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April 19, 2002
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Bakersfield Fire Department
Environmental Services
1715 Chester Avenue, 3n1 Floor
Bakersfield, CA 93301
Attn: Inspector Steve Underwood
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SUBJECT: Tank Removal and Remedial Excavation Report
Fonner Texaco Station
2601 White Lane
Bakersfield, California
Dear Inspector Underwood:
WGR Southwest, Inc. is forwarding the attached copy of the Tank: Removal and Remedial
Excavation Report for the above referenced site. Should you have any questions or require
any additional infonnation, please contact me at (562) 799-8510 or Ed Paden, Project
Coordinator, Shell Oil Products US at (310) 816-2075.
Enc.
cc: Ed Paden, Shell Oil Products US
Marvin Katz, Shell Oil Products US
Lany Turner, Shell Oil Products US
Y ogendra & Yatendra Solanki
11021 Winners Circle, Suite 101 · Los Alamitos, CA 90720 · (562) 799-8510 · Fax (562) 799-8556
Los Alamitos, CA · Bothell, WA · Lodi, CA
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,
Tank Removal and
Remedial Excavation
Report
at
u
Fonner Texaco Station
- ,
2601 White Lane
B~rstield, CA
"
April 8, 2002
for
,
Mr. Ray Alyeshmemi
Shell Oil Products
P.O'-Box 7869
Burbank, CA 91510-7869
prepared by:
- V\V (Gr]R..
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Somthwest:r Inc.
11021 Wmners Circle, .Suite 101
Los Alamitos, CA 90720
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Tank Removal and
Remedial Excavation
Report
at
Former Texaco Station
2601 White Lane
Bakenfield, CA
April 8, 2002
for
Mr. Ray Alyeshmemi
Shell Oil Products
P.O. Box 7869
Burbank, CA 91510-7869
prepared by:
~v {Gr]Rl
SOUJIthwest, Inc.
11021 Wmners Circle, Suite 101
Los Alamitos, CA 90720
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WGr]R.
Southwest, IDe
TABLE OF CONTENTS
INTRODUCTION
SITE mSTORY
ÇEOWGY AND HYDROGEOLOGY
HEALTH AND SAFETY PLAN
TANK REMOVAL AND DISPOSAL
1
1
2
2
2
SOn. SAMPLE COLLECTION AND ANALYSIS
3
ANALYTICAL RESULTS OF SOn. SAMPLES
STOCKPILING AND DISPOSAL
SOURCE REMOVAL - SOn. EXCAVATION AND STOCKPn.ING
DELINIATION SAMPLING
ANALYTICAL RESULTS OF DELINIATION SOIL SAMPLES
EXCAVATION BACKFD..L AND COMPACTION
4
4
4
5
5
6
SUMMARY
6
FIGURES
FIGURE I:
FIGURE 2:
FIGURE 3:
FIGURE 4:
Site Vicinity Map
Soil Sample Locations
Remedial Excavation Areas
Delineation Sample Locations
Appendix A
Appendix B
Appendix C
APPENDICES
UST Disposal Documentation
Soil Disposal Documentation
Laboratory Analytical Report
Chain of Custody Record
419.EQL.00
April 8, 2002
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Southwest, Ine
Tank Removal and
Remedial Excavation Report
Former Texaco Station
2601 White Lane at EI Potrero Lane
Bakersfield, California
INTRODUCTION
The site is a fonner Texaco retail service station located at 2601 White Lane in a commercial
area of Bakersfield, California (Figure 1). The site is situated in the southwest corner of the
intersection of White Lane and EI Potrero, approximately!l.t of a mile east of the Highway 99.
Four 10,000 gallon, double-walled fiberglass underground fuel storage tanks (UST's) were
removed from the site on March 4, 2002. In addition, four dispenser islands and associated
product piping were removed during the field operations. A remedial excavation was
petfonned from March 11, 2002 to remove the hydrocarbon impacted soil. The excavation
and removal of the tanks was petfonned by L. C. Services. This report docwnents the tank
removal operation, discusses the methods of the associated environmental work, and presents
the environmental data generated during the field investigation.
SITE HISTORY
In December 1999, Artemis conducted a Phase I ESA at the subject site to detennine whether
any current or past uses hazardous materials resulted in impacted site soils and/or groundwater.
According to the ESA report, a site assessment investigation was conducted at the site in 1985.
IT Corporation drilled one soil boring and installed four monitoring wells on the site.
Aanalytical results of soil samples indicated no detectable concentrations of petroleum
hydrocarbons were found. Based on a review of the project results, The County of Kern sent a
letter to Texaco in December 1985 stating that no significant soil impact had resuhed from fuel
tank leakage and that the case was considered closed (Artemis, 1999).
As part of the ESA, Artemis searched several databases containing infonnation regarding
leaking tanks, Superfund sites, hazardous waste generation and handling, etc. Neither the
subject site nor the surrounding properties were included in the databases with the exception of
five sites with state-registered USTs and two sites identified as small quantity generators. No
active Leaking Underground Storage Tank (LUST) cases were identified.
419.EQL.00
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GEOLOGY AND HYDROGEOLOGY
The geologic conditions in the site vicinity are characterized by alluvial deposits underlain by
marine and non-marine sedimentary units, metamorphic rocks, and crystalline basement
material.
Surface and near-swface soil is designated by the U.S. Geological Survey (USGS) as older
alluvium, deposited in northwest-dipping alluvial fans resulting ffom outwash ffom the Sierra
Nevada mountain range to the east. This alluvium is composed primarily of poorly-graded and
unconsolidated sands, sandy gravels, and occasional discontinuous lenticular bodies of sandy
clay and silt. Regionally, the surface of these old alluvial fans is undulatory, with a distinct dip
toward the Kern River to the northwest of the site. The site itself is located along one of the
crests of the alluvial fan surface 'ripples', at an elevation of approximately 393 feet above mean
sea level (MSL). The total thickness of the alluvial fan deposits is estimated to range ffom
approximately 600 feet west of the site to over 4,000 feet near the Sierra Nevada Mountains
(IT, 2oo1a).
The site lies within the Edison hydrogeologic sub-area of the Edison-Maricopa area.
Uppermost groundwater within this area occurs within the old alluvial fan deposits. In the site
vicinity, deeper aquifers of limited areal extent are present in the consolidated non-marine
sedimentary units and within fracture zones of the crystalline basement rock (IT, 2oolb).
According to the County of Kern Health Department, the depth to ground water near the
subject site is approximately 250 feet below land swface with a local flow direction toward the
northwest (IT, 2000). The most prominent subswface features controlling the groundwater
flow direction are the groundwater barriers fonned by the northwest -to-southeast trending
Edison fault and subparallel splays of this fault, located south and north of the site, respectively
(IT,2oo1b).
HEALTH AND SAFETY PLAN
A site specific Health and Safety Plan detailing known or potential hazards and emergency
response procedures was prepared prior to field operations. On-site personnel reviewed the
plan and a "tailgate" safety meeting was conducted prior to initiation of field activities. The
plan was maintained on-site throughout the duration of field activities. A copy of the Health
and Safety Plan utilized during the assessment activities is available upon request.
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Southwest, Jfnc
TANK REMOVAL AND DISPOSAL
On March 4,2002, three 10,000 gallon gasoline and one 10,000 gallon diese~ double-walled
fiberglass underground fuel storage tanks (UST's) were removed ftom the site. Four product
dispenser islands and associated product piping were also removed (Figure 2). To render the
fuel USTs inert prior to removal the tanks were triple rinsed and degassed prior to removal.
After an acceptable LEL level was reached, the tanks were removed ftom the excavation. The
tanks appeared to be intact with no observed holes. The removed tanks were transported by
Ecology Control Inc., to their facility for disposal. Copies of the Unifonn Hazardous Waste
Manifests for the tank rinsate and the tank disposal fonns will be forwarded upon receipt and
included in Appendix A.
SOIL SAMPLE COLLECTION AND ANALYSIS
Immediately following the tank removal, soil samples were collected below each end the USTs
at depths of 15 and 19 feet below surface grade (BSG) (samples designated IA-15', IA-19',
IB-15', IB-19', 2A-15', 2A-19', 2B-15', 2B-19', 3A-15', 3A-19', 3B-15', 3B-19, 4A-15',
4A-19', 4B-15', and 4B-19') under the direction of Mr. Steve Underwood of the City of
Bakersfield Fire Department. Additionally two soil samples were collected ftom below each of
the four fuel dispensers at depths of2 feet and 6 feet BSG(samples designated D-I-2', D-l-6',
D-2-2', D-2-6', D-3-2', D-3-6', D-4-2' and D-4-6'). The sample locations are indicated on
Figure 2. Stockpile samples were also collected in order to characterize the excavated
material.
The UST and dispenser soil samples were analyzed for total petroleum hydrocarbons as
gasoline (TPH-g) by the CA DOHS approved method 8015M and for Benzene, Toluene,
Ethylbenzene, Xylene (BTEX), and Methyl-tert-Butyl Ether (MTBE) by EPA Method 8260B.
Dispenser samples and tank 4 samples were also analyzed for TPH as diesel by the CA DOHS
approved method 8015M.
The samples were collected in laboratory supplied Core-PaklM glass jars with Teflon coated
lids or 2-inch diameter by 6-inch long brass sample tubes. Following collection each end of the
brass sample tube was sealed with Teflon and a plastic end cap. All samples were labeled with
all pertinent sampling infonnation, and then placed immediately on ice and chilled to 4 °C for
storage and subsequent delivery to the analyzing laboratory. All field operations were
conducted under the supervision of a California Registered Geologist.
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ANALYTICAL RESULTS OF SOIL SAMPLES
Underground Storage Tanks
A total of 16 samples were collected ITom the UST excavation immediately following the tank
removal. No TPH-g or BTEX concentrations were reported in any of the tank excavation
samples. TPH-d was not detected in any of the samples collected beneath tank 4. MTBE was
detected in eight of the 16 samples with concentrations ranging ftom 5.5 µglkg (4B-19') to
130 µg/kg (3B-19').
Dispenser Samples
A total of eight samples were collected ftom below the fuel dispensers. A TPH-g
concentration of 9.1 mglkg was detected in sample D-l-6'. Two samples contained detectable
TPH-d: sample D-1-6' with 170 mglkg and sample D-4-6' with 76 mglkg. None of the
samples contained detectable benzene or toluene concentrations. Sample D-1-6 contained a
detectable ethyl benzene concentration of 24 µglkg and a total xylene concentration of 460
µglkg. Only one of the dispenser samples contained a detectable MTBE concentration;
sample D-2-6' with 6.9 µg/kg.
Table 1, included in the Attachments section of this report, summarizes the compliance soil
sample analyses.
STOCKPILING AND DISPOSAL
Five soil samples (designated SP-I, SP-2A, SP-2B, SP-3A and SP-3B) were collected ftom
the stockpile material ftom the uncovering of the tanks and product lines to characterize the
material excavated. None of the samples contained any detectable concentrations ofTPH-g or
BTEX. MfBE was reported in one sample, SP-1, at a concentration of 41 uglkg. The
impacted stockpile material was separated and stockpiled separately. The clean stockpile
material (approximately 150 cubic yards) as determined by the sample analysis was used as
backfill. Table 2 summarizes the analytical results of the stockpile samples.
SOURCE REMOVAL - SOIL EXCAVATION & STOCKPILING
Due to the presence of detectable hydrocarbon concentrations in the compliance samples
collected ftom below the storage tanks, removal of the impacted material was deemed
appropriate.
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Since the tank pit area was open, the remedial efforts consisted of removing material from
below the storage tanks. The impacted soil in the tank pit was removed to a total depth of 23
feet BSG. Once completed, delineation soil samples were collected to verifY removal of the
impacted material. Figure 3 depicts the aerial extent of the remedial excavations.
A track-mounted excavator was utilized to remove overburden and the impacted material. A
rubber tired front-end loader was utilized to assist with soil handling. South Coast Air Quality
Management District Rule 1166 mOIÚtoring was conducted by WGR Southwest, Inc.
personnel during all soil handing activities.
Once the impacted material was excavated from the tank pit and surrounding area, the
impacted material was temporarily stockpiled on the east side of the property for
characterization and subsequent off-site disposal. Copies of the soil disposal documentation
are attached as Appendix B.
DELINEATION SAMPLING
Once impacted material was removed, soil samples were collected from the bottom of the
excavated area under the inverts of the former UST's in order to confirm the removal of
hydrocarbon impacted material. Soil samples 3AA and 3BB were collected at 23 feet BSG in
the UST pit. The samples were collected in laboratory supplied Core-PakTM glass jars with
Teflon coated lids. The samples were labeled with pertinent infonnation and then placed
immediately on ice and chilled to 4°C for storage and subsequent delivery to the analyzing
laboratory. All field operations were conducted under the supervision of a California
Registered Geologist.
The locations of the delineation soil samples are shown on Figure 4. Soil samples were
analyzed for TPH-g by the CA DOHS approved method 8015M and for Benzene, Toluene,
Ethylbenzene, Xylene (BTEX), and Methyl-tert-Butyl Ether (MTBE) by EP A Method 8260B.
ANALYTICAL RESULTS OF DELINEATION SOIL SAMPLES
A total of two tank pit and three dispenser delineation soil samples were collected to verifY
successful removal of impacted material. There were no TPH-g or BTEX concentrations
detected in soil samples 3AA or 3BB. MTBE was not detected in sample 3M An MTBE
419.EQL.00
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April 8, 2002
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concentration of23 µgIkg was detected in sample 3BB.
Table 3 summarizes the delineation soil samples analytical results.
The analytical results of all the soil samples are summarized in Tables 1, 2, and 3 of tlùs
report. Copies of the laboratory reports and chain-of-custody records for the soil samples are
included in Appendix C.
EXCAVATION BACKFILL AND COMPACTION
Upon removal of impacted material, the excavation pit was backfilled with imported material.
The imported material that was used as backfill contained no debris or rocks greater than 3"
diameter. The surface was left in a smooth graded condition with ground swface at its original
elevation. All backfill procedures were confumed tested for compaction compliance by a
geotechnical consultant.
SUMMARY
· Three 10,000 gallon gasoline and one 10,000 gallon diese~ double-walled fiberglass
underground fuel storage tanks (UST' s), four product dispensers and associated product
piping were removed during the field operations conducted on March 4, 2002.
· Immediately subsequent to tank removal, soil samples were collected from below the UST
inverts, dispensers, product lines and stockpiled material.
· Detectable hydrocarbon concentrations were reported in eight of the sixteen UST samples
and in three of the eight dispenser samples.
· A remedial excavation was conducted from March II, 2002 to remove the hydrocarbon
impacted soil from beneath the UST's. Results of delineation samples indicated the
maximum MTBE concentration remaining in the soil were 23 µglkg at a depth of 23 feet
BSG.
· Approximately 522.25 tons of impacted material was removed from the site as a result of
the UST removal and remedial excavation. The impacted soil was transported under
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Southwest, ]{nc
manifest to the TPS Technologies Inc. disposal facility in Adelanto, CA.
WGR Southwest, IDe.
Prepared by:
Approved by:
Ryan~~Scienrim
419.EQL.00
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April 8, 2002
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I ATTACHMENTS
FIGURES
I TABLES
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11021 Winners CircJe. Suite 101
Los Alamitos. CA 90720
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DATE PROJECT NUMBER
4/8/02 419.EQL.OO
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DATE PROJECT NUMBER
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Table 1
UST REMOVAL SOIL SAMPLE ANALYTICAL SUMMARY
Texaco Service Station
2601 White Lane
Bakersfield, California
8015M EPA METHOD 8260B
Ethyl Total
Sample Depth TPH-d TPH-g Benzene Toluene Benzene Xylenes MTBE
Number (Ft) Date (mg/kg) (mglkg) (µg/kg) (µgIkg) (µgIkg) ( µg/kg) (µg/kg)
IA 15 3/4/02 NA ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND< 1 0 8.1
19 3/4/02 NA ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<10 ND<5.0
IB 15 3/4/02 NA ND<O.50 ND<5.0 ND<5.0 ND<5.0 ND<10 ND<5.0
19 3/4/02 NA ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<lO ND<5.0
2A 15 3/4/02 NA ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<10 6.5
19 3/4/02 NA ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND< 1 0 ND<5.0
2B 15 3/4/02 NA ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<10 ND<5.0
19 3/4/02 NA ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<10 ND<5.0
3A 15 3/4/02 NA ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND< 10 26
19 3/4/02 NA ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<10 13
3B 15 3/4/02 NA ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<10 68
19 3/4/02 NA ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<10 130
4A 15 3/4/02 ND<5.0 ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND< 1 0 7.3
19 3/4/02 ND<5.0 ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<10 ND<5.0
4B 15 3/4/02 ND<5.0 ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND< 1 0 ND<5.0
19 3/4/02 ND<5.0 ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND< 1 0 5.5
D-I 2 3/4/02 ND<5.0 ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<10 ND<5.0
6 3/4/02 170 9.1 ND<10 ND<10 24 460 ND<10
D-2 2 3/4/02 ND<5.0 ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<10 ND<5.0
6 3/4/02 ND<5.0 ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<10 6.9
D-3 2 3/4/02 ND<5.0 ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<10 ND<5.0
6 3/4/02 ND<5.0 ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND< 1 0 ND<5.0
D-4 2 3/4/02 ND<5.0 ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<10 ND<5.0
6 3/4/02 76 ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<10 ND<5.0
NA - Not Analyzed
ND - Not Detected
-------------------
Table 2
STOCKPILE SAMPLE ANAL YTICAL SUMMARY
Texaco Service Station
2601 White Lane
Bakersifield, California
8015M EPA METHOD 8260B
Ethyl Total
Sample TPH-g Benzene Toluene Benzene Xylenes MTBE
Number Date (mg/kg) (µglkg) (µg/kg) (µg/kg) (µglkg) (µg/kg)
SP-l 3/4/02 ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND< 1 0 41
SP-2A 3/4/02 ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<lO ND<5.0
SP-2B 3/4/02 ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<10 ND<5.0
SP-3A 3/4/02 ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<lO ND<5.0
SP-3B 3/4/02 ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<lO ND<5.0
NA - Not Analyzed
ND - Not Detected
-------------------
Table 3
DELINIA TION SOIL SAMPLE ANALYTICAL SUMMARY
Texaco Service Station
2601 White Lane
Bakersfield, California
8015M EPA METHOD 8260B
Ethyl Total
Sample Depth TPH-g Benzene Toluene Benzene Xylenes MTBE
Number (Ft) Date (mglkg) (µg/kg) (µglkg) (µglkg) (µglkg) (µglkg)
3AA 23 3/11/02 ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND< 1 0 ND<5.0
3BB 23 3/11/02 ND<0.50 ND<5.0 ND<5.0 ND<5.0 ND<lO 23
NA - Not Analyzed
ND - Not Detected
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I APPENDIX B
SOIL DISPOSAL
I MANIFESTS
I
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I
I 419.EQL.00 April 8, 2002
I
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. _. UjD.Þ/o~
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Customer Job Report
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A07·- 1I1O:¡81'EXACO N61O-S800-14()(, RIPR#I002' SAP#12lO17 rNCDNT#9714BAK.ERSPI¡¿L..U CA ~:i30'"
Loa4 1# Date k Tirt1è Out 'Tr.U1~portC"'· # Truck & TTlliler Nlurlber OlOSt! TaT\,: N~t Nrt Wt
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2. 04/01/0209: Hi 7000193 12<) - 02 SO, I ~OM 31,9~OM 48. 2()C I 24.111
, 1)4/01 102 01]: 17 7000l!)) 127··02 79,R40M J2,OOOM 11,~40 ¡J.92
3 04/0 I¡()2 09:34 7000193 2 74,660M J 1.220M 43,4411 21.72
4 04/0110209:35 7000193 )3W al,16OM .:¡.~,7g()M 47,,;80 2~.69
5 (14/0l102 09: 55 7110m 93 129M 80,440M 21f,420M 52,020 26.01
6 04/0U02n9:sg 7000193 . 77,420M 32,ClZOM 4j,40() 22.70
7 04/01/0210:11 700œ 93 111 -219 83,420M 21C,S8ùM S4,K4() 27.42
9 04/01/0210:39 7000193 W9 RO,tif,aM 27,l40M 53,.520 2ó.7f:
8 ()4/011U210:4() 7000 }I)'3 '7 - ~l.600M ~1,420M ~O, I~{\ 25.09
10 04/01102 I 1:23 7000193 3U 76,200M 31,360M 44.I4U 22.42
14 11410110212:09 70001 !)J 7ClO 77,1$2UM ~I,9~M 4~.MO 22.92
11 04/0 I /02 12: 11 700019] ¥O 76,7401\1 32,880M 43.860 21.93
12 04/01/0212:34 1000193 51 79,SSOM 33,KlCOM 4~,70( 22.8~
13 04/OI/U212:36 7000] 93 38 77,300M 31,340M 45.960 22,'J!
15 04101102 I S:30 7000193 129 - U2 79,~OOM J2.K20M 46,680 23.34
16 0410110215::.13 '7000 193 127 - 02 M.040M 32,OOOM 4K,(4Q 24.m
17 04101/021(,:5& 7000193 2 !iI, 800M 30,gOOM Sl,OOO 25.50
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APPENDIX C
LABORATORY REPORTS AND CHAIN-OF-CDSTODY RECORD
419 .EQL. 00 April 8, 2002
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c: a/science
I:Environmental
'- aboratories, Inc.
March 07, 2002
Dave Williams
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Subject: Calscience Work Order No.:
Client Reference:
Dear Client:
f
!
¡
02-03-0130
2601 White Ln, Bakersfield
Enclosed is an analytical report for the above-referenced project. The samples
included in this report were received 3/5/02 and analyzed in accordance with
the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the
guidelines established in our Quality Assurance Program Manual, applicable standard
operating procedures, and other related documentation. The results in this analytical
report are limited to the samples tested and any reproduction thereof must be made in
its entirety.
If you have any questions regarding this report, please do not hesitate to contact the
undersigned.
C Is Ie c nvironmental
Laboratories, Inc.
Larry Lem
Project Manager
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,
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Michael,J. risostomo
Quality As urance Manager
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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WGR Southwest, Inc.
11021 Winners Circle, Suite 101
os Alamitos, CA 90720-0000
'"-= a/science
ß:~nVironmenta/
Laboratories, Inc.
. .
ANALYTICAL REPORT
roject: 2601 White Ln, Bakersfield
lient Sample Number
4A 15'
Parameter
IPH as Diesel
SurrOQates:
IecachlorobiPhenYI
Parameter
IPH as Diesel
SurroQates:
ecachlorobiphenyl
4815'
I Parameter
TPH as Diesel
I Surrogates:
ecachlorobiphenyl
B 19'
Parameter
IH as Diesel
Surrogates:
IcachlorobiPhenYI
I
:\j.
Result
ND
REC(%)
92
Result
ND
REC (%)
93
Result
ND
REC(%)
88
Result
ND
REC (%)
90
Lab Sample
Number
: 02-03-0130-13
RL
5.0
Control
Limits
45-149
DF
02-03-0130-14
RL
5.0
Control
Limits
45-149
DF
02-03-0130-15
RL
5.0
Control
Limits
45-149
DF
02-03.0130-16
RL DF
5.0
Control
Limits
45-149
RL - Reporting Limit, DF - Dilution Factor, Qual - Qualifiers
Matrix
Solid
Qual Units
mg/kg
Qual
Solid
Qual Units
mglkg
Qual
Solid
Qual Units
mg/kg
Qual
Solid
Qual Units
mg/kg
Qual
Date Reœived:
Work Order No:
Preparation:
Method:
03/05/02
02-03-0130
Ext. + 0/1
. EPA8015M
Page 1 of 4
Date Date Date
Collected Prepared Analyzed QC Batch ID
03104102 03/05102 03105102 02030503s8 ,
03/04102
03105/02 03/05102
02030503sa
03/04102, 03/05102 03/05102' 02030503sa
03/04/02
03/05102 03/05102
02030503sa
f
\
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I ~= a/science
I ANAL YTICAL REPORT
I:§nvironmenta/
I Laboratories, Inc.
WGR Southwest, Inc. Date Received: 03/05/02
11021 Winners Circle, Suite 101 Work Order No: 02-03-0130
os Alamitos, CA 90720-0000 Preparation: Ext. + DII
Method: EPA 8015M
Iroject: 2601 White Ln, Bakersfield Page 2 of 4
Lab Sample Date Date Date
lient Sample Number Number Matrix Collected Prepared Analyzed QC Batch ID
0-12' ·'·s· 02-G3-G13o.:.17 Solid 03/04102 03/05102 , 03105102 02030503sa
I Parameter Result RL DF Qual Units
PH as Diesel ND 5.0 mglkg
SurrOQates: REC(%) Control Qual
lecachlorobiPhenYI Limits
88 45-149
0-16' . ,02-G3-G130-18 Solid 03/04102 03105102 03/05102 02030503sa
Parameter Result RL DF Qual Units
IPH as Diesel 170 5 mg/kg
REC(%) Control Qual
SurroQates: Limits
ecachlorobiphenyl 91 45-149
D-22' 02.:03.:0130-19 Solid 03/04102 03/05102 03/05/02 ' 02030503sa'·
I Parameter Result RL DF Qual Units
TPH as Diesel ND 5.0 mglkg
I SurroQates: REC (%) Control Qual
Limits
Decachlorobiphenyl 77 45-149
D-26' 02-G3-0130-20 Solid 03/04102 03/05/02 03/05/02 02030503sa
Parameter Result RL DF Qual Units
JH as Diesel ND 5.0 mg/kg
SurroQates: REC(%) Control Qual
JcachlorobiPhenYI Limits
90 45-149
RL - Reporting Limit. DF - Dilution Factor, Qual- Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I ' , .
. =alscience
I ANALYTICAL REPORT
I/!;snvironmental
I Laboratories, Inc.
WGR Southwest, Inc. Date Received: 03/05/02
111021 Winners Circle, Suite 101 Work Order No: 02-03-0130
Los Alamitos, CA 90720-0000 Preparation: Ext. + 0/1
Method: EPA 8015M
Iproject: 2601 White Ln, Bakersfield Page 3 of 4
Lab Sample Date Date Date
lient Sample Number Number Matrix Collected ' Prepared Analyzed, QC Batch ID
. 02-03-0130-21 Solid 03104102 '03105102 '. 03106102 ' , 0203050~",
'L Parameter Result RL DF Qual Units
PH as Diesel ND 5.0 mglkg
SurroQates: REC (%) Control Qual
IcecachlorobiPhenYI Limits
77 45-149
D-36' 02-03-0130-22 Solid 03104102 03105102 03106102 ' 02030503sa
Parameter Result RL DF Qual Units
rPH as Diesel ND 5.0 mg/kg
REC(%) Control Qual
SurrOQates: Limits
ecachlorobiphenyl 85 45-149
D-42' 02-03-0130-23 Solid 03/04102 03/05102 03/06/02 02030503sa
I Parameter Result RL DF Qual Units
TPH as Diesel NO 5.0 mg/kg
I SurroQates: REC (%) Control Qual
Limits
Decachlorobiphenyl 90 45-149
D-46' 02-03-0130-24 Solid 03104/02 03/05/02 03106/02 02030503sa
Parameter Result RL DF Qual Units
IPH as Diesel
76 5 mg/kg
Surrogates: REC(%) Control Qual
lecachlorobiPhenYI Limits
87 45-149
I
RL - Reporting Limit. DF - Dilution Factor. Qual- Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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~= a/science
I:;g¡gnvironmenta/
'- aboratories, Inc.
ANALYTICAL REPORT'
. .
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Project: 2601 White Ln, Bakersfield
Date Received:
WorkÚrder No:
Preparation:
Method:
03/05/02
02-03-0130
Ext. + D/I
EPA 8015M
Page 4 of 4
Client Sample Number
. Method Blank
Parameter
Result
TPH as Diesel
ND
SurrOQates:
REC (%)
Decachlorobiphenyl
77
Lab Sample
Number
< '098-O3"()()2-1 ,689
Matrix
Date
Collected
'. "N/A
Solid
RL
5.0
DF
Qual Units
mg/kg
Control
Limits
45-149
Qual
RL - Reporting Limit. DF - Dilution Factor, Qual- Qualifiers
Date
Prepared
03/05102
Date
Analyzed QC Batch JD
03/06/02 ' ; <. 02030503sa
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I C a/science
I ANALYTICAL REPORT
6!;gnvironmenta/
I '- aboratories, Inc.
WGR Southwest, Inc. Date Reœived: 03/05/02
I 11021 Winners Circle, Suite 101 Work Order No: 02-03-0130
Los Alamitos, CA 90720-0000 Preparation: EPA 5030B
Method: EPA 8015M
I Project: 2601 White Ln, Bakersfield Page 1 of 7
lab Sample Date Date Date
I Client Sample Number Number Matrix Collected Prepared Analyzed QC Batch ID
"* ',.
1A is' . ,02~3~13O-1' Solid ' '03104102 ' NJA 03/05102 02030501 sa
I Parameter Result Rl DF Qual Units
TPH as Gasoline ND 0.50 mglkg
Surrogates: REC (%) Control Qual
I limits
1 ,4-Bromofluorobenzene 91 21-159
I 1A 19' " 02~3~130-2 Solid 03104102 N/A 03/05102 ' 02030S01sa
Parameter Result RL DF Qual Units
I TPH as Gasoline ND 0.50 mglkg
SurrOQates: REC (%) Control Qual
limits
I 1,4-Bromofluorobenzene 68 21-159
1815' 02~3-o130-3 Solid 03104/02 N/A 03105102 02030501 sa
I Parameter Result Rl DF Qual Units
TPH as Gasoline ND 0.50 mg/kg
I Surrogates: REC (%) Control Qual
limits
1 ,4-Bromofluorobenzene 86 21-159
I 1B 19' 02-03-0130-4 Solid 03/04102 N/A 03105/02 02030501sa
Parameter Result RL DF Qual Units
I TPH as Gasoline ND 0.50 mglkg
Surrogates: REC (%) Control Qual
I limits
1,4-Bromofluorobenzene 86 21-159
I
I
RL - Reporting Limit DF - Dilution Factor Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 . TEL: (714) 895-5494 . FAX: (714) 894-7501
I ( = a/science
I ANALYTICAL REPORT
I:; nvironmenta/
I Laboratories, Inc.
WGR Southwest, Inc. Date Received: 03/05/02
I 11021 Winners Circle, Suite 101 Work Order No: 02-03-0130
Los Alamitos, CA 90720-0000 Preparation: EPA 5030B
Method: EPA 8015M
I Project: 2601 White Ln, Bakersfield Page 2 of 7
Lab Sample Date Date Date
I Client Sample Number Number Matrix Collected Prepared Analyzed QC Batch ID
'2A1S' 02-o3-Ó13G-S . ". Solid ·,.,03/04102 WA 03105102 ." '02030S01sa
I Parameter Result RL DF Qual Units
TPH as Gasoline ND 0.50 mglkg
I Surrogates: REC(%) Control Qual
limits
1 ,4-Bromofluorobenzene 89 21-159
I 2A19' .. . 02-03-0130-6 ,Solid 03104102 WA 03/05102 02030501 sa
Parameter Result RL DF Qual Units
I TPH as Gasoline ND 0.50 mglkg
SurroQates: REC(%) Control Qual
limits
I 1 ,4-Bromofluorobenzene 93 21-159
2B 15' : 02-03-0130-7 Solid 03/04102 N/A 03105102 . 02030501 sa
I Parameter Result RL OF Qual Units
TPH as Gasoline ND 0.50 1 mglkg
I Surrogates: REC (%) Control Qual
limits
1 ,4-Bromofluorobenzene 85 21-159
I 2B19' 02-03-0130-8 Solid 03/04102 N/A 03105102 02030501 sa
I Parameter Result RL OF Qual Units
TPH as Gasoline NO 0.50 mglkg
. Surrogates: REC (%) Control Qual
I Limits
1 ,4-Bromofluorobenzene 52 21-159
I
I
RL - Reporting limit . DF - Dilution Factor. Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I . = a/science
I ANALYTICAL REPORT
I!;gnvironmenta/
I Laboratories, Inc.
WGR Southwest, Inc. Date Received: 03/05/02
I 11021 Winners Circle, Suite 101 Work Order No: 02-03-0130
Los Alamitos, CA 90720-0000 Preparation: EPA 5030B
Method: EPA 8015M
I Project: 2601 White Ln, Bakersfield Page 3 of 7
Lab Sample Date Date Date
I Client Sample Number Number Matrix Collected Prepared Analyzed _ QC Batch ID
3A1S' ' 02-03-0130-9 'Solid .'. 03104102 NlA' 03/06/02' . 02030501 sa
I Parameter Result RL DF Qual Units
TPH as Gasoline ND 0.50 mglk.g
I Surrogates: REC (%) Control Qual
Limits
1,4-Bromofluorobenzene 76 21-159
I 3A 19' 02~3-o130-1.0 Solid 03104102 NIA 03/06/02 " 02030S01sa
Parameter Result RL DF Qual Units
I TPH as Gasoline ND 0.50 mglk.g
SurroQates: REC (%) Control Qual
Limits
I 1,4-Bromofluorobenzene 78 21-159
3B 1S' , 02-03-0130-11 Solid 03/04102 " N/A , 03/06/02 02030S015a
I Parameter Result RL DF Qual Units
TPH as Gasoline ND 0.50 mg/kg
I SurroQates: REC(%) Control Qual
Limits
1,4-Bromofluorobenzene 83 21-159
I 3B 19' 02-03-0130-12 Solid 03/04/02 N/A 03/06/02 02030S015a
I Parameter Result RL DF Qual Units
TPH as Gasoline ND 0.50 mg/kg
. SurroQates: REC(%) Control Qual
I Limits
1,4-Bromofluorobenzene 80 21-159
I
I
RL - Reporting Limit DF - Dilution Factor Qual - Qualifiers
7440 Lincoln Way, Garden Grove. CA 92841-1432 . TEL: (714) 895-5494 . FAX: (714) 894-7501
I C a/science
I ANALYTICAL REPORT
l::j1vironmenta/
I LaboratOries, Inc.
WGR Southwest, Inc. Date Received: . 03/05/02
I 11021 Winners Circle, Suite 101 Work Order No: 02-03-0130
Los Alamitos, CA 90720-0000 Preparation: EPA 5030B
Method: EPA 8015M
I Project: 2601 White Ln, Bakersfield Page 4 of 7
Lab Sample Date Date Date
I Client Sample Number Number Matrix Collected Prepared Analyzed QC Batch ID
4A1S' '. (j2,,()3.o130~13 Solid 03104102 NJA 03106102 ' 02030501 sa'
I Parameter Result RL DF Qual Units
TPH as Gasoline ND 0.50 mg/kg
I SurroQates: REC (%) Control Qual
Limits
1 ,4-Bromofluorobenzene 88 21-159
I 4A19' 02..()3..()130-14 Solid ,03/04102 ' NJA 03/06102 . .020305015a
Parameter Result RL DF Qual Units
I TPH as Gasoline ND 0.50 mg/kg
SurrOQates: REC (%) Control Qual
Limits
I 1,4-Bromofluorobenzene 87 21-159
4B is' .. 02"()3..()130-1S Solid ' 03Ì04/02 'N/A' . 03/06/02 02030501 sa
I Parameter Result RL DF Qual Units
TPH as Gasoline ND 0.50 mg/kg
I SurroQates: REC (%) Control Qual
Limits
1,4-Bromofluorobenzene 92 21-159
I 4B 19' 02"()3-0130-16 Solid 03/04102 N/A 03/06/02 02030S01sa
I Parameter Result RL DF Qual Units
TPH as Gasoline ND 0.50 mg/kg
Surrogates: REC(%) Control Qual
I Limits
1,4-Bromofluorobenzene 90 21-159
I
I
RL - Reporting Limit DF - Dilution Factor Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 . TEL: (714) 895-5494 . FAX: (714) 894-7501
I
. = a/science
I/; nvironmental
I.. aboratories, Inc.
I
I
ANALYTICAL REPORT
WGR Southwest, Inc.
111021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
I Project: 2601 White Ln, Bakersfield
Date Received:'
Work Order No:
Preparation:
Method:
03/05/02
02-03-0130
EPA 5030B
EPA 8015M
Lab Sample
Number
, : 02-03-0130-17'
Page 5 of 7
Date Date Date
Matrix Collected Prepared Analyzed QC Batch ID
Solid ' 03104102·: NIA 03106/02 02030501 sa
-The sample chromatographic pattem for TPH does not match the chromatographic pattem of the specified
standard. Quantitation of the unknown hydrocarbon(s) in the sample was based upon the specified standard.
Result RL DF Qual Units
I Client Sample Number
D-12'
I Parameter
TPH as Gasoline
I Surrogates:
1 ,4-Bromofluorobenzene
Result
ND
REC (%)
77
I
D-16'
Comment(s):
Parameter
I TPH as Gasoline
Surrogates:
11,4-Bromofluorobenzene
9.1
REC(%)
85
D-22'
I
Parameter
Result
I TPH as Gasoline
Surrogates:
ND
REC(%)
1 ,4-Bromofluorobenzene
I D-2 6'
77
RL
0.50
DF
Qual Units
mg/kg
Qual
Control
Limits
21-159
02-03-0130-18
, Solid
NIA
03104102
03106102
02030501 sa
0.5
mglkg
Control
Limits
21-159
Qual
, 02-o3~130-19
Solid
03/04/02
N/A
. 03/06/02
02030501 sa
RL DF
0.50
Qual Units
mglkg
Control
Limits
21-159
Qual
02-03-0130-20
Solid 03/04/02
02030501 sa
N/A
03/06/02
Result
Qual Units
I Parameter
TPH as Gasoline
ND
I Surrogates:
1,4-Bromofluorobenzene
REC (%)
74
RL - Reporting limit .
RL
0.50
DF
mglkg
Control
Limits
21-159
Qual
DF - Dilution Factor. Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I .... '..
I t...= a/science ANALYTICAL REPORT
~ nvironmenta/
I '- aboratories, Inc.
WGR Southwest, Inc. Date Received: 03/05/02
I 11021 Winners Circle, Suite 101 Work Order No: 02-03-0130
Los Alamitos, CA 90720-0000 Preparation: EPA 5030B
Method: EPA 8015M
I Project: 2601 White Ln, Bakersfield Page 6 of 7
Lab Sample Date Date Date
I Client Sample Number Number Matrix Collected Prepared Analyzed QC Batch ID
"D-32' ^ '02-03-0130-21 Solid 03104102 ',NIA 03/05102 02030401 sa
I Parameter Result RL DF Qual Units
TPH as Gasoline ND 0.50 mglkg
I SUIToQates: REC (%) Control Qual
Limits
1 ,4-Bromofluorobenzene 89 21-159
I D-36' 02-03-0130-22 Solid' . 03/04102 N/A " 03105102 02030401 sa
Parameter Result RL DF Qual Units
I TPH as Gasoline ND 0.50 mglkg
Surrogates: REC (%) Control Qual
Limits
I 1,4-Bromofluorobenzene 93 21-159
1>-42' 02-03-0130-23 Solid 03/04102 N/A 03/05/02 02030401 sa
1 Parameter Result RL DF Qual Units
TPH as Gasoline ND 0.50 mg/kg
I Surrogates: REC (%) Control Qual
Limits
1,4-Bromofluorobenzene 81 21-159
I 1>-46' 02-03-0130-24 Solid 03104102 N/A 03/05102 02030401 sa
Parameter Result RL DF Qual Units
I TPH as Gasoline
ND 0.50 mg/kg
, SurroQates: REC(%) Control Qual
11 ,4-Bromofluorobenzene Limits
88 21-159
RL - Reporting Limit, DF - Dilution Factor, Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
~=alscience
ß!;ggnVironmental
Laboratories, Inc.
ANALYTICAL REPORT
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Project: 2601 White Ln, Bakersfield
Date Received:
Work Order No:
Preparation:
Method:
03/05/02
02-03-0130
EPA 5030B
EPA 8015M
Page 7 of 7
Client Sample Number
Method Blank
'. -".'. '> ~ <
, ,098-03-00,8-1;881
Lab Sample
Number
Parameter
Result
TPH as Gasoline
ND
SurroQates:
REC (%)
87
1 ,4-Bromofluorobenzene
";Method Blank
Parameter
Result
TPH as Gasoline
ND
SurroQates:
REC(%)
77
1,4-Bromofluorobenzene
RL
0.50
Control
Limits
21-159
DF
09/J-03-o08-1,883
RL
0.50
Control
Limits
21-159
DF
RL· Reporting Limit, DF· Dilution Factor, Qual· Qualifiers
Matrix
Date
Collected
'N/A
Date Date
Prepared Analyzed
.'.. ,N/A "03/04102
NJA
NlA 03105102
QC Batch ID
,,02030401.Sa
02030501 sa
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
Solid
Qual Units
mg/kg
Qual
Solid,
Qual Units
mg/kg
Qual
I
· - a/science
I:; nvironmenta/
Laboratories, Inc.
I
I WGR Southwest, Inc.
11021 Winners Circle, Suite 101
I Los Alamitos, CA 90720-0000
ANALYTICAL REPORT
Date Received:
Work Order No:
Preparation:
Method:
I Project: 2601 White Ln, Bakersfield
Lab Sample
Number
'Ô2~3~13o.;1X< '.>,
Matrix
Date Date
Prepared Anal ed QC Batch ID
'I
I Parameter
Benzene
Ethylbenzene
I Toluene
SurroQates:
Dibromofluoromethane
I 1,4-Bromofluorobenzene
Parameter
I Benzene
Ethylbenzene
Toluene
I SurroQates:
Dibromofluoromethane
1,4-Bromofluorobenzene
I
Parameter
I Benzene
Ethylbenzene
Toluene
I SurroQates:
Dibromofluoromethane
1 ,4-Bromofluorobenzene
I 1819'
Parameter
I Benzene
Ethylbenzene
Toluene
SurroQates:
Dibromofluoromethane
1.4-Bromofluorobenzene
..., \NiÂ;< . ».03/Q5t02"{Q30@2AS..
.'.... ,"' .:.'. >~- . .";.\ .",/ ,:- ::
····:SolidF<
03/05/02
02-03-0130
N/A
EPA 8260B
Page 1 of 7
Result RL DF Qual Units Parameter Result RL DF Qual Units
ND 5.0 uglkg p/m-Xylene ND 5.0 ug/kg
ND 5.0 uglkg o-Xylene ND 5.0 ug/kg
ND 5.0 uglkg Methyl-t-Butyl Ether (MTBE) 8.1 5.0 ug/kg
REC(%) Control Qual Surrogates: REC (%) Control Qual
Limits Limits
105 80-120 Toluene-d8 109 81-117
92 74-121
Result
ND
NO
ND
REC(%)
107
92
Result
NO
ND
ND
REC (%)
108
92
. .-:-::<,/." "'.. ~.
'c;C)~::03-9130':2' . ..
. >·C)3/Ø4l02~·. ·<.':···.:::$òlid:-...···' :,,:·-;'·<:~F-NJÁ::
RL DF Qual Units Parameter Result
5.0 ug/kg p/m-Xylene NO
5.0 ug/kg o-Xylene ND
5.0 ug/kg Methyl-t-Butyl Ether (MTBE) ND
Control Qual Surroç¡ates: REC(%)
Limits
80-120 Toluene-d8 108
74-121
P2-o3.,o130-3 03/04/02 Solid
RL OF Qual Units Parameter Result
5.0 uglkg p/m-Xylene ND
5.0 uglkg o-Xylene ND
5.0 ug/kg Methyl-t-Butyl Ether (MTBE) ND
Control Qual SurroQates: REC (%)
Limits
80-120 Toluene-d8 107
74-121
02-03-0130-4 03/04/02 >'Solid NJA
Result RL DF Qual Units Parameter Result
ND 5.0 ug/kg p/m-Xylene ND
ND 5.0 uglkg o-Xylene ND
ND 5.0 uglkg Methyl-t-Butyl Ether (MTBE) ND
REC(%) Control Qual Surrogates: REC(%)
Limits
109 80-120 Toluene-d8 107
91 74-121
RL - Reporting Limit. DF - Dilution Factor. Qual - Qualifiers
·[<03l.ÒŠ/Ó~ <0305021.5
RL DF Qual Units
5.0 uglkg
5.0 ug/kg
5.0 ug/kg
Control Qual
Limits
81-117
03/05/02. . '. 030502AS
RL DF Qual Units
5.0 uglkg
5.0 ug/kg
5.0 uglkg
Control Qual
Limits
81-117
03/05102 030502AS
RL DF Qual Units
5.0 ug/kg
5.0 uglkg
5.0 ug/kg
Control Qual
Limits
81-117
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
I
E -a/science
I:ænvironmental
Laboratories, Inc.
ANALYTICAL REPORT
I WGR Southwest, Inc.
11021 Winners Circle, Suite 101
I Los Alamitos, CA 90720-0000
Date Received:
Work Order No:
Preparation:
Method:
03/05/02
02-03-0130
N/A
EPA 8260B
I Project: 2601 White Ln, Bakersfield
Page 2 of 7
I Client Sample Number
Date
Collected Matrix
03/04/02 <Solid
Date
Prepared
~,;:;:,?N/Å' .
Date
Analyzed QC Batch ID
. ..... ....,. .....- ,."?, ,".
;03105102';' )'030502AS'
I Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units
Benzene ND 5.0 uglkg p/m-Xylene ND 5.0 uglkg
Ethylbenzene ND 5.0 uglkg o-Xylene ND 5.0 ug/kg
I Toluene ND 5.0 uglkg Methyl-t-Butyl Ether (MTBE) 6.5 5.0 uglkg
Surrogates: REC (%) Control Qual Surrogates: REC (%) Control Qual
Limits Limits
Dibromofluoromethane 112 80-120 Toluene-d8 108 81-117
1,4-Bromofluorobenzene 89 74-121
I «'Solid} . NlA . .. >'0~/05l02 .... <Ò305Ø2A.S .....
. ~,;,
/",<..,'
I Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units
Benzene NO 5.0 uglkg p/m-Xylene ND 5.0 ug/kg
Ethylbenzene NO 5.0 uglkg o-Xylene ND 5.0 ug/kg
Toluene ND 5.0 ug/kg Methyl-t-Butyl Ether (MTBE) ND 5.0 ug/kg
I Surrogates: REC (%) Control Qual Surrogates: REC(%) Control Qual
Limits Limits
Dibromofluoromethane 112 80-120 Toluene-d8 107 81-117
1,4-Bromofluorobenzene 90 74-121
I }···..·....·.02:'O3.,()130-7. ) Solid ............ ....;NIA.··... . '..03/05102 '. :030502AS
Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units
I Benzene ND 5.0 ug/kg p/m-Xylene NO 5.0 ug/kg
Ethylbenzene ND 5.0 uglkg o-Xylene ND 5.0 ug/kg
Toluene ND 5.0 uglkg Methyl-t-Butyl Ether (MTBE) NO 5.0 ug/kg
I SurroQates: REC (%) Control Qual Surrogates: REC(%) Control Qual
Limits Limits
Dibromofluoromethane 113 80-120 Toluene-d8 106 81-117
1,4-Bromofluorobenzene 91 74-121
I 2B 19' 02:,03:,0130-8 03/04/02 'N/A 03/05102 030S02AS
Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units
Benzene NO 5.0 ug/kg pIm-Xylene ND 5.0 uglkg
Ethylbenzene ND 5.0 ug/kg o-Xylene ND 5.0 ug/kg
Toluene ND 5.0 uglkg Methyl-t-Butyl Ether (MTBE) ND 5.0 ug/kg
SurroQates: REC (%) Control Qual SurroQates: REC (%) Control Qual
Limits Limits
Oibromofluoromethane 119 80-120 Toluene-d8 101 81-117
1,4-BromofJuorobenzene 95 74-121
RL - Reporting Limit, OF - Dilution Factor. Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
. =alscience
I/:, nvironmental
LaboratOries, Inc.
I
I WGR Southwest, Inc.
11021 Winners Circle, Suite 101
I Los Alamitos, CA 90720-0000
ANALYTICAL REPORT
I Project: 2601 White Ln, Bakersfield
Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units
Benzene ND 5.0 uglkg p/m-Xylene ND 5.0 ug/kg
Ethylbenzene ND 5.0 uglkg o-Xylene ND 5.0 ug/kg
Toluene ND 5.0 uglkg Methyl-t-Butyl Ether (MTBE) 26 5. uglkg
Surrogates: REC(%) Control Qual Surrogates: REC (%) Control Qual
Limits Limits
Dibromofluoromethane 117 80-120 T oluene-d8 108 81-117
1,4-Bromofluorobenzene 90 74-121
I
I
I
13A 19'
......,..,.;·.c,' .
. '-"":";'::':"';';,:"'::"
Parameter
I
Result
Benzene
Ethylbenzene
Toluene
I Surrogates:
ND
NO
ND
REC (%)
117
95
Dibromofluoromethane
1,4-Bromofluorobenzene
I
Parameter
Result
I Benzene
Ethylbenzene
Toluene
I Surrogates:
ND
ND
ND
REC(%)
112
99
Oibromofluoromethane
1,4-Bromofluorobenzene
I
3819'
Parameter Result
I Benzene ND
Ethylbenzene ND
Toluene ND
Surrogates: REC(%)
Dibromofluoromethane 118
1,4-Bromotluorobenzene 90
RL - Reporting Limit ,
',"," .
> ":::." ,~::.':/--'::/.'
Lab Sample
Number
j{\,p21J3~j~~~\:
Date Received:
Work Order No:
Preparation:
Method:
03/05/02
02-03-0130
N/A
EPA 8260B
.,,::.<~<>, ..
:-. -.'.-:-: ::-/.-.:':.:'-.,.. ,< . ..,.-..-.....- .
,. :::iþ2..()~130:-10/
Page 3 of 7
Date
Collected Matrix
;'·03/04102 ·;<~ôlid·.·
Date Date
Prepared Analyzed QC Batch ID
?;}' .. NiA'L )~:;O~/o5iô~::6ò3~502AS' .
""<";'-,;'';
DF Qual Units
RL
5.0
5.0
5.0
Control
Limits
80-120
74-121
······:··/<.02:;ij3-Ò130-11
uglkg
uglkg
uglkg
Qual
. ". .
. 03104102; :.: .·:Sol.l~ .:'.'
)~/AC,; 93/05lô2': 030502AS
'-'","
. ..
Parameter Result RL DF Qual Units
p/m-Xylene NO 5.0 ug/kg
o-Xylene ND 5.0 ug/kg
Methyl-t-Butyl Ether (MTBE) 13 5 ug/kg
Surrogates: REC(%) Control Qual
Limits
Toluene-d8 108 81-117
03/04102 .' ····;;Solid
'-' " , .
. . ·'()3/07J02.>,,030702As
··,··,·':NlA
RL DF Qual Units Parameter Result RL DF Qual Units
5.0 uglkg p/m-Xylene NO 5.0 ug/kg
5.0 uglkg o-Xylene NO 5.0 ug/kg
5.0 uglkg Methyl-t-Butyl Ether (MTBE) 68 5 ug/kg
Control Qual Surrogates: REC(%) Control Qual
Limits Limits
80-120 Toluene-d8 99 81-117
74-121
. .
...... >.02"03"013G-12 03105102 030502AS
RL DF Qual Units Parameter Result RL DF Qual Units
5.0 uglkg p/m-Xylene NO 5.0 ug/kg
5.0 uglkg o-Xylene ND 5.0 ug/kg
5.0 ug/kg Methyl-t-Butyl Ether (MTBE) 130 5 ug/kg
Control Qual Surrogates: REC(%) Control Qual
Limits Limits
80-120 Toluene-d8 94 81-117
74-121
DF - Dilution Factor. Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
: "
I
. = a/science
'=g¡nvironmenta/
I. aboratories, Inc.
ANALYTICAL REPORT
I WGR Southwest, Inc.
11021 Winners Circle, Suite 101
I Los Alamitos, CA 90720-0000
Date Received:
Work Order No:
Preparation:
Method:
03/05/02
02-03-0130
N/A
EPA 8260B
I Project: 2601 White Ln, Bakersfield
Page 4 of7
I
Lab Sample
Number
Date
Collected
Date
Matrix Prepared
pSOIl«Í<.i/.'NJA
Date
Analyzed QC Batch ID
ò3Í0~Ò2>.:0305()2AS
. . >, -~: '.
:\\·02~3.:oÚO~13/ .... .... ." 03/04102.
I Parameter
Parameter
I Benzene
Ethylbenzene
Toluene
I SurroQates:
Dibromofluoromethane
1,4-Bromofluorobenzene
I 4B 19'
Parameter
I Benzene
Ethylbenzene
Toluene
SurroQates:
I Oibromofluoromethane
1,4-Bromofluorobenzene
Result RL OF Qual Units Parameter Result RL DF Qual Units
ND 5.0 ug/kg p/m-Xylene ND 5.0 uglkg
ND 5.0 uglkg o-Xylene ND 5.0 ug/kg
ND 5.0 uglkg Methyl-t-Butyl Ether (MTBE) 7.3 5.0 uglkg
REC (%) Control Qual Surrogates: REC (%) Control Qual
Limits Limits
117 80-120 Toluene-d8 108 81-117
85 74-121
'":;",'; . ,.,. . . . ., . . ,.. .
.. .. ;'02~~130~14 .............. .03/04/02 03!OS/Q2" "03ÓS02As .,...
Result RL DF Qual Units Parameter Result RL DF Qual Units
ND 5.0 ug/kg p/m-Xylene ND 5.0 ug/kg
ND 5.0 uglkg o-Xylene ND 5.0 ug/kg
ND 5.0 ug/kg Methyl-t-Butyl Ether (MTBE) ND 5.0 ug/kg
REC (%) Control Qual Surrogates: REC(%) Control Qual
Limits Limits
120 BO-120 Toluene-dB 107 B1-117
86 74-121
·02~3~130-1S· ; 030502AS .'
~ ~' ..
Result RL DF Qual Units Parameter Result RL DF Qual Units
ND 5.0 ug/kg p/m-Xylene NO 5.0 uglkg
ND 5.0 ug/kg o-Xylene NO 5.0 ug/kg
ND 5.0 ug/kg Methyl-t-Butyl Ether (MTBE) NO 5.0 uglkg
REC(%) Control Qual Surrogates: REC(%) Control Qual
Limits Limits
96 80-120 Toluene-d8 95 81-117
95 74-121
02-03'-0130-16 03/04/02 Solid N/A 03/0S/02 030502AS
Result RL DF Qual Units Parameter Result RL OF Qual Units
ND 5.0 uglkg p/m-Xylene ND 5.0 ug/kg
ND 5.0 uglkg o-Xylene ND 5.0 ug/kg
ND 5.0 ug/kg Methyl-t-Butyl Ether (MTBE) 5.5 5.0 ug/kg
REC (%) Control Qual SurroQates: REC(%) Control Qual
Limits Limits
94 80-120 Toluene-d8 87 81-117
96 74-121
Benzene
Ethylbenzene
Toluene
I Surrogates:
Dibromofluoromethane
11.4-BromOflUOrObenzene
Parameter
I
Benzene
Ethylbenzene
Toluene
I Surrogates:
I
Dibromofluoromethane
1,4-Bromofluorobenzene
RL - Reporting Limit .
DF - Dilution Factor. Qual - Qualifiers
7440 Lincoln Way, Garden Grove. CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501
I
· =a/science
I:¡¡;gnvironmental
'- aboratories, Inc.
I
ANALYTICAL REPORT
I WGR Southwest, Inc.
11021 Winners Circle, Suite 101
I Los Alamitos, CA 90720-0000
I Project: 2601 White Ln, Bakersfield
I
Lab Sample
Number
'02~3~1àO:-:~i /.
I
I
I 'D-1 6'
".:
., ..
i:,;02~~13ô-18
<t> .,.,.::::.:...:.:':,.-.,........-.
,".",
-"-".",';,:<",:.
,"
..
Parameter
I
Result RL DF Qual Units
ND 10 2 ug/kg
24 10 2 uglkg
ND 10 2 ug/kg
REC(%) Control Qual
Limits
97 80-120
97 74-121
Benzene
Ethylbenzene
Toluene
I Surrogates:
Dibromofluoromethane
1 ,4-Bromofluorobenzene
I
",'
~/..;< .<~-~..
;,-."
. {:;02.:o3~13Ô:19 <,. .
Parameter
I Benzene
Ethylbenzene
Toluene
I SurroQates:
Dibromofluoromethane
1 ,4-Bromofluorobenzene
I D-26'
Parameter
I Benzene
Ethylbenzene
Toluene
I Surroqates:
Dibromofluoromethane
1,4-Bromofluorobenzene
I
Result RL DF Qual Units
ND 5.0 uglkg
ND 5.0 uglkg
ND 5.0 uglkg
REC (%) Control Qual
Limits
97 8Q..120
92 74-121
: 02-03-0130-20
Date Received:
Work Order No:
Preparation:
Method:
03/05/02
02-03-0130
N/A
EPA 8260B
Page 5 of 7
Date
Collected
03104102
Date Date
Matrix Prepared Analyzed QC. Batch ID
. Solid i,;) ,;::NíÁ(;:,'~{0~()~å2;r:03Q50~S .'
,;.,'<:".
;'·.":03/04102,
$olid ..
N/A ,. '.' "";' 03/o§i02/,ó~Ôs02AS:
Parameter
Result
Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units
Benzene ND 5.0 uglkg p/m-Xylene ND 5.0 uglkg
Ethylbenzene ND 5.0 uglkg o-Xylene ND 5.0 uglkg
Toluene ND 5.0 uglkg Methyl-t-Butyl Ether (MTBE) ND 5.0 ug/kg
Surroqates: REC (%) Control Qual SurroQates: REC (%) Control Qual
Limits Limits
Dibromofluoromethane 96 8Q..120 Toluene-d8 85 81-117
1,4-Bromofluorobenzene 94 74-121
p/m-Xylene
o-Xylene
Methyl-t-Butyl Ether (MTBE)
SurroQates:
180
280
ND
REC (%)
Toluene-d8
102
Parameter
Result
p/m-Xylene
o-Xylene
Methyl-t-Butyl Ether (MTBE)
Surrogates:
ND
ND
ND
REC(%)
Toluene-d8
97
03/04102
Solid
NIA
Result RL DF Qual Units Parameter Result
ND 5.0 ug/kg p/m-Xylene ND
ND 5.0 ug/kg o-Xylene ND
ND 5.0 uglkg Methyl-t-Butyl Ether (MTBE) 6.9
REC (%) Control Qual Surrogates: REC(%)
Limits
97 8Q..120 Toluene-d8 88
94 74-121
RL - Reporting Limit, DF - Dilution Factor, Qual - Qualifiers
I
RL DF Qual Units
10 2 ug/kg
10 2 ug/kg
10 2 ug/kg
Control Qual
Limits
81-117
'. "03/05102. .··.·Ó30502AS
RL DF Qual Units
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
Control Qual
Limits
81-117
03/05/02 030502AS
RL DF Qual Units
5.0 ug/kg
5.0 ug/kg
5.0 ug/kg
Control Qual
Limits
81-117
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
(.= a/science
I:ggnVironmental
'- aboratories, Inc.
I
I WGR Southwest, Inc.
11021 Winners Circle, Suite 101
I Los Alamitos, CA 90720-0000
1 Project: 2601 White Ln, Bakersfield
I
:';:>~ :.<
.... . ,'-' ...-,
:. . ;:.<:>'('!:: «~>~:
" ~ .'- "
r~' '.
ANALYTICAL REPORT
Date Received:
Work Order No:
Preparation:
Method:
03/05/02
02-03-0130
N/A
EPA 8260B
Page 6 of 7
;.::f:~i'-;::::-:·:' ;.
.,..y,....,.....,
Lab Sample
Number
.:)i:Ö2;:03f(),3G,;21.·.
Date
Collected
Matrix
Date Date
Prepared Analyzed QC Batch ID
''';';«>N1Â:j'ò;eio3/Ô5l02 :·5>Ô30Sò2AS '
'i.:.~ :-;-:~~!{}
'03/04102 '.
:1'; '·.:;;$ö'~d;·:
.;:.:>:,:~~;.::)
Benzene
Ethylbenzene
Toluene
I Surrogates:
Result RL DF Qual Units Parameter Result RL DF Qual Units
ND 5.0 ug/kg p/m-Xylene ND 5.0 ug/kg
ND 5.0 ug/kg o-Xylene ND 5.0 ug/kg
NO 5.0 uglkg Methyl-t-Butyl Ether (MTBE) NO 5.0 uglkg
REC (%) Control Qual Surrogates: REC (%) Control Qual
Limits Limits
97 80-120 Toluene-d8 103 81-117
92 74-121
I Parameter
Dibromofluoromethane
1,4-Bromofluorobenzene
I
: '..';~::::'" ::v,:. ~'>"~< '::,~~
...
Parameter
I
"
-{->.-.;.;--, .
. . " .
·Ó2-oj.;o1.30~22>S,)03l04l02,' . '.' 'Solid .,'
//<,,:;
N/A<,:;;C)3/psíoî( : 030502AS
"',
" ".:'y.,:.~
Benzene
Ethylbenzene
Toluene
I Surrogates:
Result RL DF Qual Units Parameter Result RL DF Qual Units
NO 5.0 ug/kg p/m-Xylene ND 5.0 ug/kg
NO 5.0 uglkg o-Xylene ND 5.0 ug/kg
ND 5.0 ug/kg Methyl-t-Butyl Ether (MTBE) ND 5.0 uglkg
REC(%) Control Qual Surrogates: REC{%) Control Qual
Limits Limits
97 80-120 Toluene-d8 85 81-117
89 74-121
Dibromofluoromethane
1 ,4-Bromofluorobenzene
1
Parameter
Result
I Benzene
Ethylbenzene
Toluene
1 Surrogates:
ND
ND
NO
REC (%)
Oibromofluoromethane
1,4-Bromofluorobenzene
98
88
I
D-46'
Parameter
1 Benzene
Ethylbenzene
Toluene
Surroqates:
'I Díbromofluoromethane
1,4-BromofJuorobenzene
Result
ND
ND
NO
REC (%)
97
91
RL - Reporting Limit ,
, 0 03l04/02S¡)Ud:. "NIA _ o;03/oSio2-;030502AS
RL DF Qual Units Parameter Result RL DF Qual Units
5.0 uglkg p/m-Xylene NO 5.0 ug/kg
5.0 ug/kg o-Xylene NO 5.0 ug/kg
5.0 ug/kg Methyl-t-Butyl Ether (MTBE) ND 5.0 ug/kg
Control Qual Surrogates: REC(%) Control Qual
Limits Limits
80-120 Toluene-d8 104 81-117
74-121
,< 02-03,.0130-24 NfA 03f05l02 . 030502AS
RL DF Qual Units Parameter Result RL DF Qual Units
5.0 ug/kg p/m-Xylene ND 5.0 ug/kg
5.0 ug/kg o-Xylene ND 5.0 ug/kg
5.0 ug/kg Methyl-t-Butyl Ether (MTBE) ND 5.0 ug/kg
Control Qual Surrogates: REC (%) Control Qual
Limits Limits
80-120 Toluene-d8 86 81-117
74-121
7440 Lincoln Way. Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501
DF - Dilution Factor ,
Qual - Qualifiers
I
I
. =alscience
I:æn vironmen tal
Laboratories, Inc.
ANALYTICAL REPORT
I WGR Southwest, Inc.
11021 Winners Circle, Suite 101
I Los Alamitos, CA 90720-0000
Date Received:
Work Order. No:
Preparation:
Method:
03/05/02
02-03-0130
N/A
EPA 8260B
I Project: 2601 White Ln, Bakersfield
Page 7 of 7
I Client Sample Number
Method Blank',: '<!'/<
'-'.'<-
.'-,'"","" ,"<.:"/',.:.:-
lab Sample
Number
". ····.+L.)('i)g~~1~Ôf2.~69··..
Date
Collected
Date Date
Matrix Prepared Analyzed QC Batch ID
····,Sòlid·.··;',;;'ÜiJÁ·..····.· ·{>\;C)3I05l02·.,:·'030s02ÄS···
,","
I Parameter Result Rl DF Qual Units Parameter Result RL DF Qual Units
Benzene ND 5.0 ug/kg p/m-Xylene ND 5.0 uglkg
Ethylbenzene ND 5.0 uglkg o-Xylene ND 5.0 ug/kg
I Toluene ND 5.0 uglkg Methyl-t-Butyl Ether (MTBE) ND 5.0 uglkg
Surrogates: REC (%) Control Qual Surrogates: REC(%) Control Qual
Limits Limits
Dibromofluoromethane 90 80-120 Toluene-d8 101 81-117
1,4-Bromofluorobenzene 94 74-121
I . Method Blank ..Solid." MIA? ", .-.03/05102 . .
",.,<. . ..
I Parameter Result Rl DF Qual Units Parameter Result Rl DF Qual Units
Benzene ND 5.0 uglkg p/m-Xylene ND 5.0 uglkg
Ethylbenzene ND 5.0 uglkg o-Xylene ND 5.0 ug/kg
Toluene ND 5.0 uglkg Methyl-t-Butyl Ether (MTBE) ND 5.0 uglkg
I Surrogates: REC (%) Control Qual Surrogates: REC (%) Control Qual
limits limits
Dibromofluoromethane 103 80-120 Toluene-d8 108 81-117
1,4-Bromofluorobenzene 93 74-121
I ,"-;...,' .:', .. '.,',' -. -.' -. ,...,...... ',",.. . .. ··'.Soiid>.· . .. ..
Method Blank·' . ~ '"',"' ; ::.::" ~.':,. ," ';':-'-(:. :"":{::;, " "999~10..o()s..2,680.é ........ .'. MIA , >NJA> ' .~:: , ' 03/07/02 030702AS
:..<:'" f.': :''';:-, ','
Parameter
Result RL DF Qual Units Parameter Result RL DF Qual Units
ND 5.0 uglkg p/m-Xylene ND 5.0 ug/kg
ND 5.0 ug/kg o-Xylene ND 5.0 ug/kg
ND 5.0 uglkg Methyl-t-Butyl Ether (MTBE) ND 5.0 ug/kg
REC (%) Control Qual Surrogates: REC (%) Control Qual
limits limits
109 80-120 T oluene-d8 103 81-117
97 74-121
I Benzene
Ethylbenzene
Toluene
I Surrogates:
Dibromofluoromethane
1,4-Bromofluorobenzene
I
I
I
I
RL - Reporting limit ,
DF - Dilution Factor, Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
I
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. = a/science
I/!; nvironmenta/
I.. aboratories, Inc.
Quality Control - Spike/Spike Duplicate
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Date Received:
Work Order No:
Preparation:
Method:
03/05/02
02-03-0130
EPA 5030B
EPA 8015M
Project: 2601 White Ln, Bakersfield
Quality Control Sample ID
I02~3-o11~¿1""" ""'.i
Date Date MSIMSD Batch
Prepared Analyzed Number
;;NJÀ . '", '/03/0002' v(02~~Ó1~sl
,
Matrix Instrument
':'~Iià"" <GC 5'
Parameter
MS %REC
MSD %REC
%REC CL
RPD
RPD CL
Qualifiers
TPH as Gasoline
87
83
75-125
4
0-29
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
4' =alscience
I:!;§nvironmental
'- aboratories, Inc.
Quality Control - Spike/Spike Duplicate
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Date Received:
Work Order No:
Preparation:
Method:
Project: 2601 White Ln, Bakersfield
03/05/02
02-03-0130
EPA 5030B
EPA 8015M
.... .. ·.···GC5 .... ..... '. '. ···tiJA,·'/,« '.j»3/ô5/02 .... ·;Ò263Ò5Óf~s"
Quality Control Sample ID
.àÂ19.>;q ., ,. i. . .., .
Date
Prepared
Date
Analyzed
Matrix
Instrument
< -:. ','.",/ ,< <:
, .",", {/,,:.,
''-'",', .
/.
'--""';"","'.>'<:> '
····$Olid.··c)......
Parameter
MS %REC
MSD %REC
%REC CL
RPD
RPD CL
TPH as Gasoline
91
75-125
2
93
MSIMSD Batch
Number
Qualifiers
0-29
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
'"-= a/science
I/;~nvironmenta/
Laboratories, Inc.
Quality Control - LCS/LCS Duplicate
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Project: 2601 White Ln, Bakersfield
Date Received:
Work Order No:
Preparation:
Method:
03/05/02
02-03-0130
EPA 50308
EPA 8015M
Quality Control Sample ID
'. o~8~~-ooá~1,å8r/' . "."
Date
Prepared
Date LCS/LCSD Batch
Analyzed Number
. ':03lc)4l02' ....... .....: '02c)3ÎJ401$a'»\}
..
Matrix Instrument
, , ,." ,. . .". ':'., '-. ':~',. -," -. ,",.
,<...·$()lid ...... ..... .·t:;ês·.·· ". .
Parameter
TPH as Gasoline
LCS %REC
97
,'. . ,. ..-'-
. <.N/A··
(¡f·:,..-<····
LCSD %REC
97
%REC CL
79-124
RPD
RPD CL Qualifiers
0-21
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
~=a/science
I::, nvironmental
Laboratories, Inc.
Quality Control - LCS/LCSDuplicate
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Date Received:
Work Order No:
Preparation:
Method:
Project: 2601 White Ln, Bakersfield
03/05/02
02-03-0130
EPA 5030B
EPA 8015M
Quality Control Sample ID
..·098-ó3:-008?ì.ts~á'
:,-:/,-,' ,
.,
r':-:,"·.;", ,
Parameter
TPH as Gasoline
(>;"
~', ,:- ::...::-:
. .' \'~
Matrix
Date Date
Prepared Analyzed
.·.····./NiÁ··...·£¡¿(·étÕ3l~5!Ô2..·
LCS/LCSD Batch
Number
. "v.··· . ,0203ØSô1$å:'",.1h;
RPD CL Qualifiers
0-21
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
Instrument
:'>Š-à!ìd:O}.;U; ,,' '.
·'.'~C5
LCS %REC
97
LCSD %REC
96
%REC CL
79-124
RPD
o
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
~= a/science
=
I!:sn vironmen tal
'- aboratories, Inc.
Quality Control - Spike/Spike Duplicate
'.(,.,
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Date Received:
Work Order No:
Preparation:
Method:
Project: 2601 White Ln, Bakersfield
03/05/02
02-03-0130
Ext. + 011
EPA 8015M
Quality Control Sample ID
Date
Prepared
······':'03íó5102"/
Matrix
Instrument
Parameter
MS %REC
MSD %REC
%REC CL
TPH as Diesel
83
78
49-139
Date
Analyzed
MSIMSD Batch
Number
.-.'- '. ..- ."
',-' '. ....... -',.---'. ."-'-',
> ..Ó3J()6/02··:(·:s02030503~s
RPD
RPD CL
Qualifiers
0-28
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
6
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
~= a/science
I:jlVironmental Quality Control - Laboratory Control Sample
'- aboratories, Inc.
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Project: 2601 White Ln, Bakersfield
Date Received:
Work Order No:
Preparation:
Method:
03/05/02
02-03-0130
Ext. + DII
EPA 8015M
Quality Control Sample ID
Matrix
LCS Batch Number
.. . ," . .
...,_. '.', ," .
.' ()9s.:93.()()2~1.689 .. .....
Parameter
TPH as Diesel
Instrument
Date Analyzed
Lab File ID
.. "024F0201:<
%Rec
77
%Rec CL
65-124
".:-".-:.,...,':
.·iiÔ2~~~5.Öª~>.·.·.;;.·.
. ·····/···03106102>\
.' . ." .
Cone Added
400
Cone Recovered
310
~
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
I
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I
I
I
~= a/science
l:;¿gnVironmenta/
Laboratories, Inc.
Quality Control - Spike/SpikeDuplicate
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Date Received:
Work Order No:
Preparation:
Method:
Project: 2601 White Ln, Bakersfield
03/05/02
02-03-0130
N/A
EPA 8260B
MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers
108 106 72-127 1 0-25
101 100 70-130. 1 0-25
96 95 72-131 1 0-25
105 105 70-130 0 0-25
83 85 69-127 2 0-25
107 105 75-124 2 0-25
104 104 60-137 0 0-25
91 92 70-130 1 0-25
90 93 80-120 4 0-25
Quality Control Sample ID
Date
Prepared
Date
Analyzed
Matrix
Instrument
.' ...... ··..vGCNlŠÔ':···\/;·.NIA../·\······
.. ...-:-::<','>::
···03/c)S/Ò2.
Parameter
Benzene
Carbon Tetrachloride
Chlorobenzene
1,2-Dichlorobenzene
1,1-Dichloroethene
Toluene
Trichloroethene
Vinyl Chloride
Methyl-t-Butyl Ether (MTBE)
MSIMSD Batch
Number
... ,
:~: ::~ ':: /:)~:: <~-,:,~~,i/:~:' :,;:":: /.-. :.:
'0203013001' ....
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
1
I
I·
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I
I
I
L=alscience
I!f;§nvironmental
'- aboratories, Inc.
..
Quality Control - Spike/Spike Duplicðte
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Project: 2601 White Ln, Bakersfield
Date Received:
Work Order No:
Preparation:
Method:
03/05/02
02-03-0130
N/A
EPA 82608
Quality Control Sample ID
Matrix
Parameter
MS %REC
MSD %REC
Benzene
Carbon Tetrachloride
Chlorobenzene
1,2-Dichlorobenzene
1 ,1-Dichloroethene
Toluene
Trichloroethene
Vinyl Chloride
Methyl-t-Butyl Ether (MTBE)
80
83
84
84
81
88
90
80
89
Instrument
Date
Prepared
Date
Analyzed
MSIMSD Batch
Number
'. ...... ",-.,'.
.", .., ,'.-
"GC/MSS
;,.>('., .~ -: /
'. ····ò3Îò5ío2 "<':'0'20'3013015
%REC CL RPD RPD CL Qualifiers
72-127 11 0-25
70-130 . 5 0-25
72-131 3 0-25
70-130 2 0-25
69-127 0 0-25
75-124 14 0-25
60-137 1 0-25
70-130 2 0-25
80-120 1 0-25
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
72
87
87
86
81
77
92
82
89
I
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I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
~ =alscience
Cgnvironmental
I.. aboratories, Inc.
Quality Control - Spike/Spike Duplicate
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Date Received:
Work Order No:
Preparation:
Method:
Project: 2601 White Ln, Bakersfield
03/05/02
02-03-0130
N/A
EPA 8260B
MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers
102 99 72-127 3 0-25
104 103 70-130 ' 2 0-25
100 100 72-131 0 0-25
99 103 70-130 3 0-25
107 107 69-127 0 0-25
102 98 75-124 4 0-25
101 99 60-137 2 0-25
102 103 70-130 1 0-25
107 105 80-120 1 0-25
Quality Control Sample ID
02.-03lo1~0~1' ','>' .'.. '
Date
Prepared
Date
Analyzed
Matrix
Instrument
"/N/A '"
.'...:/',:."
':03/07/02
Parameter
Benzene
Carbon Tetrachloride
Chlorobenzene
1.2-Dichlorobenzene
1 ,1-Dichloroethene
Toluene
Trichloroethene
Vinyl Chloride
Methyl-t-Butyl Ether (MTBE)
MSIMSD Batch
Number
,. . '. '<o:iÖ;~;';)1<:
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
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I
I
I
I
I
I
I
I
I
I
I
I
I
~=alscience
6/;ggnVironmental
Laboratories, Inc.
Quality Control - LCS/LCS Duplicate
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Date Received:
Work Order No:
Preparation:
Method:
Project: 2601 White Ln, Bakersfield
03/05/02
02-03-0130
N/A
EPA 8260B
Quality Control Sample ID
Ó~-10.:oÖs;.2,6'73 ....... ...../....
Date
Prepared
/.:fµþ,;.....
Date
Analyzed
,"i i"03l0$!02····
LCS/LCSD Batch
Number
.. ········..·:Ôªo~iAS.:;;i·fiI:0;8·;::):
Matrix
. . ···<,>::t~~lld >;/M
Instrument
<;CIMSQ
. .";
Parameter LCS %REC LCSD %REC %REC CL RPD
Benzene 104 105 72-127 1
Carbon Tetrachloride 97 99 70-130 1
Chlorobenzene 93 94 72-131 0
1,2-Dichlorobenzene 105 103 70-130 2
1,1-Dichloroethene 83 83 69-127 . 0
Ethanol 97 98 60-140 1
Toluene 105 105 75-124 0
Trichloroethene 103 103 60-137 1
Vinyl Chloride 87 88 79-118 2
Methyl-t-Butyl Ether (MTBE) 87 89 80-120 2
Tert-Butyl Alcohol (TBA) 96 97 60-140 1
Diisopropyl Ether (DIPE) 93 95 60-140 2
Ethyl-t-Butyl Ether (ETBE) 103 106 60-140 3
Tert-Amyl-Methyl Ether (TAME) 111 113 60-140 2
RPD CL
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
0-25
Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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~= a/science
I:: nvironmental
'- aboratories, Inc.
Quality Control - LCS/LCS Duplicate
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos. CA 90720-0000
Date Received:
Work Order No:
Preparation:
Method:
Project: 2601 White Ln, Bakersfield
03/05/02
02-03-0130
N/A
EPA 8260B
Quality Control Sample ID
099-10'()O~2,669""" ,
Date Date
Matrix Instrument Prepared Analyzed
. ....;; / '.:¿<.:;Ø~~jì~·.;Æ.j; "'}W>GBíMs'S"<;Y:/N/þ.>i.:iiid :;;'ij3íifØ/Ò2 . ...... ......
lCS/lCSD Batch
Number
'·Q3ò~~4;~t;¡.;::j . .
Parameter LCS %REC LCSD %REC %REC Cl RPD RPD CL Qualifiers
Benzene 82 72 72-127 14 0-25
Carbon Tetrachloride 95 91 70-130 3 0-25
Chlorobenzene 93 92 72-131 1 0-25
1,2-Dichlorobenzene 101 96 70-130 5 0-25
1,1-Dichloroethene 86 81 69-127. 6 0-25
Ethanol 81 75 60-140 8 0-25
Toluene 93 80 75-124 15 0-25
Trichloroethene 98 100 60-137 2 0-25
Vinyl Chloride 83 80 79-118 4 0-25
Methyt-t-Butyl Ether (MTBE) 85 81 80-120 4 0-25
Tert-Butyl Alcohol (TBA) 80 76 60-140 6 0-25
Diisopropyl Ether (DIPE) 86 80 60-140 8 0-25
Ethyl-t-Butyl Ether (ETBE) 82 76 60-140 7 0-25
Tert-Amyl-Methyl Ether (TAME) 90 80 60-140 12 0-25
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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,,-= a/science
I/:,gg nvironmenta/
Laboratories, Inc.
Quality Control - LCS/LCS Duplicate
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Date Received:
Work Order No:
Preparation:
Method:
Project: 2601 White Ln, Bakersfield
03/05/02
02-03-0130
N/A
EPA 8260B
Quality Control Sample ID
Date
Prepared
'·,;tNlA;t:
" ,
Date
Analyzed
ôiiôl/oi7
"/;.- .
LCSILCSD Batch
Number
·~3~!Ó~.»¡?;/,(fi'; /Y.
Matrix Instrument
$âlidi{!}/ ',GClMSO ,
:099~10,,()OS.2,680 ..'
,"', '. . ;, ...:,;:-;¡;:.:;<'-::':;:'~';.: ::-:
.~ -»> ,':;...., ;:-.,,</<. '/-::::~;~:::~:;i\;::~:<:><-
Parameter LCS %REC LCSD %REC %REC CL RPD RPD CL Qualifiers
Benzene 102 99 72-127 3 0-25
Carbon Tetrachloride 101 102 70-130 0 0-25
Chlorobenzene 100 98 72-131 2 0-25
1,2-Dichlorobenzene 100 100 70-130 0 0-25
1,1-Dichloroethene 104 105 69-127 . 1 0-25
Ethanol 106 103 60-140 3 0-25
Toluene 100 100 75-124 1 0-25
Trichloroethene 100 100 60-137 1 0-25
Vinyl Chloride 101 103 79-118 2 0-25
Methyl-I-Butyl Elher (MTBE) 102 104 80-120 2 0-25
Tert-Butyl Alcohol (TBA) 100 102 60-140 3 0-25
Diisopropyl Ether (DIPE) 110 100 60-140 10 0-25
Ethyl-t-Butyl Ether (ETBE) 101 103 60-140 1 0-25
Tert-Amyl-Melhyl Elher (TAME) 99 100 60-140 0 0-25
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501
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-..-,
¡¡=
..a/science GLOSSARY OF TERMS AND QUALIFIERS
I:;fEnvironmenta/ .
Laboratories, Inc.
Work Order Number: 02-03-0130
Qualifier
Definition
ND
Not detected at indicated reporting limit.
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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CLlENT:JJJ C, R_
I . TEMPERATURE - SAMPLES RECEIVED BY:
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Cooler --L of
SAMPLE RECEIPT FORM
WORK ORDER #: 02.[0 ŒJ· [g[J[1J [g
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DATE:
~
Chilled, cooler with temperature blank provided.
Chilled, cooler without temperature blank.
Chilled and placed in cooler with wet ice.
Ambient and placed in cooler with wet ice.
Ambient temperature.
LABORATORY (Other than Calscience Courier):
o C Temperature blank.
3. 0 C IR thermometer.
Ambient temperature.
CALSCIENCE COURIER:
o C Temperature blank.
Initial:~.
CUSTODY SEAL INTACT:
/..,
Sample(s):
Cooler:
No (Not Intact) :
Not Applicable (N/A):
·Initial:~
SAMPLE CONDITION:
Chain-Of-Custody document( s) received with samples.........................
Sample container label(s) consistent with custody papers.....................
Sample container( s) intact and good condition...... .. .. .. .. .. .. .. .. .. .. .. .. .. ...
Correct containers for analyses requested, . .,. .. . . . . ... .. . . . .. . . .... . . ...... . .. . ..
Proper preservation noted on sample label( s).... .. .... .. ..... .. .... .... .. .. .. ....
VOA vial(s) free of headspace. .......................................................
Tedlar bag(s) free of condensation.. ... ............................. .... .............
Yes
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Initial:
COMMENTS:
~LS"EE"'m~"'L - ._. ,- E!!ftV~rv. L~Ch"" O~st-- RMrd- - - .,.
LABORATORIES, INC. oay
7440 Lincoln Way
Garden Grove, CA 92841-1432
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7440 Lincoln Way
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( -a/science
I:;§nvironmenta/
Laboratories, Inc.
March 14,2002
Dave Williams,
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Subject: Calscience Work Order No.:
Client Reference:
02-03-0487
2601 White Lane, Bakersfield, CA
Dear Client:
Enclosed is an analytical report for the above-referenced project. The samples
included in this report were received 3/12/02 and analyzed in accordance with
the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the
guidelines established in our Quality Assurance Program Manual, applicable standard
operating procedures, and other related documentation. The results in this analytical
report are limited to the samples tested and any reproduction thereof must be made in
its entirety.
If you have any questions regarding this report, please do not hesitate to contact the
undersigned.
Mich21:::::
Quality Assurance Manager
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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~ -a/science
I!!;ggnVironmenta/
Laboratories, Inc.
ANALYTICAL REPORT
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Date Received: .
Work Order No:
Preparation:
Method:
03/12/02
02-03-0487
EPA 5030B
EPA 8015M
Project: 2601 White Lane, Bakersfield, CA
Page 1 of 1
Client Sample Number
Lab Sample Date Date Date
Number Matrix Collected Prepared Analyzed QC Batch ID
'>"{~';1,\?(;1Q,~~~~~i:1,;;j¡::~':';S ;{\;; !)i~li~ . '<::';~Í11(Ô2\!);\J;'\N,JÂ: Ii,:'.', 03112102. i;~';:;~203~ 201~ .
Parameter
Surrogates:
Result RL OF Qual Units
ND 0.50 mg/kg
REC (%) Control Qual
limits
26 21-159
TPH as Gasoline
1,4-Bromofluorobenzene
.3BB.
;;:'~:~;~~j>~~'1'~2;;j\~}
>,X:,,_ ._
~)~:t> ;~_.'-.:~.'
..,s'ónti;:; ';:~~/11~Ò2;;:'..;1;L · .~t}¡1-;
03/12102'oìó31201Sa' '.
Parameter
SurrOQates:
Result RL DF Qual Units
ND 0.50 mglkg
REC(%) Control Qual
limits
87 21-159
TPH as Gasoline
1,4-Bromofluorobenzene
Method Blank
,<¡),Ò9íÌ4032óoS;1;903 ...·.......·..i...~...',;.: ".'. :.....,.. .....
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Parameter
Surrogates:
Result RL DF Qual Units
ND 0.50 mglkg
REC (%) Control Qual
limits
95 21-159
TPH as Gasoline
1,4-Bromofluorobenzene
Rl - Reporting limit. DF - Dilution Factor, Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
Ii -a/science
I::. nvironmenta/
Laboratories, Inc.
ANALYTICAL REPORT
I
I WGR Southwest, Inc.
11021 Winners Circle, Suite 101
I Los Alamitos, CA 90720-0000
Date Received:
Work Order No:
Preparation:
Method:
I Project: 2601 White Lane, Bakersfield, CA
I
03/12/02
02-03-0487
N/A
EPA 8260B
Page 1 of 1
Matrix
Date Date
Prepared Analyzed QC Batch ID
Result RL DF Qual Units Parameter Result RL DF Qual Units
ND 5.0 uglkg p/m-Xylene ND 5.0 uglkg
ND 5.0 uglkg o-Xylene ND 5.0 uglkg
ND 5.0 uglkg Methyl-t-Butyl Ether (MTBE) ND 5.0 uglkg
REC(%) Control Qual Surrogates: REC (%) Control Qual
Limits Limits
102 80-120 Toluene-d8 105 81-117
84 74-121
I Parameter
Benzene
Ethylbenzene
I Toluene
Surrogates:
Dibromofluoromethane
I 1.4-Bromofluorobenzene
Parameter
I Benzene
Ethylbenzene
Toluene
I Surrogates:
Dibromofluoromethane
1,4-Bromofluorobenzene
Result
DF Qual Units Parameter
Result
RL
ND
ND
ND
REC(%)
p/m-Xylene
o-Xylene
Methyl-t-Butyl Ether (MTBE)
Surrogates:
ND
ND
23
REC (%)
5.0
5.0
5.0
Control
Limits
80-120
74-121
;~i';\¡;0:i;lt,~';:I'¡AiI¡';'ó99¿1º~º~~;11i1¡:.¡'/;::i'.;.NÎ$.·.···,
uglkg
uglkg
uglkg
Qual
108
82
Toluene-d8
102
RL DF Qual Units
5.0 ug/kg
5.0 uglkg
5 uglkg
Control Qual
Limits
81-117
'"'"
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Parameter
Result RL DF Qual Units Parameter Result
ND 5.0 uglkg p/m-Xylene ND
ND 5.0 uglkg o-Xylene ND
ND 5.0 uglkg Methyl-t-Butyl Ether (MTBE) ND
REC(%) Control Qual Surrogates: REC(%)
Limits
98 80-120 Toluene-d8 86
81 74-121
I Benzene
Ethylbenzene
Toluene
I SurroQates:
Dibromofluoromethane
1 ,4-Bromofluorobenzene
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RL - Reporting Limit .
DF - Dilution Factor, Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
RL DF Qual Units
5.0 uglkg
5.0 ug/kg
5.0 uglkg
Control Qual
Limits
81-117
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(...= alscience
l1!;¡¡gnvironmental
Laboratories, Inc.
Quality Control - Spike/Spike Duplicate
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Date Received:
Work Order No:
Preparation:
Method:
Project: 2601 White Lane, Bakersfield, CA
03/12/02
02-03-0487
EPA 5030B
EPA 8015M
Quality Control Sample ID
Date
Prepared
Date
Analyzed
Matrix
Instrument
Parameter
MS %REC
MSD %REC
%REC CL
RPD
RPD CL
TPH as Gasoline
75-125
62
68
9
MSIMSD Batch
Number
Qualifiers
0-29
3
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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.. = a/science
I:gn vironmen tal
Laboratories, Inc.
Quality Control - LCS/LCS Duplicate .
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Date Received:
Work Order No:
Preparation:
Method:
03/12/02
02-03-0487
EPA 5030B
EPA 8015M
Project: 2601 White Lane, Bakersfield, CA
Quality Control Sample ID
Parameter
LCSD %REC
93
LCS %REC
92
%REC CL
79-124
RPD
RPD CL Qualifiers
0-21
TPH as Gasoline
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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t... =alscience
C§nVironmental
'- aboratories, Inc.
Quality Control - Spike/SpikeDuplic;ate
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Date Received:
Work Order No:
Preparation:
Method:
Project: 2601 White Lane, Bakersfield, CA
03/12/02
02-03-0487
N/A
EPA 8260B
Quality Control Sample ID
Date
Prepared
Date
Analyzed
Matrix
Instrument
MSIMSD Batch
Number
Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers
Benzene 106 98 72-127 7 0-25
Carbon Tetrachloride 96 99 70-130· 3 0-25
Chlorobenzene 97 94 72-131 3 0-25
1,2-Dichlorobenzene 90 89 70-130 1 0-25
1,1-Dichloroethene 101 102 69-127 1 0-25
Toluene 103 97 75-124 6 0-25
Trichloroethene 94 93 60-137 1 0-25
Vinyl Chloride 100 105 70-130 5 0-25
Methyl-t-Butyl Ether (MTBE) 111 109 80-120 2 0-25
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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S - a/science
I:;Eiff nvironmental
Laboratories, Inc.
Quality Control - LCS/LCSDuplicate
WGR Southwest, Inc.
11021 Winners Circle, Suite 101
Los Alamitos, CA 90720-0000
Date Received:
Work Order No:
Preparation:
Method:
Project: 2601 White Lane, Bakersfield, CA
03/12/02
02-03-0487
N/A
EPA 8260B
Date
Prepared
LCS/LCSD Batch
Number
Parameter LCS %REC LCSD %REC %REC CL RPD RPD CL Qualifiers
Benzene 115 96 72-127 18 0-25
Carbon Tetrachloride 103 101 70-130 3 0-25
Chlorobenzene 103 103 72-131 1 0-25
1,2-Dichlorobenzene 99 99 70-130 0 0-25
1,1-Dichloroethene 107 105 69-127 . 2 0-25
Toluene 115 96 75-124 18 0-25
Trichloroethene 105 90 60-137 16 0-25
Vinyl Chloride 109 106 79-118 3 0-25
Methyl-t-Butyl Ether (MTBE) 103 100 80-120 3 0-25
Tert-Butyl Alcohol (TBA) 109 125 60-140 14 0-25
Diísopropyl Ether (DIPE) 100 103 60-140 2 0-25
Ethyl-t-Butyl Ether (ETBE) 99 96 60-140 4 0-25
Tert-Amyl-Methyl Ether (TAME) 101 92 60-140 9 0-25
Ethanol 103 96 60-140 7 0-25
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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(,,;alscience GLOSSARY OF TERMS AND QUALIFIERS
6::,gggnVironmental
Laboratories, Inc.
Work Order Number: 02-03-0487
Qualifier
Definition
3
Spike or Spike Duplicate compound was ouiof'control due to matrix
interference. The associated LCS and/or LCSD was in control and,
therefore, the sample data was reported without further clarification.
Not detected at indicated reporting limit.
ND
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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WÓRK ORDER #: 02.[QJ [3]. [g[±] ~ŒJ
Cooler -L oft
SAMPLE RECEIPT FORM
LlENT:
WG,(Z
DATE:
3)2/0'2-
, EMPERATURE - SAMPLES RECEIVED BY:
IfALSCIENCE COURIER:
, ____ ChIlled, cooler with temperature blank provided.
I' Chilled, cooler without temperature blank.
1== Chilled and placed in cooler with wet ice.
I Ambient and placed in cooler with wet ice.
'I Ambient temperature. ,
o C Temperature blank.
LABORATORY (Other than Calscience Courier):
o C Temperature blank.
3 0 C IR thermometer.
Ambient temperature.
Initial:
IVL-
---.
USTODY SEAL INTACT: ,
---
No (Not Intact) :
Not Applicable (N/A): ~ _.
Initial: I'vé-
Cooler:
AMPLE CONDITION:
~llain-Of-CustodY document(s), receiV~d with samples.. ........ ............ ...
~ample container label( s) consistent with custody papers.....................
Sample container(s) intact and good condition........................... '" .. ... / . . . . ..
orrect containers for analyses requested......................................... - /....,..
Proper preservation noted on sample label(s).....................................
VOA vial(s) free of headspace. .......................................................
edlar bag(s) free of condensation..... ......... ..,.............. ...... ..............
Yes
/.....
/
No
N/A
--
--
---
/
---
~
Initial:
¡JC
--_. -------
COMMENTS:
-
-
-
-----
CALSCIENCE ENVIRONMENTAL
LABORATORIES. INC.
-----------
EQUIV A Services LLC Chain Of Custody Record
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7440 UncoIn Way l]¡(sci£HCii~:EjijGiN£ERi~
Garden Grove, CA 92841-1432()i¢:íHîéN;s~>
(714) 895-5494 (714) 894-7501 fax I[jCiiMr::~~>.. .'. ,1
11021 Wlnnerl Circle, Suite 101, LOI Alamlto., CA
PAOÆC1 CONT-'C1 _.. _ "- to):
'\)¿t \!'t.. W"\ \ \ ~.> SAMPLER NAME(S) (1'...):
(;-8510 1(;2)199-8566 r:·\l\\~s~r-WA'" ~\Gtv\" J()."
TURNAROUND 11ME (BUSINESS DAYS): J
o 10 DAYS 0 S DAYS 0 72 HOURS ]a{ ~ HOORS [J 24 HOURS [J LESS THAN 24 HOURS
o LA - RWQC8 REPORT FORMAT [J UST AGENCY:
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LOO COQE:
W/:,Jl-A-
WGR Southwelt, Inc.
>COM",
GClMS t.lTBE CONF1f\MÞ.i1ON: HIGHEST
HIGHEST per BORING _ALI._
TEMPERATURE ON RECEIPT CO
SPECIAL INSTRUCTIONS OR NOTES:
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ONLY
SAMPLING MAT~IX
DATE TIME
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