t:~dt:ll..'o4>
"''''''y .
i? c.. ,/!."... ~ ¡:,,'~ lei
0'10", D$'- S H- 1..
Technician
~It#"~ rlqet::._-."
x
WeJlbox - OIher Aclion
Water BaJled Cap Loclt Taken
From Components Replaced Replaced (explain
Wellbox Cleaned below)
X
I
Well Not
Inspected Repair Order
(explain SubmiUed
below)
-
. ,
'.
..
WeJllnspecfed -
No Corrective
Action RequIred
)(
NOTES:
I
I
I
I
BLAII, E TECH SERVICES; II·IC.
SAr,) JOSE
SACRAMEI,'TO
LOS ANGELES
SAN DIEGO
W'.vw,blainotac:ll,COn\
I
I
I
I
I
I
I
I
I
"
SITE INSPECTION CHECKLIST.
Client S.(e//
Site Address 5..3'2/
~/e
. //¿"Y
Date ~..zr; .2~)'
,
ß~.5r&R /!"o..
Job Number
l/. ?oB' 2...$"'" - ~IZ. ~
Technician
~h;:. ~~
Site Status
,
T~D
Branded Station
Vacant Lot
Other
Inspec:ted I Labeled I Cleaned - All Wells on Scope Of Work
l3'
W
G--'.
[H/'
~
o
NJA
Inspected I Cleaned Components - All Other Identifiable Wells
Inspected Site for Investigation Related Trip Hazards
Addre~sed All Outstanding Wellhead Repair Order{s)
N/A
Completed Repair Data Sheet(s)
N/A
I' Inspected Treatment I Remediation System Compound For Secu~itYI
Cleanliness and Appearance .
Ilnspe~ted Vacant Lot for Signs of Habitation, Hazardous Materials or
Terrain, Overgrown Vegetation and Security
I. PLEASE BE ADVISED THAT, UNLESS OTHERWISE INST~UCTED, NO REPAIRS ARE PLANNED FOR THE ISSUES DESCRIBED BELOW
~
D
rN/0
I Outstanding p~oblems / Comments
'. - . ð-l( M()~
(in addlllon to other issues, note all SOW wellboxes that, by design, are not securable)
A-~/es D-1.
.
PJf-If:' ~t'- A1eé Ii'- 7Z./ ,j¿",.¿;Ht./)
~ðr
~¿
A.)tY(-
/.
A--t( ß,eJ(..J- N>/¡:ç
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Vrt-/~ '¿'ð
I
PROJECT COORDINATOR ONLY
Checklist RevieWed
&iJ 1-3-1) ;,/
Initial/Date
Note$
I
BLAINE TECH SERVICES, lNG,
SAN JOSE
SACRAMENTO
LOS ANGELES
SAN DIEGO
www.bl~ir)e ech.ccm
-
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public water
suppl,Y well
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LUFT site
LUIS
-
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LEGE N 0
.MW-1
Proposed G(\').mdwa!er
Monitoring Well
Map Not To Scale
SHEll OIL PRODUCTS US
TEXACO SERVICE STATION
BAKERSFIELD,C ALIFORNI A
SITE MAP WITH PROPOSED WELL LOCATION
5321 STOCKDALE HIGHW A Y
BAKERSFIEt.D, CA
DAlE
11116102
PROJED
FIGLÆ
2
081.5321
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REPAIR DATA SHEET
Page ...1.... of ~
Client .:5 he-If Date rky z.s¡'ZðCI)
Site Address S-3<:.¡ 5'f-s~t!?· IIw"¡ ß~k-/~ L?~.
Job Number D:Sog:z..S--M~ 'Z.. Technician ~k ~A~
Repair Loc:alion
/1(w-z.
Defidencies Corrected
~It. ~Æ£"~
Þ'1t~ðP A-te.ì
Iv~(¿ ¡:¡,¡:..
~
jhrr~s
Materials Used
Repair Loc:alion
PtlV;..-3
/2e/'~
O/~~
Deficiendes Corrected
~
Malerials Used
/ ~A-t!~
~ / 4<=-é.
Repair Loc¿¡lion (f;;)
s~~
ßLYf .f- L. IE.
c¥- IH) De.o ..3.
~·Il 1!J1rl-
Deficiencies Corrected
ß&'~
- , ,
" .
Materials Used
3 ß~j/j
aLAINE TECH SERVICES. INC.
SAN JOSE
SACRAMENTO
Repair LocaUon fttt.J - /
.
Deficiencies Corrected ~~
.
I&~ ·S~/
Materials Used
, 11. \ 1M.. . Se>4- (
Repair Location ø
Deficiencies Corrected
¿ ~ oS tf- .Iff>D
2..... g~(./- ~/~ Wcx,¡j,¿
L . ßcYlfs
..-.=." --,
. w . _ __. ~ . ~
Materials Used
? ßt!) (its
Repair LacaUan (%;).
Deficiencies Corrected
I IZE'h'fP ~ '4- J4.0'i>e.D
s P.,rt//- k-IE ~ ¿,'Ò
./ ßð-N'
6"'¡", ¿:"'1.c!"
------
Materials Used
/ &/i4
LOS ANGELES
SAN DIEGO
w·.·.w.blainetcth.com
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REPAIR DATA SHEET
Page '2. of-L
I
Client :5 hl:?/I
Site Address S-3Z./' ~~G
Job .Number ð3 0"8 zs-- ¡,aIL (
Date
~
ZS2ct)..3
,
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Jluy
ß~¡::-G://¿ &...
Technician p¡¡b£ ~Ae.L
RepairLo~Uon @
Repair Location
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{.:? . ßer/,I- krle tJttt4¿
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Deficiencies Corrected
Deficiencies Corrected
Materials Used I ß¿J If
Materials Used
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Repair LOl?8tion Repair Loc:aUon
Defic:lencies Corrected Deficienc1es ¡Corrected
, ,
Materials Used Materials Used
I
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Repair LOI?8Uon Repair Location
Deficiencies Corrected Deficiencies Corrected
Materials Used Materials Used
I
I
I
BLAINE TECH SERVICES, II·IC,
SAN JOSE
SACRAMENTO
LOS ANGELES
SAI' DIEGO
W'./NI.bCain£!tf!ch.com
I
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WELL GAUGING DATA
Project # a:5 0" 0 '3 ~ S,,·~
Date If· '3 - ;:I c>ø"3;
Client ~ "e If
Site 53'" stot:.f<d....lc. Hw"l r1...~~~.r.~t!'rd
,
Thickness Volume of
Wel1 Depth to of Immiscibles Survey
Size Sheen I Immiscible Immiscible Removed Depth to wáter Depth to wen Point: TOB
Well ID (in.) Odor Liquid (ft.) Liquid (ft.) (ml) (ft) bottom (ft.) or éE.QC:::>
P1W·' L( n '2. bst- I '-I? '-1'1 T t> c:.
"" Wi ~ 'Z. I.f 1"3(, :¡.q J'15.3f-
t"'\\Ai- '3 LI r "?/."N I 'I S-. II -'""::....
1 ,.
Mw...t..I y I J r.2 b I '/Ý. h2.
,
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Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (408) 573~0555
I
I
BTS #: &:7 "3oCf O""!.· S tot - '2.
I· Samp' l~r:'s
'.. . ,. t.o
. Well LD.: Mw- ,
I Total Well Depth (TD): I.,? "'1
SHELL WELL MONITORING DATA S1fEET
Site: ':) "z.'
~+c>c:\= e\
Date: q. "3. 3.00'
Well Diameter: 2
3
€D
6
8
Depth to Water (DTW): 1""3"l. lol1'
I Depth to Free Product: Thiclmess of.Free Product (feet):
Referenced to: ~ Grade D.O. Meter (lfreq'd): ' YSI
I DTW with 80% Recharge [(I-Ieight of Water ColuTIm x 0.20) + DTW]: 1,$.
HACH
Purge Method:
I
I
Bailer
Disposable Baíler
Positive Air Displacement
)( Electric Submersible
WaleITa
Perislaltic
Extraction Pump
Other
Sampling Method:
Bailer
'Þ<Disposable Bailer
Extraction Port
Dedicated Tubing
Other:
<=t. (, (Gals.) X 5
J Case Volume S ecified Volumes
)) .8'" Gals.
Calculated Volume
Well Diameter
I"
2"
3"
Multiplier
0.04
0.16
0.37
Well Diameter Multiplier
4" 0.65
6" 1.47
Other rodius2 + 0.163
Condo Turbidity
Time Temp (oF) pH (mS or~ (NTUs) Gals~ Removed Observations
".'
?~.8 (,..g ?8) ~ L" q. b
12.3 lø . 8"" ~80 (..ö IQ."3
-=11. it ~ .g- ,.,"'tq b4~ ;>q.c>
Yes
<lSP
Gal lOllS actually evacuated: ;>". &>
Sampling Date: '1- 3, aoo'3 Sampling Time: o~' ~o
1 I D Laboratory:
amp e . .: I"1w- ,
Depth to Water:¡ s "!o. I "
<C~CI~ Co1umbia' Other
nalyzed for: TPH-G BTEX MTBE TPH-D Oxygenates (5) Other: Sf!'f" ~Þ<.N
-<B I.D, (if applicable):
nalyzed for: TPH-G BTEX
@
Time
Duplicate I.D. (if applicable):
Oxygenates (5) Other:
J'vfTBE TPH-D
D.O. (ifreq'd):
.R.P. (ífreq'd):
Pre-purge:
Pre-purge:
mg/L
Post-purge:
mg/L
mV
Post-purge:
mV
rlaine Tech Services, Inc. 1680 Rogers Ave., sa," Jose, CA 95112 (800) 54~-7558
I
I - ,
BTS #: () '30'1 0 "'?. S to¡ - '2.
I Sampler: ~l.
Well ID.: MW. do
I Total Well Depth (TD): NS".."'1-
SHELL WELL lVIONITORlNG DATA SHEET
Site: $ "l. 1
Stoc,," c\ ,
Dat~: q . 3- a-c 0
Well Diameter: 2
3
ø
6
8
Depth to Water (DTW): I~'.T,
I Depth to Free Product: Thiclmess of Free Product (feet):
Referenced to: ~ Grade D.O. Meter (ifreqtd): YSI
I DTW with 80% Recharge [(Height ofVvater Column x 0.20) + DTWJ: I ~ L/. S I
HACH
Purge Method:
I
I
I
Bailer
Disposable Bailer
Positive Air Displacement
~Electric Submersible
Waterra
Peristal tic
Extraction Pump
Other
Sampling Method:
BaiJer
,,<DìsposabJe Bailer
Extraction Port
Dedicated Tubing
Other:
Well Diameter MulLiDlier Well Diameter MultiDlier
'" 0.04 4" 0.65
<¡·It (Gals.) X 5 ;) G.. c.l Gals. 2" 0.16 6" 1.47
= radiusl .. 0.163
1 Case Volume Sœcified Volumes Calculated Volum... 3" 0.37 Other
I Condo Turbidity
Time Temp (oF) pH (mS or ~ (NTUs) j Gals: Removed Observations
91. Cf <'.ct , 1- -=1- ' , i.}?
I oq'3s 3>"2-
o""1~ =1f. "'!. ¿'.ct 5-s.5 ?'øt,;Oo ,'1-..
I ....11"'1 =/0.":1- b .g- S"JLf ....' Co) O~ jr..·S
I
I Did well dewater? Yes cWÞ Gallons actually evacuated: ~ b. S
,
Sampling Date: '1- 3- ,;)00'3 Sampling Time: o.:tçC) Depth to Water: ( ""3':'. 4f::¡-
I Sample 1.D.: ¡VI t..J - do- Laboratory: ~cle~ Columbia Other
I Analyzed for: TPH-G BTEX MTBE TPH-D Oxygenates (5) Other: S'c."'t'" çbv.J
EB I.D. (if app1icable): @ Duplicate I.D. (if appl1cable):
Time
I Analyzed for: TPH-G BTEX MTBE TPH-D Oxygenates (5) Other:
D.O. (ifreq'd): Pre-purge: mf!,/l- Post-purge: mg/L
I O.R.P. (ifreq'd): Pre-purge: mV Post -purge: mV
I Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (800) 545~ 7558
I
I
I
I
I
I
Purge Method:
I
I
I
SHELL WELL lVIONITORING DATA SHEET
BTS #: ð '30'1 0 ""!. S 1-1 ~ '2.. Site: '5' "t-z. , Stce"'- 0:\_1_ ""-,u R". ~~...~ "'·.leI
Sampler: S (.'''''..... .rI ,"" -- Date: q - 5Þ a.oc.....
Wen I.D.: MW <~ Well Diameter: 2 3 (D 6 8
Total Well Depth (TD): I l./ ~. 1/ Depth to Water (DTW): I -St. 4'-'
Depth to Free Product: Thiclmess of Free Product (feet):
Referenced to: ~ Grade D.O. Meter (ifreq'd): YSI HACH
DTW with 80% Recharge [(Height of Water Column x 0.20) + DTW]: 1'1".1"':1-
Bailer
Disposable Bailer
Positive Air Displacement
~Iectric Submersible
Waterra
Peristaltic
EXITaction Pump
Other
Sampling Method:
Bailer
K'Disposable Bailer
Extraction Port
Dedicated Tubing
Other:
Well Diameter Multiplier Well Diameter Multiplier
\" 0.04 4" 0.65
1;-, 9' (Gals.) X S. ;).(. . ":/ Gals. 2" 0.]6 ,6" 1.47
= radius2 + 0.16J
1 Case Volume Specified Volumes Calculated Volume J" 0.]7 Other
I Condo Turbidity
Time Temp (oF) pH (mS or~ (NTUs) Gals: Removed Observations
....
I lonG,. =t 1.. 3 ' ~.o >'S '1~> q.t>
,ooq "':Jo. '-I lÞ.~ '3 , , '390 1&-.0
I '0("2- ?O.I t...q "310 "3yg- ~'"i.o
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I Did well de'water? Yes ~ Gallons achtally evacuated: ~ r. t>
Sampling Time: Depth to Water:
Sampling Date: "'- S' ~oo:3 ID:::Jc:> "'3 '1. ~ "i
I Sample I.D.: ~ w - 3 Laboratory: ~Cl~ Columbia Other
I Analyzed for: TPH-G' BTEX MTBE TPH-D Oxygenates (5) Other: 5"~f!' ~Þvo.f
EB I.D. (if applicable): @ Duplicate I.D. (if applicable):
Time
I ' .
Analyzed for: TPH-G BTEX MTBE TPH-D Oxygenates (5) Other:
D.O. (ifreqrd): Pre-purge: mg/L Post-purge: mg/L
I O.R.P. (ifreq'd): Pre-purge: mV Post-purge: mY
I Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (800) 545e7558
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Ptirge Method:
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SHELL WELL lVIONITORING DATA StrEET
BTS #: 030" O~. 5H-, Site: S "1"2. , Stø~\c 0::\.....,- ,",,,,,,,.. Rðo I.!~"''' r...././
San1pler: ~ (.n..... ,¡ ,h ,.. Dat,e: '\. "'3- 3.00....
Well I.D.: I"fw- L/ Well Diameter: 2 3 €> 6 8
Total Well Depth (TD): I 'I &(. lD ~ Depth to Water (DTW): ( "3,. ? ~
Depth to Free Product: Thiclmess of Free Product (feet):
Referenced to: ~ Grade D.O. Meter (ifreq'd): YSI BACH
DTW with 80% Recharge [(Height of Water Column x 0.20) + DTW]: \")"1.9'7 .
Bailer
Disposable Bailer
Positive Air Displacement
;<Electric Submersible
Waterra
Peristaltic
Extraction Pump
Other
Sampling Method:
Bailer
~Disposable Bailer
Extraction Port
Dedicated Tubing
Other:
Well Diameler Multiplier Well Diameter Multiplier
. 0.65
I" 0,04 4"
&-.~ (Gals,) X S. ~ lÞ. ( Gals. 2" 0.16 6" 1.47
= radius1 + 0,163
1 Case Volume Specified Volumes Calculated Volume 3" 0.37 Other
I Condo Turbidity
Time Temp (oF) pH (mS or~) (1'{TUs) Gals~ Removed Observations
I 'c> o;r: q ?-'2. , , <...<=t 500 ?, D"O ·'·'fi t 8' S.. 'of... / r...., 6..J
b.f I ~ ":1- ,t \ I
,nUl. ~o. , 5DS" ?tOoo
I It
~~.q ~.R" "'3 o~ ,~ s, ;)fÞ . S ,-
f c> t.( lø
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I Did well dewater? Yes @õ) Gallons actually evacuated: .:l c.. S"
Sampling Date: ~ - '5' .7 bÞ '3 Sampling Time: to s- S' Depth to Water:
13~ 1.01
I Sample I.D.: ""tAP 1./ Laboratory: ~c~ Columbia Other
I Analyzed for: TPH-G BTEX MTBE TPH-D Oxygenates (5) Other: S'~t" ~O¥J
EB I.D. (if applicable): @ . Duplicate I.D. (if applicable):
lImo
I Analyzed for: TPH-G BTEX MTBE TPH-D Oxygenates (5) Other:
mg/L mg/L
D.O. (ifreq'd): Pre-purge: Post-purge:
O.R.P. (ifreq'd): Pre-purge: mV Post-purge: 'mV
I Blaine Tech Services, Inc. 1680 Rogers Ave., San Jose, CA 95112 (800) 545-7558
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ApPENDIX B
FIELD PROCEDURES
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1680 ROGERS AVENUE
SAN JOSE, CA 95112-1105
(408) 573-7771 FAX
(408) 573-0555 PHONE
CONTRACTOR'S LICENSE #746684
www.blainetech.com
BLAINE
TECH SERVICES,,,,.
September 25,2003
Tony Palagyi
Shell Oil Products US
P.O. Box 7869
Burbank, CA 91510-7869
Third QUaIier 2003 Groundwater Monitoring at
Shell-branded Service Station
5321 Stockdale Highway
Bakersfield, CA
Monitoring perfonned 011 September 3,2003
Groundwater Monitoring RepOli 030903-SH-2
This repOli covers the routine monitoring of grolindwater wells at this Shell,-branded facility. In
accordance with staI1dard procedures that conform to Regional Water Quality Control Board
requirements, routine field data collection includes depth to water, total well depth, thickness of
any separate inllniscible layer, water colunm volume, calculated purge volume (if applicable),
elapsed evacuation t~me (if applicable), total volume of water removed (if applicable), and
standard water parameter instrument readings. Sample material is collected, contained, stored,
and transpOlied to the laboratory in confom1ance with EP A staI1dards. Purgewater (if applicable)
is, likewise, collected and traI1sported to D.K. Enviromnental. '
Basic field infoTInation is presented alongside analytical values excerpted from the laboratory
repOli in the cumulative table of WELL CONCENTRATIONS. The full analytical repoli for
the most recent samples aI1d the field data: sheets are attached to this report.
At a minimum, Blaine Tech Services; Inc. field persolmeI are certified on completion of a forty-
hour Hazardous Materials and Emergency Response training course per 29 CFR 1910.120. Field
personnel are also enrolled inannual eight-hour refresher courses.
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Blaine Tech Services, Inc. conducts sampling and documentation assignmentsofthis type as an
independent third party. Our activities at this site consisted of objective data and sample
collection only. No interpretation of analytical results, defining of hydrological conditions or
fonnulation of recoII1lllendations was perfonned.
Please call if you have any questions.
Yours truly,
Francis Thie
Vice President
·FT /ks
attachments: Cumulative Table of WELL CONCENTRATIONS
Certified Analytical Report
Fielçl Data Sheets
cc: Kathryn Ewing
KHM Environmental Management, Inc.-
911 S. Primrose Ave., Suite K
Monrovia, CA 91016
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'APPENDix C
WASTE DISPOSAL DOCUMENTS
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.~
j) NO. 639294
NON-HAZARDOUS WASTE DATA FORM
EPA
I.D.
NO,
SHELL OIL PRODUCTS US
VIIC:# S-?Z/ HDr:~""fl!.
/1.....'1'
f1a..I£.ersf:e:rdr <::./J
NAME
P.O. BOX 7869
PROFILE
NO.
ADDRESS
BURBANK, CA 91.51.0-7ß69
CITY. STATE, ZIP AlTf\! r
713 241-151.6
PHONE NO, (
';':) I '
I tJlI'I I "'- '\."j Y ;
CONTAINERS: No.
If ç; Û....\
VOLUME
WEIGHT
TYPE:
!}Q ~Ö~IC 0 ~Wlf~(
o OTHER
o DRUMS 0 CARTONS
NON-HAZARDOUS GROUNDWATER
PURGED GRDUNDif\JATER
WASTe DESCRIPTION GENERATING PROCESS
COMPONENTS OF WASTE PPM qb COMPONENTS OF WASTE PPM %
WATER 99-100% SAP.:#:
1. s.
TPH -:: 10/0 I INCIDENT#' c¡ =t-'t ,",,::n '2. 7-
2. 6.
RIPR :#=
3. 7.
BES! #
4, .... 10 vv a.
.r Ô"" lIaUID 0 0 0
PROPERTIES: pH_ 0 SOLID SLUpGE SLURRY OTHER
HANDLING INSTRUCTIONS:
24-HOUR EI\1ERGENCY PHONE {BOOj 424-51"300
THE GENERATOR CERTIFIES THAT THE
WASTE AS DESCRIBED IS 100%
NON·HAZARDOUS.
Ç40f'¡'" /lctc: ,i:::.;.,..,~
~!I~
TYPED OR PRINTED FULL NAME & SIGNATURE
{On behalf of SOP US} V:(O;-
DATE
NIETO AND SONS TRUCKl[1JG, INC.
NAME
5T TRAN5P~!, I
Blaine Tech 5el'\1lces.
G merCÿ Plaœ
?036Q fa OSRfYICE ORDER N .
Torrance. CA 9 ::>
10)782-2465 ,
(3 _ ,,,,S/GIWP'EJA'TË."-
1281 BREA CANYON ROAD
ADDRESS
BREl...., CALlFORNIß.. 9282.1
CITY, STATE, ZIP
(714) 990-6855
f"HONE NO.
TRUCK, UNIT, I,D. NO.
D/K ENVIRONMENTAL
TYPED OR PRINTED ~ULL NAME & SIGNATURE
NAME
~PA
I.D.
NO.
36.50 E. 261H STREET
.DISPOSAL METHOD
o LANDFILL 0 OTHER
ADDRESS
L02. ANGELE2., CA 90023
CITY. STATE. ZIP
(323) 268-50.56
PHONE NO,
TYPED OR PRINTED FULL NAME & SIGNATURE
DATE
GEN OLD/NEW L A TONS
TRANS S 8
RT/CD HWDF
c/o NONE DISCREPANCY
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ApPENDIX D
LABORATORY REpORT AND
CHAIN-OF-CUSTODY DOCUMENTS
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~ -a/science·
l:,j¥nVironmenta/
,£. aboratories, Inc.
September 10, 2003
Nick Sudano
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Subject: Calscience Work Order No.:
Client Reference:
03-09-0129
5321 Stockdale Highway, Bakersfield, CA
Dear Client:
Enclosed is an analytical report for the above-referenced project. The samples'
included in this report were received 9/3/2003 and analyzed in accordance with
the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the
guidelines established in our Quality Assurance Program Manual, applicable standard
operating procedures, and other related documentation. The original report of any
subcontracted analysis is provided herein, and followS the standard Calscience data
package. The results in this analytical report are limited to the samples tested and any
reproduction thereof must be made in its entirety.
-, If you have any questions regarding this report, please do not hesitate to contact
'the undersigned.
M:dfl¿
Quality Assurance Manager
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494.,· FAX: (714) 894-7501
'_'_"'_".._ ___.._. ___._.._...____..~. _..,__ .._._ ...._._.. _._.,..~ ...__ M_._____....,.___...._._..__.~~_....__...._, .._.._......... __..____,...._..__.._..~.... ...~....." .... ....., .._._.__......_...._... ,_._..' ...._.... .,.,~__,.. _. 'M__"'..__'" ._.__,__....'...___h..._.._......_ ... .,.
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¡¡ - a/science
I::, nvironmenta/
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
ANALYTICAL REPORT
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I
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
EPA5030B
DHS LUFT
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Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
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Client Sample Number
Matrix
Date Date
Prepared Analyzed QC Batch 10
,:: :;~f#~,*j;~'::'ii~ìifii¡~~:):t~~~öfi~,~:#0::'~:.,,~"·'·':
I
Parameter Result RL DF
TPH as Gasoline ND 50
SurroQates: REC(%) Control
Lim its
1,4-Bromofluorobenzene 97 49-133
Qual
Units
ugIL
Qual
I
·..··;~l~~~tU',;.,ii~~ª~~~~;:63~i~þ.~~'· ..
:t" .
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Parameter Result RL OF
TPH as Gasoline ND 50
SurroQates: REC(%) Control
Limits
1,4-Bromofluorobenzene 95 49-133
Qual
Units
ug/L
I
Qual
I
;v·'qi:¡;~:;~~4~~~.~1 .
1,4-Bromofluorobenzene
NO
REC (%)
91
RL
50
Control
Limits
49-133
'"~~i2i!ik~' 'C'
DF
Q!@!
Units
Parameter
Result
I
TPH as Gasoline
Surroaates:
ug/L
Qual
I
'::.:~t!:1~~J:'~,'
.', '<:~~l~:;:;à;¿1~~(~~~¡~~'~~~'~f3o.1· ,"
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Parameter Result RL OF Qual Units
TPH as Gasoline NO 50 ug/L
SurroQates: REC (%) . Control Qual
Limits
1,4-Bromofluorobenzene 83 49-133
Åiiûi~i!ìi1!t!~1:::[::~.:··:;,~}:~~~,~,:.
, . .,,~. ."'. ,..:-"
. , .::::·:~~f¥;~é+'~q'~i'~~¡9'ii"j;~~t!!l~Yi>::~h:q~#~ ,..
.,,~t~;~)i .·',q9,tlp~~~!~~~~~()4Bø1'.
I
" ~ <S'.~~~:h~.~:
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Parameter Result RL OF Qual Units
TPH as Gasoline NO 50 ug/L
SurroQates: REC(%) Control Qual
Limits
1,4-Bromofluorobenzene 92 49-133
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. ,RL - Reporting Limit ,
DF - Dilution Factor, Qual - Qualifiers
I
7440 Lincoln Way, Garden Grove,CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
. .. . '-_'~'__~_'_'_"'~_'___'__'__"''''_'' _.__~._",,_..__. _ _. .,_____._ ._w..__~~____..._..-.._··__~··_·. ..~.__..___.~_ _,___",_,_._.
,....,- .'-. -...... . .....-...............-.-.-.. ".--.-- ,.-......;.----..--...-.--.-.--- .." -.------.-----..--.. ,"..-. .
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æ - a/science
I:,ªn vironmen tal
Laboratories, Inc.
ANALYTICAL REPORT
I
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
EPA 5030B
EPA 8260B
I
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Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 5
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Lab Sample Date Date Date
Number Collected Matrix Prepared Analyzed
:.; I:îDt0¡~;:f:;~~~\~t;r¡~i1iI1,~f~~lf~0~;~)f:~;s.:~~i:lt~~~t~~~~ijl;~é~:~~~~~1!,~:~:"~I;~:~?~:~~
QC Batch ID
,^p~~(q~~8j~'::<¡:
I
Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units
Acetone ND 10 1 ug/L 1,1 "Dichloropropene ND 1.0 1 ug/L
Benzene ND 0,50 1 ug/L c-1,3-Dichloropropene NO 0.50 1 ug/L
Bromobenzene NO 1.0 1 ug/L t-1,3-Dichloropropene NO 0.50 1 ug/L
Bromochloromethane NO 1.0 1 ugfL Ethylbenzene ND 1.0 1 ugfL
Bromodichloromethane ND 1.0 1 ugfL 2-Hexanone NO 10 1 ug/L
Bromoform ND 1.0 1 ug/L Isopropyl benzene NO 1.0 1 ugfL
Bromomethane NO 10 1 ug/L p-Isopropyltoluene NO 1.0 1 ug/L
2-Butanone NO 10 1 ugfL Methylene Chloride NO 10 1 ugfL
n-Butylbenzene ND 1,0 1 ug/L 4-Methyl-2-Pentanone ND 10 1 ug/L
sec-Butylbenzene NO 1.0 1 ug/L Naphthalene ND 10 1 ugfL
tert-Butylbenzene NO 1,0 1 ugfL n-Propylbenzene ND 1.0 1 ug/L
Carbon Disulfide ND 10 1 ug/L Styrene ND 1.0 1 ugfL
Carbon Tetrachloride NO 0.50 1 ug/L 1,1,1,2-Tetrachloroethane ND 1.0 1 ug/L
Chlorobenzene NO 1,0 1 ug/L 1,1,2,2-Tetrachloroethane ND 1.0 1 ug/L
Chloroethane NO 1.0 1 ug/L T etrachloroethene NO 1,0 1 ug/L
Chloroform ND 1.0 1 ug/L Toluene ND 1,0 1 ug/L
Chloromethane ND 10 1 ug/L 1,2,3· T richlorobenzene ND 1.0 1 ug/L
2-Chlorotoluene NO 1.0 1 ug/L 1,2,4- Trichlorobenzene NO 1.0 1 ug/L
4-Chlorotoluene ND 1.0 1 ugfL 1,1,1- Trichloroethane NO 1.0 1 ug/L
Dibromochloromethane ND 1:0 1 ug/L 1,1,2- Trichloroethane ND 1,0 1 ugfL
1,2-0ibromo-3-Chloropropane NO 5.0 1 ug/L Trichloroethene NO 1,0 1 Ug/L
1,2-Dibromoethane' NO 1.0 1 ug/L Trichlorofluoromethane ND 10 1 ugfL
Dibromomethane ND 1.0 1 ug/L 1,2,3- Trichloropropane ND 5.0 1 ug/L
1,2-0ichlorobenzene NO 1.0 1 ug/L 1,2,4- Trimethylbenzene NO 1.0 1 ug/L
1,3,Dichlorobenzene ND 1.0 1 ug/L 1,3,5- Trimethylbenzene NO 1,0 1 ugfL
1,4-0ichlorobenzene . NO 1.0 1 ug/L Vinyl Acetate NO 10 1 ug/L
Oichlorodifluoromethane NO 1.0 1 ugfL Vinyl Chloride NO 0.50 1 ugfL
1,1-Dichloroethane NO 1.0 1 ug/L p/m-Xylene ND 1,0 1 ug/L
1,2-Dichloroethane NO 0.50 1 ug/L o-Xylene NO 1,0 1 ug/L
1,1-Dichloroethene NO 1.0 1 ugfL Methyl-t-Butyl Ether (MTBE) ND 1,0 1 ug/L
c-1,2-0ichloroethene NO 1.0 1 ug/L Tert-Butyl Alcohol (TBA) NO 10 1 ugfL
t-1,2-Dichloroethene NO 1.0 1 ug/L Diisopropyl Ether (DIPE) NO 2.0 1 ug/L
1,2-Dichloropropane ND 1.0 1 ug/L Ethyl-I-Butyl Ether (ETBE) NO 2.0 1 ug/l
1,3-0ichloroproparie NO 1.0 1 ug/L Tert-Amyl-Methyl Ether (TAME) NO 2.0 1 ug/l
2,2-Dichloropropane ND 1.0 1 ug/L Ethanol NO 100 1 ug/L
Surròaates: REC (0/0) Control Qual Surroaates: REC(O/O) Control Q!m!
Limits
Oibromofluoromethane 105 86-118 Toluene-d8 99 88-110
1,4-Bromofluorobenzene 100 86-115
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RL - Reporting Limit ,
DF - Dilution Factor .
Qual - Qualifiers
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7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494
.
FAX: (714) 894-7501
".h.._....__·,__._._. ._"...
_ .~.~ .,~. P. "_." . ....._~_., .".._............~._ ~._........._...~..__....__,....._.., _,_J,__..,.......__.._...._J~ _..,.______ .... __~, ...._~... ,"w. ..._ .~_..._......_.... _.... ,n _"....._......". .._._.....-_.._....~_...._.-_.. .. .- '.._~.
,". -.-.... -....." .
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S - a/science
I:En vironmen tal
Laboratories, Inc.
ANALYTICAL REPORT
I
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Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
. Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
EPA 5030B
EPA 8260B
I
Project: 5321 Stockdale Highway, Bakersfield, CA Page 2 of 5
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Oate Oate
Matrix Prepared Analyzed QC Batch 10
·,..i;::')f~'~f!:~r:OJ' '~Ä~\~;¡[$~(5,~~ì;i;,;;~':Ci"
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Parameter Result RL OF Qual Units Parameter Result RL QE Qual Units
Acetone NO 10 1 ug/L 1,1-0ichloropropene NO 1.0 1 ug/L
Benzene NO 0.50 1 ug/L c-1,3-0ichloropropene NO 0.50 1 ug/L
Bromobenzene NO 1.0 1 ug/L t-1,3-0ichloropropene NO 0.50 1 ug/L
Bromochloromethane NO 1.0 1 ug/L Ethylbenzene NO 1,0 1 ug/L
Bromodichloromethane NO 1.0 1 ug/L 2-Hexanone NO 10 1 ug/L
Bromoform NO 1.0 1 ug/L Isopropyl benzene NO 1.0 1 ug/L
Bromomethane NO 10 1 ug/L p-Isopropyltoluene NO 1,0 1 ug/L
2-Butanone NO 10 1 ug/L Methylene Chloride NO 10 1 ug/L
n-Butylbenzene NO 1.0 1 ug/L 4-Methyl-2-Pentanone NO 10 1 ug/L
sec-Butylbenzene NO 1.0 1 ug/L Naphthalene NO 10 1 ug/L
tert-Butylbenzene NO 1.0 1 ug/L n-Propylbenzehe NO 1.0 1 ug/L
Carbon Disulfide NO 10 1 ug/L Styrene NO 1.0 1 ug/L
Carbon Tetrachloride NO 0.50 1 ug/L ~ ,1.1,2-Tetrachloroethane NO 1.0 1 ug/L
Chlorobenzene NO 1.0 1 uglL 1,1,2,2- Tetrachloroethane NO 1,0 1 ug/L
Chloroethane NO 1.0 1 ug/L Tetrachloroethene NO 1.0 1 ug/L
Chloroform NO 1.0 1 ug/L Toluene NO 1.0 1 ug/L
Chloromethane NO 10 1 ug/L 1,2,3- Trichlorobenzene NO 1.0 1 ug/L
2-Chlorotoluene NO 1.0 1 ug/L - 1,2,4-Trichlorobenzene NO 1;0 1 ug/L
4-Chlorotoluene NO 1.0 1 ug/L 1,1,1-Trichloroethane NO 1,0 1 ug/L
Oibromochloromethane NO 1.0 1 ug/L 1,1,2- Trichloroethane NO 1,0 1 ug/L
1,2-0ibromo-3-Chloropropane NO 5.0 1 ug/L Trichloroethene NO 1;0 1 ug/L
1,2-0ibromoethane NO 1,0 1 ug/L Trichlorofluoromethane NO 10 1 ug/L
Oibromomethane NO 1.0 1 ug/L 1,2,3-Trichloropropane NO 5.0 1 ug/L
1,2-0ichlorobenzene NO 1.0 1 ug/L 1,2,4,Trimethylbenzene NO 1.0 1 ug/L
1,3-0ichlorobenzene NO 1.0 1 ug/L 1,3,5- Trimethylbenzene NO 1.0 1 ug/L
1,4-0ichlorobenzene NO 1,0 1 ug/L Vinyl Acetate NO 10 1 ug/L
. Oichlorodifluoromethane NO 1.0 1 ug/L Vinyl Chloride NO 0.50 1 ug/L
1,1-0ichloroethane NO 1.0 1 ug/L p/m-XyleÍ1e NO 1.0 1 ug/L
1,2-0ichloroethane NO 0.50 1 ug/L o-Xylene NO 1.0 1 ug/L
1,1-0ichloroethene NO 1.0 1 ug/L Methyl-t-Butyl Ether (MTBE) NO 1.0 1 ug/L
c-1,2-0ichloroethene NO 1.0 1 ug/L Tert-Butyl Alcohol (TBA) NO 10 1 ug/L
t-1,2-0ichloroethene NO 1,0 1 ug/L Oi!sopropyl Ether (OIPE) NO 2.0 1 ug/L
1,2-0ichloropropane NO 1.0 1 ug/L Ethyl-t-Butyl Ether (ETBE) NO 2.0 1 ug/L
1,3-0ichloropropane NO 1.0 1 ug/L Tert-Amyl-Methyl Ether (TAME) NO 2.0 1 ug/L
2,2-0ichloropropane NO 1.0 1 ug/L . Ethanol NO 100 ,1 ug/L
Surroaates: REC(%) Control Qual Surrooates: REC(%) , Control Qual
Limits
Oibromofluoromethane 105 86-118 Toluene-d8 99 88-110
1,4-Bromofluorobenzene 99 86-115
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RL . Reporting Limit ,
OF - Dilution Factor ,
Qual - Qualifiers
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7440 Lincoln Way, Gardèn Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: ((14) 894-7501
....,..._._....~.........,~..~_. '"'''' ...._._ ......__ "'h.___._..,,___._,., ~._ __~____~___,_"_"",,_,,~~~,,._.._~_ .._"'_ ._,.. .__._.__,....__....H..
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I,
I
sa/science
I:,~nvironmental
Laboratories, Inc.
ANALYTICAL REPORT
I
I
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Mett)od:
09/03/03
03-09-0129
EPA 5030B
EPA 82608
I
Project: 5321 Stockdale Highway, 8akersfiéld, CA
Page 3 of 5
I
Oate
I
Parameter Result RL OF Qual Units Parameter Result RL OF QMill Units
Acetone NO 10 1 ugfL 1,1-0ichloropropene NO 1.0 1 ugfL
Benzene NO 0.50 1 ugfL c-1,3-0ichloropropene NO 0.50 1 ugfL
Bromobenzene NO 1.0 1 ugfL t-1,3-0ichloropropene NO 0.50 1 ugfL
Bromochloromethane NO 1.0 1 uglL Ethylbenzene NO 1.0 1 ugfL
Bromodichloromethane NO 1.0 1 ugfL 2-Hexanone NO 10 1 ugfL
Bromoform NO 1,0 1 ugfL Isopropytbenzene NO 1,0 1 ugfl
Bromomethane NO 10 1 ugfL p-Isopropyltoluene NO 1.0 1 ugfL
2-Butanone NO 10 1 uglL Methylene Chloride NO 10 1 ugfL
n-Butylbenzene NO 1.0 1 ugfL . 4-Methyt-2-Pentanone NO 10 1 ugfL
sec-Butylbenzene NO 1.0 1 ugfL Naphthalene NO 10 1 ugfL
tert-Butylbenzene NO 1.0 1 ug/L n-Propylbenzene NO 1.0 1 ug/L
Carbon Disulfide NO 10 1 ug/L Styrene NO 1.0 1 ugfL
Carbon Tetrachloride NO 0,50 1 ug/L 1,1.1,2-Tetrachloroethane NO 1.0 1 ugfL
Chlorobenzene NO 1,0 1 ugfL 1,1,2,2-Tetrachloroethane NO 1.0 1 ugfL
Chloroethane NO . 1.0 1 ugfL Tetrachloroethene NO 1.0 1 ugfL
Chloroform NO 1.0 1 ugfL - Toluene NO 1,0 1 ugfL
Chloromethane NO 10 1 ugfL 1,2,3-Trichlorobenzene NO 1.0 1 ugfL
2-Chlorotoluene NO 1.0 1 uglL 1,2,4-Trichlorobenzene NO 1.0 1 ugfL
4-Chlorotoluene NO 1,0 1 ugfL 1,1,1-Trichloroethane NO 1.0 1 ugfL
Oibromochloromethane NO 1,0 1 ugfL' 1,1,2- Trichloroethane NO 1,0 1 ugfL
1,2-Dibromo-3-Chloropropane NO 5.0 1 ug/L Trichloroethene NO 1.0 1 ug/L
1,2-Dibromoethane NO 1,0 1 ug/L Trichlorofluoromethane NO 10 1 ug/L
Oibromomethane NO 1.0 1 ug/L 1,2,3-Trichloroprbpane ,NO 5.0 1 ug/L
1,2-0ichlorobenzene NO 1.0 1 ug/L 1,2,4- Trimethylbenzene NO 1.0 1 ug/L
1,3-Dichlorobenzene NO 1.0 1 ugfL 1,3,5-Trimethylbenzene NO 1,0 1 ugfL
1,4-0ichlorobenzene NO 1.0 1 ugfL Vinyl Acetate ND 10 1 ugfL
Oichlorodifluoromethane NO 1,0 1 ug/L Vinyl Chloride NO 0,50 1 ug/L
·1,1-0ichloroethane NO 1.0 1 ugfL p/m-Xylene NO 1.0 1 ug/L
1,2-0ichloroethane NO 0.50 1 ugfL o-Xylene NO 1.0 1 ugfL
1,1-0ichloroethene NO 1.0 1 ug/L Methyl-t-Butyl Ether (MTBE) NO 1.0 1 ugfL
c-1,2-0ichloroethene NO 1.0 1 ug/L Tert-Butyl Alcohol (TBA) NO 10 1 ug/L
t-1,2-0ichloroethene NO 1.0 1 ug/L Oiisopropyt Ether (OIPE) NO 2.0 1 ugfL
1,2-0ichloropropane NO 1.0 1 uglL Ethyl-t-Butyl Ether (ETBE) NO 2,0 1 uglL
1,3-0ichloropropane NO 1.0 1 ug/L Tert-Amyl-Methyl Ether (TAME) NO 2.0 1 ug/L
2,2-0Ichloropropane NO 1.0 1 ugfL Ethanol NO 100 1 ugfL
Surrogates: REC(%) Control Quat Surroaates: REC(%) Control QMill
Limits
Oibromofluoromethane 104 86·118 Toluene-dB 99 B8-110
1,4-Bromofluorobenzene 99 86-115
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RL - Reporting Limit ,
DF, Dilution Factor ,
Qual, Qualifiers
I
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
'.-., ._._.._..~.._._..._. - .. ....-..-----..- .~....,_. ....~~~.. -, ".'- _............... .,.__.~_............~.,~..._-..- ".....,_.,.~."
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..... .._.' .""-"-'.' -.-.....--. .
.. ... ."_' _O·_"·n..'.·
I
I
I
IE -a/science
I:,#fpvironmenta/
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance,CA 90501-1511
ANALYTICAL REPORT
I
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
EPA 5030B
EPA 8260B
I
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 4 of 5
I
Client Sample Number
. Lab Sample
Number
QC Batch 10
I
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Parameter Result RL OF Qual Units Parameter Result RL OF Q!!ill Units
Acetone NO 10 1 ug/L 1,1~Oichloropropene NO 1.0 1 ug/L
Benzene NO 0,50 1 uglL c-1,3-Dichloropropene NO 0.50 1 ug/L
Bromobenzene NO 1.0 1 ug/L t-1,3-0ichloropropene NO 0,50 1 ug/L
Bromochloromethane NO 1,0 1 uglL Ethytbenzene NO 1.0 1 ug/L
Bromodichloromethanè NO 1.0 1 ug/L 2-Hexanone ND 10 1 ug/L
Bromoform NO 1.0 1 ug/L Isopropylbenzene NO 1.0 1 ug/L
Bromomethane NO 10 1 ug/L p-Isopropyltoluene NO 1.0 1 uglL
2-Butanone NO 10 1 ug/L Methylene Chloride NO 10 1 ug/L
n-Butytbenzene NO 1.0 1 ug/L 4-Methyl-2-Pentanone NO 10 1 ug/L
sec-Butylbenzene ND 1,0 1 ug/L Naphthalene ND 10 1 ug/L
tert-Butyfbenzene NO 1,0 1 ug/L n-Propylbenzene NO 1,0 1 ug/L
Carbon Disulfide ND 10 1 ug/L Styrene NO 1,0 1 uglL
Carbon Tetrachloride NO 0.50 1 uglL 1 ,1,1,2- Tetrachloroethane NO 1.0 1 ug/L
Chlorobenzene NO 1,0 1 ug/L 1,1,2,2-Tetrachloroethane NO 1,0 1 ug/L
Chloroethane NO 1,0 1 ug/L T etrachloroethene NO 1.0 1 ug/L
Chloroform NO 1.0 1 ug/L Toluene NO 1.0 1 ug/L
Chloromethane NO 10 1 ug/L 1,2,3-Trichlorobenzene NO 1.0 1 ug/L
2-Chlorotoluene NO 1.0 1 uglL 1,2,4- Trichlorobenzene NO 1,0 1 ug/L
4-ChlorotoJuene NO 1.0 1 ug/L 1,1,1- Trichloroethane ND 1.0 1 ug/L
Oibromochloromethane NO 1.0 1 ug/L 1,1,2-Trichloroethane NO 1,0 1 ug/L
1,2-0ibromo-3-Chloropropane ND 5.0 1 ug/L Trichloroethene ND 1.0 1 ug/L
1,2-0ibromoethane NO 1.0 1 ug/L Trichlorofluoromethane NO 10 1 ug/L
Dibromomethane ND 1.0 1 ug/L 1,2,3- Trichloropropane NO 5.0 1 ug/L
1,2-Dichlorobenzene NO 1.0 1 ug/L 1,2.4- T rimethylbenzene NO 1.0 1 ug/L
1,3-0ichlorobenzene NO 1.0 1 ug/L 1,3,5- Trlmethylbenzene NO 1.0 1 ug/L
1,4-0ichlorobenzene NO 1.0 1 ug/L Vinyl Acetate NO 10 1 ug/L
Oichlorodifluoromethane NO 1.0 1 ug/L Vinyl Chloride ND 0.50 1 ug/L
1,1-0ichloroethane NO 1,0 1 ug/L p/m·Xylene NO 1,0 1 ug/L
1,2-0ichloroethane NO 0,50 1 uglL o-Xylene NO 1.0 1 ug/L
1,1-0ichloroethene NO 1.0 1 ug/L Methyl-t-Butyl Ether (MTBE) NO 1.0 1 ug/L
c-1,2-0ichloroethene NO 1,0 1 ug/L Tert-Butyl Alcohol (TBA) NÒ 10 1 uglL
t-1,2:Dichloroethene NO Ù 1 ug/L Diisopropyl Ether (DIPE) NO 2,0 1 ug/L
1,2-Dichloropropane NO 1.0 1 ug/L Ethyl-t-Butyl Ether (ETBE) ND 2.0 1 ug/L
1,3-0ichloropropane NO 1,0 1 ug/L Tert-Amyl-Methyl Ether (TAME), NO 2.0 1 ug/L
2,2·0ichloropropane NO 1.0 1 ùg/L Ethanol ND 100 1 ug/L
Surrooates: RECI%) Control Qual Surrooates: RECI%) Control Qual
Limits
Dibromofluoromethane 106 86-118 Toluene-d8 99 88-110
1,4-Bromofluorobenzene 99 86-115
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RL - Reporting Limit ,
DF - Dilution Factor .
Qual - Qualifiers
I
7440 Lincoln Way, Garden Grove, CA 92841-1432 · ,TEL: (714) 895-5494 · FAX: (714) 894·7501
. ____'_'_"" ........_..~.u ',__ _._. ~ ___.__._.,_._____.~_.___.___~___. ..__......____~____._._w___....._.hfi_.__.___._.__.. ._....~___~.__...._~_....._ _.._._..-......... ...... ...._.. ..__ ..._.....___........_ .._.._..._~... "._h'· ..~ ..~.,_~ ,..........__.....-. ... .-_. '.'
I
I
~ = a/science
I!:;ggovironmental
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
ANALYTICAL REPORT
I
I
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
EPA 50308
EPA 8260B
I
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 5 of 5
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Client Sample Number
Lab Sample
Number
Date
Date
I
Parameter Result RL OF Qual Units Parameter Result RL OF QYID Units
Acetone ND 10 1 ug/L 1,1-Dichloropropene ND 1.0 1 uglL
Benzene ND 0.50 1 ug/L c-1,3-0 chloropropene ND 0.50 1 ug/L
Bromobenzene ND 1.0 1 ug/L t-1,3-0ichloropropene ND 0.50 1 ug/L
Bromochloromethane ND 1.0 1 uglL Ethylbenzene ND 1,0 1 ug/L
Bromodichloromethane ND 1.0 1 ug/L 2-Hexanone NO 10 1 ug/L
Bromoform NO 1.0 1 ug/L Isopropyl benzene ND, 1.0 1 uglL
Bromomethane NO 10 1 ug/L p-Isopropyttoluene ND 1,0 1 uglL
2-Buìanone NO 10 1 ug/L Methytene Chloride NO 10 1 ug/L
n-Butylbenzene NO 1.0 1 ug/L 4-Methyl-2-Pentanone NO 10 1 ug/L
sec-Butylbenzene NO 1.0 1 ug/L Naphthalene ND 10 1 , ug/L
tert-Butylbenzene ND 1.0 1 ug/L n-Propylbenzene NO 1.0 1 ug/L
Carbon Disulfide NO 10 1 ug/L Styrene NO 1.0 1 ug/L
Carbon Tetrachloride NO 0.50 1 ug/L 1,1,1,2- Tetrachloroethane NO 1.0 1 ug/L
Chlorobenzene ND 1.0 1 ug/L 1,1,2,2-Tetrachloroethane NO 1.0 ' 1 ug/L
Chloroethane NO 1.0 1 ug/L Tetrachloroethene NO 1.0 1 ug/L
Chlorofonn NO 1.0 1 ug/L Toluene ND 1.0 1 ug/L
Chloromethane NO 10 1 ug/L 1.2,3- Trichlorobenzene NO 1.0 1 ug/L
2-Chlorotoluene NO 1.0 1 ug/L 1,2,4- Trichlorobenzene NO 1.0 1 ug/L
4-Chlorotoluene NO 1.0 1 ug/L 1,1,1- Trichloroethane ND 1.0 1 ug/L
Oibromochloromethane NO 1.0 1 ug/L 1,1,2- Trichloroethane NO 1.0 1 ug/L
1,2-0ibromo-3-Chloropropane NO 5.0 1 ug/L Trichloroethene NO 1.0 1 ug/L
1,2-0ibromoethane NO 1.0 1 ug/L TrichlorofluoromE¡!thane NO 10 1 ug/L
Dibromomethane ND 1.0 1 ug/L 1,2,3- Trichloropropane ND 5.0 1 ug/L
1,2-0ichlorobenzene NO 1.0 1 ug/L 1,2,4-Trimethylbenzene NO 1.0 1 ug/L
1,3-Dichlorobenzene ND 1.0 1 ug/L 1.3,5- Trimethylbenzene NO 1,0 1 ug/L
1 ,4-0ichlorobenzene NO 1,0 1 ug/L Vinyl Acetate ND 10 1 ug/L
Oichlorodifluoromethane NO 1.0 1 . ug/L Vinyl Chloride NO 0.50 1 ug/L
1,1·0ichloroethane NO 1,0 1 ugfL :ifm-Xylene NO 1.0 1 ug/L
1,2-0ichloroethane NO 0.50 1 ug/L . o-Xylene NO 1.0 1 ug/L
1 ,1-0ichloroethene NO 1,0 1 ug/L Methyl-t-Butyl Ether (MTBE) NO 1.0 1 ug/L
c-1,2-0ichloroethene NO 1.0 1 ug/L Tert-Butyl Alcohol (TBA) NO 10 1 ug/L
t-1,2-0ichlorœthene NO 1.0 1 ugfL Oiisopropyl Ether (OIPE) NO 2.0 1 ug/L
1,2-0ichloropropane NO 1.0 1 ugfL Ethyl-t-Butyl Ether (ETBE) NO '2,0 1 ugfL
1,3-0ichloropropane NO 1.0 1 ug/L Tert-Amyl-Methyl Ether (TAME) NO 2.0 1 ug/L
2,2-0ichloropropane NO 1,0 1 ug/L Ethanol NO 100 1 ug/L
Surrocates: REC(%) Control Qual Surrocates: REC(%) Control Qual
Limits
Oibromofluoromethane 105 86-118 Toluene-d8 101 88-110
1,4-Bromofluorobenzene 100 86-115
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RL - Reporting Limit ,
OF - Dilution Faclor ,
Qual - Qualifiers .
I
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
... '.'~__~.._..,_. __ .._.~._.._. .~._..._'..~. ._~..._ __._.._......,._.___..~__.. __._______.___.____.M"_..__........"_.__.._.~_...__,~.._._..~..,. .w__...n~". _~_.... ......_____..", ..._~..~MM_···_· _.._......,.....__ ..._'" ....._..__._____ ...-... -----".... ....--... ..'
I
I
I
I
L- a/science
~nVironmental
I., aboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
ANALYTICAL REPORT
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
EPA 3005A Fill.
EPA 601 OB
I
I
I
I
I
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Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 2
Client Sample Number
Lab Sample
Number
Date Date
Matrix Prepared, Analyzed QC Batch ID
" ',' '5?~:t:,g~!iiq~I~~M@1tJlf~ii~~è~~:,;'::~~~1
Parameter
Lead
Result
NO
RL OF Q1@! Units
0.0100 1 mg/L
;};!{i~}jIII.tl:~iM~~·;·j~'~~:~'
";"¡'~~H:~~$;:~~~~:~X~,~1~t
Parameter
Lead
Result
NO
RL OF Qual Units
0.0100 1 mgfL
Parameter
Lead
Result
NO
RL OF Qual
0.0100 1
I
I
Parameter
Lead
Result
NO
RL DF Qual Units
0.0100 1 mgfL
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I
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I
I
RL - Reporting Limit, DF - Dilution Factor" Qual - QualifierS
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
- _. ,~~_.-..._-- - _.......
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... ......__ _ .~_... .'._.~_" ....·h_' ..... ". _. ....
I
I
iE - a/science
l::iËnvironmental
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
ANALYTICAL REPORT
I
I
. Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
EPA 3010A Total
EPA 601 OB
I
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 2 of 2
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Lab Sample
. Number
Date
Analyzed QC Batch ID
tiûí~!ªt'~~ijþ~~~'j~.:·;::·;,~
I
Parameter
Manganese
Potassium
Sodium
Result
ND
2.06
40.3
RL OF Qual Units Parameter Result RL DF Qual Units
0.00500 1 mg/L Calcium 30.8 0.1 1 ' mg/L
0.50 1 mglL Iron ND 0.100 1 mg/L
0.5 1 mg/L Magnesium 5.45 0.101 mglL
·,;:;,;;::~j!~!~H~t!i;,~'~~~~lrf!~~;]__~~Hi~{'''~ro~;Xt~~~~tiq~~~i;·;...,,~q~~~~
I
I
Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units
Manganese ND 0.00500 1 mg/L Calcium 32,6 . 0.1 1 mg/L
Potassium 2.34 0.50 1 mg/L Iron ND 0.100 1 mg/L
Sodium 34.0 0.5 1 mg/L Magnesium 5.94 _ 0.10 1 mg/L
1::~~~;J¡ï~!1~~i¡!'k!!:]':.':;~t;1;:;;;,~t~~f~~~~1:~j~1m,~1r=~¡I~m§ø~~~~('W(ic!t~~';};..'i'i~~~*~~;\:'¡9,f&i~~q2"".' .
I
I
Result
ND
2,01
41.0
RL DF
0.00500 1
0.50 1
0.5 1
Qual Units
mglL
mg/L
mg/L
Parameter
Calcium
Iron
Magnesium
Result RL Units
30.5 0.1 mg/L
ND 0.100 mg/L
5.48 0.10
','.. ", '~"'~~.,..
Result RL DF Qual Units
ND 0.00500 1 mgfL
ND 0.500 1 mgfL
NO 0,500 1 mgfL
I
I
Parameter .Result RL DF Qual Units Parameter
Lead NO 0.0100 1 mg/L Manganese
Calcium NO 0.100 1 mg/L Potassium
Iron ND 0.100 1 mg/L Sodium
Magnesium ND 0.100 1 mg/L
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Rl - Reporting limit, OF - Dilution Factor, Qual - Qualifiers
I
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
." .-_.__."-...._- .--.-.-' ......- _. ._.-.. '- .. ........ -..- ".- .......-....,.. ......~ ......-.. ..,.-..... .... ... ....
-.. -'-~ . ._~....."..- - -- ................ ".... .--..., '..-. '-' .......-..-.-.... -,..-.
........._.......-.....-...-.............
I
I
1....= a/science
6::2n vironmen tal
L aboratbries, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
ANALYTICAL REPORT
I
I
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
Ext. -+ D/I
DHS LUFT
I
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
I
Lab Sample
Number
Matrix
Date
Prepared
QC Batch ID
'~~,:, >'Q~~,~~º~
Client Sample Number
I
Parameter
Result RL DF Qual Units
ND 1000 ugfL
REC(%) Control Qual
Limits
93 51-141
:':~~d~~ ~-:<W>:&~">.., Y.w.< y" -t'
~&3?09'ii012912> ';"":
" ",t",,,;j '" ~ ","'~' ~
Result RL DF Qual Units
ND 1000 ugfL
REC(%) Control Qual
Limits
84 51-141
TPH as Diesel
SurrOQates:
I
Decachlorobiphenyl
I
Parameter
I
TPH as Diesel
SurrOQates:
I
Decachlorobiphenyl 1
, ,',
......... .
I
Parameter Result RL OF
TPH as Diesel NO 1000
SUrroQates: REC (%) Control
Limits
Decachlorobiphenyl 97 51-141
Qual
Units
ugfL
Qual
I
,:~tiv~':'~: ,,~~jr~."" ,r'
;' 'R~qØ,~BÓ3.
Parameter
Result RL OF
NO 1000
REC(%) Control
Limits
86 51-141
Qual
Units
I
TPH as Diesel
Surroaates:
ugfL
Qual
I
Decachlorobiphenyl
"~!t~r~{~I¡~L ' ;~
',·,:~'::~¡i~~~äfiç,":~':~;·,::;~ti,~~~9~l,·r1.i): " ',.' ~!i'I;c;;:I;~1U¡~.~ø~:;:Y~{~9~{~£,;{:~~~CWÔ3 .'
" ,,",
i~~q904Bº3
Parameter
Result RL DF Qual Units
NO 1000 ugfL
REC (%) Control Qual
Limits
99 51-141
I
TPH as Diesel
Surroaates:
Decachlorobiphenyl' '
I
I
Rl - Reporting Limit. DF . Dilution Factor, Qual - Qualifiers
I
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
.....-.-.....----..-..--.- _.._~._.~~..~. .-..--..--.. -............-,.--... ...,.__._......~.__._.... -------..-,,---.-.--.......--.- .-----.- _._..~...,~-. _.... .~...... .. _. . "'~"""'-' .--..... ."-' ...
I
I
Ii -a/science
C~nv;ronmental
I.. aboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place.
Torrance, CA 90501-1511
I
I
I
ANALYTICAL REPORT
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
N/A
EPA 300.0
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
I
Lab Sample Date Date
Number Collected Matrix Prepared
y,"';+0Þ:~,:~%'~Jr:íil~1i!11~\~t;;~;~èi;';'i;:~!~!iª~~I~~~~~¡,~t~'.,,;
I
Parameter .
Nitrite (as N)
Result
ND
Parameter
Nitrate (as N)
I
Parameter
Chloride
Result
26
I
I
Parameter
Nitrite (as N)
Result
ND
I
Parameter
Chloride
,Result
26
RL
10
DF Qual Units Parameter Result RL DF Qual Units
10 D mg/L Sulfate 27 10 10 D mglL
~~{;',.~.:';:~~il~;>~l~~&~,;~~;I:~~~~)~\;'fr.~}i'~'<·:·,..'''.::'Ø,Iii.~i)3;·.:~;(~¡gj09~.:i(01
I
·1W:+f\.1:;~~d~t:~L~;;j~ "¡".:"
Parameter
Nitrite (as N)
Result
ND
RL
0.10
DF Qual Units Parameter Result RL DF Qual Units
1 mg/L Nitrate (as N) 1,5 0.1 1 mg/L
·'~;,::·;i~!&'i~&q!t~~Ó~:~:,,~iil"~~%¡~~ij~~l,*'j::,~;.:,,:i:Bj~¡¡t9~;Ai;ø~q~pªL01. ".'
I
, QC Batch ID
RL DF Qual Units
0.10 1 mg/L
'Result RL DF Q!@! Units
1.6 0.1 1 mglL
,1t~~:i:X{"';~;¡~,':',2!'i~,:!Iì,~$Ri~¡\~~"q9{¡:}IL01 . , .....
RL DF Qual
10 10 D
Parameter
Sulfate
Result RL DF Qual Units
27 10 10 D mg/L
':~~,i,~~,:"~~i~;:f~0~', .. ,'C~~~i:Ø3LØ1:' '."
RL DF.Q!ml Units Parameter Result RL DF Qual Units
0.10 1 mg/L Nltrate(asN) 1.6 0.1 1 mg/L
, "....,;j'),¡:,:2~~;'~f9~~I~je~:j;M~IT~ì~~,~e~,\:4£~¡ill~~~f~1~¡fA<.i~\¡~tt~At.;,~~!tÚ:;,ß~~~~Ó~...
I
'"..,/A, H ,;jA*,~\i<i~~kE';::;'\~/~YY
I
Parameter
Chloride
Nitrite (as N)
Result
ND
ND
I
I
I
Parameter
Sulfate
RL DF Qual Units
10 10 D mg/L
¡",,}~{ô,~ffi~,,', 'O~O~03L~1
Result
26
RL
1.0
0,10
DF Qual Units
1 mg/L
1 mg/L
Parameter
Nitrate (as N)
Sulfate
Result
ND
ND
RL
0.10
1.0
DF Qual Units
1 mg/L
1 mg/L
Qual - Qualifiers
RL - Reportin9 Limit. DF - Dilution Factor
I
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
_...~-_. ... .. _........_...._.._......_ ._..._._....__..____._.._ h._."_..._. ,. .. ._~~. .0-._" .~_______..,__...J_..._. ...~._._.__.__._..~,..u_._..~._'_.~.. ._.. ._,____, .....·..:.__......._.H....._ "._ __ .....'__...",....._..___.. .~._._... '" _..__.,..',",~ --...."" '-'-"~.~'
I
I
Š - a/science
lJ:_nvironmental
L aboratories,lnc.
BlaineTech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
ANAL. YTICAL REPORT
I
I
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
N/A
EPA 351.3
I
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
I
I
I
Client Sample Number
Lab Sample
Number
Date Date Date
Collected Matrix Prepared Analyzed QC Batch ID
, . "i )!iÑ{ÂtJ4ì:~~ø!iî~M~"~~<m~§~: ,'.
Parameter
Result
Total Kjeldahl Nitrogen
ND
RL DF
0.50
Qual Units
mg/L
~" i¡~)9t!!iiïiY:é/ ~ªB~~~N~2
Parametèr
Result
I
Total Kjeldahl Nitrogen
ND
RL OF
0.50
Qual Units
mg/L
;~~~~j?~ìlè~iì'.iil;i~~~~,::~~il~t:;~::~~:;::·,:
Total Kjeldahl Nitrqgen
ND
RL
0.50
OF
Qual
Units
I
Parameter
Result
I
mglL
'" ':ï~itiMij,j)~~j;~1;:;~5\~iÄ;,;. '.:~[~i?!~.~~~.~,!~;';3~~~~~~:l
ND
RL
0.50
DF
Qual
Units .
Parameter
Result
Total Kjeldahl Nitrogen
mg/L
I
I
I
I
I
I
I
RL - Reporting Limit, OF - Dilution Factor, Qual - Qualifiers
I
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
~~_.w.... _. _ ._......_, __.___.._~,____ _. .____n_..__._,.....___._.__. ~._._.~~__.~..~._.....___.___. __ .._.""_ '.u" "._. '._ _.____._.~ .____... .. .....__.... ._,.. .~..... ...~.. ~._.
.. _~._.... h..·~ ....*..,.,.._....... "'_"'~" ~.' ,.~~. ..
I
I
j¡' - a/science
I::ªnvironmenta/
L aboratories, Inc~
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
ANALYTICAL REPORT
I
I
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
N/A
SM 23208
I
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
I
Lab Sample Dáte
Number Collected
':~~~",,\,;¡;~~1Ii~
Matrix
Date
Prepared
QC Batch ID
I
I
Parameter
Result
100
RL
5.0
DF
Qual
Units
Alkalinity, Total (as CaC03)
mg/L
Parameter
Result
RL
DF
Qual
Units
I
Alkalinity, Total (as CaC03)
100
5.0
mg/L
: ....;.<:~!!~~ r·~..n:~·:'1~::·:>:.:;:·:. '~.."
I
Parameter
Result
RL
DF
Qual
Units
Alkalinity, Total (éJs CaC03)
80
1.0
mg/L
I
I
I
I
I
I
I
I
RL - Reporting Limit. DF - Dilution Factor, Qual - Oualifiers
I
7440 Lincoln Way, Garden Grove, CA 92841-1432 '. TEL: (714) 895-5494 · FAX: (714) 894-7501
......... .-.------- _......__._......__.~.- ..-.- -_..~-.._~~-----. --~-----.~_.__..._-"'.._.~.....-.._--.-._._. -....... .. ..~_._--_.' -...,___'._._._--_.~,._---~ _..~._._----_..._---- ~-".""-_. ..._. ,.-.- ".--- .-" .......- ..
I
I
C a/science
I:j1Vironmental
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
ANALYTICAL REPORT
I
I
Date Received:
Wark Order No:
Preparation:
Method:
09/03/03
03-09-0'129
N/A
S'M 2320B
I
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
I
Lab Sample
Number
Date Date
Matrix Prepared Analyzed QC Batch ID
~!{t~:~if!i~ú;,",;.ô~jb4tÖ3<:<';~9!~~g~~EfX;¡
I
Parameter
Result
Bicarbonate (as CaC03)
100
RL
5.0
DF
Qual
Units
, mg/L
I
,i;~~~;;~;}ir~a~:;,::,tii~~,~1iÇ'i~~<:
Parameter
Result
I
Bicarbonate (as CaC03)
100
RL
5.0
DF
Qual
Units
mg/L
YJ.(Ä,',~,~l;&e- '~~'E~1\j~;~. t.);.y..!;~:~~.~:t :~;:::': < ";::?:.?< :~~. Y:~:'··~·..""·jߪ~iK~¡1!t2.~~j;~~~~,~:: ÞU.t2ú"^W;,~~Ûþ\~¡¿H;~;;;:~1:,1)~ .4.'~t:#~~itl¿~i;~~~~Zt\~~~~~~~f':~~, ::::~;~"'-'{~.~,._~-,,,f.::~'~;;<~ i~<;:;^(n:·;~:;·.\~, .; :::.Tjø·r~Þ:r;~~:·~':~'~(~·: :.' ",
,"iV,,·...'....·..! '."," ".,. ". ',. ". .... . M.' d""'\'" :AJ3ægilh2H' .<;~,,;, .~, '''''OQIA!VM,x.O¡.. ,,'!il:í-i ' ''''''hø:d¡w¡Æ!l\ff,iI''''"''' .y'" "09IQjt/03"'"";309ft'''~';iK ' ..."..,. ','
._,·::r;.-:?{;:<,,··~t~·1~\~1'·\::.:~·,:·;: \,: :.:" . .:..", ,::.", ·~·::<:":\·",;'·,::'þ'·,<:~y·.:{.;,-;:·..;<,;/h,h0i'"t?lt\}·;'ã;;~-{:~{,~;¡~g1r~V~~~,,·::,:'+:~t~~· )'~ ,,;<~~fÆ::~~N:;~:::-:~\:'~'~'~"'~; "~~";~ .,.,-",>:/< . ,¿" t':.:. ;":> ...i,; ~:>:'''.<,¡¿~;-i{ ~~.: . :
I
Parameter
Result
80
RL
1,0
DF
.Q!.@!
Units
Bicarbonate (a~ CaC03)
mg/L
I
I
I
I
I
I
I
I
RL . Reporting Limit, DF - Dilution Factor, Qual - Qualifiers
I
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
...-_~.._. ..__..~N_...._"~~_'_' _.._,... 'H '" "_.._, ~"'" ..~_~~..,. .. ". ._._,"', ~~.~ .__~..,~.... ,,_... ,............~....... ......~...__.._~..._ ...._,~__...~~,_ .~....___.A'.".'"_..' ..... "' ..~... ..........'.._.._.~_ _,_",__ __. _. ._._..._...._..__... ......__ . '.." "~H.. .. .
I
I
I
I
~- a/science
I:; nvironmental
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
ANALYTICAL REPORT
Date Received:
Work Order No:
Preparation: .
Method:
09/03/03
03-09-0129
N/A
SM 2320B
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
Lab Sample
Date
Oate
Client Sample Number
Matrix
QC Batch 10
:'.;
Parameter
Result
RL
OF
Qual
Units
Carbonate (as CaC03)
NO
1.0
mg/L
'~;;~<~~:~~~ .
Parameter Result RL OF Qual Units
Carbonate (as CaC03) NO 1.0 mg/L
:1~kp1:::~'ê"!
Parameter Result RL OF Qual Units
Carbonate (a~ CaC03) NO 1.0 mg/L
RL - Reporting Limit, DF - Dilution Faclor, Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
~.. ~ .....~_._._.._. '.__'_._M__"'_._~____.______._~.__.. __________.__....___.__._...~..._~._..........,_...._._._~_~. ~....._..... .,._.__...___. ........_.."...,.__,_.~._~.~w ._......_,". _.._....,,_._.~...-._.....--~.... ".'
I
I
I
I
I
I
E - a/science'
I:,¡gpvironmental
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
ANALYTICAL REPORT
Date Received:
Work Order No:
Preparation:
,Method:
09/03/03
03-09-0129
N/A
SM 2320B
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
,Date Date Date
Collected Matrix Prepared Analyzed QC Batch 10
·>;y::!,~¿~~~~qi1~~fl:~ii.¡~.i!,,;;;':,~{Æj~¡~¡q~l~q~~jj(S>~,~i«L~~,~"'~'!.,,
I
Parameter
Result
Hydroxide (as CaC03)
NO
RL
1.0
OF
Qual
Units
I
I
I
I
I
Parameter
Result
RL
OF
Qual
Units
Hydroxide (as CaC03)
NO
1.0
'T::~¡::~i?!lt~~~~¡;;ii;'~i*64Aû~1" . ,
Parameter
Result
RL
OF
Qual
Units
Hydroxide (a~ CaC03)
ND
1.0
mg/L
I
I
I
I
I
I
I
RL - Reporting Limit, DF - Dilution Factor, Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
_'_~.__._.. ......~__.~ "_,'_,_~._.__~._,,,_ .._,~. ~ .._...",....._...__..__"'·.N'~.............".,.._....~..____.._._,_,_,_...__.~_..._...~__,._...~ .__~._,_..._._ __.. .._._........ ...-, _."_""_" .........~,-__.___... ._- -----. "~._"-"-""_._""" ... _....~.~, ... "...
'I
I
L- a/science
I::: nvironmental
Laboratories, Inc.
Blaine Tech Services; Inc
20360 Gramercy Place
Torrance, CA 90501-1511
ANALYTICAL REPORT
I
I
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
N/A
EPA 120.1
I
Project: .5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
I
Matrix
Date 'Date
Prepared Analyzed QC Batch ID
>·':<:i;;;;:~i.ò¥ )~tí~~~~~gfJ~:':·.
I
Parameter
Result
RL
DF
Qual
Units
Specific Conductance
350
1.0
umhos/cm
I,
't:,~,.~~!Q,~q:i~~\:,:i~~g~r~l&>';;~::¿~
I
350
RL
1,0
DF
Qual
Units
Parameter
Result
Specific Conductance
umhos/cm
·~6iíj1G:'ji;it9!rW!~~·~:)¡i~~Þ.t~~~~jÞ~1~:·'.·,~
Specific Con~uctance
350
RL
1.0
DF
Qual
Units
I
Parameter
Result
umhos/cm
I
I
I
I
I
1
I
I
Rl - Reporting Limit, OF ~ Oilulion Factor, Qual· Qualifiers
I
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
. ....~'".~.~~...__....~~...~ ....._._ U".. '..' ......~. _. __.r ,·~__w~ _".' ._ .~.~_.~.... ~_._",_,_~~., ........_.~_.__ ,... nO' .. '..__, _. ., .....w....._.'" ......'~,._ ......_. _....__". ....._. .__.._. .."-"..._,,....~.._.... ......-...._-~.~-_._.__..._..~.__._..~_._---_.... -"-"~""'. .....~._- ......... .-.
I
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I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
æ -a/science
I:ªnvironmental
, Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
ANALYTICAL REPORT
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
N/A
EPA 130.2
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
Matrix
Date Date
Prepared Analyzed QC Batch 10
¡, t ,:3()!IMHARB1 M ''" .
" ¡I-: /tS,~;ìi'.':t ¡~~~''''w
Parameter Result RL OF Qual Units
Hardness, Total 110 2
~fj·*:l.·~~Qf4~~)t')'~"él
Parameter Result RL OF Q¡@ Units
Hardness, Total 100 2 mg/L
Pàrameter
Result
RL
Qual
Units
DF
96
2
1 mg/L
.:~~~~f::~' ,:)\9)~ì~::{:~;+i~~~
····/i<~~i~~!if~~~~,~iåMij~~
Parameter
Result
RL
Qual
Units
DF
Hardness, Total
2,0
mg/L
NO
RL - Reporting Limit, DF - Dilution Factor, Qual - Qualifiers
7440 Lincoln Way. Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
'~_".__'h"~__ _ __"_." .., _..._. _ <,-.___._.~ . _.._~._,__~_AO_' ..____.___~.._..__.. _~_...."__~_..____.__.._.___..____..._ _ ____.......__._,........ .'_....._......J ." ..__....... ._. e,__" _ .'^~_. _
"'.' .....--.-...,,--.-.........
I
I
I
I
I
§ a/science
I:;§nvironmental
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
ANALYTICAL REPORT
Date Received:
Work Order No:
. Preparation:
Method:
09/03/03
03-09-0129
N/A
EPA150.1
"Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
I
Parameter
, Result
I
I
I
I
I
pH
6.31
RL
0.01
DF
Qual
Units
Parameter
Result
RL
DF
Qual
Units
6.36
0.Q1
pH units
6.43
RL
0.01
DF
Qual
Units
Parameter
Result
pH
pH units
I
I
I
I
I
I
I
I
RL - Reporting Limit. DF - Dilution Factor. Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
..,.. --"--~'-'-~~~'~-'--'''''''''-''-'''-''-'''- '-".',
.._......~.^,....,._------..-._-----_.---.~_._,,-_.._._- ...-......-.-..----.. -. - -'-'-. '-"'~ .....-._-"..,,-_.~........~_. .-....---.,.. -.... --.-.... .-...~._..- -.. .....~. ....-
I
I
I
t.....= a/science
I:: nvironmental
Laboratories, Inc.
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA90501-1511
ANALYTICAL REPORT
"
I
I
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
N/A
EPA 160.1
Project: 5321 Stockdale Highway, Bakersfield, CA
Page 1 of 1
I
Lab Sample Date Date Date
Client Sample Number Number Collected Matrix' Prepared Analyzed QC Batch 10
·..4i~..~~\ìrBI~i0Æ~eii~¡i;"",',";;)!i':W~J¡~jJ.Ø.~fj~~~i¡~,j,'~~:,0;:~'~'~~~Ár,;?{:Ø~~~~1j)1
Parameter
Result
I
I
I
I
Solids, Total Dissolved
220
RL
1.0
OF
Qual, Units
mg/L
~11~~$D1I: .
Parameter
Result
Solids, Total Dissolved
220
RL
1,0
OF
Qual Units
mg/L
:::;~!ß¡1~~~t:~~"\'11IJ.!Ii~~~fã~;61?;..
220
RL
1,0
OF
'Qual Units
Parameter
Result
Solids, Tot~1 Dissolved
mg/L
I
I
I
I
I
I
I
I
I
RL . Reporting limit, OF - Dilution Factor, Qual - Qualifiers .
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
.. ... _._".._._...... ..._...._..... ~'__.."._.--.. .. _,,,_._..__._ ....__.._._._.~...._.. ,',"~____~'-""'_____,'-'-'__. ___ ,..~__._~..__.,,_._.._ ..._'_~... _ ,.. ... ___. _, ."_. ~'_"'_'_'_"_'__'__."_'_'. __..__._._.._.......H.._..._.____..__~.~.._.. _.__.... ... .~_.
I
I
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I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
ii - a/science
, I::ffffnvironmental
I.. aboratories, Inc.
Quality Control - Spike/Spike Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
EPA 50308
DHS LUFT
Project: 5321 Stockdale Hiç¡hway, Bakersfield, CA
Quality Control Sample ID
Matrix
Date
Prepared
Date
Analyzed
MS/MSD Batch
Number
Instrument
, ". ,., ·09/ô4i.Ø~~t~J~t~ijiÖ9i>4SÖ1,;'
Parameter
MS %REC
%REC CL
Qualifiers
MSD %REC
RPD
RPD CL
TPH as Gasoline
103
0·17
99
70-112
5
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894·7501
.. ..._~__..~..__. _.~__~______,,~.__..__.._.~~___...___.___..___.......__.,_. ~_......._~....___,..._.........._ .~.~._........,~..~.....~, ._.~_u__" .......____ ~..n....'__~._"._...__·...___·__·___a___.._....___. ,-,
I
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I
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I
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I
I
I
I
I
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I,
I
I
I
jj -a/science
I:~nvjronmental
Laboratories, Inc.
Quality Control· LCS/LCS Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
. Method:
Project: 5321 Stockdale Highway, Bakersfield, CA
09/03/03
03-09-0129
EP A 5030B
DHS LUFT
Date
Quality Control Sample ID
%REC CL
RPD
LCS %REC
104
LCSD %REC
105
Parameter
TPH as Gasoline
72-114
LCS/LCSD Batch
Number
!q,~9A~,~~S~·¡¡".·.;;;riK¡:é[
RPD CL Qualifiers
0-10
7440 Lincoln Way, Garden Grove, CA 92841·1432 · TEL: (714) 895·5494 · FAX: (714) 894-7501
. '~__"_"~''':''''''M'_____'''.'~h~''__~'''___''''____'_'_'''__'___'~_____.__"W.___.__"___ '~~~__'_''-'''''~'''_'___M_~_~....~__·__...··__··",____n__~~·_._.~..._.- - ... .,eo'··
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
E - a/science
I::ª nvironmental
'- aboratóries, Inc.
Quality Control - Spike/Spike Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
EPA 5030B
EPA 82608
Project: 5321 Stockdale Hiç¡hway,Bakersfield, CA
Quality Control Sample 10
Date Date MS/MSD Batch
Matrix Instrument Prepared Analyzed Number
"{\~1'~~,,~·:· .., :. ~ ,>'/..' .: . ....,-:.': ,.) :j:~:/':,:'::Z:';Y::"·;:Y)Ú·~i".,,
.S09I061P3 ,-".;""", .,. ,03O!J(J6$02¡r,,'\í
MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers
96 95 81-123 1 0-15
94 93 61-133 1 0-17
97 97 82-124 0 0-15
97 96 82-124 1 0-16
104 102 70-136 3 0·20
95 93 87-123 2 0-15
92 90 66-108 2 0·16
99 97 61-133 2 0·20
91 91 67-127 1 0-20
102 106 20-158 4 0-41
89 87 71-125 1 0-16
90 89 69-129 1 0-19
93 92 70-124 1 0-19
95 96 39-141 1 0-53
Parameter
Benzene
Carbon Tetrachloride
Chlorobenzene
1,2-Dichlorobenzene
1,1-Dichloroethene
Toluene
Trichloroethene
Vinyl Chloride
Methyl-t-Butyl Ether (MTBE)
Tert-Butyl Alcohol (TBA)
Diisopropyl Ether (DIPE)
Ethyl-t-Butyf Ether (ETBE)
Tert-Amyl-Methyl Ether (TAME)
Ethanol
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
""_'._.._.._.~,.~._._',,_~.__. ~'__".......~_..~_._,'.'_ ..,. .... .._...._,..__.,.'__._.._,_..____._.......'"',.....~______....._...._....~__.'''__....__.._............... ""'__'_"'~'~'~ "_~'''''''.'M~.._____''_''''' _........__..w.....___..... ..._.._......~._. _. . .u......... .._.~.... . ...
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
s - a/science
~ n vironmen tal
Laboratories, Inc.
Quality Control - lCS/LCS Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torra'rice, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
EPA 5030B
EPA 82608
Project: 5321 Stockdale Highway, Bakersfield, CA
Quality Control Sample ID
Daie Date lCS/lCSD Batch
Instrument Prepared Analyzed Number
";~~é~hmt~¡,:~:¡1;~,~¡;~~\qfº'tt"i~i~¡r~~~þ,igl,.:'
Matrix
Parameter lCS %REC LCSD %REC %REC Cl RPD ' RPD CL Qualifiers
Benzene 96 96 84- 1 20 1 0-23
Carbon Tetrachloride 94 94 66-132 0 0-43
Chlorobenzene 100 97 89-119 3 0-25
1,2-Dichlorobenzene 99 97 89-119 3 0-20
1,1-Dichloroethene 105 106 80-128 1 0-28
Toluene 97 95 84-126 2 0-31
Trichloroethene 101 100 69-105 1 0-29
Vinyl Chloride 98 100 70-124 1 0-36
Methyl·t-Butyl Ether (MTBE) 92 92 68-134 1 0-25
Tert-Butyl Alcohol (TBA) 101 105 48-144 4 0-25
Diisopropyl Ether (DIPE) 88 89 79-121 1 0-27
Ethyl-I-Butyl Elher (ETBE) 91 92 74"134 1 0-34
Tert-Amyl-Methyl Ether (TAME) 95 95 73-127 0 0-38
Ethanol 93 96 49-133 3 0-25
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
,". .......-."-~~---,.............._.~..~-~---_...........~.....-._.....---. '''-'' ..--..__.._.._..~-,....~-----........_.._-_..~-----._._---,_._.,-- ---...... ~ ..... ....-.-... .. ~._. ._.,-".-...~-_........~...~~-_.-.....~_. ....~ -. .-.-. -~- -- -...........--...
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ii a/science
'6::i'E n vironmen tal
Laboratories, Inc.
Quality Control - Spike/Spike Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
N/A
EPA 300.0
Project: 5321 Stockdale Hiqhway. Bakersfield, CA
Quality Control Sample 10
Date
Prepared
Date
Analyzed
MS/MSD Batch
Number
Matrix
Instrument
'··;',¡~;~~~t;Nf~;4~(i~::);';2.jó91~ö~r~L~·':~~¡ò¡iìÖöjsò~:(.,;'!
Parameter
MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers
105 104 50-150 0 0-25
96 97 50-150 1 0-25
104 104 50-150 0 ,0-25
105 105 50-150 0 0-25
Chloride
Nitrite (as N)
Nitrate (as N)
Sulfate
7440 Lincoln Way, Garden Grove. CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
.. ·~·~··~"_'__H'_.'H"'___'_H__'__~'H._.. ._._..._........n......þ'___.. ._.__._.~_H___~________._...~_,.... H_.____......_w._....'.,~_. .....~..,_...~. _'_'H_ ....... __ H.__...........___._.____.. .........__.. 'H'___ ._."' .H._.'.......__,..·_·_ _.,._
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Jia/science .
I:. nvironmental
L aboratóries, Inc.
Quality Control - LCS/LCS Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
N/A
EPA 300.0
Project: 5321 Stockdale Highway, Bakersfield, CA
Date LCS/LCSD Batch
Parameter LCS %REC LCSD %REC %REC CL RPD RPD Cl Qualifiers
Chloride 101 101 80-120 0 0·25
Nitrite (3S N) 97 96 80-120 1 0-25
Nitrate (as N) 104 104 80-120 0 0-25
Sulfate 103 104 80-120 2 0-25
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 .. FAX: (714) 894-7501
.. ... ....._._._.~._.__..____~...~._._".._._ _. ,"," ~"_"_" .,~ ._._.. _.._.... ... ...A.....·_...___...._..__......__.___~_.___........·~__,......____._ .........-..-._ .........-.. .-. .......-... .....- .-.....,..- ...-,,_.-. ".'.. '"..---... '.-- .'..-- ...,.-....-.".--........, "'...-.. .---....., ,...
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~ = a/science
l:;¿gnVironmenta/
, Laboratories, Inc.
Quality Control - Spike/Spike Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
EPA 3010A Total
EPA 60108
Projett: 5321 Stockdale HiQhway, Bakersfield, CA
Date
Prepared
Date
Analyzed
MS/MSD Batch
Number
Matrix
Instrument
'"' ~{;f'" ~: ~ :1;-';:/ ð ~£:\¡; ~øÔ:~::::;,_. '~' .<~:.~.:!~.:; ~:.. ~:': ')~~l;:~;;~~:fi~j~~ ~..·\1:~:.~~/;;~';·:;'· ,j::.'r~'.:·:., . "
IC!i'3300 ,W" X...: ""'4Ð9/0¡t#,v<,,,,,,,,..¡,,09/pgI03,:;;;!o/,~,,;:':'O~( 904S02,,;
Parameter
MS %REC
MSD %REC
%REC CL
RPD
RPD CL
Qualifiers
Lead
96
94
80-120
3
0-20
7440 Lincoln Way, Garden Grove, CA 92641-1432 · TEL: (714) 695-5494 · FAX: (714) 694-7501
,_ __..______...__..__. ._.. ... _._._~.~.., ...... .__.~.._._. "._.. _. ~.___.__.. ___.......__._.._.___....,........._.....__.,.._.........._.._._.........~__.._...__...___._.__.__.n _.h....._.U._. ._.._~. "'__"'~'_'_~__~_.-"'.' "_'."".'~ ......_..__.-....-.~._.._.......- _..'--..- ....,~.. .~ ," .....
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L- a/science
I!;ggn vironmen tal
L aboratories~ Inc.
Quality Control - LCS/LCS Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-:1511
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
EPA 3010A Total
EPA 6010B
Project: 5321 Stockdale Highway, Bakersfield, CA
Date LCSfLCSD Batch
Analyzed Number
:;iJ:;~;;;;;;~f~>~U![trl.\q~i~);\~~? ....!;
Parameter
LCS %REC LCSD %REC %REC CL RPD RPD CL Qualifiers
107 106 80-120 1 0"20
105 105 80-120 0 0-20
108 106 80-120 2 0-20
105 105 80-120 0 0·20
110 108 80-120 1 0-20
101 101 80-120 0 0-20
108 109 80-120 1 0·20
Lead
Calcium
'ron
Magnesium
Manganese
Potassium
Sodium
7440 Lincoln Way, Garden Grove, CA 92841·1432 · TEL: (714) 895·5494 · FAX: (714) 894-7501
.. .~ "-"'_~~"'__ ..._"~...__,,.~ .,.....~__ ·_·.······__M __"__"__'_ _,"-" . ~..._.,........--.-.__..,._.,____......_~...__.......".~....."".. ..___.. _.._._.____.._...__..._._~ .-. ___ --.-.-..._.__, . ,,-,__.~ '-"'_ -.-..-.--..-.-.-.-- ....--,.-. .-..--.- ..--.... -..--..-.-... .-................
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IS - a/science '
~nvironmental
Laboratories, Inc.
Quality Control - LCS/LCS Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Date Received:
Work Order No:
Preparation:
Method:
09/03/03
03-09-0129
Ext. + 011
DHS LUFT
Project: 5321 Stockdale Highway, Bakersfield, CA
Date Date LCS/LCSD Batch
Matrix Instrument Prepared Analyzed Number
. ··:t~,,~~i,: ·';,'~~~~~:g,~;;t~1f,pjlŠ1~!!;~~,,~~~;~6i~~~¡~~b~~r',)1~!M~~ø~¡:::.:;"
n',:.", .
Parameter
LCS %REC
%REC CL
60-132
RPD
8
RPD CL Qualifiers
0-11
LCSD %REC
82
TPH as Diesel
76
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
-.." .'-'_ _'_.'_' _____'"....4~~~__.__ ~_.. _. .____.. __'._'_' _.__.'__ ..____.......~.__.._._._.._~~~___'_.~____.~...~ ,.___. ___..._.,_.__.__.__ --. --"---'"--'¥--" .. -'-'~-'''-'---''-'-''----'''--''-''-- .,_. '--'-"'-'--'_."'--.' .".-. .-.......
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L -a/science
I/:, nvironmenta/
, aborator;es~ Inc.
f'
Quality Control - Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project:
Date Received:
Work Order No:
Preparation:
Method:
5321 Stockdale Highway, Bakersfield, CA
09/03/03
03-09-0129
N/A
EPA 351.3
Quality Control Sample 10
Date
Prepared:
Duplicate Batch
Number
Matrix
Instrument
Date
Analyzed:
Parameter
RPD CL
0-25
Qualifiers
Sample Cone
DUP Cone
RPD
NA
Total Kjeldahl Nitrogen
ND
ND.
.... ''-'-''--'- .." ...-.~
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
. "'~'_"_4"~ ,_.~-',.~ ,.........__~_..___~.~_._"__...._ ___...__....____.~...._._ _.....__........._._ ....._.._._._._.....~____.__.__,...~._._._ ._._~_._,,_._... ._......-.~..._.__.______r._.. .M....._.... ._. ..... _~......,.- __.._.. ~.,..__..h.... _ ... ..._ ._. ..
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ã a/science
.1::, nvironmental
L i:Jboratories, Inc.
Quality Control - Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project:
Date Received:
Work Order No:
Preparation:
Method:
5321 Stockdale Highway, Bakersfield, CA
09/03/03
03-09-0129
N/A
SM 2320B
Quality Control Sample ID
Date
Prepared:
Duplicate Batch
Number
Matrix
Instrument
Date
Analyzed:
Parameter Sample Cone DUP Cone RPD RPD CL Qualifiers
Alkalinity, Total (as CaC03) 170 170 0-25
Bicarbonate (as CaC03) , 170 170 0 0-25
Hydroxide (as CaC03) ND NO NA 0-25
Carbonate (as CaC03) NO ND NA 0-25
7440 Lincoln Way, Garden Grove. CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
. . ... ... '__'~'._ ... .___.___._ ..._..._..________...._..__..._..... ~..__._.__~.".____,_~,_...'__ _. ..,....·...,,_....'u_._"_.__.....u~.~.,_ ..~... _..~__.,,~_.__. .._..~,.......,.......w_.·__·__ .-... _ ~ .-.-,...-.--.----.........--.-.,-~..._-~
..--.....-,..,.....-.. ,
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§ - a/science
l:j1vironmenta/
Laboratories, Inc.
Quality Control - Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project:
Date Received:
Work Order No:
Preparation:
Method:
5321 Stockdale Highway, Bakersfield, CA
09/03/03
03-09-'0129
N/A
EPA 120..1
Quality Control Sample 10
Matrix
Instrument
Date
Prepared:
Date
Analyzed:
Duplicate Batch
Number
Parameter
Samole Cone
DUP Cone
Specific Conductance
4400
, 4400
RPD
o
RPD CL
0-25
Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 . TEL:.(714) 895-5494 · FAX: (714) 894-7501
. .~_.._-- .-.------ -.--.----. ----." -'~~'--"'--"~"'--'- ... ~-~. ,,- _._.."'¥...__.~ .". .--..----.....-.- -.-......-" ....-..-.....-...- ,_..~-.._...
. ',_ "......... ____..... ._ h..u'. .,,___.. _____. __.__ __'_n__.....__,...._.._._H...__'"_~._'_ --...-, ~- -.-.,"..,
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~ - a/science
I!:ªnvironmenta/
Laboratories; Inc.
Quality Control - Duplicate
Blaine Tech Services. Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project:
. Date Received:
Work Order No:
Preparation:
Method:
5321 Stockdale Highway, Bakersfield, CA
09/03/03
03-09-0129
N/A
EPA 130.2
Quality Control Sample 10
Date
Prepared:
Duplicate Batch
Number
Matrix
Instrument
Parameter
Sample Cone
RPD CL
0-25
Qualifiers
DUP Cone
RPD
o
Hardness, Total
80
80
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
..'.. .,...__.~.,. nO" .__........ ...... __."__ "._......_..____~."_~........_____.__~__._~..._.,__...'_____"'"_'....._h._._ ...___.___.__....__._..._.._._____._.___.._......._._______.~....._..__._.U_._..H._.__._____......_·.·· .
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L- a/science
I:ªnvironmental
L aboratories, Inc.
Quality Control - Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrance, CA 90501-1511
Project:
Date Received:
Work Order No:
Preparation:
Method:
5321 Stockdale Highway, Bakersfield, CA
09/03/03
03-09:-0129
, N/A
EPA 150.1
Quality Control Sample 10
Duplicate Batch
Number
Date Date
Prepared: Analyzed:
*~iU:tiidL,..' {\~~t,,~î1~10'~rrf¡~aiii~wl~:~1i~~'ò;)":;99(~'lJI~~A"::;~j~~~ft~~,. .....
Matrix
Instrument
Parameter
SamDle Cone
DUP Cone
7.64
RPD CL
Qualifiers
RPD
o
0-25
pH
7.64
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
_~_ "'~_'~'''__'__'''_'___'_....,~..,_.__. ,......_..__..~._._...._ .......__.. _.. ,__,____.. _.__~_ _____,....._..____.___...._.M..~.. ___..__._.____~.__.._, ~___....._. ".,._. ._. ._.__~..,._.._~_,_..._..._. - '--..-.'
...._~.. ....-...-......-.... ...........--_..
... ..... .-....
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I
~- a/science
I:§n vironmen tal
I.. aboratories~ Inc.
Quality Control - Duplicate
Blaine Tech Services, Inc
20360 Gramercy Place
Torrànce,CA 90501-1511
Project:
Date Received:
Work Order No:
Preparation:
Method:
5321 Stockdale Highway, Bakersfield, CA
09/03/03
03-09-0129
N/A
EPA 160.1
Quality Control Sample 10
Date
Prepared:
Duplicate Batch
Number
Matrix
Instrument
~1~('~:ã~9.~mi~~1,:;,j
Parameter
Solids, Total Dissolved
RPD CL
0-25
Samole Conc
DUP Cone
Qualifiers
RPD
o
2800
2800
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
. _·_.·__~_·~Rr_.·.._,._, _'._~._.."___"~ ...._ _....___.._.,,~.... _'.._._._._._._.._...._.._.~._.___.__~~ ____.~.__..._......____.._ ..._..~_____. "__'.___ ._.._.. __._.,_.. _ .....___._...... _ '___," . ..."
_... .~_..".... 0"
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C,;alsclence GLOSSARY OF TERMS AND QUALIFIERS
I:; nvironmental
.. aboratories, Inc.
Work Order Number: 03-09-0129
Qualifier
Definition
D
E
NO
The sample data was reported from a diluted analysis.
Concentration exceeds the calibration range.
Not detected at indicated reporting limit.
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
.-. .".~ ....._. "'_'___'~"___"'''___'__ ~__'" .. _... _.~~ __~._~....__._.. _____ _.~.__.,~ .._.___.___._,_....,~......._..._,___.~..._._..h._._~.._.._.,.._'"__..______ __. .... _. ." ..... .___..",.___ _~__.........~....._....._ ." .._. ......... .._... ,.....__........ '. '..
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TbVfmn%::·' .,' ",. . ,·m""'/
... ... 'torIss'nc..,
. ,
WORK ORDER #:
03 -@]rn - @]OJ~[5J
Cooler
\ of
SAMPLE RECEIPT FORM
CLIENT:
ßI OVVuL T~ (,h
DATE:
O~ / 0 3/20D~
TEMPERATURE - SAMPLES RECEIVED BY:
CALSCIENCE COURIER:
Chilled, cooler with temperature blank provided.
Chilled, cooler without temperature blank.
V Chilled and placed in cooler with wet ice.
Ambient and placed in cooler with wet ice.
Ambient temperature.
2 0 C Temperature blank:
LABORATORY (Other than Calscience Courier):
o C Temperature blank,
o C IR thermometer.
Ambient temperature.
Initial: -i1ß
CUSTODY SEAL INTACT:
Sample(s):
Cooler:
No (Not Intact) :
Not Applicable (N/A): ~
Initial: ...}J.Å--
SAMPLE CONDITION:
Chain-Of-Custody document(s) received with samples... ......................
Sample container label(s) consistent with custody papers.... ..' .', ... .., .., ,.
Sample container(s) intact and good condition.. '........;.......................
Correct containers for analyses requested...... ,................, '..'...... .'.' ".
Proper preservation noted on sample label(s).....................................
VOA vial(s) free of headspace, ............ ... ..........................,..... ..... '"
Tedlar bag(s) free of condensation...... ......... ...... ......... ... ..................
Yes
\/
J
~/ .......
J'
./
V
No N/A
J
. Initial: J, ~
COMMENTS:
.
-LAB~¡.5£~£t- -
lab Identification (If necessary):
Address:
cny. Stale. Zip:
SAMPUNC3 COMPANY:
Blaine Tech Services, Inc.
ADDRESS;
-
-
-
~,-
-
-, - - - - - ..- .-
SHELL Chain Of Custody Record
-
'Shell Project Manager to be Invoiced:
1J.~n¿¡6.kÜ~;j$~~Üij~~ Tony Palagyi
Infui¡ï«¡ii($~~~~:::::¡
ID~M6#Þ.~~>~}}1
lOG CODE:
BTST
20360 Gramercy Place, Torrance, CA 90501-1511
PROJECT CONTACT (Hwdcopy or PDF Repon. to):
Nick Sudano
SITE ADDRESS \Streetand City):
:::::,J\jŠ!Þ~t!@~@~!(~~9~r~::::
97467222
:\¡#ffl\~:B~MÎ~~M#~~:~t~r:~~M~:¡
DATE: q-s-jf:)('3
(
PAGE:
of
GL.OBA.I..tDNO.:
5321 Stockdale Highway, Bakersfield
EO'DE1.IVI!AA8l.E.~R£PORTTO~'"-tr.~): PHONE NO.:
Pending
E-MftIL;
Kathrvn Ewlna
SAMPLER NAME(S) (Pr1nl):
TELEPHONE: I FAX.:.
310-782-2465 1310'.782-2958
TURNAROUND TIME (BUSINESS DAYS):
~ 10 DAYS 0 5 DAYS 0 72 HOURS 0 48 HOURS 0 24 HOURS 0 lESS THAN 24 HOURS
o LA· RWQCB REPORT FORMAT 0 UST AGENCY:
GC/MS MTBE CONFIRMATION: HIGHEST
SPECIAL INSTRUCTIONS OR NOTES:
E-MAIL:
nsudano@blalnetech.com
>::c'f+
HIGHEST per BORING
CHECK BOX IF EDD IS HQI NEEDED U
'All
(' "-
~";
~ ) ,
~ - .
íiì ;¡'"
0 ~
<II '"
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;¡;¡ !!!. I:)
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II. 0
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IIÌ N .:'J
.. N !2. .. Õ
C) !!!. c c
. ~ w OJ ..
J: ,II '" .<:
D. !ii ... ~ ..
... :=;¡ 0 :=;¡
HN03 poly's)were field filtered prior to preservation
·Must state whether bicarbonate Is repo~ed as either calcium carbonate
(CaC03), or bicarbonate (HC03)
i~\\
iÓNty::
Field Sample Identification
::::f:::::::
~) :nn
.........
:::¡µ:¡
¡dÜ
.:.:.:.:-:
fYlw-1
""w-"1.
mw -J
¥.!ml
(VI UJ . -{
I·,:·:,:.;·
::::::;:::
.:.;.:.:-:
..........
..........
II
SAMPLING
DATE TIME
9-3
1.""3 < lO
\
J
1.
qso
105T
Relinj=lgna¡;~j..~
Relinquished by. (Stgnature)
(1 ,1 ",0)
RelinQ l(ïs; :hlL- .
DISTRIBUTION: White with final report, Green to F.ile. Yellow and Pink to Client.
MATRIX
NO. OF
CONT.
w
(0 X X- X X.
Ib X X- X. X
1'- X >< X '.,<
It-, )( [)< '1< K
¥.-/
¡OU)
'v--(
w
(;// I /Í11
RecrlfJ~%(
Recèivo!a by: (Signature)
Received by: (Signature)
~
V/'A__L
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íiì
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626·256-6662
IE CONSULTANT PROJE.CT NO.:
c:> -ro<jC'-;·· Ç'H'1..
kewlna@deltaenv.com BTS 1/
111~llttllllll~I~!II¡iJ¡I¡
REQUESTED ANALYSIS
General Minerals
Ê . ~
on Ê
.... !
<> .. .!,!
!2. c ër .. "
0 0 ! ..
.. € u .c .. ..
.. E ..
;¡;¡ :3 u .2- ! c E
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10116100 Revision