HomeMy WebLinkAboutMITIGATION
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ENVIRONMENTAL MANAGEMENT, INC.
April 25, 2003
KHM Project D81-2600WL
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Mr. Steve Underwood
City of Bakersfield Fire Department
Preventative Services
1715 Chester Avenue, 3 rd Floor
Bakersfield, California 93301
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Re: GRASP Site Assessment Report
Shell Service Station
2600 White Lane
Bakersfield, California
Dear Mr, Underwood:
KHM Environmental Management, Inc. (KHM), on behalf of EqiÜlon Enterprises LLC dba
Shell Oil Products US (SHELL), has prepared this GRASP Site Assessment Report for the above
referenced site (Figure 1). The Groundwater Assessment Program (GRASP) activities
initiated at the above referenced site on January 20, 2003, revealed no detectable
concentrations of petroleum hydrocarbons in the subsurface soil, which are detailed in this
report,
BACKGROUND
GRASP is a voluntary initiative by SHELL to install groundwater monitoring wells at
numerous retail service stations nationwide that do not have any active release cases' but
have been identified to be in close proximity to one or more public water supply wells, The
purpose of this program is to proactively monitor the groundwater beneath these sites and,
in the event of a subsurface release, to respond quickly to protect pùblic wells from this
impact.
GRASP ASSESSMENT
On January 20, 2003, KHM supervised the drilling of one exploratory soil boring (SB-1),
Groundwater was not encountered and drilling was terminated at 111 feet below ground
surface, 'Exploratory boring lithology and field observations are documented in a boring log
presented in Appendix A. The ~aste inventory record sheet is included as Appendix B.
911 S. PRIMROSE AVENUE, SUITE K . MONROVIA; CALIFORNIA . 91016 . PHONE: (626) 256-6662 . FAX: (626) 256-62~3
REDMOND, WASHINGTON .
(425) 558'0134
PORTLAND, OREGON -' CROCKETT, CALIFORNIA
(503) 233·4068 (510) 787·6756
SAN JOSE, CALIFORNIA
(408) 224·4724
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April 25, 2003
Page 2
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ANALYTICAL FINDINGS
Selective soil samples were taken during the drilling ohhis boring and subsequently
analyzed for chemical impacts, The soil analytical results are summarized in Table 1 and
presented in Figure 2, Certified analytical results andëhain-of-custody documentation for
soil are presented in Appendix C.
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If you have any questions regarding this site, please çontact Brad Clark (KHM) at
(626) 256-6662 or Tony Palagyi (SHELL) at (425) 377-8530.
Sincerely,
. KHM ,Environmental Management, Inc.
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Shelby Valenzuela
Staff Geologist·
Bradley E, Clark, P.E.
Senior Project Engineer
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cc: Tony Palagyi, Shell Oil Products US (PDF byemail without appendices)
Isabel Mejia, Shell Oil Products US
\ \Scrver\KI-IM_Data \Clicnis\....Shell\_Shell GRASP\_GRASP Sites\26QQ White Lane\2003-04.25_She-Assessment Report\Site Assessment Report(2600).doc
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ATTACHMENTS:
· Table 1 - Soil Analytical Data
· Figure 1 - Site Location Map
· Figure 2 - Hydrocarbon Distribution in Soil Map
· Appendix A - Boring Log
· Appendix B - Waste Inventory Sheet
· Appendix C - Soil Laboratory Report and Chain-of-Custody Documentation
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TABLE
l_
1-
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Table 1
Soil Analytical
2600 White Lane,
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Data
Bakersfield, California
ND<0.25
ND<O,25
ND<0.25
ND<0.25
ND<0.25
ND<0.25
ND<O.OlO
ND<O.OlO
ND<O,OlO
ND<O,OlO
ND<O,OlO
ND<O.OlO
ND<O.OlO
ND<O,OlO
ND<O.OlO
ND<O,OlO
ND<O,OlO
ND<O.OlO
ND<O.OlO
ND<O~010
ND<O,OlO
ND<O,OlO
ND<O.OlO
ND<O.OlO
ND<O,050
ND<O,050
ND<O,050
ND<0.050
ND<O,050
ND<0.050
ND<O,0050
ND<O,0050
ND<0.0050
ND<O,0050
ND<O,0050
ND<O,0050
ND<O,0050
ND<0.0050
ND<0.0050
ND<O,0050
ND<0.0050
ND<0.0050
ND<O,0050
ND<O,0050
ND<O,0050
ND<0.0050
ND<O,0050
ND<0.0050
ND<0.0050
ND<O,0050
ND<0.0050
ND<0.0050
ND<O,0050
ND<O.0050
ND<0.0050
ND<O,0050
ND<O,0050
ND<O,0050
ND<0.0050
ND<O,0050
ND<O,50
ND<O,50
ND<O,50
ND<O,50
ND<0.50
ND<0.50
25
30
35'
40
45
50
of 1
Page
DIPE - Di-isopropyl ether
ETBE - Ethyl tert-butyl ether
TAME - Tert-amyl methyl ether
TRPH - Total Recoverable Petroleum Hydrocarbons
TPH- g and TPH- d quantified using EPA Method 8015M modified
BTEX Compounds, MTBE, TBA, DIPE, ETBE, and TAME analyzed using EPAMethod 8260B
1 {2600LSoil Anal Data
\\Khmserver\_KHMServer\..OataIClients\....5hell\..Shell GRASP\..GRASP Sitesl2600 White Lane\2003-04-xx_Site Assessment Reportl Table
Notes:
mg/kg - milligrams per kilogram
ND - Not detected, see CARS for method detection limits
NA - Not analyzed
TPH-g - Total Petroleum Hydrocarbons as gasoline
TPH-d - Total Petroleum Hydrocarbons as diesel
MTBE - Methyl tert-butyl ether
TBA - Tert-butvl alcohol
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FIGURES
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119°03'00" W
WGS84 119°00'00" W
119°02'00" W
119°01'00" W
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Printed fmm TOPO! C2001 NðÛDnIIl Geographic HoJdings (www.topo.com)
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SHEll Oil PRODUCTS US
SHEll SERVICE STATION
BAKERSFIELD, CALIFORNIA .
N
FIGURE 1
SITE LOCATION MAP
2600 WHITE LANE
BAKERSFIELD, CALIFORNIA
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N
W<:>E
S
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-
-
-
-
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. SB-
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(TYP)
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LEGEND
EXPLORA TORY
SOIL BORING
LOCA TION AND
DESIGNA TION
TOTAL PETROLEUM
HYDROCARBONS
AS GASOLINE
METHYL
TERT -BUTYL
ETHER
SB-1.
TPH-g
MTBE
TRASH ENCLOSURE
TBA
mg/kg
----wI
NïR0:õ50
ND<0.050
ND<0.050
ND<O,050
ND<0.050
ND<0.050
- t'iA
/22/2003
MTBE
mg/kg
~
mRo.õ05o
ND<0:0050
ND<O,0050
ND<O,0050
ND<0.0050
ND<0.0050
NA
SB-1
Benzene
mg/kg
~
NïRõ:õ05o
ND<O,0050
ND<0.0050
ND<O,0050
ND<0.0050
ND<0.0050
NA
TPH-g
mg/kg
NA
ND<O,50
ND<O,50
ND<O,50
ND<0:50
ND<0.50
ND<O,50
NA
ö
Depth
(feét)
10-20
25
30
35
40
----;rs
50
55-1
Ii;
D
W
'"
U
W
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U
~a
:~
~
D~
TERT -BUTYL
ALCOHOL
TBA
o
MILLIGRAMS PER
KILOGRAM
NOT ÀNAL YZED
NOT DETECTED
"
30
00
mg/kg
NO
NA
CANOPY
(TYP)
SIGN
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DD
[D D DDI
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D D
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SHELL OIL PROOUCTS US
SHELL SERVICE STATION
BAKERSFIELD, CALIFORNIA
SCALE:
FIGURE 2
HYDROCARBON DISTRIBUTION
IN SOIL MAP
2600 WHITE LANE
BAKERSFIELD, C!,-lIFORN\A
PClG
035
MAP,dwg, 5/25/20031:50:49 PM, RlCOH AlIcia
SOIL
\\5erver\khm_data\ClientsLSheIlLShelf GRASPLGRASP Sltes\2600 White Lane\2003·04·x,,-Slte Assessment Report\Figure 2(2GOOLHYDROCARBON DISTRIBUTION IN
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ApPENDIX A
BORING LOG
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PROJECT NO: D81-2600 CLIENT: Shell Oil Products (US) I~ORING NO: SB-l
LOGGED BY Jim Harms LOCATION: 2600 White Lane, Bakersfield PAGE 1 OF 6
KHM DRILLER: BC2 DATE DRIUED: 1/20/2003 LOCATION MAP
DRILLING METHOD: HSAlCME 95 BOREHOLE DIAMETER: 8" OD of auger See Figure 2 (Site Map) for location
SAMPLING METHOD: SS Cal. Mod. BOREHOLE DEPTH: 111 ft of well.
ENVIRONMENTAL CASING TYPE: N/A WELL DIAMETER: N/A
MANAGEMENT SLOT SIZE: N/A WELL DEP1H N/A
INCORPORATED GRAVEL PACK: N/A CASINGSTICKUP: N/A
ELEVATION NORTHING EASTING
Not Available Not Available Not Available
Wen Completion M I:: ,..... -Z-
4.> .... I:: ,8 ç.... 4.> Sample "
Water ... I:: .:a ,..... ~ 0..
::I .... "-
ß '" S '" '" >. ?' LITHOLOGY I DESCRIPTION
~ 4.> b ~ ... -;;;
a b() a t:: 0::: 0.. -£
.5 Level 'õ 0 ð " 0 4.> ;>- -
"t'; ..!<i ,;:E u Q t:: _ c... ;>- ... 'õ
'" 0
'" U 4.> ...0 ". u ß '"
'" U '" ¡¡: 0.."-' Q 4.> ..s
p:¡ p:¡ 0:::
Asphalt Cap & Base
1
2
3
damp 4- SM SAND, silty sand, brown, loose, fine to medium grained,
silt 15%, trace clay, 40% medium sand, 40% fine sand,
5 micaceous 5%.
6
7
8
9
.
10
-
damp O· 11 11 SM SAND, light grey fine to medium sand 60%, silt 40%, soft, .
loose, no dry strength.
12
13
14-
...... -------------------------------
. .
15 ,
,"
dry 0 17 16 SP SAND, tan fine to medium sand 90%, silt 10%, trace
'-'-+ coarse sand, soft, no dry strength.
-
17
18
19
"=-
.
dry 0 26 21 SP SAND, as above.
22
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I.. PROJECT NO: 081-2600
. LOGGED BY: Jim Harms
I KHM ~~~::~ METHO~C2 HSNCME 95
SAMPUNG METHOD: SS Cal. Mod,
ENYIR.ONMENTAL CASING TYPE:' N/A
I MANAGEMENT, SLOT SIZE: N/A
~ INCOR.PORATED GRAVEL PACK N/A
ELEVATION
Not Available
CliENT: Shell Oil Products (US)
LOCATION: 2600 White Lane, Bakersfield
DATE DRILLED: 1/20/2003
. BOREHOLE DIAMETER: . 8" 00 of auger
BORE'HOLE DEPTH: 111 ft
WHL DIAMETER: N/A
. \NEU DEPTH: N/A
CASING STICKUP: N/A
NORTHING EASTING
Not Available Not Available
Well Completion' t>.O ¡:: ""' 'Z' Sample
I!) .... ¡:: 0'- I!) I!)
Water .... ¡:: .:e â '~ ~ ~ ¡::..
..a I!) ~ ....... >-. >-.
t>.O æ '" .... I!) þ '" .... ""; f-
a ,~ Level 'õ ¡:: c:G ¡::.. I!)-~ -£ I!) >
~ ~ 0 ð ¡:: ....s > .... 'õ
u u ::;E u a ¡::.. 0 I!)
~ I!) -6 I!) u .... en
~ U ~ 5: 0.. a I!) ..s
o:¡ o:¡ c:G
23
24
25
damp
o
damp
o
damp
moist
o
moist 0
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19 26
27
28
29
30
26 31
32
33
34
35
21 36
37
38
39
40
17 41
42
43
44
BORING NO: SB-t
PAGE 2 OF 6
LOCATION MAP
See Figure 2 (Site Map) for location
of well.
LITHOLOGY I DESCRIPTION
SP SAND, as above,
SP SAND, tan fine grained sand 90%, silt 10%, soft
no dry strength.
SP SAND, tan fine to medium sand 95%, silt 5%, soft,
no dry strength,
SP SAND, as above,
SM SILT, reddish brown silt 80%, 20% fine sand, very stiff,
trace clay, no dry strength,
I PROJECT NO: D81-2600 CliENT: Shell Oil Products (US) BORING NO: SB-l
LOGGED BY: Jim Harms LOCATION: 2600 White Lane, Bakersfield PAGE 3 OF6
KHM DRIUER: BC2 DATE DRILLED: 1/20/2003 LOCATION MAP
I DRILliNG METHOD: H5NCME 95 BOREHOLE DIAMETER: 8" OD of auger See Figure 2 (Site Map) for location
SAMPliNG METHOD: S5 CaL Mod, BORE'HOLE DEPTH: 111ft of well.
ENVIR.ONMENT AL CASING TYPE: N/A \NELL DIAMETER: N/A
I MANAGEMENT SLOT SIZE: N/A WELL DEPTH N/A
INCORPORATED GRAVEL PACK N/A CASING STICKUP: N/A
ELEVATION NORTHING EASTING
Not Available Not Available Not Available
I Well Completion t>() ¡:: ---- -¡;-- Sample
" 1:: ¡:: o - " "
.... .:a ---- .- - ~ 0...
Water .µ '-
B " '" S '" '" ---- >-. >-. LITHOLOGY I DESCRIPTION
t>() .µ " b ~ .... -;;; ¡-
~ ~ '" ¡:: 0:: 0... -£ "
.~ Level . 'õ >
0 ð " 0 0... > .... 'õ
u u ~ u a ¡:: - 0 "
I '" "'0 '" " ..J:¡ " u .µ Cl)
¡:¡:¡ u ¡:¡:¡ ö: 0... ---- a " ..5
0::
4-5
I damp 0 25 4-6 SM SILT, as above,
4-7
I 4-8
I 4-9
-------------------------------
50 ".,..
I damp 0 23 51 ML SILT, reddish brown silt 60%, 40% fine sand, trace clay,
slight plasticity, very stiff, low dry strength.
52
I 53
54-
-------------------------------
".,..'
dry 0 32 56 SP SAND, reddish brown to light grey medium sand 60%,
coarse sand 20%, fine sand and silt 20%, trace fine gravel,
57 soft, loose, no dry strength.
58
59
60
dry 0.1 32 61 SP SAND, reddish brown fine to medium sand 90%, silt 10%
trace coarse sand, soft, no dry strength,
62
63
64-
65
dry 0 31 66 SP SAND, tan medium sand 60%, 40% fine sand and silt,
soft, no dry strength.
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PROJECf NO: DB1-2600
LOGGED BY: Jim Harms
KHM DRILLER: BC2
I· . DRIUlNG METHOD: HSA/CME 95
SAMPLING METHOD: SS Cal. Mod.
ENVIR.ONMENT AL CASING TYPE: N/A
MANAGEMENT SLOT SIZE: N/A
INCORPORATED GRAVEL PACK: N/A
£lEV A TIO~.,
Not Available
CLIENT: Shell Oil Products (US)
LOCATION: 2600 White Lane, Bakersfield
DATE DRILLED: 1/20/2003
BOREHOLE DIAMITER: B" 00 of auger
BOREHOLE DEPTH 111 ft
WELL DIAMETER: N/A
WELL DEPTH N/A
CASING STICKUP: N/A
NORTHING EASTING
Not Available Not Available
BORING NO: SB-1
PAGE 40F 6
LOCATION MAP
See Figure 2 (Site Map) for location
of well.
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I 0() t:: '-'" Z' Sample
Com letion (1) ... t:: 0 (1) (1)
Water .... t:: .:.a Ê :;::: 1.0 J: 0...
B (1) co ...... t' ~
... (1) co '" ....... -¡¡; E-
O() ~ '" t:: IX: 0... .b ~ -£ (1)
,5 Level 'õ 0 ð- (1) > >
0 .... 'õ
'" u ::E u Q t:: 0... 0 (1)
'" co (1) :::ë (1) u ... rJJ
U c:¡ ¡¡: CJ... ....... Q (1) ..s
IX:
67
68
69
dry
0.2
. 70
25 71
72
73
74
75
17 76
77
78
79
80
24 81
82
83
84
85
25 86
87
88
dry
0.2
dry
0,6
damp
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LITHOLOGY / DESCRIPTION
SP SAND, as above, grey in color.
SP SAND, as above, trace coarse sand,
SP SAND, tan medium sand 80%, 10% silt, 10% coarse sand,'
trace fine gravel, soft, no dry strength,
------------------------------
......
SM SAND, grey fine sand 60%, silt 40%, soft, no dry
strength,
PROJECT NO: D81-2600
. LOGGED BY: Jim Harms
DRILLER: BC2
DRILLING MITHOD: HSAlCME 95
SAMPLING MITHOD: SS Cal. Mod.
ENVIRONMENTAL CASING TYPE N/A
MANAGEMENT SLOT SIZE: N/A
INCOR.PORATED GRAVEL PACK: N/A
ELEVATION
Not Available
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BORING NO: SB-1
PAGE 5 OF 6
CLIENT: Shell Oil Products (US)
LOCATION: 2600 White Lane, Bakersfield
DATE DRILLED: 1/20/2003
BOREHOLE DIAMETER: 8" OD of auger
BORE'HOLE DEPTH: 111 ft
WELL DIAMETER: N/A
WELL DEPTH: N/A
CASING STICKUP: N/A
NORTHING EASTING
Not Avàilable Not Available
e
0{) :: .--. Z' Sample
Com letion <j) .µ :: 0 <j) I!)
.:a -
Water ..... :: â '¡oj ....... ~ c..
=' I!) '" '" >-, ~
~ .µ <j) .þ OJ '-' .... '" ¡.....
0.0 ~ :: c... ~ .p
<= ,5 Level '8 IX <j) >
0 ð I!) 0 > .... -
OJ u ::E u Q :: ¿ c... 0 <j) '8
'" "'. <j) <j) u .µ VJ
U c::¡ P::: c.. Q <j) ..s
IX
89
90
damp 0
damp 0
damp 0
damp 0
23
25
42
35
91
92
93
94-
95
96
97
98
99
100
101
102
103
104-
10?
106
107
108
109
110
LOCATION MAP
See Figure 2 (Site Map) for location
of well.
LITHOLOGY I DESCRIPTION
SM SILT, grey silt 60%, fine sand 40%, tight, medium stiff,
no dry strength, trace clay and very slight
plasticity ,
SM SILT, as above,
SM SILT, grey silt 80%, fine sand 20%, soft, no dry
strength, minor iron staining. .
SM SAND, light brown to grey fine sand 80%, silt 20%, soft,
no dry strength.
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PROJECT NO: 081-2600 CLIENT: Shell Oil Products (US) I BORING NO: SB-l
--" LOGGED BY: Jim Harms LOCATION 2600 White Lane, Bakersfield. PAGE 6 OF 6
KHM DRILLER: BC2 DATE DRILLED: 1/20/2003 LOCATION MAP
DRILLING METHOD: HSAlCME 95 BOREHOLE DIAMETER: 8" 00 of auger See Figure 2 (Site Map) for location
SAMPLING METHOD: SS Cal. Mod, BOREHOLE DEPTH: 111 ft of well.
ENVIRDNMENT AL CASING TYPE: N/A WELL DIAMETER: N/A
I MANAGEMENT SLOT SIZE: N/A WELL DEPTH: N/A
INCOR-PORA TED GRAVEL PACK N/A (ASING STICKUP: N/A
ELEVATION NORTHING EASTING
I Not Available Not Available Not Available
WeB t:>() ~
Completion ¡::: ¡::: ..-... Sample (1)
(1) ..j .:.e o - (1)
Water .... c:: ..-... .- - ~ 0...
..... ""-
- .z (1) os S os '" >-, >-, LITHOLOGY / DESCRIPTION
..... (1) .... '" ¡-
~ t:>() <2 '" c:: c:>:: 0... !:3 ;: ~ (1)
,5 Level 'õ >
~ 0 0... (1) 0 > .... 'õ
I~ '" ¿¡ U 0'-' c:: _ 0... 0 (1)
os '" (1) ..0 " u ..j (/)
U C:Q 5: 0... '-' CI " oS
c:>::
dry 0 36 111 SM SAND, as above.
I -
112
I 113
114
115
116
I 117 .
,
I 118
119
I 120
1 121
,
122
'-
I 123
124
I 125
I 126
127
'I 128
129
I 130
1 131 .
132
1- .
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APPENDIX B
WASTE INVENTORY SHEET
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WASTE INVENTORY RECORD'
Page /, òf I
I/U /0 -:5 .
r. ..
'D%I-~~D
'2-(pCO LV h/1-¿ WUtL: 1x:, ~(" 5/-;'(/4 .
, . ,
Location/SS#
Date Generated
Project No.
.5helJ
Client
ç¡; 0'\1' Har i'Y1 .::>.
Date Removed
FiEild Technician
Well or Depth Type of Waste Dê!te Drum & ID q"t" Comments'
Bo(ing 10 . . (Interval) Waste Volume Generated Stock Pile and (wet,odof,chemical
1 Designation constituents, etc.)
5Þ- J D-Z-t> '5 f); I ,Sqq! . II~D Þæ~ I .5:>,. I C V 1i-11'1 I? 5-
- I
to - LIt> I DI<.-2
l/() -.It- tJ Þ ", -3' I
- Cto...~D . Df(-'1 I
.. Vt-~'7 J
SO - 1'00 ,
St? - , 100 - II 0 D~·Co '5Da -t flIt;. sftc
~- -- ()Ja~· DC-J ~'rð~" ~4~
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Sketch, Locations of Waste
·f
tJ·
\\,\'J' ~ ~~~7
\j\j - , i?
G:-I·~(1
. {V _
~. K.
"
w",
Stock Pile on site
. 8. Volume
T atal Number of
Drumsat.Site
7
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ApPENDIX C '
SOIL LABORATORY REPORT
AND CHAIN'-OF-CUSTODY DOCUMENTATION
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s ' _a/science
- ~nvironmenta/
.. aboratories, Inc.
. January 28, 2003
Brad Clark' ,
KHM Environmental Management
911 South Primrose Avenue, Unit K
Monrovia, CA 91016-0000
Subject: Calscience Work Order No.:
Client Reference:
03-01-1094
2600 White Lane, Bakersfield, CA
Dear Client:
Enclosed is an analytical report for the above-referenced project. The samplès
included in this report were received 1/22/2003 and analyzed in accordance with
the attached chain-of-custody,
Unless otherwise noted, all analytical testing was accomplished in accordance with the
,guidelines established in our Quality Assurance Program Manual, applicable standard
operating procedures, and other related documentation. The original report of any
. subcontracted analysis is provided herein, and follows the standard Calscience data
package. The results in this analytical report are limited to the samples tested and any
reproduction thereof must be made in its entirety.
If you have any questions regarding this report, please do not hesitate to contact
the undersigned.
Michae J Crisostomo
Quality A surance Manager
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
I' iÆ _ alscience ANAL YTICAL REPORT
- §nvironmental
I S aboratories, Inc.
KHM Environmental Management Date Received: 01/22/03
911 South Primrose Avenue, Unit K Work Order No: 03-01-1094
I Monrovia, CA 91016-0000 Preparation: EPA 50308
Method: EPA 8015M
I Project: 2600 White Lane, Bakersfield, CA Page 1 of 2
Lab Sample Date Date Date
I Client Sample Number Number Collected Matrix Prepared Analyzed QC Batch ID
I Parameter Result RL DF Qual Units
TPH as Gasoline ND 0,50 mg/kg
Surrooates: REC (%) Control Qual
I Limits
1,4-Bromofluorobenzene 89 44-122
I Parameter Result RL DF Qual Units
TPH as Gasoline ND 0,50 mglkg
I Surrooates: REC(%) Control Qual
Limits
1.4-Bromofluorqbenzene 87 44-122
I Parameter Result RL DF Qual Units
I TPH as Gasoline ND 0,50 mg/kg
Surrooates: REC(%) Control Qual
Limits
1,4-Bromofluorobenzene 92 44-122
I
Parameter Result RL DF Qual Units
I TPH as Gasoline ND 0,50 mg/kg
Surrooates: REC(%) Control Qual
Limits
I 1,4-Bromofluorobenzene 90 44-122
I Parameter Result RL DF Qual Units
TPH as Gasoline ND 0,50 mg/kg
Surrooates: REC(%) Control Qual
I Limits
1,4-Bromofluorobenzene 90 44-122
I
RL - Reporting Limit OF . Dilution Factor , Qual - Qualifiers
I 7440 Lincoln Way, Garden Grove, CA 92841-1432 . TEL: (714) 895-5494 . FAX: (714) 894-7501
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æ _a/science
- §nvironmenta/
.. aboratories, Inc.
KHM Environmental Management
911 South Primrose Avenue, Unit K
Monrovia, CA 91016-0000
ANALYTICAL REPORT
Date Received:
Work Order No:
Preparation:
Method:
01/22/03
03-01-1094
EPA 5030B
EPA 8015M
Project: 2600 White Lane, Bakersfield, CA
Page2of2
Client Sample Number
Lab Sample
Number
Date
Collected
Matrix
Date Date
Prepared Analyzed QC Batch 10
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Parameter Result RL OF Qual Units
TPH as Gasoline . NO 0,50 mg/kg'
Surrooates: REC(%) Control Qual
Limits
1 ,4-Bromofluorobenzene 87 44-122
Parameter Result RL OF Qual Units
TPH as Gasoline NO 0,50 mg/kg
Surrooates: REC(%) Control Qual
. Limits
1 ,4-Bromofluorobenzene 82 44-122
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RL - Reporting Limit, OF -Dilution Factor. Qual - Qualifiers
7440 Lincoln Way, Garden Grove,CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
I
I !E _a/science ANAL YTICAL REPORT
... nvironmental
I .. aboratories, Inc.
KHM Environmental Management Date Received: 01/22/03
911 South Primrose Avenue, Unit K Work Order No: 03-01-1094
I Monrovia, CA 91016-0000 Preparation: EPA5030B
Method: EPA 8260B
I Project: 2600 White Lane, Bakersfield, CA Page 1 of 3
Lab Sample Date Date
I Client Sample Number Number Collected Matrix Prepared QC Batch 10
I Parameter Result RL OF Qual Units Parameter Result RL OF Qual Units
Benzene NO 0,0050 mg/kg Tert-Butyl Alcohol (TBA) NO 0.050 mg/kg
Ethylbenzene NO 0.0050 mg/kg Oiisopropyl Ether (OIPE) NO 0.010 mglkg
I Toluene NO 0.0050 mg/kg Ethyl-t-Butyl Ether (ETBE) NO 0.010 mg/kg
p/m-Xylene NO 0.0050 mg/kg Tert-Amyl-Methyl Ether (TAME) NO 0.010 mg/kg
o-Xylene NO 0.0050 mg/kg Ethanol NO 0.25 mg/kg
Methyl-t-Butyl Ether (MTBE) NO 0.0050 mg/kg
I Surrooates: REC(%) Control Qual Surrooatés: REC (%) Control Qual
Limits Limits
Oibromofluoromethane 99 79-127 Toluene-d8 97 84-114
1,4-Bromofluorobenzene 89 68-116
I Parameter. Result RL DF Qual Units Parameter Result RL DF Qual Units
I Benzene NO 0.0050 1 mg/kg Tert-Butyl Alcohol (TBA) ND 0.050 mg/kg
.Ethylbenzene NO' 0,0050 1 mg/kg Oiisopropyl Ether (DIPE) ND 0,010 mg/kg
Toluene NO 0.0050 1 mg/kg Ethyl-t-Butyl Ether (ETBE) NO 0.010 mg/kg
p/m-Xylene NO 0,0050 1 mg/kg Tert-Amyl-Methyl Ether (TAME) NO 0.010 mg/kg
I o-Xylene NO 0.0050 1 mg/kg Ethanol ND 0,25 mg/kg
Methyl-t-Butyl Ether (MTBE) NO· 0.0050 1 mg/kg
Surrooates: REC(%) Control Qual Surrooates: REC(%) Control Qual
Limits Limits
I Oibromofluoromethane 101 79-127 Toluene-d8 96 84-114
1 ,4-Bromofluorobenzene 89 68-116
I Parameter Result RL OF Qual Units Parameter Result RL DF Qual Units
Benzene NO 0.0050 mg/kg Tert-Butyl Alcohol (TBA) ND 0.050 mg/kg
I Ethylbenzene NO 0.0050 mg/kg Oiisopropyl Ether (DIPE) NO 0,010 mg/kg
Toluene ND 0.0050 mg/kg Ethyl-t-Butyl Ether (ETBE) NO 0,010 mg/kg
p/m-Xylene NO 0.0050 mg/kg Tert-Amyl-Methyl Ether (TAME) NO 0,010 mg/kg
o-Xylene NO 0,0050 mg/kg Ethanol NO 0,25 mg/kg
Methyl-t-Butyl Ether (MTBE) NO 0.0050 mg/kg
I Surro~ates: REC (%) Control Qual Surrooates: REC(%) Control Qual
Limits Limits
Oibromofluoromethane 104 79-127 Toluene-d8 96 84-114
1,4-Bromofluorobenzene 90 68-116
I
I
RL - Reporting Limit OF - Dilution Factor Qual - Qualifiers
I 7440 Lincoln Way, Garden Grove.CA 92841-1432 . TEL: (714) 895-5494 . FAX: (714) 894-7501
I
I
æ _a/science
- gnvironmenta/
.. aboratories, Inc.
KHM Environmental Management
911 South Primrose Avenue, Unit K
Monrovia, CA 91016-0000
ANALYTICAL REPORT
I
I
Date Received:
Work Order No:
Preparation:
Method:
01/22/03
03-01-1094
EPA 5030B
EPA 8260B
I
Project: 2600 White Lane, Bakersfield, CA
Page 2 of 3
I
Client Sample Number
Lab Sample
Number
Oate
Collected
Matrix
Oate Oate
Prepared Analyzed QC Batch 10
I
Parameter Result RL OF Qual Units Parameter Result RL OF Qual Units
Benzene NO 0.0050 mg/kg Tert-Butyl Alcohol (TBA) NO 0.050 rnglkg
Ethylbenzene NO 0,0050 mg/kg Oiisopropyl Ether (OIPE) NO 0,010 mg/kg
Toluene NO 0.0050 mg/kg Ethyl-t-Butyl Ether (ETBE) NO 0,010 mg/kg
p/m"Xylene NO 0,0050 mg/kg Tert-Amyl-Methyl Ether (TAME) NO 0.010 mg/kg
o-Xylene NO 0,0050 mg/kg Ethanol NO 0.25 mg/kg
Methyl-t-Butyl Ether (MTBE) NO 0.0050 mg/kg
Surroqates: REC(%} Control Qual Surroqates: REC(%} Control Qual
Limits Limits
Oibromofluoromethane 98 79-127 Toluene-d8 . 96 84-114
1,4-Bromofluorobenzene 90 68-116
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Parameter Result RL OF Qual Units Parameter Result RL OF Qual Units
Benzene NO 0.0050 mg/kg Tert-Butyl Alcohol (TBA) NO 0,050 1 mg/kg
Ethylbenzene NO 0,0050 mg/kg Oiisopropyl Ether (OIPE) NO 0.010 1 mg/kg
, Toluene NO 0,0050 mg/kg Ethyl-t-Butyl Ether (ETBE) NO 0.010 1 mglkg
.p/m-Xylene NO 0.0050 mg/kg Tert-Amyl-Methyl Ether (TAME) NO 0,010 1 mg/kg
o-Xylene NO 0.0050 mg/kg Ethanol NO 0,25 1. mg/kg
Methyl-t-Butyl Ether (MTBE) NO 0,0050 mg/kg
Surroqates: REC(%} Control Qual Surroqates: REC(%} Control Qual
Limits , Limits
Oibromofluoromethane 100 79-127 Toluene-d8 96 84-114
1 ,4~Bromofluorobenzene 90 68-116
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Parameter Result RL OF Qual Units Parameter Result RL OF Qual Units
Benzene NO 0.0050 mg/kg Tert-Butyl Alcohol (TBA) NO 0,050 mg/kg
Ethylbenzene NO 0,0050 mg/kg Oiisopropyl Ether (OIPE) NO 0.010 mg/kg
Toluene NO 0.0050 mg/kg Ethyl-t-Butyl Ether (ETBE) NO 0.010 mg/kg
p/m-Xylene NO 0.0050 mg/kg Tert-Amyl-Methyl Ether (TAME) NO 0,010 mg/kg
o-Xylene NO 0,0050 mg/kg Ethanol NO 0.25 mg/kg
Methyl-t-Butyl Ether (MTBE) NO 0.0050 mg/kg
Surroqates: REC(%) Control Qual Surroqates: REC(%) Control Qual
Limits Limits
Oibromofluoromethane 98 79-127 Toluene-d8 97 84-114
1,4-Bromofluorobenzene 89 68-116
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RL - Reporting Limit. DF - Dilution Factor .
Qual - Qualifiers
I
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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f!j _a/science
- j'vironmenta/
&. aboratories, Inc.
KHM Environmental Management
911 South Primrose Avenue, Unit K
Monrovia, CA 91016-0000
ANALYTICAL REPORT
Date Received:
Work Order No:
Preparation:
Method:
01/22/03
03-01-1094
EPA 5030B
EPA 8260B'
Project: 2600 White Lane, Bakersfield, CA
Page 3 of 3
Client Sample Number
Lab Sample
Number
Date
Collected
Matrix
Date Date
Prepared Analyzed QC Batch ID
Parameter Result RL DF Qual Units Parameter Result RL DF. Qual Units
Benzene ND 0.0050 mg/kg Tert-Butyl Alcohol (TBA) ND 0.050 mg/kg
Ethylbenzene ND 0.0050 mg/kg Diisopropyl Ether (DIPE) ND 0,010 mg/kg
Toluene ND 0.0050 mg/kg Ethyl-t-Butyl Ether (ETBE) ND 0,010 mg/kg
p/m-Xylene ND 0,0050 mg/kg Tert-Amyl-Methyl Ether (TAME)' ND 0,010 mg/kg
o-Xylene ND 0,0050 mg/kg Ethanol ND 0.25 mg/kg
Methyl-t-Butyl Ether (MTBE) ND 0,0050 mg/kg
Surrooates: REC(%) Control Qual Surrooates: REC(%) Control Qual
Limits Limits
Dibromofluoromethane .97 79-127 Toluene-d8 96 84-114
1,4-Bromofluorobenzene 90 68-116
RL - Reporting Limit, OF - Dilution Factor, Qual - Qualifiers
7440 Lincoln Way, Garden Grove, CA92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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æ _a/science
- iffnvironmenta/
... aboratories, Inc.
Quality Control - Spike/Spike Duplicate
KHM Environmental Management
911 South Primrose Avenue, Unit K
Monrovia, CA 91016-0000
Date Received:
Work Order No:
Preparation:
. Method:
01/22/03
03-01-1094
EPA 5030B
EPA 8015M
Project: 2600 White Lane, Bakersfield, CA
Quality Control Sample 10
Date
Prepared
Date
Analyzed
MS/MSD Batch
Number
Matrix
Instrument
Parameter
MS %REC
%REC CL
RPD CL
MSD %REC
RPD
Qualifiers
TPH as Gasoline
63-123
11
0-20
99
89
"
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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æ _a/SCience
- ªnvironmenta/
.. aboratories, Inc.
Quality Control - LCS/LCS Duplicate
KHM Environmental Management
911 South Primrose Avenue, Unit K
Monrovia, CA 91016-0000
Date Received:
Work Order No:
Preparation:
Method:
01/22/03
03-01-1094
EPA 5030B
EPA 8015M
Project: 2600 White Lane, Bakersfield, CA
Quality Control Sample ID
Date
Prepared
LCS/LCSD Batch
Number
Matrix
Instrument
Date
Analyzed
Parameter
LCS %REC
110
LCSD %REC
101
RPD
9
RPD CL Qualifiers
0-21
%REC CL
TPH as Gasoline
71-125
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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iË _ a/science
. - gnvironmenta/
£,; aboratories, Inc.
Quality Control - Spike/Spike Duplicate
KHM Environmental Management
911 South Primrose Avenue, Unit K
Monrovia, CA 91016-0000
Date Received:
Work Order No:
Preparation:
Method:
Project: 2600 White Lane, Bakersfield, CA
Instrument
Date
. Prepared
Date
Analyzed
Quality Control Sample ID
Matrix
01/22/03
03-01-1094
EPA 5030B
EPA 8260B
MS/MSD Batch
Number
Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers
Benzene 98 98 72-127 0 0-25
Carbon Tetrachloride 87 87 70-130 0 0-25
Chlorobenzene 102 101 - 72-131 1 0-25
1,2-Dichlorobenzene 100 101 70-130 1 0-25
1,1-Dichloroethene 107 106 69-127 1 0-25
Toluene 97 97 75-124 0 0-25
Trichloroethene 84 83 60-137 1 . 0-25
Vinyl Chloride' 107 112 70-130 4 0-25
Methyl-t-Butyl Ether (MTBE) 91 91 80-120 0 0-25
Tert-Butyl Alcohol (TBA) 80 82 60-140 2 0-25
Diisopropyl Ether (DIPE) 102 101 60-140 1 0-25
Ethyl-t~Butyl Ether (ETBE) 96 96 60-140 0 0-25
Tert-Amyl-Methyl Ether (TAME) 86 87 60-140 1 0-25
Ethanol 97 98 60-140 0 0-25
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714)895-5494 · FAX: (714) 894-7501
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~ a/science
- jlvironmental
... aboratories, Inc.
Quality Control - LCS/LCS Duplicate
KHM Environmental Management
911 South Primrose Avenue, Unit K
Monrovia, CA 91016-0000
Date Received:
Work Order No:
Preparation:
Method:
01/22/03
03-01-1094
EPA 5030B
EPA 8260B
Project: 2600 White Lane, Bakersfield, CA
Quality Control Sample ID
Date
Prepared
LCS/LCSD Batch
Number
Matrix
Instrument
Date
Analyzed
Parameter LCS %REC LCSD %REC %REC CL RPD RPD CL Qualifiers
Benzene 99 100 72-127 1 0-25
Carbon Tetrachloride 88 89 70-130 1 0-25
Chlorobenzene 106 105 72-131 1 0-25
1,2-Dichlorobenzene 104 104 70-'130 1 0-25
1,1-Dichloroethene 109 108 ·69-127 0 0-25
Toluene 99 99 75-124 0 0-25
Trichloroethene 86 86 60-137 0 0-25
Vinyl Chloride 114 113 79-118 1 0-25
Methyl-t-Butyl Ether (MTBE) 93 94 80-120 1 0-25
Tert-Butyl Alcohol (TBA) 84 86 60-140 2 0-25
Diisopropyl Ether (DIPE) 103 104 60-140 1 0-25
Ethyl-t~Butyl Ether (ETBE) 98 99 60-140 1 0-25
Tert-Amyl-Methyl Ether (TAME) 90 90 60-140 1 0-25
. .
Ethanol 99 105 60-140 6 0-25
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501
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1\
~alsèience GLOSSARY OF TERMS AND QUALIFIERS
- gnvironmental
I., aboratories, Inc.
Work Order Number: 03-01-1094
Qualifier
Definition
ND
Not detected at indicated reporting limit.
7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501
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. WORK ORDER #: 03·0 [2] . [Z] lQ] [fJ [iJ
Cooler -L of-l--
SAMPLE RECEIPT FORM
CLIENT:
/(/1»1
DATE:
. ..
TEMPERATURE - SAMPLES RECEIVED BY:
CALSCIENCECOURIER:
Chilled, cooler with temperature blank provided.
. ..9b-il1ed,cOOler without temperature blank.
~Chilled and placed in cooler with wet ice.
Ambient and placed in cooler with wet ice,
'.--;:-;- Ambient temperature.
~ °c Temperature blank,
LABORATORY (Other than Calscience Courier):
°c Temperature blank.
° C IR thermometer.
Ambient temperature.
\
Initial:~
Sample(s): .
Cooler:
No (Not Intact) :
Not Applicable (N/A):
Initial:
CUSTODY SEAL INTACT:
SAMPLE CONDITION: . ~.
Chain-Of-Cust~dy docurnent(s) received with samplesuuu.uu.u....u. ~..... No NJA
Sample container label(s) consistent with custody papers.", '.. ,., ,,' .., ",., --------u /. .,...
Sample conta.iner(s) intacfandgoodcondition.... ,........... ...... ...,;. '" ,...,~:...
Correct containers for analyses requested,.. ,.. .., '" ." ,., ". ." '" .., .,.....,.., ... .~. ,
Proper preservation noted on sample label(s)..........;."..,..,.....; '...,.,.... . ... . . . .
VOA vial(s) free of headspace. '" ,., '" ". .., ,., ". ... .",.; ,,' .,.., ,,' .., ... "... ".
. ..
Tedlarbag(s) free of condensation.., ,'. ... ,,' ... .., ...... ... ... .,. ..".~ ... ... .,....
Initial:
COMMENTS:
..
_.
-
II~ P"-ctJle's dflfn cftus\!Øy Record-
INCIDENT NUMQER (S&EÓNL Y)
~1
lI!ft'e
Manager to be invoiced
-
-'
~\";I~NV-'EN~
, LABORATORIES,INC .
DATE:_1'20/03
_1_ -' I
I CONSULTANT PROJECT NO,
D81-2600 WL
7440 Lincoln Way
Garden Grove, CA 92841-1432
(714) 895·5494 (714) 894-7501 fax
SAMPUNG COMPANY:
KHM Environmental Management
ADDRESS:
911 S. Primrose Ave., Monrovia CA
PROJECT CONTACT (HarticoPY 01' PDF Report to):
Brad Clark
,_ì
PAGE:
;.:~1P;i~~ CRMT 'NUMBER(TS/CRMT)
. 1 3T5rõT6/a
~ding
E-MAIL:
THONE NO.
1626-256-6662
Tony Palagyi
,
SITE ADDRESS (Street and City):
2600 WHite Lane, Bakersfield
EDF OEUVERABL:E TO (Responsib)e Party or Designee):
LAB USE ONLY
0/ -/07;/
bclark@khm1,com
REQUESTED ANALYSIS
,
Brad Clark
Jim Harms
FA>< E-MAIL:
626-256-6662 626-256-6263 bclark@khm1,com
TURNAROUND TIME (BUSINESS DAYS):.
o 10 DAYS 0 5 DAYS 0 72 HOURS 0 48 HOURS 0 24 HOURS 0 lESS TItAN 24 HOURS
o LA - RWQCB REPORT FORMAT DUST AGENCY:
FIELD NOTES
Container/Preservative
or PID Readings
or Laborato.ry Notes
TEMPERATURE ON RECEIPT C'
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CHECK BOX IF EDD IS NOT NEEDED 0
NO. OF
CONT,
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Field Sample Identification
GCIMS MTBE CONFIRMATION: HIGHEST
SPECIAL iNSTRUCTIONS OR NOTES:
Please fax to Brad Clark ASAP
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