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HomeMy WebLinkAboutUNDERGROUND TANK #2-C-08/21/01 BUSlNESS/DEAPRTMENT NAME: ADDRESS: PROJECT DESCRIPTION: PROJECT NUMBER: 14-47 po --'1JCf1:J:) TIME DATE: NAME: CHGD: COMMENTS: (n/;Ù/OI .~ 4!..r íZ<..,'w - $a../.. ~<$ &.ãrre.u ""Þ1rß¡; ···7-r~-DI }__J1 cft~ Q $ K()::: ~ 3?-D [!J , ~/?A(01 ~ . Z i--..r: \).")cv» W ('RwG::K:ß éf c5<;ae cJcJ'SuV'c- (e:t/~ 1/-1-01 MJ;J~/~(;)$Ø)~JJ 16ø é2d ", ' I ' I PROJECT COMPLETION: . DATE: / I I I I I I I I I I I I I - I I I I I . the(,f;grOUR IT Corporation 3452 East Foothill Boulevard, 9th Floor Pasadena, CA 91107-3159 Tel. 626.304.1500 Fax. 626.535.9076 11 Mcmber of' l1Je IT Group April 25, 2001 IT Project No. 822407 Mr. Steve Underwood Bakersfield Fire Department Office of Environmental Services 1715 Chester Avenue Bakersfield, California 93301 Re: UNDERGROUND STORAGE TANK CLOSURE REPORT Fonner Shen-Branded Service Station 101 South Union Avenue at Brundage Lane Bakersfield, California Bakersfield Fire Department Removal Pennit No. BR-0273 Dear Mr. Underwood: On behalf ofEquiva Services LLC (EQUIV A), IT Corporation (IT) has prepared this report summarizing the removal and excavation of underground storage tanks (USTs), product dispensers, product piping, and one hydraulic hoist £Tom the above-referenced site (Figure 1). This work was completed under the direction of Mr. Steve Underwood from the Bakersfield Fire Department Office of Environmental Services (BFD). BACKGROUND Site Description The site is currently vacant and completely fenced; three USTs, four dispensers, one hydraulic hoist, and an associated piping have been removed. The site is located on the southwest comer of the intersection of Union Avenue and Brundage Lane, in Bakersfield, California (Figure 1). Figure 2 illustrates the approximate site layout and location of the soil sampling. Subsurface Lithology The soils encountered during recent site activities consist of sandy silt and clayey silt to an approximate depth of 25 feet bgs. Below the silt layers, the soil consists of poorly sorted sands with varying amounts of silt and fine gravel. Groundwater was not encountered during the excavation activities. I I I I I I I I I I I. 'I I I I I I I I J Page 2 Previous Assessment On July 10, 1998, Cambria Environmental Technology, Inc. (Cambria) observed upgrade activities at the Site, including instal]ation of secondary containment to the existing dispensers and gasoline turbines. Cambria subsequently collected soil samples from beneath all dispensers. Total petroleum hydrocarbons as gasoline (TPH-g) was detected at concentrations ranging from non-detect to 2,600 milligrams per kilogram (mglkg) (D- 4-2, 1998). Dispenser samp]es were collected at 2 feet be]ow the dispensers. Table 1 summarizes analytical results from Cambria's July 1998 assessment. In June and July of 1999, Pacific Environmental Group (PEG/IT) advanced five soil borings to depths ranging from 20 to 40 feet below ground surface (bgs). Soil samples were collected during drilling activities at 5-foot depth interva]s. TPH-g, BTEX, and MtBE compounds were not detected above laboratory detection ]imits. Soil analytical results from the soil borings are summarized in Table 1. The locations of the soil borings are designated on Figures 2 and 3. PERMITTING ACTIVITIES EQUIV A's general contractor, L.c. Services, Inc., obtained Tank Removal Pennit No. BR-0273 from the BFD. The following documents pertaining to the removal of the USTs are included in Attachment 1: . Tank removal pennit · Waste manifests for UST transport FIELD ACTIVITIES USTs, Dispensers, Product Piping, and Hydraulic Hoist Removal and Soil Sampling On January 29, 2001, L.c. Services uncovered three 12,000-gallon, double-walled fiberglass gasoline USTs, the product dispensers, and associated product piping. On February 1, 2001 the empty USTs were rendered inert with carbon dioxide bricks and removed for disposal by Ecology Control Industries (ECI). The three gasoline USTs were located in the northwest comer of the property and appeared to be in good condition at the time of removal with no visible holes or cracks. Inspector Steve Underwood of the BFD observed the removal of the USTs on February 1, 2001. The origina] dimension and outline ofthe UST complex is shown in Figure 2. IT collected soil samples beneath the gasoline USTs, four product dispensers, and product piping as specified by Steve Underwood. IT personnel conducted soil sampling under the oversight of a California Registered Geologist. A total of 42 soil samp]es were colJected for laboratory analysis. All UST, dispenser, and product piping soil samples were collected using an excavator bucket. Twenty soil samples were collected beneath the fonner gasoline USTs on February 1, 2001, at depths of approximately 16 and 24 feet bgs. High VOC concentrations were N:\dara\PROJEC1ì705-equiva\Union-131 \822407\Tank Closure Report - 3-29-01 - 101 Union.doc I I I II I I I I I I II I '. I I I I. I I I Page 3 recorded by the photo-ionization detector (PID) during headspace analysis of the excavated soils. Limited over-excavation in the northwest comer of the UST pit was completed in order to constrain the vertical extent of hydrocarbon impacted soil beneath the tanks. Two confinnation samples (T-lA-24 and T-2A-23) were collected at the floor of the limited over-excavation areas. Ten soil samples were col1ected beneath or in the immediate vicinity of the fonner dispensers at depths of approximately 2, 6, and 10 feet bgs and two soil samples were col1ected from beneath the fonner product piping at approximately 3 feet bgs. On February 15, 2001, five additional soil samples were collected approximately 4 feet bgs beneath the fonner product piping at or in the immediate vicinity of the piping elbow locations, Destruction and removal of the fonner station building, car wash, and associated concrete pad revealed an abandoned hydraulic hoist. On February 15, 2001, the hydraulic hoist was removed. One soil sample (H-I-I0) was col1ected two feet below the footing of the removed hydraulic hoist. One background sample (B-G-4) was collected on February 15, 2001 on the southern property line behind the fonner service station. A summary of soil analytical results is included in Table 1. Soil sampling locations and designations are presented in Figure 2. Over-Excavation Activities On February 15,2001, IT personnel observed over-excavation activities at the northeast comer of the UST pit. Over-excavation was advanced to a total depth of 24 feet bgs, at which time IT Personnel col1ected two confinnation soil samples (T1A-24C and T2A- 24C) [Soil analytical results are summarized in Table 1 and sample locations with analytical results are shown on Figure 4]. Over-excavation of the northern sidewall of the UST pit was advanced approximately five feet to the north (over-excavated area is shown on Figure 4). Confinnation samples were collected upon completion of sidewall over-excavation activities ITom the western and northern sidewalls (SW-W-18 and SW-N-18). Soil analytical results from the sidewall samples are summarized in Table 1 and shown on Figure 4. The extent of over- excavation is illustrated in Figure 4. The soil removed during over-excavation was stockpiled on site pending transport and disposal by Belshire Environmental Services, Inc (BESI). GROUNDWATER INFORMATION Groundwater was not encountered during over-excavation activities. Groundwater in the vicinity ranges ITom approximately 175 to 195 feet bgs (Pers. Comm., Zack Smith; Kern County Water Agency). N:\data\PROJECT\705-equiva\Union-I3I\822407\Tank Closure Report - 3-29-01 - 10] Union.doc I I I I I I I I I I I I I 'I I I I I I Page 4 LABORATORY ANALYSES Soil samples collected during site activities were submitted to Calscience Environmental Laboratories, Inc. (CEL), in Garden Grove, a California state-certified laboratory. Soil samples were analyzed for total petroleum hydrocarbons as gasoline (TPH-g) using EP A Method 8015-Modified; and for benzene, toluene, ethylbenzene, total xylenes (BTEX compounds), and methyl tert-butyl ether (MtBE) using EPA Method 8021. Select soil samples with detectable concentrations of MtBE were confinned for MtBE using EPA Method 8260B. The soil sample co]]ected from beneath the hydraulic hoist was analyzed for total recoverable petroleum hydrocarbons (TRPH), BTEX, and California Code of Regulations Title 22 Metals (CAM Metals). A background soil sample was analyzed for BTEX and total lead. A summary of the soil analytical results is included in Table 1. Certified analytical reports and chain-of-custody documentation are included in Attachment 2. ANALYTICAL RESULTS Former Gasoline Fuel UST Area. Soil samples collected from the floor of the UST excavation ranged in TPH-g concentrations from non-detect to 14,000 mglkg [T-2A~16]. Benzene and MtBE were not detected above laboratory detection limits in any samples collected. Soil analytical results are summarized in Table 1 and are displayed on a hydrocarbon concentration in soil map in Figure 3. Former Gasoline Fuel UST Over-Excavation Area. TPH-g, Benzene, and MtBE were not detected above laboratory detection limits in any samples collected from the over- excavated areas. Soil analytical results are summarized in Table I and are displayed on a hydrocarbon concentration in soil over-excavation map in Figure 4. Former Dispenser Area. Soil samples co]]ected beneath or in the vicinity of the fonner product dispensers ranged in TPH-g concentrations from non-detect to 9,100 mglkg (D-4- 2). MtBE was detected at concentrations ranging from non-detect to 0.87 mglkg (D-I-6). Benzene was not detected above laboratory detection limits in any soil sample (Table 1 and Figure 3). Former Product Piping Area. Soil samples collected beneath or in the vicinity of the fonner product piping location ranged in TPH-g concentrations from non-detect to 1.1 mglkg (P-I-I). Benzene was detected at concentrations ranging from non-detect to 0.OÌ3 mglkg (P-I-I). MtBE was detected at concentrations ranging from non-detect to 1.2 mglkg (P-1-1) [Table 1 and Figure 3]. Fonner product piping locations are illustrated in Figures 2 and 3. Former Hydraulic Hoist Area. TRPH, benzene, and MtBE were not detected above laboratory detection limits (Table I and Figure 3). All Title 22 Metals (CAM Metals) did not exceed ten times the Soluble Threshold Limit Concentrations (STLC). N:\data\PROJEClì705-equiva\Union-131 \822407\Tank Closure Report - 3-29-01 - 101 Union.doc I I I I I I I I I I I I I I I I I I I Page 5 Background Sample. The background soil sample contained 0.27 mg/kg of lead (Table 1). UST RINSATE, UST DESTRUCTION AND HYDROCARBON-IMPACTED SOIL On March 1, 2001, the UST rinsate was transported to DeMenno Kerdoon of Compton, California, as flammable liquid waste. The manifest is included in Attachment 1. Approximately 600 cubic yards of pea gravel was generated during excavation of the USTs on January 29,2001. The pea gravel was stockpiled on-site. The gasoline USTs were removed from the site on February 1, 2001, transported to ECI, in Fontana, California, for decontamination, and then transported to Mid Valley Landfill for disposal. The waste manifest for tank transportation is included in Attachment 1. Approximately 475 cubic yards of hydrocarbon impacted soil was stockpiled on-site pending transport and disposal by BESI. CONCLUSIONS AND RECOMMENDATIONS The USTs, dispensers, and associated product piping were properly removed and disposed as documented in this report. Based on the results of sampling activities, IT concludes the following: · Hydrocarbon-impacted soil was not observed beneath Dispenser Island D2. · Hydrocarbon-impacted soil observed beneath the USTs and dispenser islands D1, D2, and D4 were removed during over-excavation activities. · It is IT's professional opinion that hydrocarbon-impacted soil has been adequately removed from the site. IT recommends that Site Closure be granted to the Fonner Shell Service Station located at 101 South Union A venue, Bakersfield, California. N:\data\PROJECT\705-equiva\Union-131 \822407\Tank Closure Report - 3-29-01 - 101 Union.doc I I I I I I I I I I I I I I I I I I I Page 6 This work was perfonned in accordance with generally accepted environmental consulting practices and principles. If you have any questions about this report or the infonnation presented herein, please call either Patrick McCullough [IT Project Manager] at 626-304-1520 or Edward Paden [EQUIV A Project Manager] at 310-816-2075. Sincerely, c?~~y-- IT Corporation Patrick McCullough, R.E.A., R.G. No. 7021 Project Manager Attachments: Table 1 -Soil Analytical Results Figure 1 - Site Location Map Figure 2 - Site Plan Figure 3 ....:. Hydrocarbon Concentrations in Soil Map Figure 4 - Over-Excavation and Hydrocarbon Concentrations in Soil Map Attachment 1 - UST removal pennit and UST and Rinsate Transport and Removal Manifests Attachment 2 - Certified Analytical Reports and Chain-of-Custody Documentation cc: Mr. Edward Paden - Equiva Services LLC Mr. Justin Hawkins - IT Corporation Mr. Larry Turner - Equiva Services LLC (2 copies) P+ "'žSOS; 4S ~ 07z.t, N:\data\PROJEClì705-equiva\Union-131 \822407\Tank Closure Report - 3-29-01 - 101 Union.doc I I I I I "I I I I I I I , I I I I I I I I I I I I I I ~ OJ r m (f) 905-9-91 I I I I I I I I I I I I I I I I I I I TABLE ., - - - - - - - .. - - - - - - - - - - Table 1 Soil Analytical Results Summary Former Shell-Branded Service Station WIC No. 204-4262-2100 101 South Union Avenue Bakersfield, California 8-1-5 06/15/99 5 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-1-10 06/15/99 10 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-1-15 06/15/99 15 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-1-20 06/15/99 20 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-1-25 06/15/99 25 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-2-5 06/15/99 5 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-2-10 06/15/99 10 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-2-15 06/15/99 15 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-2-20 06/15/99 20 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-3-5 07/22/99 5 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-3-10 07/22/99 10 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-3-15 07/22/99 15 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-3-20 07/22/99 20 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-3-25 07/22/99 25 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-4- 5 07/22/99 5 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-4-10 07/22/99 10 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-4-15 07/22/99 15 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-4-20 07/22/99 20 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-4-25 07/22/99 25 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-4-30 07/22/99 30 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-4-35 07/22/99 35 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-4-40 07/22/99 40 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-5-5 07/22/99 5 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8- 5-10 07/22/99 10 ND«O.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-5-15 07/22/99 15 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-5-20 07/22/99 20 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 8-5-25 07/22/99 25 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) n:/data/projectldrawings/705-equiva/I31/822407131 Table I so¡l.xls lof4 3/29/0 I ~ - - - - - - - - - - - - - - - - - - Table 1 Soil Analytical Results Summary Former Shell-Branded Service Station WIC No. 204-4262-2100 101 South Union Avenue Bakersfield, California P-2-1 02/0 I/O 1 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) P-3-4 02/15/01 4 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) P-4-4 02/15/0 I 4 ND«O.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) P-5-4 02/15/01 4 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) 0.13/0.081 * P-6-4 02/15/0 I 4 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) P-7-4 02/15/0 I 4 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) 07/10/98 2 ND«20) NA ND«O.I) ND«O.I) ND«O.I) ND«O.I) 30 / 19* D-2-2 07/10/98 2 ND«I.O) NA ND«0.005) ND«0.005) ND«0.005) ND«0.005) 0.21 D-4-2 07/10/98 2 2,600 NA ND«I.2) 2.3 L3 70 ND«6.2) D-5-2 07/10/98 2 58 NA ND«0.05) ND«0.05) ND«0.05) 1.4 3.2 D-I-2 02/0 I/O I 2 ND«O.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) D-I-6 02/0 I/O I 6 0.87 NA ND«0.005) 0.014 ND«0.005) 0.062 0.087/0.094* D-l-1O 02/0 I/O 1 10 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) D-2-2 02/0 I/O I 2 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) D-2-6 02/0 I/O I 6 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) D-4- 2 02/0 I/O I 2 9,100 NA ND«2.5)** ND«2.5)** ND«2.5)** 1 10 ND«13)** D-4-6 02/0 I/O 1 6 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) D-4-10 02/01/01 10 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) n:/datalprojectldrawingsI70S-equivaJI31/822407131 Tablel soil.xls 2of4 3/29/0\ ~ - - - - - - - - - - - - - - - - - - Table 1 Soil Analytical Results Summary Former Shell-Branded Service Station WIC No. 204-4262-2100 101 South Union Avenue Bakersfield, California D-5-2 D-5-6 UST Sam les T-IA-16 02/01/0 I 16 1,500 NA ND«0.63)** 13 18 180 ND«3.1)** T-IA-20 02/01/01 20 4,900 NA ND«2.5)** 65 74 680 ND«13)** T-IA-24 02/01/01 24 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) T-IB-16 02/01/01 16 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) T-IB-20 02/01/0 I 20 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OJO) ND«0.025) T-IC-16 02/01/0 I 16 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) T-IC-20 02/01/0 I 20 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) T-2A-16 02/01/01 16 14,000 NA ND«5.0)** II 43 1,200 ND«25)** T-2A-20 02/01/0 I 20 10 NA ND«0.005) ND«0.005) ND«0.005) 0.023 ND«0.025) T-2A-23 02/01/0 I 23 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) T-2B-16 02/01/01 16 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) T-2B-20 02/01/0 I 20 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«0.010) ND«0.025) T-2C-16 02/01/01 16 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) T-2C-20 02/01/01 20 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«0.010) ND«0.025) T-3A-16 02/01/01 16 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) T-3A-20 02/01/01 20 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OJO) ND«0.025) T-3B-16 02/01/01 16 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) T-3B-20 02/01/01 20 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) T-3C-16 02/01/0 I 16 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) T-3C-20 02/01/0 I 20 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) n:/data/projectldrawings/705-equiva/I3 1/822407131 Table 1 sniLxls 30f4 3/29/01 I - I - - - - - - - - - - - - - - - - - - Table 1 Soil Analytical Results Summary Former Shell-Branded Service Station WIC No. 204-4262-2100 101 South Union Avenue Bakersfield, California Over-Excavation Sam les T-IA-24C 02/15/01 24 T-2A-24C 02/15/01 24 SW-W-18 SW-N-18 02/15/01 02/15/01 18 18 ND«O.S) NA ND«O.OOS) ND«O.OOS) ND«O.OOS) ND«O.OIO) ND«0.02S) ND«O.S) NA ND«O.OOS) ND«O.OOS) ND«O.OOS) ND«O.OIO) ND«0.02S) ND«O.S) NA ND«O.OOS) ND«O.OOS) ND«O.OOS) ND«O.OIO) ND«0.02S) Sidewall Sample ND«O.S) NA ND«O.OOS) ND«O.OOS) ND«O.OOS) ND«O.OIO) ND«0.02S) Sidewall Sample NA NA ND«O.OOS) ND«O.OOS) ND«O.OOS) ND«O.OIO) ND«0.02S) Total lead: 0.27 mg/kg B-G-4 02/15/01 4 Notes: mg/kg = Milligrams per kilogram ND = Not detected NA = Not analyzed ** = MDL is elevated due to matrix interferences and di1ution factors. TRPH = Total recoverable petroleum hydrocarbons TPH-g = Total petroleum hydrocarbons as gasoline MtBE = Methyl tert- butyl ether * = Confinned by EPA Method 8260 n:/datalprojectldrawings/705-equivalJ 3 J /822407 J 3 J Table J soil.xls 40f4 3/29/0\ I I ; I ! I I ! I I I I I I I I I : I I ' I I I I I I ïl G) C ::u I m ! en 905-9-91 I I I I I I I I I I I I I I I I !I I . I FIGURES ,...... ~ 0 V N -r N IX) ~~ ()W WID ë3~ ~::::> o..z >- ID CI W > 0 ~ a.. a.. < I I I I I I I >- ID CI W :II:: () w I () I I I >- ID Z ~ 0:: CI I I I I I I I I I ..,~ '"A_' ß<'W ~ -:~ REFERENCE: DelORME 3-D TopoQuads CALIFORNIA SOUTH, COPYRIGHT 1999. o 1/2 1 Mile . I 0 2000 Feet I I SCALE rn IT CORPORATION EQUIVA SERVICES llC SHEll SERVICE STATION BAKERSFIELD, CALIFORNIA FIGURE 1 SITE LOCATION MAP 101 SOUTH UNION AVENUE BAKERSFIELD, CALIFORNIA / N:\CAD\DWG\8224D7\PA4D7SLM.dwg Tue. 13/Feb/D1 1D:13am kkistinger LEGEND, I SOIL BORING LOCATION AND DESIGNATION ¡ 1998 DISPENSER SOIL SAMPLE LOCATION AND DESIGNA,rION '¡ SOIL SAMPLE LOCATION AND DESIGNATION i I GASOLrnEUNDERGROUNDSTORAGETANK PIPING ¡ i DISPENS-fR / HYDRAULIC HOIST r EQUIVA SERVICES LLC SHELL SERVICE STATION BAKERSFIELD, CALIFORNIA m IT CORPORATION FIGURE 2 SITE PLAN , ¡ B-1. D-l . AÖ T P ,D H APPROXIMATE SCALE ~ ::J Z ~ >- < Z o - z :;;;;¡ ... v < -'" .-..; c:: ~ ~. < ::¿ 1 :;::: ~ o VJ v ~ V c:: ~ õ: < I I I I \ \ a 400 GAL L PROPANE BRUNDAGE LANE ----\ - --- B-4 --- - -.., DISPENSER D-l ~ ISlAND -f~ - -. -- -- 0 -. B-5 UNDERGROUND STORAGE TANKS 1 /----- ( Ö 1'1 n \ 'A - -B - -C) ~------- ( Ö 1'2 Ö a) ~ ~ ::. ::.Ir ::. ::... c.. (ana aj 'A - - B - - C I ~ ;z. .....; ;;.- f- a:: u.: ~ ~ v c:: ~ I I , I , ----------------------- BG-4 f- o ....J '- Z < v <' >- I I I I I I I I I I I I I I , I I I I I , I I I I I , I I r -I-·-~- o '<t N 1 ~ ..- I I ~ I-æ I ~~ o:::i: æ::> a.Z >- ID QL ~I 9t, I I ,I I I ,I I I I HIGH\VAY 58 I Q .... ~ ) 101 SOUTH UNION AVENUE BAKERSFIELD, CALIFORNIA 60 FEET 30 o ~ > N ~ :; t!:! !?i ¡;; '" 'äi -5i ob o !:> II) C) z ~ II: ~ U w ..., o II: ~ 3 .. Y Ž I I I I I BRUNDAGE +'1-- @ 16': ND/ND/ND @ 20': ND/ND/ND' LEGEND. 1 B-1-+- SOIL BORING LOCATION AND DESIGNATION 'I D-l. 1998 DISJ¡>ENSER SOIL SAMPLE LOCATION AND DESIGNÄTION A Ö SOIL SAi1PLE LOCATION AND DESIGNATION ¡ T GASOLINE UNDERGROUND STORAGE TANK " P PIPING ¡ i D DISPENSER 'I, H HYDRAULIC HOIST I ND/ND/ND TPH-g/BI¡NZENE/MtBE CONCENTRATION IN SOIL (mg/kg), AT DEPTH INDICATED, 2/01/01 AND 2/15/01 * CONFIJED BY EP A METHOD 8260 ~ ND NOT DET¡ECTED I NA NOT ANALYZED ! I I ¡ ! : ¡ I II ¡ ¡ I i' , @ ND/ND/ND ~ :;:¡ Z ~ > < 2: o - z :;:¡ D-4 @ 2': 9,100/ND/ND @ 6'; ND/ND/ND @ 10'; ND/ND/ND (0.094)* 3(0.081 )* ': 1.1/0.013/1.2 (1.3)* D-5 @2': 4.9/ND/0.047 (0.060)* @ 6': NDfNDfND ,~ .< ~ , I , -I , D-2 @ 2'; ND/NDfND @ 6'; ND/ND/ND , 1_.__,_- 40() GAL PROPANE BG-4 @ 4'; ND/ND/ND HIGH\VAY 58 I - , TI-B RGI OLJNl @ 16'; ND/NDfND ORA ìE @20'; ND/NDfND "ANK. I' I 1,500/ND/ND ~' 'to 4,900/ND/ND ,.- _ _ _ T2-1 NDfNDfND " : ~ j @IND/NDfND ~ = Ii = ~ @ 2' ND/ND/ND I ¡ J 2rr-- tW- !-c I > ::.B_ ::. -=..c../ @ 16'; ND/ND/ND ~73 ~ @20';ND/ND/ND -r 'A - B --C ""- /~ · C I _ T3-B 6'; ND/ND/ND @ 16': D/ND 0'; ND/NDfND f- @20'; D/ND ~ S : :J H-l-lO , . 3 I ~ STATION,' '. w ~ " 0- BUILDING > ~ D ,0- , , , , , , I , , , I , ,- BG-4 T1-A @16' @20' @24' T2-A @16' @20' @23' T3-A @ 16': ND/NDfND @ 20'; ND/ND/ND EQUIVA SERVICES LLC SHELL SERVICE STATION BAKERSFIELD, CALIFORNIA rn IT CORPORATION FIGURE 3 HYDROCARBON CONCENTRATION IN SOIL MAP 101 SOUTH UNION AVENUE BAKERSFIELD, CALIFORNIA APPROXIMATE SCALE - ~ I - 0 30 60 FEET - .. · · .. · · · · · "< , .. · , " · , · · LEGEND I D-4 Ö SOIL SAMjLE LOCATION AND DESIGNATION ND/ND/ND TPH-g/BENZENE/MtBE CONCENTRATION IN SOIL (mg/kg), AT DEPTH!INDICATED, 2/15/01 I * CONFIRMED BY EP A METHOD 8260 , , ND NOT DETECTED I ' I ( I I i ! , , I i J , I I' I , @ ¡,...; ~, .... Z ¡,...; > < Z ,-. ~ - Z -; ...; D-4-10 @ 10'; NDINDIND LANE I I I I -------------------------------~ ..... < o c:: ~ -< ;~ ~ '-' c:: ~ < I , I 1 , I I \ a 4UO GAL L PROPANE DISPENSER [SLAND DISPENSER ISLANDS BRUNDAGE -- --' r I I I I UNDERGROUND STOR:\GE ,}:'.~N KS SW-N-18 @ 18'; ND/NDIND T2A-24C " @ 24'; NDIND/ND I, OVER-EXCA VAT[ON PIT ~ Iw F- ;z: C· ~ ...J f-J :- I (- ~ ;¡ ~ I' ~ > ~ ~ - I , I I , , I I , I , I ,- SW-W-18 @ 18'; NDINDIND -I .-r--- - 0 '<t C\I C\I ~ T"" M T"" I U") o r-- 1-0:: ÜW Wee o:::i: o:::J CLZ >- ee a ~ ~í ~I ¡ I I I I II I I I I I I I , i ¡ I I HIGH\VA Y 58 I ì;! .... ~ '" EQUIVA SERVICES LLC SHELL SERVICE STATION BAKERSFIELD, CALIFORNIA rn IT CORPORATION I I, i I I ! I I FIGURE 4 OVER-EXCAVATION HYDROCARBON IN SOIL MAP 101 SOUTH UNION AVENUE BAKERSFIELD, CALIFORNIA APPROXIMATE SCALE - ~ I - 0 30 60 FEET I ï ¡ 'C g! N !1c ::; I!! !1i M "" 'äj -5i J, o !:> (f) C) z ~ a: ~ u w -, o a: 9- '" i;j ~ :ž I ,I, I I I, I I I I I I I I I I I I I I I I I I II ATTACHMENT 1 UST REMOVAL PERMIT AND UST AND RINSA TE TRANSPORT AND REMOVAL MANIFESTS 1:13/1:11.lLtJl'J1, }":1:1'::1 ~.-,.. . .___ ..~.~. 44....1,35 I_ ~. .,~- -.-. ----- ~_:': '''.''}. ~'.J It) LC SERVICES --- - ""'1."0 ."'8 _ ~ -.- ~ a,<z MAT-DIY PAGE 82 , '. w.U 32' ùl1' ; I .. .. U'I' 'HZ IIA1 Wi ' ! ~ .., 1_.- ~_U_-------;k~\fd~~",,¿;ëJ------ ¡?.n 1QJ()02 (\(61, .......1 oIe..'..ð-:'j){ ~ I \11/ /, ".,o,¡.. "CITY OF BAKERSFIELD i i 7 J. nÞ I ;;?tQ4 (f,/ ; .......¡, OFfICE OF ENVIRONMENTAL SE VICES I ~ ,Y ,,:' lil5 Che$ler Ave., Bak£uñeld. CA (80~ ,~26-39'i9 ~ë.Ø ! oÞ- P£RMrr APPUCAilON FOR ! i S\)"'I pd'tð\L I RtMO\' AI., OF ~ UNDERGROUND 5TO I: GE TANK I I grf. ~~11i - I ~IT£ . .r ~~a0._AODP.ESSjQ\ ;-, ~,~Z!l' ODEo. 'Á.CI1..JTf NA.ME __' ~ __ ('(.lOSS S'tUEi ,f1."~ ~ .. AN" OWNER!OPE-.1..fô~~1'- ~~ _- PHONË'NO' ¡:L "t"1JL' c(¡> 15'1. - I MAl UNG ~DD~ESS)(Q &--.... _ u1 '< "\ 2 " _ - . crr'l . : ZIP 'î"'\ ¡t( 11.3'1 '2.::::, 91~i1'R;\Ç,,!~''''' RMA~ .. I , COMPANY ~- '';; _Pft'OJ'ENO~ .W-n3..9 LlCfi>/s£i¥o·JJ"'~2 I ,',DtJRi.SS _ _ ?_..-~~ . -:- .. CITY ~ . ZIP .!5J.z..1. INSIJAAWCE CA¡¡¡UE1\ ~ F rid ~. :::. woJt1{ME.~S COM!' NO, I :. II I LlCENS' "o.110<;~ 2- __ l-nP~ ___ F:.a~oY~ I TA~K L l ."\,, : ,L COMPAIoOY _ _ ' - 11) 1"\ '-' I ADDREsS ..~ \J(,. --.:._ . ..c~o_ Z1P_ ,-('(fit WASTE TRANSPOB.tø.1DF.NTtF1CATlON ~1JV:aEn. C ~ ~ , \ "'''ME- Of 1\).II.s~ TE D~I, p....ClLlTY Î!2i"'~,':"" - ADDRESS ~<\ ~a.'\l. Y::J,;.\ \ C1íY I F.4C1LJTY 1D¡;;NTJ~ëAl1QN NlJMBEl' ~. Q , ~ 'Î \JJ\9 Y Z. '-\i'¡ 1\~\ ~ \ S 3 '1 ~NIi r....N$fQIITU 1"fOl\l!I" 't'O)!i ,n ¡ \ I COMPANY o¡;~ \ ~ P!1ONE NC1.>.\() 2.#>J.. ?_L:- t.1C\, ¡¡ NO, 1<\ \ 10 1L- ADOR~SS ~ =?" <;~ .~':..Fí~ . ~r \00' I.' ~ "!'ANK Des1'rN~:nON _ ;- L\ ,..-A I I I I I I APN --- zi~ ~ ~-------_. :rANK II'IFO!!l MÀ T\9fo! T"NK NO. ACe. VOLUME ~ \ . _ ~_ JQ.ro.D- -~ '$ ~ ---- JQ.~':>')\ ') _ _ __- Jg¡~O~ .___-- - ~ - ~.--" __ __ I . ~ . ... ,.~.. ... ~ .'. . l'ørOnicill. U . OA . ' , LAP pUCi<TØÍi< !:4.f..'~.[;: ; iiI;, '~¡¡),:;;F&i';;~~i~J~;'~'!#f6il ~"J,:~·,.;;:;';'¡i'~'X4~ ¡ Till'. M'I'I.1CJ\)'fr liAS 1U'£F.lVE11, !JND~r ANtIS. AND WQ:.I. cOll4l'l ,Y wrm TIlE ^ Tf AC I If'\) COl'-'nl1lO\Il5 Of 11 I/~ I'I:HMrr N.m ^~V nn \I~tt 5TA'\1.;."tX;M. AW rr;m~{t,AL l~OULA.l10NS- . , I CrŒM1CAL STOR£D ()(L~G"' ~ ------- -i:i!:. "'-. :1 , Vi t..::: oM - ¥,i.I']¿"" . _ _r~- DA. ns STœED "? - ~ I I CHEMICAL p ~VlOUSI.. '{ stOF£D n II> ,.',,.. IIA.' ",,, '" ('<,MPl. "m' UN""" pENAJ.:rt OF PE>UUR Y. ~ TO l' IE Dmör ( .< I>IY "",)\\II.l'JX¡~ IS 'rR\I\~ ^N"~' ".,,1' I ." ! 1 ...,.. . ,. '1'. ---. ..WPUtA¡.J'('. ..ìNATUJil,(~ M[ .........'....... ...................,...... .....·......'''''C.IIU. I ......c....."'III"'\!dt::'.'..., Form Approved OMB No. 2050-0039 (Expires 9-30·99) ~I print,.;"'type. Form designed For use on elite t 12-pitch} typewriter. See Instructions on bock of poge 6. UNIFORM HAZARDOUS WASTE MANIFEST 1. Generotor's US EPA ID No. Manifest Document No. 2. Page 1 Department of Toxic Substances Control Sacramento, California Information in the shaded areas is not required by Federal law. 3. Generator's Nome and Moiling Address 4. Generator's Phone ( EQUIlON PIPElINE COMPANY CADE DAVIS, ~!SP 1389K-l P.O. BOX 261tJ S. Transporter 1 Company Nome ECOLOGY CONTRa... INDUSTRIES C Slate T rein.porter'. ID. ~: :.:¿~;";':'J)': {~<;: ;~:~~_-:,)';::' - . ~:"¡'\~-',;}, ~:.;J!~~:~.7,¡,{;:~f.h~~;!:..ð·;': ..~;·~~~~1~a;::~Är.:'M!~.;:';· ..... .F:)~~,Q-~~mir),.~~.~~~_;;i;:. . G._ St~te. Facility'. I~. 7. Transporter 2 Company Name 9. Designated Facility Name and Site Address ECOLOGY CONTROl INDUSTRIES 255 PARR BLVD. 11. a. NON-RCRA HAZARDOUS WASTE SŒ.ID EMPTY lJND£RGROlIID STORAGE T ANI( (S) ¡. ¢ R 'I ~I ? R b. c. d. Facility: SERVICE STATION 101 S. UNION/BRUNDAGE BAKERSFIELD, CA 93307 16. GENERATOR'S CERTIFICATION: I hereby declare that the content. of this consignment ore fully and accurately described above by proper .hiPfing nome and ore classified, pocked, marked, and labeled, and are in all re.pect. in proper condition far transport by highway according to applicable international and nationa government regulation.. 24 HOUR E:MERGЫ;Y PHONE NUMBER (BOO) 424-9300 NOTE: ADD PROFILE .. OR DElETE THIS LINE. If I om 0 large quantity generator, I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and that I hove selected the practicable method 01 treatment, stor e, or di.posal currently available to me which minimize. the present and future threat to human health and the environment; OR, if I om 0 small quantity generator, I have mode 0 ad faith effort to minimize my waste generation and select the best waste management method that is available to me and that I con afford. ON BEHALF OF EOOIlON PIPE 19. Discrepancy Indication Space C I I y 20. Facili Owner or 0 eratar Certification of recei t of hazardous materials covered b this manifest exce t as noted in Item 19. Printed/Typed Nome Signature I CHD000274 DO NOT WRITE BELOW THIS LINE. 'TSC 8022A (4/971 PA 10-22 :.'ihô:-:::' T: TSDF .3Et· D5 ~~::s '~~:=-'?'( ~O Dr~C ','/'~,--!!"'J -30 DAYS, p,'."J 3::,. 3:~~Ú_ :),-jc:;"',~!~;r::' C¡.. :;)2~2 ate ot \..QII'arnla-cnvHanmemUI rfU1t::\.I1UI1 ,...~t::II\.r orm A proved OMB No. 2050-0039 (Expire, 9-30'99) eo rint or type. Form de,igned lor u,e on elite (12'pilch) typewriter. 1. Generator', US EPA ID No. See Instructions on bock of poge 6. UNIFORM HAZARDOUS WASTE MANIFEST Manifest Document Na. 2. Page 1 Deportment of Toxic Sub,tonce, Control Sacramento, California Information in the shaded areaS i, not required by Federal low. 3. Generator's Nome and Moiling Address 5. Transporter 1 Company Name EQUILON PIPELINE COMPANY CADE DAVIS 1 TSP 1389K 1 P.O. BOX 2048 2-2648 6. US EPA ID Number A. Generator's P},one ( ECCLOGY CONTROL INDUSTRIES 7. Transporter 2 Company Name 9. De,ignoted Facility Nome and Site Address ECOLOGY CONTROL INDUSTRIES 255 PARR BLVD. 11. NON-RCRA HAZARDOUS WASTE SŒ..ID EMPTY lJNDERGROlJND STmAGE TANK (S) o. I E i b. c. d. J ) J , , 5 ; J <: ... { , 2 { 7 24 HOtR EMERGENCY PHONE N..JMÐER (BOO) 424-9300 NOTE: ADD PROFILE II OR DELETE THIS LINE. Facility: SERVICE STATION 101 S. UNION/BRUNDAGE BAKERSFIELD, CA 9-s507 GENERATOR'S CERTIFICATION: I hereby declare thot the contents of thi, con,ignment ore fully and accurately described above by proper ,hiPfing name and are classilied, packed, marked. and labeled, and ore in all respects in proper condition for transport by highway according to applicable international and nationa government regulations. If I am a large quan,tity generator. I certify that 1 have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable Cnd that I have ,elected the practicable method of treatment, ,tar e, or di'pa,al currently available to me which minimize, the pre,ent and future threat to human health and the environment; OR, if I am a small quantity generator, I have mode 0 od faith effort to minimize my waste generation and select the best waste management method that is available to me and that I can afford. T j :> ~ E t of Material, JJ n c{ J Z 19. Di,crepancy Indication Space c . 20. Facili Owner or 0 era lor Certification 01 recei t of hazardou, material, covered b thi, manife,t exce t a, noted in Item 19. Printed/Typed Name Signature y CHD000271 DO NOT WRITE BelOW THIS LINE. DTI8022A (4/97) EP 700-22 'N~;te :0 iSDF 'Sêr-¡DS TH!S CO~,( :0 ,....-::'- .,'i'';'·-ili'; '3G D,<\'(S ?C £.0.< 3'.: :'c. S')·:r'C012C,;O· .. -\ .; 53 ~;' .......,e¡...., ......."......",'"' ......................,....., ..........11...." ,....t1I"'....., Fo......:.t"Prov~B No. 2050-0039 IExpires 9·30-99) lose print or tyPUe'NFloFrOm RdeM'ignHedAIZorAu'ReDoOn eulj'se (J 2-pi/ch) typewriter. 1. Generotor's US EPA ID No. WASTE MANIFEST See Instructions on back of page 6. Manifest Document No. 2. Page 1 Department of Toxic Substances Control Sacramento, California InFormation in the shaded areas is not required by Federal law. I 3. Generator's Nome and Moiling Address 1 EQUILON PIPELINE COMPANY CADE DAVIS, _!SP 13891(-1 P.O. BOX 2b1tS I-O.JSTOH TX 77252-2648 6. US EPA ID Number of 1 :f?¡~?Zr1~;~~E;~~ 4. Generator, Phone I 7131241-8673 5. Transporter 1 Company Name ECOLOGY CONTROL INDUSTRIES 7. Transporter 2 Company Nome 9. De'ignated Facility Name and Site Address ECOLOGY CONTROL INDUSTRIES 255 PARR BLVD. 24 HOUR EMERGENCY PHONE N.JMBER (BOO) 424-9300 NOTE: ADD PROFILE It OR DELETE THIS LINE. Facility: SERVICE STATION 101 S. UNION/BRUNDAGE BAKERSFIELD, CA 93307 16. GENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately de,cribed above by proper shipring name and are classified, packed, marked, and labeled, and are in all respects in proper condition far transport by highway according to applicable international and natiana government regulation,. If I om a large quantity generator, I certify that I have 0 program in place to reduce the volume and toxicity of waste generated to the degree 1 have determined to be economically practicable and that I have selected the practicable method of treatment, stora e, or disposal currently available to me which minimizes the present and future threat to human health and the environment; OR, iF I om 0 .small quantity generator, I hove mode 0 9 ad foith effort to minimize my waste generation and select the best waste manogement method thot is available to me and that I can afford. ON BEHALF OF EQUILON PIPE \ 19. Discrepancy Indication Space t of hazardous moteriols covered b this maniFest exce t os noted in Item 19. Signature CHD000272 DO NOT WRITE BELOW THIS LINE. Ic 8022A (4/97) 8700-22 White: To: TSDF SENDS ïHIS COP! ïO [::S,: "fi"~h:~, P.O. Bc.< 300(;, Sc:rarn·~nt,:> C/:.. )52: 2 DA.YS I· 's",~ Qr Ca ¡IoI'f\I~n~i;"'"m~o1;'~~¡~ "';.ncy .' 'r' ' . f.orm AtW.-' OI-ðß I';: Q. ¡O~O,.{Hj39 {1:1!irc, ~'30'~9') . . Plea.. PM' or t,pe, Fot'rr> d~~HI f.;>r Ii.. "" .11,. (/2·p I I I ~ .., /'0.. I ~ Q 0:) ("f")':' I;§ C) . i~ a>5 I~ ~ I G N E o N ~ E ~ R "'1 A 8 T <;0 0 ..:. R I~ w f- Z w I~ ·.:-·2· I~ z o I~ .: 15 -I' "'" .: ~ z UJ I; 11.1 I~ u ~ I I I ~ . I' See In'structions on bac;'r~ . pas_ 6. ',;·tâ:rrfr.¡ D..portm.n, W T c.ode Sub.Ia.,."; 'Colt~ &cera...n,o. California Inlctn\Gllan in tho .hQ40cl OI_ ,. lIot teqvi~ by F_"" 10.... ~rl,.,. L 'Gen.....ror·. US EP.... Ii:> No. Manile,l D"'IJ"'.~' No. 2. Pc. ¡ , UNIFORM HAZARDOUS . WASTE MANIFEST 2 0 of 1 'þ,. 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II' em 0 lore. quonlily \Je"..ro'ar, , certify '~ol "avo a prag,om in >Iøn to '"vel th. -.0/.",. ond tc~;..:1y of ......'" ge~&I'Q,"d 1'0 '¡'o desru ~eve delerr:lil1rd ro b. .conami.colly prccricoble ond '''cot I ~o.. ..10ClN ,h. p.cot/cob¡" ",.,hod 01 "'.elm.,,', ".r09", 01' di>¡><>.ol C1""""tly ""ailabl. '<> m. ..."¡do mln'm;_ Iht }lr...,., ono luMO ""'"'10 hUl\' cn hotalth ' øn<i III. ......;r..,,"'"",; ~. ill om a >man <¡""nlily ¡¡enera"'" I have meel. a 9..0<:1 fei'" .fIa" tc ""ll\i""I' my ""tWI!! g.n.rá~on ond ..1..tll~" be"",O'~ lI1enDQ1I.....nl metf1a¿ thaI ,i!I" " c.,a; oblc tc m. and .no. çan afford. '. '. .:~'-... T ~ A . I , a R f I . Pri,,""¡/Typ"'¡ Nome L ~CtJi4 i'~ 'D \1 . J . PI 1"'. i 17. T'eo, crt., 1 Ac~nQ'oooIecl ."'.n' of R6C'; ! 01 MoOlttlol. 'rinledk;yp,ed No,,!.' · {J.:¿' '"I LHJP-, 18. Tron. Mer 2 Þ.clnO"lI.d 0101."101 Rlcei 'of MCI.fIQil prin,.~I1,ptd ~mt , (;tJ£lj.J.4.~ æ. 9E.1-W..F OF f.QtfILOtf OfT w '; . , ·.t"·I('~ .. I . ... F " C I l I T y '9. elecfopO",,", ndica~on Spa.,. " , ..:....'i.!,. :~. ;-" '.~.,'~, ·~ï. I'ftD~jf.1t eJtc. t as AOMd ¡" (f.1n 19. ~o. Focili Ownor., Prillro. JT~~ No,';'. .\ ''''~~~~''.' " c. ~ . (' . .:... .:._,.... ,-,' '''--, v....··..· \ t:-;:~(~, 1'...j I¡;;h:~f fN : f;J.:~;¡, )'~¡~l.r) DO NOT WRITE BELOW THIS LIN~. ':':~'.. . "~;r~~ G",,, TRANSPORT¡;~ ~~"INS 7 . r! ,.....~~. Q ¡ Ii' 0 ~,i c~¡w:~n~NI ln~!Nn' l~~nln'J 1A1,.I ~ I . I I r.1ì 7 . (\ I . n;:u I I I I I I I II I I I I I I I I I II I I I ATTACHMENT 2 CERTIFIED ANALYTICAL REPORTS AND CHAIN-OF- CUSTODY DOCUMENTATION I' II 'I I I I I I I I I I II II I I I I E _a/science - j'vironmental Laboratories, Inc. February 05, 2001 Pat McCullough IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Subject: Calscience Work Order No.: Client Reference: 01-02-0075 101 South Union Avenue, Bakersfield, CA Dear Client: Enclosed is an analytical report for the above-referenced project. The samples included in this report were received 2/2/01 and analyzed in accordance with the attached chain of custody The results in this analytical report are limited to the samples tested and any reproduction of this report must be made in its entirety. If you have any questions regarding this report, require sampling supplies or field services, or information on our analytical services, please feel free to call me at (714) 895-5494. 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501 I I æ _a/science - ¡virOnmental .. aboratories, Inc. ANALYTICAL REPORT I IT Corporation 113452 East Foothill Blvd., 9th Floor "asadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0075 EPA 5030B EPA 8015M/8021B JrOject: 101 South Union Avenue, Bakersfield, CA Page 1 of 1 Client Sample Number: Lab Sample Date Date Date Number: Collected: Matrix: Prepared: Analyzed: QC Batch ID: ::ri1.H:::·,::::::,:::,:',::::,,:·:,:::,:::'::::::::·,::::::'::::::::::::::':::':'::::::::::::::::::::::':::.:::·,::::::::::·.::·:g1W~3iRi~f:~::::·::::::·::::::::,·::::·:9&~1/~':,::::::·:::::"~·Þ!¡~::::·:::'::::::::::::::·~(~:::::::,:::::::,::::::::::~gr9~~~~:::::::::'::::P:1~~P3Y1¡!:::::::::::::::::::::'::':: larameter Result RL DF Oual Units Parameter Result RL DF Qual Units Benzene 0.013 0.005 mglkg Xylenes (total) 0.043 0.010 mglkg J oluene 0.073 0.005 mglkg Methyl-tert-Butyl Ether 1.2 0.025 mglkg IthYlbenzene 0.0087 0.0050 mglkg TPH for Gasoline 1.1 0.5 mglkg Surroç¡ates: REC (%) Control Limits Qual Surroç¡ates: REC (%) Control Limits Qual ,4-Bromonuorobenzene 85 47-137 1,4-Bromonuorobenzene - FID 78 34-141 ...:.:.:.:.:.:.;.:.:.;.:.:.:.:.:..... .............................,.,............................................... ...................................... ......... ................. ..............:.:.:.:-:.:.:.:-:.;.:.;.;.:.;.:.;.;.:.;.:.>:.:.:.:.:.;.:.:-:.:............ ......... ... '.... ,." ..................................... ::~f**':~:::t::::::::::::::!:::'::::::::::':::::::::!::t:::::::::::::::::::!::::::!,::::::::::::::::::::::}:::::::::::::::::::~,:w~m~f!f~:::::::j'}::::!:::::-::R#/Mm,j::jL::::~Mft::~::::::::::::::::mA::{{i{{::::~w~#r~1.t:??:R1Y~9~P1~!:::::!:::::::::::::::::::: lara meter Result Rl OF Qual Units Parameter Result Rl OF Qual Units Benzene NO 0.0050 mglkg Xylenes (total) ND 0.010 mglkg 10luene NO 0.0050 mglkg Methyl-tert-Butyl Ether NO 0.025 mglkg thylbenzene ND 0.0050 mglkg TPH for Gasoline ND 0.50 mglkg Surroç¡ates: REC (%) Control limits Qual Surroç¡ates: REC (%) Control limits Qual 1,4-BrOmonuorobenzene 83 47-137 1,4-Bromonuorobenzene - FID 76 34-141 :jM~~:~ffl;~::¡:::::·::::::¡:::::!::::':::::::::¡:":::':::!:::::::!::::::::::::::::,:::::::::::::::¡::::,:'::::::::::::::::'.·:M~~'·W9~i~~~~î:::'::::::::::::':"::"~t#:::::':::::':::::::::::::~~I'~::!::::':::::::':::::::::::::l##:::::'!:'::::::::::!:::~~!:9tt~~::::::::!:::::::i,~~i~~1i~::!::::::::::::::::::::::::: arameter Result RL DF Qual Units Parameter Result RL OF Qual Units lenzene ND 0.0050 mg/kg Xylenes (total) NO 0.010 mglkg oluene ND 0.0050 mg/kg Methyl-tert-Butyl Ether ND 0.025 mglkg thylbenzene NO 0.0050 mglkg TPH for Gasoline NO 0.50 mglkg REC (%) Control Limits Qual Surroç¡ates: REC (%) Control Limits Qual 97 47-137 1,4-Bromonuorobenzene - FIO 89 34-141 I I Rl - Reporting Limit. DF - Oilution Factor. Qual - Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-750.1 Date Spiked Sample ID Matrix Instrument Prepared Date Analyzed MS/MSD Batch Number I I I I I I I I I I I I I I I I I I I Ë _a/SCienCe - pvironmental Laboratories, Inc. Quality Control - Spike/Spike Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0075 EPA 5030B EPA 8015M/8021B Project: 101 South Union Avenue. Bakersfield, CA Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers Benzene 93 93 46-136 1 0-15 Toluene 91 89 45-138 2 0-18 Ethylbenzene 92 90 62-121 2 0-17 p/m-Xylene 92 90 53-130 3 0-17 o-Xylene 94 91 64-120 3 0-13 Methyl-tert-ButyI Ether 97 92 24-144 5 0-23 TPH for Gasoline 97 96 44-122 0 0-30 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 I I I I I I I I I I I I I I I I I æ =alSCienCe - nvironmental Laboratories, Inc. Quality Control - LCS/LCS Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 101 South Union Avenue, Bakersfield, CA 02/02/01 01-02-0075 EPA 5030B EPA 8015M/8021B Project: Date Date LCSILCSD Batch LCS Sample Number Matrix Instrument Prepared Analyzed Number ::9~ª1i1~Yii~~~tt::i:::::::::i:::·::i:::~·!::!::t::!:::::!::::::::·::::::::!::::::::·:§~¡~~f:::·:::.:::::f::~:;:!i::::::::~ç¡~!~:::I::¡::¡:::i¡:::::::::::::i:Ñ!~::::::i::::¡::':::i::::::yir9gffi,:i¡:::::¡¡::!::::::::::::::i:::·::¡:::~19~9.~y.'~ii¡i::¡¡::¡i:¡¡¡¡:¡:::!:::¡!::¡:i:¡·::¡:::¡:::¡::¡ Parameter LCS %REC LCSD %REC %REC CL RPD RPD CL Qualifiers Benzene 99 99 81-111 0 0-17 Toluene 96 96 81-111 0 0-16 Ethylbenzene 98 97 78-113 0 0-17 p/m-Xylene 98 98 70-118 0 0-18 o-Xylene 99 98 77-114 0 0-17 MethyJ-tert-ButyJ Ether 105 103 65-126 1 0-27 TPH for Gasoline 109 110 57-132 1 0-13 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 Qualifier Definition I I I I I II I I I I I ! I I I I, I -II I I ~alSCience GLOSSARY OF TERMS AND QUALIFIERS ... nvironmental Laboratories, Inc. Work Order Number: 01-02-0075 NO Not detected at indicated reporting limit. 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 I I I I I I I I I I I I I I I I I I I I SAMPLE RECEIPT FORM Work Order Number: Delivery Container Type: Client Project 10: 01-02·0075 Cooler 101 South Union Avenue, Bakersfield, CA Date Received: Date Opened: Opened By: 02/02/01 02/02101 JP Section A: Pass/Fail Criteria Comments 1. Chain of custody document(s) received with samples. 2. Sample container label(s) consistent with custody papers. 3, Sample container label(s) complete (10, date, time, taken by). 4, Sample container(s) intact and in good condition. 5. If applicable, proper preservation noted on sample label(s), 6. Sufficient sample volume received for analyses requested. 7, Correct containers used for analyses requested, 8. If applicable, VOA vials free of headspace. Yes Yes Yes Yes NA Yes Yes NA Section B: Additional Observations 1. Describe packing materials used in container. 2. Was sample container('s) sealed with custody seals? 3. Were all samples sealed in separate plastic bags? 4, Measured temperature inside delivery container when opened. 5. If delivery container shipped by third-party carrier, did container come with shipping slip, airbill, etc.? If YES, attach copy of shipping slipJairbill to the back of this form. 6, Do tedlar bags show condensation? Describe below if yes. 7. Are 25.1 condensate traps immersed in dry ice? 8. Are 25.1 sampling trains intact? 9, Are 25.3 condensate vials still attached to the sampling train? 10. Are 25.3 condensate vials on wet ice? NA No No 5.0 No °C NA NA NA NA NA Section C: Additional Comments 02/02/01 10:03:15 Generated in LlMS DATE:_~~~c?/ PAGE: I of I ~;;ni~¢ pt¡~~ø~é.Ê~¡(~$ê1~W~¡ .........................r:o:cc Tech Services ~~llin~'¡~r:r~i~:~4 Equiva Project Manager to be Invoiced: Georgina E.Davlla-DIMarco 7440 Lincoln Way ~t1$~@~~~~~~~~~i~~1 Tech Selllfces Garden Grove. CA 92841-1432 :0T.~~¥iq~:~~~\1ÇRš:~·:: I ¡:C:r··..··..··········..··..·······:·;':·;·:·;·:· (714) 895-5494 . CRMf·ffOUSf.ON·.·...·...·.·.· (714) 894-7501 fax . .' d. ...... ................ Equiva Environmental Engineer. Ed Paden CCNSU. TANT couPA"": sire ADDRess '5....' Ind Clty : T CONmAFiO~Ty;227 lI.tellii~_1 101 South UnIon Ave. @ Brundage, Bakersfield CA PROÆCT CONTACT !R..... 10): ~...... T. .ce......... - SAIIPlER NANEIS) PItrf : ~(( ke4-~-e I IT Corporation 3452 E. Foothill Blvd. Pasadena, CA ADDIIESS: fe_II.: (626) 535-9076 eifi: ~6) 304-1500 .I FAX: WRNAROUNO tiME (BUSINESS DAYS): o 10 DAYS 0 5 DAYS 0 72 HOURS 0 FIELD NOTES: Contaln8rIPr8s8rvatlv8 or prD Readings or laboratory Notes oS- TIm.: <::)~ ;;;;;;: REQUESTED ANALYSIS \ - I CD ... õi to o i' Õ .2 t; II ~ Oal.: 2\ z,lo ¡;¡¡;: ;;- ... '" õ ~ I- ! .. II .. .. o 't! II .. ü: .. o "- II > E UI - ... ... ~ I- ! J: II. ~ .. o "- II > iñ Ó t=. t; :; :; I&. .. (J o > .. o "- II > iñ Ó t=. w CD I- ::E >( W I- m .. (J o > .. o "- II > .. .; ~ J: II. ~ ~ 'ü II Go ~ .. j; II ::E âj on - co ~ ¡; c .. Ii II ::E i c .. fi w âj .. N co ~ u '"' .. E o ~ :<; S .. C II '" o õi :r II (J o > --s- o Z II .. II .! '" .. . .. c ¡; ~ > Ë .2 .. c "" 0 c ... o u (J .. iiì t :; W N on . ... - co W on CD 4( I- II. ~. w 'f- 'f m co UI N ~ .. S .. C II '" "" .. o . t: :J '; I&. II (J o > âj co ... N ~ - Ë .; Eon" ~ Õ _ i c .., ED ðI ., _ _ :::ÞIII - N" II .! '" 0 _ J:I ~ + i J! w w g, :.: e e ~ t 2 ::E Q. W - _ " >( w '"" m ~by: (SIgna...) , . (\ - --- Rec.IYId by: o lESS THAN 24 HOURS HIGHEST per BORING _ ALL-1 1EMPERAWRE ON RECEIPTcoL - SAMPLING ..ATllDe NO. 01' DATE TIME CONT. ~ - 172£ ( - (2./, 172t; \ ntü.~! 48 HOURS 0 24 HOURS o LA . RWQC8 REPORT FORMAT 0 usr AGENCY: GC/MS M1BE CONFIRMATION: HIGHEST _ SPECIAL INSTRUCTIONS OR NOTES: Field Sample Identification ~ P-"L - 1 ¡i¡iii!i¡:! ~.. :::::;:::: R b (SIgna...) RoInq\jsIIId by: SIgnaue) :~\õV\ 0\ J TIm'O"" ~~ 10123100 R_'.. - - - - - - - - - - (SIgnaue Rocllvld by: (SIgna...~ / './1.1.vv.-- - - - ::::- ~r-.~ ') OISiIIir: \\1iI1''''''IInaIIlØ0'll'1 Fill, V_PItt to. _ (Slgnallr.' ..... ~ II I I I I I I I I I II I I I I I I I -- &. a/science .. nvironmental Laboratories, Inc. February 06, 2001 Pat McCullough IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Subject: Calscience Work Order No.: 01-02-0073 Client Reference: 101 South Union Avenue, Bakersfield, CA Dear Client: Enclosed is an analytical report for the above-referenced project. The samples included in this report were received 2/2/01 and analyzed in accordance with the attached chain of custody The results in this analytical report are limited to the samples tested and any reproduction of this report must be made in its entirety. If you have any questions regarding this report, require sampling supplies or field services, or information on our analytical services, please feel free to call me at (714) 895-5494. 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 I I =~= iË a/science I/:, nvironmental Laboratories, Inc. ANALYTICAL REPORT I IT Corporation 1452 East Foothill Blvd., 9th Floor asadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0073 EPA 5030B EPA 8015M/8021B Iroject: 101 South Union Avenue, Bakersfield, CA Page 1 of 12 Client Sample Number: Lab Sample Number: Date Collected: Matrix: Date Prepared: Date Analyzed: QC Batch ID: :::P~'1:~~:::::::'!:::!:::::::!::!:':::!::¡:::':::!:::::::::::::,:¡::':::::::::::¡::::::!::::;¡::::;'!:::::¡::::':::,'::::::::::::,::::,,::::::!::::::::::':!.p'1æ~;I~81:::!':::·:::::::::::¡::::':::.¡·9.YP1{~'::::::,:::::·:':::::~é¡¡i':::::':'::::::::::'::¡:"'~!i!::::::¡:'::::::::':::¡¡:'~ìr9.tti1¡¡::;::¡;¡:!:':!9,1P~9~'~!¡:¡¡:¡:¡:I::¡:¡¡::¡:'::¡: ,lara meter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 mg/kg Xylenes (total) ND 0.010 mglkg 10luene ND 0,0050 mglkg Methyl-tert-Butyl Ether ND 0.025 mglkg thylbenzene ND 0.0050 mglkg TPH for Gasoline ND 0.50 mglkg Surroç¡ates: REC (%) Control Limits Qual Surroç¡ates: REC (%) Control Limits Qual ,4-Bromofluorobenzene 93 47-137 1,4-Bromofluorobenzene - 'FID 74 34-141 ::"Þffi1~:::::::::':¡::;:¡::¡:¡:¡::::::::::::::::::::'¡::'::::!¡::,:',::::::::::'::::¡:,!:::,:'¡:!:¡::¡:¡::::¡::'::::::::::::¡:::':':!:::::::'::'::::::!::,::91:æ~$9ì~f~::::::::::::::::!::¡::::¡:,:::¡¡:¡'q~!~im"::::::::::::¡-:,':'~'~"i::¡:::'::::::::::::::"',@i::::::::::::::::::::::::':::~p~~t!~¡':':::::'::::91~~~Y'!¡::::::¡:::::::::::::!:,::: larameter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 mglkg Xy1enes (total) 0.062 0.010 mglkg 10luene 0.014 0.005 mglkg Methyl-tert-Butyl Ether 0.087 0.025 mglkg thylbenzene ND 0.0050 mglkg TPH for Gasoline 0.87 0.50 mg/kg Surroç¡ates: REC (%) Control Limits Qual Surroç¡ates: REC (%) Control limits Qual 1,4-BrOmOfluorobenzene 94 47-137 1,4-Bromofluorobenzene - FID 75 34-141 '::gat1f,:::!::::::,!::!:!!¡:!:,:::,::,::::::'!:i:!:!:::¡¡¡!:::¡:¡::::::;:;:::::;::!:;!¡::;!,:::,::!!:::;:::::;:;:;!:::::::::;::::'!::::;:'!:::::;:'::P1'æ~lî~~:::::i::::;i!:;;;::':::::!':'[~~1~1;::!;:;!'::!!:::::!::'::~g!,!::;:;:¡::!::;:!:::;::!:'i!',;¡Ûìi,::::=i;:¡:;i;::::f::::ii~~¡'9ÿ!1::i::::;:::;::ii.1~!~~~1¡~!::!::\!::::::::¡:::¡:::::!, arameter Result RL OF Qual Units Parameter Result Rl OF Qual Units NO 0.0050 mglkg Xylenes (total) ND 0.010 mglkg ND 0.0050 mglkg Methyl-tert-Butyl Ether ND 0.025 mglkg ND 0.0050 mglkg TPH for Gasoline ND 0.50 mglkg REC (%) Control Limits Qual Surroç¡ates: REC(%) Control Limits Qual 95 47-137 1,4-Bromofluorobenzene - FIO 76 34-141 lenzene oluene thylbenzene lurroç¡ates: ,4-Bromofluorobenzene I I RL - Reporting Limit, OF - Dilution Factor. Qual - Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 II -a/science I:; nvironmental Laboratories, Inc. ANALYTICAL REPORT I I I IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Project: 101 South Union Avenue, Bakersfield, CA Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0073 EP A 50308 EPA 8015M/80218 I Client Sample Number: Lab Sample Number: 1 Page 2 of 12 Date Collected: Date Prepared: Date Analyzed: ac Batch ID: Matrix: Parameter Result RL OF Qual Units Parameter Result RL OF Qual Units Benzene NO 0.0050 mglkg Xylenes (total) NO 0.010 mglkg Toluene NO 0.0050 mglkg Methyl-tert-Butyl Ether NO 0.025 mglkg Ethylbenzene NO 0.0050 mglkg TPH for Gasoline NO 0.50 mglkg Surroç¡ates: REC (%) Control limits Qual Surroç¡ates: REC(%) Control limits Qual 1.4-Bromofluorobenzene 90 47-137 1,4-Bromofluorobenzene - FIO 74 34-141 I I II ::pfil::::':¡::!::::::¡!¡:,:::::::::::¡¡¡::::::,,:::::.:::::¡:'::::::!::'!:::::!::::::::::::::::::::::::':::::::::,:::!:::::::::::,::,:::::::::::::::!,:.:::::::::::·~1~~~#!!~::::::::::::::::::::::::::::::'··~ir~1(!'::::::::::::::::::·:§:~"~':::::::::::::::::::::::-:to/.i:':::::::::::::::::::::::9,P9~(!'::::::::::::::¡:P1~i#:#:~1~~::::¡:::::::¡:::;:::::::::: Parameter ~ RL OF Oual Units Parameter Result RL OF Qual Units Benzene NO 0.0050 mglkg Xylenes (total) NO 0.010 mglkg Toluene NO 0.0050 mglkg Methyl-tert-Butyl Ether ND 0.025 mglkg Ethylbenzene NO 0.0050 mglkg TPH for Gasoline ND 0.50 mglkg Surroç¡ates: REC (%) Control limits Qual Surroç¡ates: REC(%) Control Limits Qual I .1 1,4-Bromofluorobenzene 92 47-137 1,4-Bromofluorobenzene-FID 74 34-141 I Parameter Result RL DF ~ Units Benzene NO 2.5 500 D mglkg Toluene NO 2.5 500 0 mglkg Ethylbenzene ND 2.5 500 D mglkg Surroç¡ates: REC (%) Control limits ~ 1,4-Bromofluorobenzene 102 47-137 RL - Reporting limit. DF - Dilution Factor. Qual- Qualifiers Parameter Result RL DF ~ Units Xylenes (total) 110 5 500 D mglkg Methyl-tert-Butyl Ether ND 13 500 0 mglkg TPH for Gasoline 9100 250 500 D mg/kg Surroç¡ates: REC (%) Control limits Q!!!! 1,4-Bromofluorobenzene - FID 101 34-141 1 I I .' I I I 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 I ~ã =alSCienCe ~§nvironmental Laboratories, Inc. ~T Corporation ~452 East Foothill Blvd., 9th Floor !pasadena, CA 91107 I ANALYTICAL REPORT roject: 101 South Union Avenue, Bakersfield, CA Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0073 EPA 5030B EPA 8015M/8021B Page 3 of 12 Client Sample Number: Lab Sample Date Date Date Number: Collected: Matrix: Prepared: Analyzed: QC Batch 10: arameter Result . RL OF Qual Units Parameter Result RL OF Qual Units enzene NO 0.0050 mglkg Xylenes (total) NO 0.010 mg/kg Toluene ND 0.0050 mglkg Methyl-tert-Butyl Ether ND 0.025 mg/kg ~thYlbenzene ND 0.0050 mg/kg TPH for Gasoline NO 0.50 mg/kg urroç¡ates: REC C%) Control limits lli!!! Surroç¡ates: REC C%) Control limits Qual ,4-Bromofluorobenzene 92 47-137 1,4-Bromofluorobenzene - FIO 74 34-141 lara meter Result RL DF Qual Units Parameter Result RL OF Qual Units Benzene ND 0.0050 mg/kg Xylenes (total) ND 0.010 mg/kg fo'uene ND 0.0050 mglkg Methyl-tert-Butyl Ether ND 0.025 mg/kg thylbenzene ND 0.0050 mglkg TPH for Gasoline ND 0.50 mglkg Surroç¡ates: REC C%) Control limits Qual Surroç¡ates: REC C%) Control limits Qual 11.4-BrOmOfluorobenzene 93 47-137 1.4-Bromofluorobenzene - FIO 74 34-141 arameter Result RL DF Qual Units ¡enzene ND 0.0050 1 mglkg oluene 0.083 0.005 1 mglkg thylbenzene ND 0.0050 1 mglkg REC C%) Control limits Qual 91 47-137 I I RL - Reporting Limit. DF - Dilution Factor. Qual - Qualifiers Parameter Result RL OF Qual Units Xylenes (total) 0.56 0.01 mglkg Methyl-tert-Butyl Ether 0.047 0.025 mglkg TPH for Gasoline 4.9 0.5 mglkg Surroç¡ates: RECC%) Control limits Qual 1.4-Bromofluorobenzene - FIO 77 34-141 7440 Lincoln Way, Garden Grove, CA 92841-1432 . TEL: (714) 895-5494 . FAX: (714) 894-7501 ifj a/science I:, nvironmental Laboratories, Inc. ANALYTICAL REPORT IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0073 EPA 50308 EPA 8015M/8021B Project: 101 South Union Avenue, Bakersfield, CA Page 4 of 12 I I I I I Lab Sample Date Date Date Number: Collected: Matrix: Prepared: Analyzed: QC Batch ID: Client Sample Number: Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units 8enzene ND 0.0050 mglkg Xylenes (total) ND 0.010 mglkg Toluene ND 0.0050 mglkg Methyl-tert-8utyl Ether ND 0.025 mglkg Ethylbenzene ND 0.0050 mglkg TPH for Gasoline ND 0.50 mglkg SurroQates: REC (%) Control Limits Qual SurroQates: REC (%) Control Limits Qual 1,4-8romofluorobenzene 92 47-137 1,4-8romofluorobenzene - FID 73 34-141 I I :::[i~~f'!:::::::::::::::::::::::::::::::'::::::::::-::::::::::::::::::::::::::::::::::::::;:::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::;::'9':$~wpi!i~:,::::::::::::;::::::::::-¡gii91m~::::::::::::::::::::-§þ!,~:::::::::::::t:"'g~:Î:~~m~:::::::::::::';:!ilt~1::::::::::::::::!19~~91i.:::::::::::::::::;::::::::::1 Parameter Result RL DF Qual Units Parameter Result RL DF Oual Units 8enzene ND 0.63 125 D mglkg Xylenes (total) 180 1 125 D mglkg Toluene 13 0.63 125 D mg/kg Methyl-tert-8utyl Ether ND 3.1 125 D mglkg Ethylbenzene 18 0.63 125 D mglkg TPH for Gasoline 1500 63 125 D mglkg SurroQates: REC (%) Control Limits Qual SurroQates: REC (%) Control Limits Qual 1,4-8romofluorobenzene 110 47-137 1,4-8romofluorobenzene - FID 118 34-141 I I ¡¡t¡¡:~.111i111ll¡¡iì¡¡f0ì_iifil¡¡¡¡IWiliii!ŒJ1!>Æ:4!!i:fî.¡II:.~1i1i!i¡¡'mt~¡¡iIi¡imm~!ljl..#jpg{!~..iìl Parameter Result RL DF Oual Units Parameter Result RL DF Oual Units 8enzene ND 2.5 500 D mglkg Xylenes (total) 680 5 500 D mglkg Toluene 65 2 500 D mglkg Methyl-tert-8utyl Ether ND 13 500 D mglkg Ethylbenzene 74 2 500 D mg/kg TPH for Gasoline 4900 250 500 D mglkg SurroQates: REC (%) Control Limits ~ Surrogates: REC (%) Control Limits ~ 1,4-8romofluorobenzene 107 47-137 1 ,4-8romofluorobenzene - FID 113 34-141 RL - Reporting Limit. DF - Dilution Factor. Qual - Qualifiers I I I I I ! I 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 I I .:s _a/science .. nvironmental Laboratories, Inc. ANALYTICAL REPORT I IT Corporation .452 East Foothill Blvd., 9th Floor ~asadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0073 EPA 50308 EPA 8015M/80218 lroject: 101 South Union Avenue, Bakersfield, CA Page 5 of 12 Client Sample Number: Lab Sample Number: Date Collected: Matrix: Date Prepared: Date Analyzed: QC Batch ID: .·[f:1~i:1!::::::·::~:::::::::~:~:::::::::::::::i:~:::.~::::::~::::::::::.::.~::~:::~::::::::::::::::::::::::::::::·::::::::::,::·::::::::::::91&¥.iP9Ii1~~:::::::~:::::::~:::::::::"9YP~ffi'::::~:::::::~R'¡~:::~:::::::::':::~::·::::~t,Æ::::m:::::::::~::::::::9~f:9.~(~~:t:::::::::::91~~9~'!i.::::::::\:f:~:::::::I:: larameter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 mglkg Xylenes (total) ND 0.010 mglkg Toluene ND 0.0050 mglkg Methyl-tert-B utyl Ether ND 0.025 mglkg Ithylbenzene ND 0.0050 mglkg TPH for Gasoline ND 0.50 mglkg SurroQates: REC(%) Control Limits Qual SurroQates: REC (%) Control Limits Qual ,4-Bromofluorobenzene 94 47-137 1 ,4-Bromofluorobenzene - FID 74 34-141 ........... ...........;...:.;. .....:.;.:.;<.:.;.:.;.:.:.:.:.:.:.:.;.:.:-:.:. ...:..........:.:-:.:.:.:.:.;.;.;.....:.:.;.:.:.;.;.:.:.:.;.:.;.;.;.:.;.:.;.;.:.:.:.;.;.:.;-:.:.: ......:.:.:.:.:.:.:.;.:.;.:.:.:.:.:.:.;.;.;.:.;.:.:.:.:.:.:.' ...................................................... .............................,................................................".....,..................,.,. ~:JH~~~~%%:%:::%rit{::::::t::r%%:::~:::~::::;::~:::::=m~:::~::m:::::~:~:~~::::::::~::::~::::::%%:::··~A~·~~P:p~~~'!.:::::::::::::::::::·:ß2ió1m,::.:::::::: :.: ::: ~:~"~::::::::.:::::': :··:r,#.~:::::::::~:~:::::::::!y~!ì!~:::~:::::~:::::P1~AA~~,~~::::::::~::¡~:::::~:::~:~:~ larameter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 mglkg Xylenes (total) ND 0.010 mglkg IOluene ND 0.0050 mglkg Methyl-tert-Í3utyl Ether ND 0.025 mg/kg thylbenzene ND 0.0050 mglkg TPH for Gasoline ND 0.50 mglkg SurroQates: REC (%) Control Limits Qual Surroç¡ates: REC (%) Control Limits Qual 1,4-BrOmOfluorobenzene 91 47-137 1 ,4-Bromofluorobenzene - FID 72 34-141 :::îf1éf~!:::~:::~:::~::::::::::::~::·:::::::~::::::::;::::::::::::::::::::~::~:::::::~:~::::::::::~::::~::::::~~::~::~:::::::::~::::::::::~:::::.P1t~#I~~~1i,:::~::::~::~:::::~:::··~I~m'::::::::::::::~gi¡#::::::~::::~::~::::::·:.:·&f:~'::::::::~~::~::~:::::¡::~~tMf,,1::::\:::::::::::~~P~i~P1~;::::::::::::::::::::::~~::~:: arameter Result RL DF Qual Units Parameter ND 0.0050 mglkg Xylenes (total) ND 0.0050 mglkg Methyl-tert-Butyl Ether ND 0.0050 mglkg TPH for Gasoline REC(%) Control Limits Qual SurroQates: 92 47-137 1 ,4-Bromofluorobenzene - FID Result RL OF Qual Units ND 0.010 mglkg ND 0.025 mglkg ND 0.50 mglkg REC (%) Control Limits Qual 73 34-141 fenzene oluene thylbenzene urro ates: ,4-Bromofluorobenzene I I RL - Reporting Limit, DF - Dilution Factor. Qual- Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 E a/science I:; nvironmental Laboratories, Inc. -ANALYTICAL REPORT IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0073 EPA 50308 EPA 8015M/80218 Project: 101 South Union Avenue, Bakersfield, CA Page 6 of 12 Client Sample Number: Lab Sample Number: Date Collected: Date Prepared: Date Analyzed: Matrix: QC Batch ID: Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 mglkg Xylenes (total) ND 0.010 mglkg Toluene ND 0.0050 mglkg Methyl-tert-Butyl Ether ND 0.025 mglkg Ethylbenzene ND 0.0050 mglkg TPH for Gasoline ND 0.50 mglkg SurroQates: REC (%) Control Limits Qual Surrogates: REC(%) Control Limits Qual 1,4-Bromonuorobenzene 94 47-137 1,4-Bromonuorobenzene - FID 74 34-141 I I I I I I I :::[i:~if,i::::::::::::::::::::::::::I::::::::::::::::::::!::::::!::::::::!::::::::::::::::!:::::!:::::::::!:::::::::::::::::!:!:i::::::!::::::!:!::!:::!:¡:i::!:!:::.::::-!91:P~W9!~~1í:::::::::::::::i::i:::!:::i!i:rq~r~:~m':i¡::::::::::::::::·:·.#.m¡i::::::::::::::::::::~Y~~m':i:::::::!i::::::::~~r¡mr!1.:::::i:::::::::·919~~P~;:::::!:::::!;:::::::::::::::I Parameter Result RL DF Oual Units Parameter Result RL DF Qual Units Benzene ND 5.0 1000 D mglkg Xylenes (total) 1200 10 1000 D mglkg Toluene 11 5 1000 D mglkg Methyl-tert-ButyI Ether ND 25 1000D mglkg Ethylbenzene 43 5 1000 D mglkg TPH for Gasoline 14000 500 1000D mglkg SurroQates: REC (%) Control Limits Qual SurroQates: REC (%) Control Limits lli!!! I I _;;;;¡w.I~!;"I!l.~!~'_m'j.~~~;;;;;I;.'II;;'~119~ I Parameter Result RL DF Qual Units Parameter Result Bb DF Qual Units I Benzene ND 0.0050 mg/kg Xylenes (total) 0.023 0,010 1 mg/kg Toluene ND 0.0050 mglkg Methyl-tert-ButyI Ether ND 0.025 1 mglkg Ethylbenzene ND 0.0050 mglkg TPH for Gasoline 10 0.50 1 mglkg Surrogates: REC (%) Control Limits Qual Surrogates: REC (%) Control Limits Qual 1,4-Bromonuorobenzene 89 47-137 1,4-Bromonuorobenzene - FID 85 34-141 RL - Reporting Limit. DF - Dilution Factor. Qual - Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-750 I I 1 I I I I ~- alscience :: nvironmental Laboratories, Inc. .... --'- .-.....- ANALYTICAL REPORT I IT Corporation .452 East Foothill Blvd., 9th Floor I'asadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0073 EPA 5030B EPA 8015M/8021B lreject: 101 South Union Avenue, Bakersfield, CA Page 7 of 12 Client Sample Number: Lab Sample Number: Date Collected: Matrix: Date Prepared: Date Analyzed: QC Batch ID: .................. ............:.... .......................'.......'.. .......................................... ........;.... ....... ....... ........;.;.;.;.;.;.:.;.;.:.:.;<.;.;.;.;. ........ ........ ....:::;:::::::::.;.;.;.;.;.:.;.;.;.:. ,,<:::::::::::::::;::::;:::;:::::::::::::::::;:;:::::::::::;::::::::::::::::;.'. ..... '" .... ... :tt~~~1~::::m::::::::?::::::::::::::::::::?::t:::::::::::::::::t:::::::m::tt???::t::::::::::::::::::::::::~i~~&9!~~'!:::::::::::::::i::.:9PMl~1}}:tt:,:~:~m~::):::::':::::::r:Nl~{:}:::::t:{~f(9~f,!t:m::'::::9Mf.p,~1!!M\:r:::::ttf larameter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 mglkg Xylenes (total) ND 0.010 1 mglkg Toluene ND 0.0050 mg/kg Methyl-tert-Butyl Ether ND 0.025 1 mglkg Ithylbenzene ND 0.0050 mglkg TPH for Gasoline ND 0.50 1 mglkg SurroQates: REC (%) Control Limits Qual SurroQates: REC (%) Control Limits Oual ,4-Bromofluorobenzene 90 47-137 1,4-Bromofluorobenzene - FID 73 34-141 """"2B'-~O:--:::'-:':::::':":'::::-:--:'::-'-::':-'::::" :---:.::.:::....:::-::-. : :":::.':..' '.' 0'1:';;2 ···..3 ·0 .':::-.:..::-'" .. "'.::': :::-." ·d::::::::: ::-:- NT··· .::::::::.:..::...... ·3"'0:' .:.:::.:.:::.:.:.:.:.:.:.:.:.:::::::::;:::::::::::::::::::::::··::::i::::::: A. . "!'. ............. . . '.': .' ....... .........: .... .......... ... ......... ..... -v ;;007 .2 .... ..... .'. .. 02/01i'Q~... . Soli. .:. ...:. .'. A..........:.. :6210. f. ~:. .... tl1020201:s~.. :. ......... lara meter Result RL DF Qual Units Parameter Result RL DF Oual Units Benzene ND 0.0050 mglkg Xylenes (total) ND 0.010 1 mglkg IOluene ND 0.0050 mg/kg Methyl-tert-Butyl Ether ND 0.025 1 mglkg thylbenzene ND 0.0050 mg/kg TPH for Gasoline ND 0.50 1 mg/kg SurroQates: REC (%) Control Limits Qual SurroQates: REC (%) Control Limits Qual 1,4-BrOmOfluorobenzene 92 47-137 1 ,4-Bromofluorobenzene - FID 72 34-141 :::!f~~g1Î:::::::::::::::::::::::::::::::¡::¡::¡::::::,:::::::¡::::¡:::::::::::::::.::::::::::::.:::::::::::::::::::::::::::::::::::,::¡::¡:::::::::¡::.~1·$~lii~i~'::::::::::::::::::;::·~I·~m1::::::::::::::¡:::·~~I.¡i:;::::::·::::·::::::::·m#:::¡::¡::::::':::::¡:¡~~i,9¥!1::¡::::¡::¡::¡g,,~~~~¡,!~::::¡:::¡::¡::::::::::::¡:::: arameter Result RL DF Qual Units Parameter Result RL DF Qual Units ND 0.0050 1 mglkg Xylenes (total) ND 0.010 1 mglkg ND 0.0050 1 mglkg Methyl-tert-Butyl Ether ND 0.025 1 mglkg ND 0.0050 1 mglkg TPH for Gasoline ND 0.50 1 mglkg REC (%) Control Limits Qual SurroQates: REC (%) Control Limits Qual 92 47-137 1,4-Bromofluorobenzene - FID 74 34-141 _enzene oluene thylbenzene urro ates: ,4-Bromofluorobenzene I I RL - Reporting Limit, DF - Dilution Factor. Qual - Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 -'- E - alsp!~~n~e ß:. nvïronmental Laboratories, Inc. ANALYTICAL REPORT IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0073 EP A 5030B EPA 8015M/8021B Project: 101 South Union Avenue, Bakersfield, CA Page 8 of 12 I I I I I Client Sample Number: Lab Sample Date Date Date Number: Collected: Matrix: Prepared: Analyzed: QC Batch ID: Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 mglkg Xylenes (total) ND 0,010 1 mglkg Toluene ND 0.0050 mglkg Methyl-tert-Butyl Ether ND 0.025 1 mglkg Ethylbenzene ND 0.0050 mg/kg TPH for Gasoline ND 0,50 1 mglkg SurroQates: REC (%) Control Limits Qual SurroQates: REC C%) Control Limits Qual 1,4-Bromonuorobenzene 92 47-137 1 ,4-Bromonuorobenzene - FID 72 34-141 I I Iîs~1ii:¡:::¡!:::::'¡!::::::¡::i:¡:!::¡::':::::!':::::'¡'::::::;¡::::::'!:::!::':::::¡::!::.::::'::,!'::!:::¡::::::::'::::¡:::::::!::::,::!:::!::::::!:::,:'::::::::::!:::'~':æ~ffl~r~~~!,:!::!:!'¡!:::¡:¡i!::::::¡:::::::~~.r~:1"!~::¡:::!!:::¡!:::!::,,:!,§:~¡!!::::::::,::::,::'::':,::¡::'!;itJi.i:¡¡:::¡::::::::!:¡!::¡::!:i:'¡mr!,¡I::i¡I:::9,1~~P~'!!::!:::::::::::¡t:!¡::;!:1 Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 mglkg Xylenes (total) ND 0.010 1 mg/kg Toluene ND 0.0050 mglkg Methyl-tert-ButyI Ether ND 0.025 1 mglkg Ethylbenzene ND 0.0050 mglkg TPH for Gasoline ND 0.50 1 mg/kg SurroQates: REC (%) Control Limits Qual SurroQates: REC C%) Control Limits Qual 1,4-Bromonuorobenzene 94 47-137 1 ,4-Bromonuorobenzene - FID 73 34-141 I I I :i:T5i~~~!:::':::::::::::::::::::::::::::::::::'::::::::::::::::::::!:::,::::::::::::::::::':,:;.':'::,:::::::::::::::::¡::;::::::::::::::::::::!:!:::::::::::::':::'::':91æ~pp~!:~~i,::,::::::::,::::'!::::::'::":9Ilri~:::::::::::::::::::::::,#:~¡¡#:::::::!:::::!::::::'::::::::w~:i:¡::::!::::::::::i::::::i::~WÞMi1:::::::::::::::!i~P~Þ.~P1ii.::¡:::iii::i::i:::::::ii:::: Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 mglkg Xylenes (total) ND 0.010 mg/kg Toluene ND 0.0050 mglkg Methyl-tert-Butyl Ether ND 0.025 mg/kg Ethylbenzene ND 0.0050 mglkg TPH for Gasoline ND 0.50 mg/kg SurroQates: REC (%) Control Limits .Q.!:!!! SurroQates: REC C%) Control Limits Qual 1,4-Bromonuorobenzene 94 47-137 1,4-Bromonuorobenzene - FID 74 34-141 RL - Reporting Limit, DF - Dilution Factor, Qual- Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-750 I I I I I I I I S -a/science :: nvironmental Laboratories, Inc. -'-"'-'--=- ...:....--. ---." -- ~._._. ANALYTICAL REPORT I IT Corporation 1452 East Foothill Blvd., 9th Floor asadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0073 EPA 5030B EPA 8015M/8021B Iroject: 101 South Union Avenue, Bakersfield, CA Page 9 of 12 Client Sample Number: Lab Sample Number: Date Collected: Matrix: Date Prepared: Date Analyzed: QC Batch ID: ................... .........................., .............-......... ...... ..... ... ".... . ........ ... .......... .... /t~~S1$);}}?::::)):/:(:::i::¡@:;¡:::::::::::::·:m:::::::m:m::::::::::::;:::::::::::.:::91@~æ.#t~~~!:::::;::::;:::::::::~&P~r!"::::::::::::::::·#·§,¡ª::::::;:.:::·:::::::.:.N"~¡¡;::::::::::::::::::¡::~~(9.i(~~::::::::::::::i1P:~9#'9,~!::::¡:::¡::II;::::::::: larameter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 mglkg Xylenes (total) ND 0.010 mg/kg Toluene ND 0.0050 mglkg Methyl-tert-Butyl Ether ND 0.025 mg/kg IthYlbenzene ND 0.0050 mglkg TPH for Gasoline ND 0.50 mglkg Surrogates: REC (%) Control Limits Qual Surrogates: REC (%) Control limits Qual ,4-Bromofluorobenzene 94 47-137 1 ,4-Bromofluorobenzene - FID 72 34-141 ¡.ÌŠ~~!::::::::::::::¡::::¡:¡:::;::::::::::;¡::::::¡::::::.::::::::::¡:::::¡::::::::::::::::¡:::¡::::¡:::::::¡::::;:::¡:¡:;:::::::¡:::::::¡:::::::@1"i~#PR!~:f~!::::·::::::::I::::::~#·(91&'::::::::¡:::¡::::::::~:M~::::::::¡:::::::;::¡;¡¡fiÜ~::¡:¡:::¡::::::::·:¡¡9!l!!f~~:¡::::¡:::::P1P~P~#:,~!::::t:::j:::::::::: larameter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 mglkg Xylenes (total) NO 0.010 mglkg 10luene ND 0.0050 mglkg Methyl-tert-Butyl Ether NO 0.025 mglkg thylbenzene ND 0.0050 mg/kg TPH for Gasoline NO 0.50 mglkg Surrogates: REC (%) Control Limits Qual Surrogates: REC(%) Control limits Qual 1,4-BrOmOfluorobenzene 88 47-137 1 ,4-Bromofluorobenzene - FID 82 34-141 ::¡ïfJÇ~1!:¡:¡:::::::::¡:::;:::@::::::¡:::::::::¡::¡:::::::\:::::¡:::::¡::::::::¡::::::::¡::::::::¡:::::::¡::::::¡;::¡·:¡::::·:::::::::::~1·$~j?~S~î:¡::::::::::::::¡:::::::¡:~m>1m,::::::::::::::':~~i¡i::::::::::::::i::¡::·w#i.:::::::::¡;:::::::::::::~~!9¥~~::::::::::::::::~'P~!~9j!j:::::::::::::::::::::::::: rameter Result RL DF Qual Units Parameter ND 0.0050 mg/kg Xylenes (total) ND 0.0050 mg/kg Methyl-tert-Butyl Ether NO 0.0050 mglkg TPH for Gasoline REC (%) Control limits Qual Surrogates: 88 47-137 1.4-Bromofluorobenzene - FID Result RL DF Qual Units ND 0.010 mglkg ND 0.025 mglkg ND 0,50 mglkg REC (%) Control limits Qual .83 34-141 Inzene luene hylbenzene rro ates: 4-Bromofluorobenzene I I RL - Reporting Limit, OF . Dilution Factor. Qual - Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501 c.; a/science ~§nvironmental Laboratories, Inc. ANALYTICAL REPORT IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0073 EPA 5030B EPA 8015M/80218 Project: 101 South Union Avenue, Bakersfield, CA Page 10 of 12 I I I I I Lab Sample Date Date Date Number: Collected: Matrix: Prepared: Analyzed: QC Batch 10: Client Sample Number: Parameter Result RL OF Qual Units Parameter Result RL OF Qual Units Benzene ND 0.0050 mglkg Xylenes (total) NO 0.010 1 mglkg Toluene ND 0.0050 mglkg Methyl-tert-Butyl Ether NO 0.025 1 mglkg Ethylbenzene NO 0.0050 mg/kg TPH for Gasoline NO 0.50 1 mglkg SurroQates: REC (%) Control limits Qual SurroQates: REC (%) Control Limits Qual 1,4-Bromof1uorobenzene 89 47-137 1,4-Bromof1uorobenzene - FIO 83 34-141 I I ::Jj~~i~!::::::::::::::::::::::::~:~:~:::::::::::::~:I~::::~:~::::::::::::::::::~~:::::::::::::::::::~:~:::::::~:::::::::::::::::::::::::::::I:::::':::::::::::::::::::i91i&:~~î~~~!:::::::::¡::~:~:::::::i:::::::::::~~î~:~:m,:::::::::::::::~::::::§g¡¡i:':::::~:i::::~::::::::::i:I:::i!!i:::::::::::::i::::::::::::::i!!'~!(!,:::I~:::~:i::!1PAA~9'!¡:~::¡::::::::::i::¡:::::~:::1 Parameter Result RL DF Qual Units Parameter Result RL OF Qual Units Benzene NO 0.0050 mg/kg Xylenes (total) NO 0.010 1 mg/kg Toluene ND 0.0050 mglkg Methyl-tert-ButyI Ether ND 0.025 1 mglkg Ethylbenzene NO 0.0050 mglkg TPH for Gas?line NO 0.50 1 mg/kg SurroQates: REC (%) Control limits Qual SurroQates: REC(%) Control limits Qual 1,4-Bromof1uorobenzene 89 47-137 1,4-Bromof1uorobenzene - FIO 84 34-141 I I I i::Tf1~~iÎ~:i:::i:::i:::i:::i::::::i::::::i::i:':::::;:::~::i::::::i:::i:::i;:i:::i::::::i:::::::i:~::::~:::i:i::i::::~::::i:::i::i::i:'~i:::i::~i:::::::·"i::;:i9'æ~Ii~~@¡:i~:::::~i::::::::::i:::::::;:911~~:::i;:::::::.i~::::::;:~g¡¡iji::~:':::::·::::i::~:·;::::::;!!i:::i:~:~::i:~::::::::::::::~pft9~~~:::i::::::::::;~~9~P,AA1¡!::::i::::::~i:::i::::~:::~:: Parameter Result RL OF Qual Units Parameter Result RL OF Qual Units Benzene ND 0.0050 mglkg Xylenes (total) ND 0.010 mgJkg Toluene NO 0.0050 mglkg Methyl-tert-Butyl Ether ND 0.025 mglkg Ethylbenzene ND 0.0050 mglkg TPH for Gasoline NO 0.50 mg/kg SurroQates: REC(%) Control limits Qual SurroQates: REC(%) Control limits Q!!!! 1,4-Bromof1uorobenzene 93 47-137 1,4-Bromofluorobenzene - FID 86 34-141 RL - Reporting limit. DF - Dilution Factor. Qual - Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-750 I I I I I I I -4Ë a/science I :: nvironmental Laboratories, Inc. ANALYTICAL REPORT I IT Corporation 1452 East Foothill Blvd., 9th Floor asadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0073 EPA 5030B EPA 8015M/80218 Iroject: 101 South Union Avenue, Bakersfield, CA Page 11 of 12 Client Sample Number: Lab Sample Number: Date Collected: Matrix: Date Prepared: Date Analyzed: QC Batch ID: :·M~1ij~~¡~î.~~~¡::::::::::::::::·:::::::::::::::·::::::I:::::::::::::::::::::::::::::::·::::::::::::::::::::::::·::·M~~&:1.&9.ìS~~Æ~í::::::::::::::::.::·::·:·Ñ"~¡::::::::::::::::::::::·§·~¡¡~::::::::::::::::-·Ñ!i::::::::::::::::::;::~~r9.ìœ~¡::::I::::::P19~9i.~'~!:::::::::¡::::::::::::::::: lara meter Result RL OF Oual Units Parameter Result RL OF Oual Units Benzene NO 0.0050 mglkg Xylenes (Iolal) NO 0.010 mglkg ìOluene NO 0.0050 mg/kg Methyl-tert-Butyl Ether ND 0.025 mglkg thylbenzene ND 0.0050 mglkg TPH for Gasoline NO 0.50 mglkg SurroQates: REC (%) Conlrollimits Qual SurroQales: REC (%) Control limits Qual ,4-Bromofluorobenzene 97 47-137 1,4-Bromofluorobenzene - FIO 89 34-141 :M~ml:~~#r~::i::::::::i::::::::::::::::::::::::;:.::::::::I::::i:::::¡:::::::i:::::::::::::::::::::::::::::::::¡:::::::::::::::·#~!&.1&9ii~i.~~::::·:¡::::::::::::¡:m~:::::::::::::::::::::::··§·~I¡~::¡:::::::.:::::::··mi::::::::::::::::::::::'PP9it~~¡r::::::::'9,1#g~~#1~!:::::::::::::::¡:::::::::::: lara meter Result RL OF Qual Units Parameler Result RL OF Qual Units Benzene NO 0.0050 mglkg Xylenes (Iolal) NO 0,010 mglkg IOluene ND 0.0050 mglkg Methyl-tert-Butyl Ether ND 0.025 mglkg thylbenzene NO 0.0050 mglkg TPH for Gasoline NO 0.50 mglkg SurroQales: REC(%) Conlrollimits Qual SurroQales: REC (%) Conlrollimits Qual 1,4-BrOmOfluorobenzene 99 47-137 1,4-Bromofluorobenzene - FIO 78 34-141 :;M~I:~w~~::::::::::::::::::::::::::::::::::::::::::·::::::::::.:::::::::::::::::::::::::¡::::::¡::::¡:¡::::::::::::::::¡:::::::::::::::·.#~îdH1!9~i:~~~1!:::::::::::::¡::::::::::::::;m~:::::::::::::::¡:::::::::::~~mi:::¡::¡::::::::::¡:::::.:W~:::::::::::::::::::::::::.:~~r:1!~::¡:::¡¡:¡¡::::¡pj#:~~#i1j,i::::j::::::::;:::::::::::: arameter Result RL OF Qual Units Parameter Result RL OF Qual Units NO 0.0050 mglkg Xylenes (total) NO 0.010 1 mglkg ND 0.0050 mglkg Methyl-tert-Butyl Ether NO 0.025 1 mglkg NO 0.0050 mglkg TPH for Gasoline ND 0.50 1 mglkg REC(%) Conlrollimits Qual SurroQates: REC (%) Control limits Qual 95 47-137 1,4-Bromofluorobenzene - FIO 89 34-141 lenzene oluene thylbenzene urro ates: ,4-Bromofluorobenzene I I RL - Reporting Limit. OF· Oilution Factor, Qual· Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 I I I I I Lab Sample Date Date Date Number: Collected: Matrix: Prepared: Analyzed: QC Batch ID: I I I I I I I I I I I I ¡¡ a/science ~§nvironmental Laboratories, Inc. 'ANALYTICAL REPORT IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0073 Ext + EP A 50308 EPA 8015M/80218 Project: 101 South Union Avenue, Bakersfield, CA Page 12 of 12 Client Sample Number: Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.050 10 mglkg Xylenes (total) ND 0.10 10 mglkg Toluene ND 0.050 10 mglkg Methyl-tert-Butyl Ether ND 0.25 10 mglkg Ethylbenzene ND 0.050 10 mglkg TPH for Gasoline ND 5,0 10 mglkg SurroQates: REC (%) Control limits Qual SurroQates: REC (%) Control limits Qual 1,4-Bromofluorobenzene 92 47-137 1,4-Bromofluorobenzene . FID 86 34-141 RL - Reporting Limit . DF - Dilution Factor . Qual - Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 . TEL: (714) 895-5494 . FAX: (714) 894-7501 I ~ :;c~aISCienCe - nvironmental Laboratories, Inc. I I ANALYTICAL REPORT IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 I I Date Received: Work Order No: Preparation: Method: Client Sample Number: Project: 101 South Union Avenue, Bakersfield, CA 02/02/01 01-02-0073 N/A EPA 8260B Page 1 of 1 I II Parameter Result Methyl-tert-Butyl Ether 94 SurroQates: REC (%) I Dibromofluoromethane Toluene-d8 1,4-Bromofluorobenzene 98 96 98 I Parameter I Methyl-tert-Butyl Ether I SurroQates: I Dibromofluoromethane Toluene-d8 1,4-Bromofluorobenzene I Method,Blânk I Parameter Methyl-tert-Butyl Ether SurroQates: I Dibromofluoromethane Toluene-d8 1,4-Bromofluorobenzene I I I I I Result 60 REC (%) 100 101 97 Result ND REC (%) 109 101 93 RL - Reporting limit , Lab Sample Number: 01 :.02-0073;2. Date Prepared: Date Analyzed: 01 O~I)5-ABS.'." Matrix: Date Collected: RL DF 5 Oual Units uglkg Qual Control Limits 80-120 81-117 74-121 01-02-OÒ73~9,· RL DF Qual Units 5 uglkg Control Qual Limits 80-120 81-117 74-121 099-10-005-1,023 solid RL DF Qual Units 5.0 uglkg Control Qual Limits 80-120 81-117 74-121 N/A N/A 02106/01 DF - Dilution Factor. Qual - Qualifiers 01 0205-ABS:'··· 010205-ABS 7440 Lincoln Way, Garden Grove, CA 92841-1432 . TEL: (714) 895-5494 . FAX: (714) 894-7501 I = a/science I::, nvironmenfal Laboratories, Inc. ------- -"------- I I I 02/02/01 I 01-02-0073 EPA 5030B I EPA 8015M/8021B I MSIMSD Batch Number . ._------.'-'-~ .-. ~...-~_....-......~.......- . Quality Control - Spike/Spike Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: Project: 101 South Union Avenue, Bakersfield, CA Date Spiked Sample ID Matrix Instrument Prepared Date Analyzed Parameter MS %REC MSD %REC %REC CL RPD 101 105 46-136 3 100 103 45-,138 4 99 103 62-121 4 101 105 53-130 4 99 103 64-120 4 98 101 24-144 3 104 105 44-122 1 RPD CL Qualifiers I I I I . I I I I .' I I. I II I Benzene Toluene Ethylbenzene p/m-Xylene o-Xylene Methyl-tert-ButyI Ether TPH for Gasoline 0-15 0-18 0-17 0-17 0-13 0-23 0-30 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-750 I I I I I I I I I I I I. ! I I I I I iæ _ alscience - Environmental Laboratories, Inc. .-.-----=-----... - - _......::...:....-'----------/ .. .k__""___.O..,·;;-,........-= .-..-_. _.~, =--__->._ Quality Control - Spike/Spike Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0073 EPA 5030B EPA 8015M/8021B Project: 101 South Union Avenue, Bakersfield, CA Date Spiked Sample ID Matrix Instrument Prepared ·¡·':Ó'j%¡$ði~·ti·:·::¡:¡·:'¡::¡·:·:::¡::¡:::':·:·::·:·:·:·::¡¡·¡·:::I·¡:¡.:'·:·;::·::::::·¡:::·::::=¡·::::¡::::.:.U:::::::::,:::·::~g¡~å.:¡:¡·::::::::·¡·:I':·:·¡::::·:::,:'::::::"·:â¿:~j:¡::::;::::¡:·¡::::::::·:,::::¡::,::::::., &;Â:·:,¡·::¡:·¡:'::::::·;: ¡·::¡::·:·:::::·:6 i)ÓiÎà~¡:::¡::.¡::=¡'::¡:::¡::::=¡:ij:~:Ó¡6ið:~iI:¡,:¡¡¡ Date Analyzed MS/MSO Batch Number Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers Benzene 93 93 46-136 1 0-15 Toluene 91 89 45-138 2 0-18 Ethylbenzene 92 90 62-121 2 0-17 p/m-Xylene 92 90 53-130 3 0-17 o-Xylene 94 91 64-120 3 0-13 Methyl-tert-ButyI Ether 97 92 24-144 5 0-23 TPH for Gasoline 97 96 44-122 0 0-30 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501 Date Spiked Sample 10 Matrix Instrument Prepared Date Analyzed MS/MSD Batch Number I I II I I I I I 'I I I I II I I I I I ~ _a/s~!~~~e L~nvironmental Laboratories, Inc. Quality Control - Spike/Spike Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena. CA 91107 Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0073 EPA 50308 EPA 8015M/8021B Project: 101 South Union Avenue, Bakersfield, CA Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers Benzene 94 96 46-136 2 0-15 Toluene 93 93 45-138 0 0-18 Ethylbenzene 93 95 62-121 1 0-17 p/m-Xylene 94 95 53-130 1 0-17 o-Xylene 96 96 64-120 0 0-13 Methyl-tert-ButyI Ether 91 90 24-144 1 0-23 TPH for Gasoline 101 106 44-122 5 0-30 7440 Lincoln Way. Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-750 I I I I I I I i I I I I, I II II i I I II I I I Ë a/science ::: §nvironmental Laboratories, Inc. Quality Control - LCS/LCS Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Project: Date Received: Work Order No: Preparation: Method: 101 South Union Avenue, Bakersfield, CA 02/02/01 01-02-0073 Ext + EPA 5030B EPA 8015M/8021B Date Date LCSILCSD Batch LCS Sample Number Matrix Instrument Prepared Analyzed Number :::9~i1ii~Y~~~~§'~::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::§þ¡~:::::::::::::::::::::::::':::::::::~Ç:~:1::::::::::::::::::::¡:::::·:ºy.P~l~H:::::::::::::::::::::::·º~!Mi9':::::::::::::::·:::::::::::::::::::::::::::::9@~9~~~~~:::::::::::::¡::::::::¡:¡:::::::::::::::::::::: Parameter LCS %REC LCSD %REC %REC CL RPD RPD CL Oualifiers Benzene 98 100 81-111 2 0-17 Toluene 95 96 81-111 2 0-16 Ethylbenzene 96 97 78-113 1 0-17 p/m-Xylene 97 98 70-118 1 0-18 o-Xylene 97 98 77-114 1 0-17 Methyl-tert-ButyI Ether 102 102 65-126 0 0-27 TPH for Gasoline 108 102 57-132 6 0-13 7440 Lincoln Way, Garden Grove. CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 Project: Date Received: Work Order No: Preparation: Method: 101 South Union Avenue, Bakersfield, CA 02/02/01 01-02-0073 EPA 50308 EPA 8015M/8021B I I I I I I I I I I I I I I I I I I · -a/science ~Environmenta/ Laboratories, Inc. Quality Control - LCS/LCS Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Date LCSILCSD Batch ;~¡ì¡1i~;'i:~¡¡'0~::::::::::@':::::::':::'::::::::::::':::,::::::,:::':::::::::t:,:::,::::::,:§~r.~i::::::::::::::::,:::,:::::':~¡ªi0~i:::'::,:::::::::::::::::::~:;mi:;~::::::::::::::::::::::::::::·~j~~~~~:::::::::::::::::::::::':::::::::::::::9~~¡~i~it::::::::::::::::::::::::::::::::::::::::::::: Parameter LCS %REC LCSD %REC %REC CL RPD RPD CL . Qualifiers Benzene 109 108 81-111 1 0-17 Toluene 106 107 81-111 1 0-16 Ethylbenzene 106 106 78-113 0 0-17 p/m-Xylene 107 108 70-118 1 0-18 o-Xylene 105 107 77-114 1 0-17 Methyl-tert-ButyI Ether 109 108 65-126 1 0-27 TPH for Gasoline 116 111 57-132 4 0-13 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 1_.= I . ---.-= . m'a sCIence I :: Environmental Laboratories, Inc. I I I Project: I I I I I I II I I I I I Quality Control - LCS/LCS Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 101 South Union Avenue, Bakersfield, CA 02/02/01 01-02-0073 EPA 5030B EPA 8015M/8021B Date Date LCSIlCSD Batch LCS Sample Number Matrix Instrument Prepared Anal zed Number :::g~#.;r¡¡:':&º~i~l~iî¡:¡:¡:::¡:::¡::¡¡:¡¡:¡:¡¡::¡:¡¡¡::¡¡:¡:¡:::¡,¡,¡¡¡'¡¡:¡¡:¡¡:::¡:¡:¡¡¡¡¡:¡¡:¡:¡::¡¡:¡::::¡:::¡j¡¡::§þ!@::::¡:¡:::¡::::,¡:¡:¡'¡:¡:¡¡¡¡:¡¡:j'::¡:¡:¡::::~ç¡'~:í:¡:¡::,:::¡¡,'I:¡:¡:¡::'¡:¡:¡I:¡::¡':¡Ñj¡::¡:::::::¡,:'¡:::::::¡¡:¡¡:::¡:¡:¡:::¡'º~!9,~m~:::¡:¡:¡¡:¡:¡::¡¡¡:¡:::¡:¡¡¡:::¡:j:¡'¡¡¡¡:¡:::~Hi~9~!,iiI::I¡j¡:'::¡:¡:¡:¡:::¡:¡:::¡:::¡¡j:::::::¡: Parameter LCS %REC LCSD %REC %REC CL RPD RPD CL Qualifiers Benzene 99 99 81-111 0 0-17 Toluene 96 96 81-111 0 0-16 Ethylbenzene 98 97 78-113 0 0-17 p/m-Xylene 98 98 70-118 0 0-18 o-Xylene 99 98 77-114 0 0-17 Methyl-tert-Butyl Ether 105 103 65-126 1 0-27 TPH for Gasoline 109 110 57-132 1 0-13 7440 Lincoln Way, Garden Grove. CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 101 South Union Avenue, Bakersfield, CA 02/02/01 01-02-0073 EP A 50308 EPA 8015M/8021B I I I I I I I I I I I I I I .1 I I I I ¡¡ a/science ~Environmenta/ Laboratories, Inc. Quality Control - LCS/LCS Duplicate Project: Date Date LCSIlCSD Batch Parameter LCS %REC LCSD %REC %REC CL RPD RPD CL Qualifiers Benzene 99 98 81-111 0 0-17 Toluene 96 95 81-111 1 0-16 Ethylbenzene 97 97 78-113 0 0-17 p/m-Xylene 98 98 70-118 0 0-18 o-Xylene 99 100 77-114 1 0-17 Methyl-tert-ButyI Ether 98 98 65-126 0 0-27 TPH for Gasoline 111 108 57-132 3 0-13 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) B95-5494 . FAX: (714) 894-750 I I I I I I I I .1 I I I I I I I I ._;:;I~aISCience I:. nvironmental Laboratories, Inc. Quality Control - Spike/Spike Duplicate' IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: Project: 101 South Union Avenue, Bakersfield, CA Spiked Sample ID I··········· ..... ..... .... ... .............. . ......,-. ""'-'" ',"" ·01:Ö~~1)1)()4-~ä<···;······· . Matrix Date Prepared Date Analyzed 02/02/01 01-02-0073 N/A EPA 82608 MS/MSD Batch Number . ................... ·············;········..··sb¡Id.C.·... ········..<ð2iM§t:.U>..·i.) ............ ·········N/Ä. . ·····················...·.Uö~/Óã¡I)..?';<········%..I)~óõÎl43i· <I Parameter Benzene Carbon Tetrachloride Chlorobenzene 1,2-Dichlorobenzene 1,1-Dichloroethene Toluene Trichloroethene Vinyl Chloride Methyl-tert-Butyl Ether Instrument MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers 104 102 72-127 2 0-25 97 94 70-130 3 0-25 101 100 72-131 1 0-25 105 101 70-130 4 0-25 101 101 69-127 1 0-25 100 99 75-124 1 0-25 101 102 60-137 1 0-25 101 99 70-130 2 0-25 87 85 80-120 2 0-25 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 iË a/science ::: Environmental Laboratories, Inc. Quality Control - LCS/LCS Duplicate I I I IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 101 South Union Avenue, Bakersfield, CA Project: lCS Sample Number Parameter Benzene Carbon Tetrachloride Chlorobenzene 1,2-Dichlorobenzene 1 ,1-Dichloroethene Toluene Trichloroethene Vinyl Chloride Methyl-tert-Butyl Ether 02/02/0~ 01-02-007 NI EP A 8260 lCS %REC lCSD %REC %REC Cl RPD 102 105 72-127 3 94 100 70-130 6 97 101 72-131 4 97 101 70-130 5 97 102 69-127 5 97 100 75-124 3 97 102 60-137 5 97 101 79-118 5 84 91 80-120 8 RPD Cl 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 Qualifiers I I I I I I I I I I I I 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-750 I I I I I I I 'I I II ,I I , I I I I I I I ~a/science GLOSSARY OF TERMS AND QUALIFIERS - ~nvironmental Laboratories, Inc. Work Order Number: 01-02-0073 Qualifier Definition D ND The sample data was reported from a diluted analysis. Not detected at indicated reporting limit. 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 Work Order Number: Delivery Container Type: Client Project ID: 01-02-0073 Cooler 101 South Union Avenue, Bakersfield, CA Date Received: Date Opened: Opened By: 02/02101 02/02101 JP I I I I I I I I I I I I I I I I I I I SAMPLE RECEIPT FORM Section A: Pass/Fail Criteria Comments 1. Chain of custody document(s) received with samples. 2. Sample container label(s) consistent with custody papers. 3, Sample container label(s) complete (10, date, time, taken by). 4, Sample container(s) intact and in good condition. 5, If applicable, proper preservation noted on sample label(s). 6, Sufficient sample volume received for analyses requested. 7. Correct containers used for analyses requested. 8. If applicable, VOA vials free of headspace. Yes Yes Yes Yes NA Yes Yes NA Section B: Additional Observations 1, Describe packing materials used in container. 2. Was sample container('s) sealed with custody seals? 3, Were all samples sealed in separate plastic bags? 4, Measured temperature inside delivery container when opened. 5. If delivery container shipped by third-party carrier, did container come with shipping slip, airbill, etc.? If YES, attach copy of shipping slip/airbill to the back of this form, 6. Do tedlar bags show condensation? Describe below if yes. 7. Are 25.1 condensate traps immersed in dry ice? 8. Are 25.1 sampling trains intact? 9. Are 25,3 condensate vials still attached to the sampling train? 10. Are 25,3 condensate vials on wet ice? NA No No 5.0 No °C NA NA NA NA NA Section C: Additional Comments 02/02/01 09:49:04 Generated in LlMS CALSCIENCE ENVIRONMENTAL - _RA"'S,I~ - - _ EiiWIVilienills IIIIfì CIiW1 Cìlliu~y iIIor" - - -- I Equiva Project Manager to be invoiced: Georgina E.Davila-DiMarco :::::'~Þ:!~Nt~H~ê~~¡(~~g~~y'~¡¡¡~ ;¿ It ¡(; 7440 Lincotn Way ttj$g~~C;Î{~)~~íN.i:~#.i~~1 Tech Services Tech Services DATE: ( Garden Grove, CA 92841-1432 r0T.EÄffl..itq.;~~.~Rý¡:~~.Š:~·:::·1 ::¡~If¡~r¡~~tj~~~~Wt*~fflMr~j: I .3 l:d:Ç~Í1#.i#9Ïii::<:::::::::~:1 PAGE: of (714) 895-5494 (714) 894-7501 fax Equiva Environmental Engineer: Ed Paden 1 3 5 0 7 4 CONSIA.rNT COMPANY: SirE ADORESS (StrHtand ClIy : IT Corporation 101 South Union Ave. (fi) Brundaoe AOORESS: Bakersfield CA. I 3452 E. Foothill Blvd. PROJECT CONTACT (R.port 10): P.trlck T. MeCua.ugh CONSULTANT PROJECT NO.: 822407 - 822/10 7 CITY: I Pasadena. CA SAMPlER NAME(S) (PrH): 11·.illl·.~.i TElEPHONE: I FAX: E-MAIL: L~( /<.eç.se ( I ~626) 304-1500 (626) 535-9076 lURNtROUND T1ME (BUSINESS DAYS): ....- o 10 pAYS 0 S DAYS 0 72 HOURS 0 48 HOU~0 24 HO~ lESS THAN 24 HOURS REQUESTED ANALYSIS o LA ¡ RWQCB REPORT FORMAT ~ - o UST AGENCY: iiì iiì iiì ;;; = = z N ¡¡; I '" '" II VI - ... AllL- N II II = Ó GCIMS MTBE CONF'RMA llON: HIGHEST HIGHEST per BORING N ~ U) :¡; ~ ;;; en FIELD NOTES: ~ l=- e VI VI ë .. u - SPECIAL INSTRUCTIONS OR NOTES: 1EMPERAnJRE ON RECEIPTC· Ê S õ .. w 0 S 0 > .. iiì Ê :E Container/Preservative (onÞ,-(VV\ 0.1) {)H~E ~~ Ê .. .. m l=- V! .. C .. .. E V! l- I- wI EP^82~ V! ;; C II Ê .e 0 - '" ! I or PID Readings iiì II '" ~ = :z 1ii ; ;; ~ '" "" c !!- - m or Laboratory Notes "" u:: ::; ... ... ~ N .. .. c 0 ~ >< VI - II = 0 0 0 'IS S Õ w :; :E II II ¡¡ + U u C ~ l- I- VI ¡;; ¡¡ ~ + .. .. .. m II. ! .. 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PROÆCT CONTACT tR.....Io):Potrlctl T~ -- CrTANTCOMI'ANY: ~: I aT: I ~~) 304-1500 L (626) 535-9076 mRNAROUND liME (BUSINESS DAYS): 0110 DAYS 0 5 DAYS 0 72 HOURS 0 48 HOURS 0 24 HOURS 0 lESS THAN 24 HOURS i q LA - RWQC8 REPORT FORMAT 0 UST AGENCY: GCJMS MTBE CONFIRMA liON: HIGHEST I SPECIAL INSTRUCTIONS OR NOTES: E.....IL: Pasadena, CA 3452 E. Foothill Blvd. ~\a(UI V "*' i)~rVn;~::i LL\" \"naln UI \.IUStoay KeCOra Equiva Project Manager to be invoiced: Georgina E.Davila-DiMarco :f¡~~!AA!\!t~~~~¢~~(~~g~~nU l:q~9~N~:~;~~~~4i~~1 Tech Services Tech Services I DATE: r~::~~::i~~~i~~;;~·;1 ';:$~:*n:~m~ffl~#ffl~~~*~~Mñ¡¡ PAGE: . ........................ E uiva Environmental En ineer: Ed Paden 4 srre ADDRESS CS1r..tl.d City): 2-œl Z- of .2 IT Corporation (714) 894-7501 fax (714) 895-5494 GardenGrove, CA 92841-1432 7440 Lincoln Way LABORATORIES, INC. .. 7440 Lincoln Way Garden Grove, CA 92841-1432 CONSU.jANT COMPANY: AODRESS: I aTV: I IT Corporation 3452 E. Foothill Blvd. Pasadena. CA ertt:\a(u~;~::;~a~M~~~~.~=;g.¡~r~ (;;~) 304-1500 I FAX: (626) 535-9076 I E-MAIL: 1URNtROUND liME (BUSINESS DAYS): o 10 DAYS 0 S DAYS 0 72 HOURS 0 48 HOURS 0 24 HOURS 0 lESS THAN 24 HOURS I o LA ¡ RWQCB REPORT FORMAT 0 UST AGENCY: I GClMS¡MTBE CONFIRMAll0N: HIGHEST SPECIAL INSTRUCTIONS OR NOTES: ilrRATORIES, I. ~uiv ct l:tj~9~i-í~:~:~~~~#.i~~1 ¡:Ëj 1~~tiiiiq¡~:~~~Y!:~~S::':::'1 (714) 895-5494 (714) 894-7501 fax ¡:dç~~~~~~{{{{:1 Tech Services - - .... Tech Services ::¡W:~:~~:~~¡~PM~ffi~j~~@,~~t~¡: 1-/1/6 I .3 or.3 , DATE: PAGE: Eauiva Environmental Engineer: Ed Paden SirE ADDRESS IStr..land clIy : 1 3 5 o 7 4 101 South Union Ave. tm Brundaoe Bakersfield CA. PROJECTCONTACT(Reportto~ SAMPLER NAIIE(S) (Pritt): L~[( kv;sfl./( CONSULTANT PROÆCT NO.: a22407 ~ZZ,<{c>7 ¡¡¡i¡t~.I, ~I.I.:" HIGHEST per BORING ALL_ 1EMPERA1URE ON RECEIPTC' . 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X 'X 'i. )( )( y 'X X- X Y X 'y: IX 1)( I'{ )<' '/. I\~ AI N'ý.,...ìì;;'\... I r I r I I I I ( ! 'Ie RøcøIvød by: (Slgna~ -"< ^ n Racølvød by: (Slgnabn) Racølvød by: (Slgnabn) -'- .)} ~A/~~ ...... REQUESTED ANALYSIS - iD ;;; .. CD N .. '" 0 ... FIELD NOTES: :!. ;;; en u I::- .. Õ "" iD w 0 Ê :IE Contaln..rlPr..s..",atlv.. .. E on ca l::- I- I- tD ! or PID Readings 0 .. :IE 1;; .. I .:r '" ca :!. - ... or Laboratory Notes :;; )( :; ... .. ... - .s õ w -; :IE co ¡; c ~ l- I- .. .. .. ID IL ! .. .. c .¡; Ü C) 0 " ... .. .. "C a- '" CD CD 0 :IE ... .. u U J: co is ¡; ~ ... 0 g I!. Ie J: Õ ~ > l- ii: ~ .. ~ ~ ~ ~ .2 .. c j! J: 0 0 0 0 1;; u .. I!. Q. Q. Q. Q. g .¡; co II:: .. .. .. .. CD w :IE I- > > > > l- . \,' Dat.: lime: "'\~O,I a~'. Qr5' Date: lime: Dî\ a<.,\~\ 11mø: O~ : aS- 10123/00 Revision ·1 I I I I I I I I I I I I I I I I ;'a/science ::: nvironmental Laboratories, Inc. February 06, 2001 Pat McCullough IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Subject:Calscience Work Order No.: 01-02-0075 Client Reference: 101 South Union Avenue, Bakersfield, CA Dear Client: Enclosed is an analytical report for the above-referenced project. The samples included in this report were received 2/2/01 and analyzed in accordance with the attached chain of custody The results in this analytical report are limited to the samples tested and any reproduction of this report must be made in its entirety. If you have any questions regarding this report, require sampling supplies or field services, or information on our analytical services, please feel free to call me at (714) 895-5494. 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 'I I !Ë a/science .;:: §nvironmenta/ Laboratories, Inc. ANALYTICAL REPORT ---.., I IT Corporation I 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0075 EP A 5030B EPA 8015M/8021B I Project: 101 South Union Avenue, Bakersfield, CA Lab Sample Number: Page 1 of 1 Client Sample Number: I I Parameter Benzene Toluene I Ethylbenzene Surrogates: I 1,4-Bromofluorobenzene I Parameter Benzene I Toluene Ethylbenzene Surrogates: I 1,4-Bromofluorobenzene ,- - ..... ,. , -.".. ,,,êthocJ.Blårik .... ......... ... . I Parameter Benzene I Toluene Ethylbenzene Surrogates: I 1,4-Bromofluorobenzene I Date Collecled: Matrix: Date Date Prepared: Analyzed: QC Batch ID: Result RL DF Qual Units 0.013 0.005 mg/kg 0.073 0.005 mg/kg 0.0087 0.0050 mglkg REC (%) Control Qual Limits 85 47-137 Parameter Result RL DF Qual Units Xylenes (total) 0.043 0.010 mglkg Methyl-tert-Butyl Ether 1.2 0.025 mglkg TPH for Gasoline 1.1 0.5 mglkg Surrogates: REC (%) 1 ,4-Bromofluorobenzene - FIO 78 Control Limits 34-141 Qual )·...N/A .....: ..,....,;....-.'-,.,...'. ,", ," . ··:\::-//Q2íO'2ió~;:./:.'::· :·Ø:~¡'~2020~-~.:::::<"· Result RL DF Qual Units Parameter Result RL DF Qual Units ND 0.0050 mg/kg Xylenes (total) ND 0.010 mglkg ND 0.0050 mglkg Methyl-tert-Butyl Ether ND 0.025 mglkg ND 0.0050 mglkg TPH for Gasoline ND 0.50 mg/kg REC (%) Control Qual Surrogates: REC(%) Control Qual Limits Limits 83 47-137 1,4-Bromofluorobenzene - FIO 76 34-141 ... ···,.O~8.:o1-00~-2,64'7N/A . 'Sòlid ... .. . ..",.. .-. ...,.,.-....-.-,. ;-......::.:-:,.',<>:..:-,.:.:-.,:-.:-.,',.,-:.':..'.'.,:........:.. . ......... ··,."A·< <.ó2¡ò2to1. .Q1()~ )~01'å>< ... Result RL OF Qual Units Parameter Result RL DF Qual Units ND 0.0050 mg/kg Xylenes (total) ND 0.010 mglkg ND 0.0050 mglkg Methyl-tert-Butyl Ether ND 0.025 mglkg ND 0.0050 mglkg TPH for Gasoline ND 0.50 mglkg REC(%) Control Qual SurroQates: REC (%) Control Qual Limits Limits 97 47-137 1,4-Bromofluorobenzene - FID 89 34-141 I RL - Reporting Limit, DF - Dilution Factor , Qual - Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: I I 02/02/01 I 01-02-0075 N/A I EPA 8260B ã a/science ::: §nvironmehtal Laboratories, Inc. ANALYTICAL REPORT Project: 101 South Union Avenue, Bakersfield, CA Client Sample Number: lab Sample Number: Matrix: Solid Date Collected: 02/01/01·,. Date Date Prepared: Analyzed: QC Batch ID: N/Ai>" tÎ2.J06/01Zj '()102Q5.A~·f' '" Page 1 of 1 I Parameter Surro!1ates: Result Rl DF 1300 10 2 REC(%) Control limits 101 80-120 101 81-117 96 74-121 Qual Units Methyl-tert-Butyl Ether uglkg I I Qual Dibromofluoromethane Toluene-d8 1,4-Bromofluorobenzene , "'èthôdBlank" .,' , 09.9.1Ô-ôô~h,923· '", '02lÖ6/Ø1/:::\,::':' 01'Ò20~ÀBS:::'; .. Parameter Result Methyl-tert-Butyl Ether ND Rl 5.0 DF Qual Units uglkg Qual I I I I I Surro!1ates: REC(%) Dibromofluoromethane Toluene-d8 1,4-Bromofluorobenzene 109 101 93 Control limits 80-120 81-117 74-121 I I RL - Reporting Limit, DF - Dilution Fador, Qual- Qualifiers I I 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-750 '1 I I I I I I I I I I I I I I I' ,I Ëi _a/science - EnVironmental Laboratories, Inc. Quality Control - Spike/Spike Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0075 EPA 5030B EPA 8015M/8021B Project: 101 South Union Avenue, Bakersfield, CA Spiked Sample ID 1~_~31)""" Matrix Date Prepared Date Analyzed MS/MSD Batch Number Instrument . ..0.-.·...__ ._'"..', . "-"" ."., .--. ............ ....-.. ,"' ... ......" . '-"-"-'..-"-",,".",-,",'" ·..··'sõnd .. ... "...,. ,..". <> :\':::::-'ci6::'2'1\':::'::: :-):::'<~>:/:: :«-'::·:::N:/Â~::t· .........., .. .············:··1 .~ -:;'''";''02iO"2iÖ1:':::';':/::':': <;::;'::h1:Ô~:6žö:1:iri~ , ... ,.. .".." . .... . . .:'-'->~.' Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers 93 93 46-136 1 0-15 91 89 45-138 2 0-18 92 90 62-121 2 0-17 92 90 53-130 3 0-17 94 91 64-120 3 0-13 97 92 24-144 5 0-23 97 96 44-122 0 0-30 Benzene Toluene Ethylbenzene p/m-Xylene o-Xylene Methyl-tert-Butyl Ether TPH for Gasoline 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 ¡¡ a/science :: n vironmen tal Laboratories, Inc. Quality Control - LCS/LCS Duplicate I ·1 I IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 101 South Union Avenue, Bakersfield, CA Instrument Date Prepared LCSIlCSD Batch Number 02/02/01 01-02-00751 EPA 5030B EPA 8015M/8021B I I Qualifiers I I I I I II I i I I II I I RPD CL Project: Parameter LCS %REC LCSD %REC %REC CL RPD Benzene 99 99 81-111 0 Toluene 96 96 81-111 0 Ethylbenzene 98 97 78-113 0 p/m-Xylene 98 98 70-118 0 o-Xylene 99 98 77-114 0 Methyl-tert-Butyl Ether 105 103 65-126 1 TPH for Gasoline 109 110 57-132 1 0-17 0-16 0-17 0-18 0-17 0-27 0-13 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501 'I I I I I I I I I I I I I I I I I .. a/science ;: pvironmentål Laboratories, Inc. Quality Control - Spike/Spike Du·plicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: Project: 101 South Union Avenue, Bakersfield, CA Spiked Sample ID Instrument Date Prepared Date Analyzed Matrix 02/02/01 01-02-0075 N/A EPA 82608 MS/MSD Batch Number Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers Benzene 104 102 72-127 2 0-25 Carbon Tetrachloride 97 94 70-130 3 0-25 Chlorobenzene 101 100 72-131 1 0-25 1,2-Dichlorobenzene 105 101 70-130 4 0-25 1,1-Dichloroethene 101 101 69-127 1 0-25 Toluene 100 99 75-124 1 0-25 Trichloroethene 101 102 60-137 1 0-25 Vinyl Chloride 101 99 70-130 2 0-25 Methyl-tert-Butyl Ether 87 85 80-120 2 0-25 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) B95-5494 · FAX: (714) 894-7501 · =alSCience tL: nvironmental Laboratories, Inc. Quality Control - LCS/LCS Duplicate· I· I I IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Project: Date Received: Work Order No: Preparation: Method: 101 South Union Avenue, Bakersfield, CA lCS Sample Number 1:()~~~1Ò"º(¡~H,Oî3'Y>.·. Date Prepared Date Analyzed ...., - - - . ,. ..... ... ............ ··Šc:>IÎét.·.· .....··.·.····..·..·...··.····GêIMSl.·..y·.>;· ·········Ní~············ ·········>..···....·.Ó2/0~;¡)1;··./ ····>............()1.Ö2.()$~AØ$. Matrix Instrument .... Parameter lCS %REC lCSD %REC %REC CL RPD 102 105 72-127 3 94 100 70-130 6 97 101 72-131 4 97 101 70-130 5 97 102 69-127 5 97 100 75-124 3 97 102 60-137 5 97 101 79-118 5 84 91 80-120 8 Benzene Carbon Tetrachloride Chlorobenzene 1,2-Dichlorobenzene 1,1-Dichloroethene Toluene Trichloroethene Vinyl Chloride Methyl-tert-Butyl Ether LCS/LCSD Batch Number RPD CL 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 0-25 02/02/01 01-02-007:1 N/Þ:. EPA 8260 ;.:",:-,:., ,:\ I ...-.'.,'.-.....;.- Qualifiers I I I I I I I I I I I I 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 I I I I I I I I I I I I I I I I I &-a/science GLOSSARY OF TERMS AND QUALIFIERS ~Environmenta/ Laboratories, Inc. Work Order Number: 01-02-0075 Qualifier Definition NO Not detected at indicated reporting limit. 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 Equlva Project Manager to be Invoiced: Georgina E.Davlla-DIMarco ·¡H¡il\l~ i*l\It~iiiÞ!iè.~i.t¡($$~~Il:~¡¡¡¡ 2/; lð / .................................................................... I 7440 Lincoln Way 1"0........··..····.... ....\ Tech Services Tech Services I DATE: I ;$q~~.ê;(~;®~~~i~~ Garden Greve. CA 92B41~1432 [0~~j~~:~~~Yi:i:~~.:?~·1 :[[~~¡~m~~¡~~#~~¡~*~~~Ð:¡¡ I I Itl..··············..··..î PAGE: of ~714) 895-5494 (714) 894-7501 fax : ç~~#9!f:::::}::::::: EQuiva Environmental Enaineer: Ed Paden 31 1 5 0 7 4 COt&SIA.TAjCOW'_: Sin! ADORI!SS II"'"' Iftd CIIy : IT Corporetlon 101 South Union Ave. @ Brundøae -I Bøkersfteld CA. 3452 E. Foothill Blvd. "",OJECT CONTACT ..........,:~.... T...edIeuth CONSU. T ANT "",OJECT NO.: 122.07 C11V: I - ?Z7.. Y07 Pasadena, CA SAIIPlER NAMEfSI PIfrf : ke.:;.;;-e ! .II.¡IIIIII~_II IB.EI'HONE: I FAX: I E-MAIL: ~(( (&26) 304-1500 (626) 535-9076 I 1\JRNA~OUND liME (BUSINESS DAYS): REQUESTED ANALYSIS ::J 10 DAYS 0 S DAYS 0 72 HOURS 0 48 HOURS o 24 HOURS 0 lESS THAN 24 HOURS I I i; m :J LA· RWQCB REPORT FORMAT o UST AGENCY: m m íñ . I <> Z - iê <> '" II .. N - I '" N II '" å .. :;ClMS M1BE CONFIRMA110N: HIGHEST HIGHEST per BORING N II ... FIELD NOTES: I ALL_ ~ ~ ., ;; ~ !::. íñ Õ .. " u - l'NSTRUCTIONS OR NOTES, TEMPERA "lURE ON RECEIPT CO .. J! ~ '5 .. w Ó ¡ J! > " m 2 Cont.'norlPro.orv.tIve Ê " " ... E UI !::. E l- i i " 2 '" I- '" ! or prD R.edlng. '" ;; E " ;; 2 1;; - , ;; m '" '" ... ~ .. UI or Leboratory Not.. ~ >- "" Ii ~ ::¡ ... .. - >0 " :;; .. ~ N " 0 8 .. "!I )( 2! .. - .. '" 0 u s I!! -; .. '11 II j ~ . . u " " i ~ I&. I- " .. ~ u m t r: ~ Ü UI ! 0 ° " w w .. It II u III e ::; CI '" II II - II II " '" " I- '" W ° 2 II. .,¡ U U :z: .. is ~ t 2! 2! -; N '" '11 ~ ~ 0 0 e: " ~ ... 'i > > ü: ... 0.. W - I&. '" :z: .. .e '" ~ ... ~ Is ~¡¡ I . . )( )( .. w .. i jJ :z: ° Field Sample Identification SAMPLING NO. 01' % % W I!! u III ~ U 0.. 00. 00. t 00. " IlAT"DI CONT. e: e: I- 0 I- 0.. 0 ~ II !; " " " II DATE TIME III CD > 2 W > w 2 > > > > ~ r':': 1 p- -1 2/, 172( ~ X ~ 'f- ...... r ::::: ~. a/I X 'f 'f .:';.:: I P-'t. - I l?zÇ ( .::::~: ::::::: I mw~ Wm¡ I i mm¡ I ....... mm~ I . :.:.:.: I ,¡,¡,¡. I ~~~¡~n .:.:.:. I ....... ....... H~~H~ ¡mm I mm~ I ^ I ^ TIme: :~ f1(S1rna1ln1 ~II /" ~o A Á 0 \<. R~ ..a by: (SIgna,"' 01": 1'\ 2.\-z.lo( ~~ . a~ ~'~ )( . "- TIme: 01": I......... by: (SItna'") ...... "- RICIhMd by: (SIgna,"' I -- DI"L\ðl;\ 0\ TIme: I .ISGN"'·) ~ RICIhMd by: ISD"I,"\.....)} ¿ 01', 0)- ~'-- --~~ . ~-- ~, I" \l./ 1012:VOO R_lan I ... I s_ WW¡¡¡¡¡ ""ort. GrHn to FIll, YIIow ItId PIIt to Ct"". I - - - - - - - - - - - - - - · '1 I I I I I I I I I ¡I II I I I II i I I if a/science ;;; gnvironmental Laboratories, Inc. February 06, 2001 Pat McCullough IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Subject:Calscience Work Order No.: 01-02-0074 Client Reference: 101 South Union Avenue, Bakersfield, CA Dear Client: Enclosed is an analytical report for the above-referenced project. The samples included in this .report were received 2/2/01 and analyzed in accordance with the attached chain of custody The results in this analytical report are limited to the samples tested and any reproduction of this report must be made in its entirety. If you have any questions regarding this report, require sampling supplies or field services, or information on our analytical services, please feel free to call me at (714) 895-5494. William H. Christensen Quality Assurance Manager 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 '1 I I I I I I I I I I I I I I I I ~ = alscience ::: Environmental Laboratories, Inc. Analytical Report Page 1 of 1 LABORATORY ID: 01-02-0074 Method: OOHS LUFT Organic Lead Matrix: Soil/Solid Results CLIENT: IT Corporation PROJECT: 101 South Union Avenue, Bakersfield, CA Sample 10 Organic Lead Dilution Date Date (mg/kg) Factor Extracted Analyzed SP-1.2.3 NO 1 02/06/01 02106/01 Method Blank NO 1 02/06/01 02/06/01 Reporting Limit: 1.0 I Quality Assurance and Control Information Matrix Sample Spike 10: SP-1.2,3 Batch 10: Spike LCS RPO 010206 Conc. Result Control ppm ppm Limits Organic Lead 25.0 21.5 0-20 Ke: Rec=Recove ND=Not Detected at the re ortin level 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 !Ë _a/science - nvironmental '- aboratories, Inc. ANALYTICAL REPORT 02/02/01 01-02-0074 Total Digestion EPA 6010B I I I I . I I I I I I I I I I I I I I I IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Client Sample Number: Project: 101 South Union Avenue, Bakersfield, CA Date Received: Work Order No: Preparation: Method: Page 1 of 1 Parameter Result Lead 18.4 i. Method Bíank Parameter Result Lead ND Lab Sample Number: 01~02-0074-4 RL 0.5 DF '.':.<:.',< Matrix: ..···Sol·¡i:t.. Date Collected: Date Prepared: Qual Units mglkg Qual Units mglkg RL - Reporting Limit 0 DF - Dilution Factor. Qual- Qualifiers 097-01-002-2,095 . RL 0.500 DF 02105/01 Date Analyzed: QC Batch ID: 02105/01' .··;()102ö5jê3a;:;· . 02105101 <0102051h3a 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 'I I s. =alSCienCe - pvironmental Laboratories, Inc. ANALYTICAL REPORT I IT Corporation .452 East Foothill Blvd., 9th Floor "asadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0074 EPA 5030B EPA 8015M18021B Iroject: 101 South Union Avenue, Bakersfield, CA Page 1 of 2 Client Sample Number: lab Sample Number: Date Collected: Matrix: Date Prepared: Date Analyzed: QC Batch ID: :§R:~'¡:::::::::::::::¡:::::::::::::::::::::::::::::::::::::::::¡\:':::::::::::::::::..::::::::::::::::.:::::::::::::::::::::::·::::::::::·::::::P1&á&P!¡f,1.:::::::I:::::::::::':':'::¡:9YP,1îª,::::::::::::::::~'~!,ª::::::{:::::::::::'~(i:::::::::::::::::'p,~r9~!~1::::¡::::::¡):P1P~P,#,Y'~!::::::::::::::::::::::::::·: larameter Result RL DF Qual Units Parameter Benzene ND 0.0050 mglkg Xylenes (total) tOlUene ND 0.0050 mg/kg TPH for Gasoline thy1benzene ND 0.0050 mglkg SurroQates: REC (%) Control Limits Qual SurroQates: ,4-Bromofluorobenzene 93 47-137 1,4-Bromofluorobenzene - FID Result RL DF Qual Units 0.033 ND 0.010 0.50 1 1 mglkg mglkg REC (%) Control Limits Qual 86 34-141 :.~Bt~::::::::::::::::·:::·:::::::::::::::::::::::::::'::::::::::::::':.::::::::::::::.:::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::·.P1W~PR!!f,~:::::::::::::::::::¡::::::.:~~!~~!iH::::::::::::::::·§·~\,~:::::::::::·::::::::::·.mi::::::::::::::::::·:¡·p,~(:~~!~1:::::::::::·P,1P~P~P1~!::::::¡::::::::::::::::::::. larameter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 mglkg Xylenes (total) 0.68 0.01 mglkg 10luene 0.044 0.005 mglkg TPH for Gasoline 25 0.50 mglkg thylbenzene 0.020 0.005 mglkg SurroQates: REC (%) Control Limits Qual S urroQates: REC (%) Control Limits Qual 1,4-BrOmOfluorobenzene 94 47-137 1 ,4-Bromofluorobenzene - FID 96 34-141 :'"i.!#:::::¡:::::::¡::¡:::::::::::::::::¡::::¡:::::::::::::::::¡::):::::::::::::::::::::::::::::::::::::¡:::::::::::::·:::::::::::::::::¡:::::::::::::::::::··P1P~$~r'M:::::::::::::::::¡::::::::::~I:~m~::::::::::::::::::::·§~!¡,,¡:::::::::¡·:·:::.:·::::¡·wi::::¡:::::::::::::;:::9~(9&!!::¡:::::::::::P:1P~~#'P1~':::::::::::::::::::::::::::: arameter Result Rl DF Qual Units Parameter Result Rl DF Qual Units ND 0.0050 mglkg Xylenes (total) 0.018 0.010 mglkg ND 0.0050 mglkg TPH for Gasoline ND 0.50 mglkg ND 0.0050 mglkg REC(%) Control Limits Qual SurroQates: REC (%) Control Limits Qual 72 47-137 1,4-Bromofluorobenzene - FID 67 34-141 lenzene oluene thy1benzene urro ates: ,4-Bromofluorobenzene I I RL - Reporting Limit, DF - Dilution Factor, Qual- Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 Project: 101 South Union Avenue, Bakersfield, CA Page 2 of 2 I I I I I I I I I I I I I I I I I I I Ë _a/Science - jlvironmental Ë aboratories, Inc. ANALYTICAL REPORT IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0074 EP A 50308 EPA 8015M/8021B Client Sample Number: Lab Sample Number: Date Collected: Matrix: Date Date Prepared: Analyzed: QC Batch ID: :"M~!~~~::~~~~~::::::::::¡:¡:¡:::¡::¡:::::::::::::::::::::::.:::¡:::¡::::::::::::::¡:::::::¡:::::¡::¡:::::::::::::::¡::::::::::i:··~~'~·1·~9.~S~~~!?::::I::¡::·:::::¡:::::::::·~!i:::¡:::::::::::::::::::::::·:~:~i.¡~:::::::::::¡:::::::::::::::::&i¡::::::::::::¡:¡::::::::::::::9,Y9.i(":::::::¡::::::::P1PªP~'~!::::::::::::::::::::::::::::: Parameter Result RL DF Qual Units Parameter Result Rl OF Qual Units Benzene NO 0.0050 mglkg Xylenes (total) ND 0.010 mglkg Toluene NO 0.0050 mg!kg TPH for Gasoline ND 0.50 mglkg Ethylbenzene NO 0.0050 mg/kg Surroç¡ates: REC (%) Control Limits Qual Surroç¡ates: REC(%) Control Limits . Qual 1,4-Bromonuorobenzene 97 47-137 1.4-Bromonuorobenzene - FID 89 34-141 RL - Reporting Limit. DF - Dilution Factor. Qual - Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 "I I I I I I I I I I I I I I I I I æ a/science ::: ¡virOnmental Quality Control- Laboratory Control Sample I.. aboratories, Inc. IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/02/01 01-02-0074 Total Digestion EPA 60108 Project: 101 South Union Avenue, Bakersfield, CA lCS Sample Number Matrix Instrument Date Analyzed lab File ID lCS Batch Number Parameter Cone Added Cone Recovered O/oRec %Rec CL Oualifiers Lead 50 53.7 107 80-120 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 Date Spiked Sample 10 Matrix Instrument Prepared 1':M'%~%hitii::·::'·::::::·:'·:::·:·:.':::::·:·:::·:::.':',:,::::.'.:':::.::::'.:::.:.::,:::.:-¡:.[.:.:.::::.::::::::·[:·',:::·'::::::':~~¡ia:-¡:::,::.:::·:·::·:::::::::,:,:::::'::'¿¿::~~·:;:.::'I·::::·:t:::.::·:::·:¡:-¡,·'&jÂ'::.::·'·::·:I·:·:,"::.¡·:::·::fóiih~ìJ~:.:':::::':'¡'::¡::::':::':':-¡:~'öióiöqMt:':¡::1 Date Analyzed I I I 02/02/01 I 01-02-0074 EPA 50308 I EPA 8015M/8021 8 I I I I I I I I I I I I I MS/MSD Batch Number ¡¡ _a/SCienCe ~Jlvironmenta/ Laboratories, Inc. Quality Control - Spike/Spike Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: Project: 101 South Union Avenue, Bakersfield, CA Parameter MS %REC MSD %REC %REC CL RPD RPD CL Oualifiers Benzene 93 93 46-136 1 0-15 Toluene 91 89 45-138 2 0-18 Ethylbenzene 92 90 62-121 2 0-17 p/m-Xylene 92 90 53-130 3 0-17 o-Xylene 94 91 64-120 3 0-13 TPH for Gasoline 97 96 44-122 0 0-30 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 "I I I I I I I I I I I I I I I I I !Ii _a/science - nvironmenta/ ... aboratories, Inc. Quality Control - LCS/LCS Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Project: Date Received: Work Order No: Preparation: Method: 101 South Union Avenue, Bakersfield, CA 02/02/01 01-02-0074 EPA 5030B EPA 8015M/8021B Date Date LCSILCSD Batch Parameter LCS %REC LCSD %REC %REC CL RPD RPD CL Qualifiers Benzene 99 99 81-111 0 0-17 Toluene 96 96 81-111 0 0-16 Ethylbenzene 98 97 78-113 0 0-17 p/m-Xylene 98 98 70-118 0 0-18 o-Xylene 99 98 77-114 0 0-17 TPH for Gasoline 109 110 57-132 1 0-13 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 Qualifier Definition I I I I I I I I I I Ii I I I I I I I I ~alSCience GLOSSARY OF TERMS AND QUALIFIERS - n vironmen tal . - Laboratories, Inc. Work Order Number: 01-02-0074 NO Not detected at indicated reporting limit. 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-750 -I I I I I I I I I I I I I I I I I I ;""'_aISCience GLOSSARY OF TERMS AND QUALIFIERS - j'vironmental £. aboratories, Inc. Work Order Number: 01-02-0074 Qualifier . Definition ND Not detected at indicated reporting limit. 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 Work Order Number: Delivery Container Type: Client Project ID: 01·02·0074 Cooler 101 South Union Avenue, Bakersfield, CA Date Received: Date Opened: Opened By: 02/02/01 02/02101 JP I' I I 1 1 I I I I 1 I I I I I I I 1 I SAMPLE RECEIPT FORM Section A: Pass/Fail Criteria Comments 1. Chain of custody document(s) received with samples. 2. Sample container label(s) consistent with custody papers. 3. Sample container label(s) complete (ID, date, time, taken by). 4, Sample container(s) intact and in good condition. 5. If applicable, proper preservation noted on sample label(s). 6. Sufficient sample volume received for analyses requested. 7. Correct containers used for analyses requested. 8, If applicable, VOA vials free of headspace, Yes Yes Yes Yes NA Yes Yes NA Section B: Additional Observations 1, Describe packing materials used in container. 2. Was sample container('s) sealed with custody seals? 3, Were all samples sealed in separate plastic bags? 4. Measured temperature inside delivery container when opened. 5, If delivery container shipped by third-party carrier, did container come with shipping slip, airbill, etc.? If YES, attach copy of shipping slip/airbill to the back of this form. 6, Do tedlar bags show condensation? Describe below if yes. 7. Are 25,1 condensate traps immersed in dry ice? 8, Are 25.1 sampling trains intact? 9. Are 25,3 condensate vials still attached to the sampling train? 10, Are 25,3 condensate vials on wet ice? NA No No 4.0 No DC NA NA NA NA NA Section C: Additional Comments 02/02/01 10:02:17 Generated in LlMS ~~) 304-1500 1 FAX: (626) 535-9076 ruRN~ROUND TIME (BUSINESS DAYS): o 10 DAYS 0 5 DAYS 0 72 HOURS 0 48 HOURS 0 24 HOURS 0 lESS THAN 24 HOURS I o LA - RWQCB REPORT FORMAT 0 UST AGENCY: I GClMS MTBE CONFIRMATION: HIGHEST I SPECIAL INSTRUCTIONS OR NOTES: !¡~!! I Field Sample Identification ~:'¡I:::;!:¡: I :::: :::: ::::.:::: m~¡~ ;¡¡f( I :H¡!!i~:: ¡m¡¡¡m ¡ mmm¡ ¡¡¡¡¡¡Wi I \;\;);\=¡\; I ¡¡¡¡¡¡¡m I ¡¡:¡W¡:¡ mmm¡ II) ~ /\ .~ y ,(SØfllmYJ? /7/ I J :¡ f-u Jot> Y ) )(() Á ...I 0 V I - I CONSU.jANT CO.....ANY: ADDRESS: I CI~ I _..~--. ""'. "'.,....~, ..,,"". - --- -.. - --- . ---- --.... ............ ~. .........~.'"''--¥ . ,,,,,"'. u - - - -"iva_ct~rt~voi~eor...Da__Mar..'t!~~_~M.;.:.:...:.:...;M~:H 7440 Lincoln Way :ëi$~~:~~~¡~~~i~G Tech SerVIces Tech Services Garden Grove, CA 92841-1432 r~~~~~:~.~~~~é·:::: 1.:¡~~:Rr:~~:~~~~~:Œ~r~ffl~t~:¡ (714) 895-5494 (714) 894-7501 fax lø!Íffl){~ijQf{:»~: ~ Equiva Environmental Engineer: Ed Paden SITE ADDRESS (Str..'.nd CIty : - PAGE: ~/ð -;- I of I . -- . DATE: . 1 3 5 o 7 4 IT Corporation 3452 E. Foothill Blvd. 101 South Union Ave. @ Brundaoe, Bakersfield CA PROJECT CONTACT (Report fa): ".trlck T. .cCUlough CONSUlTANT PROJECT NO.: 822<07 2'2-2, 0/" 7 !¡¡iatiliiiffiilllii¡ - Pasadena, CA SAMPlER NAMErS) (I'Ifrt): L6'WeU ke7sv( I e-MAIL: HIGHEST per BORING ALL_ TEMPERATURE ON RECEIPT C. REQUESTED ANALYSIS ~ - m m m v; 1:0 Z Ñ ¡¡; ~ 1:0 ID co .. ID N co 1:0 0 .. N co en FIELD NOTES: ~ ~ III ;; ~ l::- v; Õ .. .. u .. .s ¿ õ ... 0 Ê .s 0 > .. iõ w :II ContalnerlPreservatlve E .. .. ... E III l::- E l- I/') c .. .e I/') I- ID ~ or PID Readings '" C; i .. E 0 C; :II 1;; - I C; m 01 01 .:r .. III ~ "" "" ... c ~ - :; ... .. or Laboratory Notes ~ Ñ .. .. c 0 :a >( .. - co .. 0 0 0 ... S õ w '; ::IE It ;; u .. co :¡;¡ ~ + 0 .. .. c $ l- I- .. .. :ã J! + 1;; iõ t c .. III II. ! 0 0 If W W It fi Ü co u III III :; .. 01 It It - II II " Ii- ~ .. l- I- ID W 0 :II ... .; 0 0 :t: It Õ t '; N I/') ¡¡ ~ - 0 0 ... .. :> :II :II ~ ... :!. > > l- i! .. ... W - - II. .. :t: Õ II .e , , >( >( .. w I/') II C ! :t: .. .. .. .. 0 III < 0 .. 0 0 0 0 1;; :t: :r: w w ... ... ... ... Q. I!: I!: l- I- 0 I- ... 0 fi co a: .. If If If It III III > ::IE w > w :IE I- > > > > I- IX iìG IX 5f-( ~ ¡)- L ~p-- "3 SAMPLING DATE TIME -¿/, 152; -ili ~(¡() 31 'Þ30 "2- "2.- 'Z- MATRIX NO. OF CONT, v RICIIIwd by: (Sl \lIm) Dal.: TIme: <s; ^ {)(T--..., ~, Qt.1 0 I <J~:Q S- ,~ Roc"'" by: (SpUo Dalo: TIme: Roc"'" by: (SIpUo) ~k!"'f-" ~: <J'Lt C)\ TIm.: O~ ':. Ö.)- 10123100 Revlslon V by: (SI IIIm '- J R~ "I'..\y ~\ ~ I I DISTRIBUTION: WIlli...... final report, Groon 10 Fill, Yellow Ind Pint 10 Cion!. I · I I I I I I I I I I I I I I I I I = a/science ~ ænvironmentål Laboratories, Inc. February 20, 2001 Pat McCullough IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Subject: Calscience Work Order No.: Client Reference: 01-02-0744 101 South Union, Bakersfield, CA Dear Client: Enclosed is an analytical report for the above-referenced project. The samples included in this report were received 2/16/01 and analyzed in accordance with the attached chain-of-custody. The results in this analytical report are limited to the samples tested and any reproduction of this report must be made in its entirety. If you have any questions regarding this report, require sampling supplies or field services, or information on our analytical services, please feel free to call me at (714) 895-5494. 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 I I II _a/science LjJvironmental I aboratories, Inc. ANALYTICAL REPORT I IT Corporation ~452 East Foothill Blvd., 9th Floor .Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0744 EP A 50308 EPA 8015M/80218 ~roject: 101 South Union, Bakersfield, CA Page 1 of 4 Client Sample Number: Lab Sample Date Date Date Number: Collected: Matrix: Prepared: Analyzed: QC Batch ID: Parameter Result Rl OF Oual Units Parameter Result Rl OF Qual Units Benzene ND 0.0050 mglkg Xylenes (total) NO 0.010 mg/kg Toluene ND 0.0050 mg/kg Methyl-tert-ButyI Ether ND 0.025 mg/kg IEthylbenzene ND 0.0050 mg/kg TPH for Gasoline NO 0.50 mg/kg Surroç¡ates: REC (%) Control Limits Qual Surroç¡ates: REC(%) Control limits Qual ,4-Bromofluorobenzene 99 47-137 1,4-Bromofluorobenzene - FIO 95 34-141 Jarameter Result Rl OF Qual Units Parameter Result Rl OF QY!l Units Benzene NO 0.0050 mg/kg Xylenes (total) NO 0.010 mg/kg fOluene ND 0.0050 mglkg Methyl-tert-Butyl Ether NO 0.025 mg/kg . thylbenzene ND 0.0050 mg/kg TPH for Gasoline NO 0.50 mg/kg Surroç¡ates: REC (%) Control Limits Qual Surroç¡ates: REC (%) Control Limits Qual 1,4-BrOmOfluorobenzene 97 47-137 1,4-Bromofluorobenzene - FID 93 34-141 arameter Result Rl DF Qual Units Parameter Result Rl DF Qual Units ~enzene ND 0.0050 mg/kg Xylenes (total) NO 0.010 mg/kg oluene ND 0.0050 mg/kg Methyl-tert-B utyl Ether NO 0.025 mg/kg _thylbenzene ND 0.0050 mg/kg TPH for Gasoline ND 0.50 mg/kg REC (%) Control Limits Qual Surroç¡ates: REC (%) Control Limits Qual 103 47-137 1 ,4-Bromofluorobenzene - FID 99 34-141 I I RL - Reporting Limit, OF - Dilution Factor, Qual- Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501 == == · a/science '= nvironmental Laboratories, Inc. ANALYTICAL REPORT IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 02/16/01 01-02-0744 EPA 50308 EPA 8015M/80218 Date Received: Work Order No: Preparation: Method: Project: 101 South Union, Bakersfield, CA Page 2 of 4 I I I I I Client Sample Number: Lab Sample Date Date Date Number: Collected: Matrix: Prepared: Analyzed: QC Batch ID: ::'Î;~~~ç:i::::::::::'::::::::i::::::::::::':':::::::::::::::::':':i::;::::::::::i:::i::::'::::::::::::::::::::::::":::::':::':::::'::i:::::';::':::"·::'@':ffi~æ?;m~::,:,::::::'::::::::::':',::::::::'9.?J1~œ'::'::::::::::'::i:'::,:~'~¡¡i:::::::,:::':::::::':::::¡':,"N,(~:::::::::::::::::::'::::i::'Pî.f1!~9'-i:::i:i:::':::::~1#~:~'~P'!i.::::::::::::::::::I::::lil Parameter Result RL DF Oual Units Parameter Result RL DF Qual Units Benzene ND 0,0050 mg/kg Xylenes (total) ND 0.010 mglkg Toluene ND 0.0050 mglkg Methyl-tert-Butyl Ether ND 0.025 mglkg Ethylbenzene ND 0.0050 mglkg TPH for Gasoline ND 0.50 mglkg Surrogates: REC(%) Control Limits Qual Surrogates: REC (%) Control Limits Qual 1,4-Bromofluorobenzene 99 47-137 1 ,4-Bromofluorobenzene - FID 94 34-141 :::éêå::::::i,::iI:::i:¡i¡':::::,:::::¡:::'::':':::::':::;i:::::¡::¡:'::::,'::¡:'::¡¡,:::::::::,::¡::i:::::::::',:::::::¡:;.:¡:::::¡:::¡¡::¡':::¡:::'91:ffi~wîli:::::'¡¡:':,:::::I::::::,::'pì~1~m':,:::::::::::¡:::':~~"~:::::::::::::":::¡:':·:'.@~:¡:::i:::¡:;:i'::':::¡::::¡¡~P1~!'!~¡::I:¡¡:::::~1P~:î~y,!¡::¡::::::::::'i::¡:::¡::¡:: Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 mglkg Xylenes (total) ND 0.010 mglkg Toluene NO 0.0050 mglkg Methyl-tert-Butyl Ether ND 0.025 mglkg Ethylbenzene NO 0.0050 mglkg TPH for Gasoline NO 0.50 mglkg Surrogates: REC(%) Control Limits Qual Surrogates: REC(%) Control Limits Qual 1,4-Bromofluorobenzene 94 47-137 1 ,4-Bromofluorobenzene - FID 89 34-141 i::rª~i::::::;:¡:!!::!¡:¡¡¡::!::::::::::'::::::!:;!::!:::;¡:,!,:,i:,¡i:!:¡!:':,:'i::,::::i::'::::::·¡::':':¡:::i::i:i::':i:i::::::::::::::::::i:::::'i::::::::,':@1'ffi~wîl~::¡:::,::,::::¡;::::::,:::::'~~1im~:¡i:::':::i'::::::,:::~:Mªi!::::':':':::,:::I::::,"g::::,::::::::::::¡i::::::i:~~?"l{~1::::::i::!:!::::i1P~:':~Y'¡'Î:::::::::::::::::::i::'!:::: Parameter Result RL OF Qual Units Parameter Result RL OF Qual Units Benzene NO 0.0050 mglkg Xylenes (total) NO 0.010 mglkg Toluene NO 0.0050 mglkg Methyl-tert-ButyI Ether ND 0.025 mglkg Ethylbenzene NO 0.0050 mglkg TPH for Gasoline ND 0,50 mglkg Surrogates: REC C%) Control Limits Qual Surrogates: REC (%) Control Limits Qual 1,4-Bromofluorobenzene 93 47-137 1,4-Bromofluorobenzene - FID 89 34-141 RL - Reporting Limit. DF - Dilution Factor, Qual - Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-750 I I II I I I I I 'I I I I I I II a/science ~ ntiironmenta/ Laboratories, Inc. ANALYTICAL REPORT II I IT Corporation 83452 East Foothill Blvd., 9th Floor Irasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0744 EPA 50308 EPA 8015M/80218 "roject: 1 01 South Union, Bakersfield, CA Page 3 of 4 Client Sample Number: Lab Sample Date Date Date Number: Collected: Matrix: Prepared: Analyzed: QC Batch 10: ~arameter Result RL OF Qual Units Parameter Result RL OF Qual Units enzene NO 0.0050 mglkg Xylenes (total) NO 0.010 1 mglkg Toluene NO 0.0050 mglkg Methyl-tert-Butyl Ether 0.13 0.02 1 mglkg ~thylbenzene NO 0.0050 mg/kg TPH for Gasoline NO 0.50 1 mglkg urroQates: REC (%) Control limits Qual SurroQates: REC (%) Control limits Qual ,4-Bromofluorobenzene 97 47-137 1,4-Bromofluorobenzene - FIO 93 34-141 lara meter Result RL OF Qual Units Parameter Result RL DF Oual Units Benzene NO 0.0050 mg/kg Xylenes (total) NO 0.010 mg/kg 'Oluene NO 0.0050 mg/kg Methyl-tert-Butyl Ether NO 0.025 mglkg thylbenzene NO 0.0050 mglkg TPH for Gasoline NO 0.50 mglkg SurroQates: REC(%) Control limits Oual SurroQates: REC (%) Control limits Oual 1,4-BrOmOfluorobenzene 95 47-137 1,4-Bromofluorobenzene - FIO 91 34-141 :::~+,iiî:;:::;¡;:::¡:;:::::::':::¡:::::::::::;::::,:':::::::::::::;:::::;:::::::::::,,::::::::::;:;:;:;::¡':::;:::::;;:::::;:::::':::::::,':,::::;;:;:::;:'::::::,:::':;';:::#:1'm~~iHf!',:::i:,i::::::¡,::¡::,i';:i:¡¡~Ü1!ø~:¡¡:::¡::::::'::'::::;:#:~!!!:::'::;;;:::::.::::'::';:¡@~::::;:::;::::::::::::::::::~#,¡'1l!~1::::::::¡:;::::i1P,!':~~Œ~~:::¡:j::::¡::;::j¡::;:t;· arameter Result RL DF Qual Units Parameter Result RL DF Qual Units _enzene NO 0.0050 mg/kg Xylenes (total) NO 0.010 mg/kg oluene ND 0.0050 mg/kg Methyl-tert-Butyl Ether NO 0.025 mglkg thylbenzene NO 0.0050 mgfkg TPH for Gasoline NO 0.50 mglkg REC(%) Control limits Qual Surroç¡ates: REC (%) Control Limits Qual 95 47-137 1 ,4-Bromofluorobenzene - FIO 91 34-141 I I RL - Reporting Limit, OF - Dilution Factor. Qual- Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501 E _a/science .. nvironmental Laboratories, Inc. ANALYTICAL REPORT IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0744 EPA 50308 EPA 8015M/80218 Project: 101 South Union, Bakersfield, CA Page 4 of 4 Client Sample Number: Lab Sample Number: Date Date Prepared: Analyzed: ac Batch ID: Date Collected: Matrix: ::M~1~9.~'§t~ht:,::::::::::::::::::::::::::::::::::::::::@::,:::::j::::::::::::',:¡:':::::::::':::'::"::::::::::::::::::::'::::::·:·9~!89·1:ffi91~~;ÆAA:':::::::::::::'::'::::::::·~(í:',:'::::::::::::::::::::·:::::~P:!i~;::::::::::::::::::::::::::::::"~(í::':::::::::::::::::'::::::::º,P:1itq':::'::::::::::::P19~:':M'~~::::::::::::::::::::::::::::. Parameter Result RL DF Oual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 mg/kg Xylenes (total) ND 0.010 mg/kg Toluene ND 0.0050 mglkg Methyl-tert-Butyl Ether ND 0.025 mglkg Ethylbenzene ND 0.0050 mglkg TPH for Gasoline ND 0.50 mglkg SurroQates: REC (%) Control Limits Qual SurroQates: REC (%) Control Limits Qual 1,4-Bromofluorobenzene 102 47-137 1 ,4-Bromofluorobenzene - FID 99 34-141 RL - Reporting limit. DF - Dilution Factor. Qual - Qualifiers 7440 Lincoln Way. Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-750 II II I I I I I I I I I I I I I I I I I I I IT Corporation f452 East Foothill Blvd., 9th Floor asadena, CA 91107 ~ -a/science I:; nvironmental Laboratories, Inc. ANALYTICAL REPORT Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0744 N/A EPA 8260B Client Sample Number: reject: 101 South Union, Bakersfield, CA Page 1 of 1 Parameter lethYI-tert-ButYI Ether SurroQates: libromofluoromethane oluene-d8 1,4-Bromofluorobenzene r..~tHþèfBìélnk··;,/:>:;,;,!, Parameter lethYI-tert-ButYI Ether SurroQates: libromofluoromethane oluene-d8 1,4-Bromofluorobenzene I I I I I I lab Sample Number: Date Date Date Collected: Prepared: Analyzed: QC Batch ID: Solid" .02115/.01 N/A02l19io,1{ '()1ó~19AS ' , .01-.02-.0744-7 Result Rl 5 DF Qual Units 81 uglkg REC(%) 104 103 99 Control limits 80-120 81-117 74-121 Qual ~".'-';':'. ", -', \~:«::-:<:::1: :::'::;,:'\(ri:{-'F) " :;;:><~;~;;;. ..' ',! ..... º~9:11?~.o()5-1;~)7~« ..... 's¿lid<); .N/ÍJ.:f';j'{ >o211'9¡ò'!<i;\:.~,o1ô21'9AsY:'{·; Nil') ~,- :';'-'.: ..", f'~:' .' .---,-.;, ,,"' '.<\:,':':':":'.'-", ":"-~ ".><. Result RL DF Qual Units ND 5.0 uglkg REC (%) Control Qual limits 105 80-120 102 81-117 100 74-121 RL - Reporting Limit, DF - Dilution Factor, Qual - Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0744 EPA 5030B EPA 8015M/8021B I I I I I I II I I I I .. I I I I I I Iii a/science ~::, J1vironmental Laboratories, Inc. Quality Control - Spike/Spike Duplicate Project: 101 South Union, Bakersfield, CA Date Date Analyzed MSIMSD Batch Spiked Sample ID Matrix Instrument Prepared Number Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers Benzene 95 95 46-136 0 0-15 Toluene 92 92 45-138 0 0-18 Ethylbenzene 94 94 62-121 1 0-17 p/m-Xytene 94 95 53-130 1 0-17 o-Xytene 95 96 64-120 1 0-13 Methyl-tert-ButyI Ether 88 90 24-144 2 0-23 TPH for Gasoline 107 106 44-122 0 0-30 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 I I I I I I I I I I I I I. !. I I I ~ =alSCienCe . - nvironmental Laboratories, Inc. Quality Control - LCS/LCS Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0744 EPA 5030B EPA 8015M/8021B Project: 101 South Union, Bakersfield, CA Date Date lCSIlCSD Batch LCS Sample Number Matrix Instrument Prepared Analyzed Number ::9~~2M:St!9~2~;~:i::::::::::.::::I::::::·::::::::·::·::::::::::::::::::::.:.:·:::·::::;:;:::;::::§è'~:::·::::::::::;:::::::::::.::·::::§Ç:~:1::::::::·::::::::::::::::::::i::::ÑtÅ::::::::::::::::::::::'::::::::::::"qir1~{9'·::::::::::::::::::::::::::::::::::::::::::::P19~:1·~P.'~':¡:::::::::::¡:::::::::::::¡:::::::::::::¡:::::: Parameter lCS %REC LCSD %REC %REC CL RPD RPD Cl Qualifiers Benzene 96 97 81-111 1 0-17 Toluene 93 94 81-111 1 0-16 Ethylbenzene 94 96 78-113 1 0-17 p/m-Xylene 95 96 70-118 1 0-18 a-Xylene 96 97 77-114 1 0-17 Methyl-tert-Butyl Ether 100 98 65-126 1 0-27 TPH for Gasoline 107 105 57-132 2 0-13 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501 ~ =alSCienCe - j'vironmental Laboratories, Inc. Quality Control - Spike/Spike DuplOicate 02/16/01 01-02-0744 N/A EPA 82608 I I I I I I I I II I I. I I I I I 1 I IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: Project: 101 South Union, Bakersfield, CA Spiked Sample ID Date Prepared Date Analyzed Matrix Instrument MS/MSD Batch Number Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers Benzene 99 101 72-127 2 0-25 Carbon Tetrachloride 98 106 70-130 9 0-25 Chlorobenzene 100 101 72-131 1 0-25 1,2-Dichlorobenzene 98 98 70-130 1 0-25 1,1-Dichloroethene 94 100 69-127 6 0-25 Toluene 99 101 75-124 2 0-25 Trichloroethene 113 117 60-137 3 0-25 Vinyl Chloride 91 86 70-130 6 0-25 Methyl-tert-Butyl Ether 95 98 80-120 3 0-25 7440 Lincoln Way, Garden Grove, CA 92841·1432 · TEL: (714) 895-5494 · FAX: (714) 894·7501 I I I I I I I I I I I I I I I I I II _a/science ... nvironmental I aboratories, Inc. Quality Control - LCS/LCS Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0744 N/A EPA 8260B Project: 101 South Union, Bakersfield, CA lCS Sample Number Matrix Parameter lCS %REC lCSD %REC %REC Cl RPD RPD Cl Qualifiers Benzene 101 99 72-127 2 0-25 Carbon Tetrachloride 111 112 70-130 0 0-25 Chlorobenzene 102 102 72-131 0 0-25 1,2-Dichlorobenzene 100 101 70-130 2 0-25 1,1-Dichloroethene 91 96 69-127 6 0-25 Toluene 102 101 75-124 1 0-25 Trichloroethene 103 101 60-137 2 0-25 Vinyl Chloride 91 94 79-118 3 0-25 Methy/-tert-Butyl Ether 97 99 80-120 2 0-25 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 Qualifier Definition I II I I Ii I I I I I I' I i I I .1 I I I I I,,;alscience GLOSSARY OF TERMS AND QUALIFIERS I::, nvirorimenfal L aborafories, Inc. Work Order Number: 01-02-0744 ND Not detected at indicated reporting limit. 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-750 I I I I I I I I I I I I I' I I I I I I SAMPLE RECEIPT FORM Work Order Number: Delivery Container Type: Client Project 10: 01·02·0744 Cooler 101 South Union, Bakersfield, CA Date Received: Date Opened: Opened By: 02/16/01 02/16/01 JP Section A: Pass/Fail Criteria 1. Chain of custody document(s) received with samples, 2. Sample container label(s) consistent with custody papers. 3. Sample container label(s) complete (10, date, time, taken by), 4. Sample container(s) intact and in good condition. 5. If applicable, proper preservation noted on sample label(s). 6. Sufficient sample volume received for analyses requested. 7. Correct containers used for analyses requested, 8. If applicable, VOA vials free of headspace. Comments Yes Yes Yes Yes NA Yes Yes NA Section B: Additional Observations 1. Describe packing materials used in container. 2. Was sample container('s) sealed with custody seals? 3. Were all samples sealed in separate plastic bags? 4. Measured temperature inside delivery container when opened. 5, If delivery container shipped by third-party carrier, did container come with shipping slip, airbill, etc.? If YES, attach copy of shipping slip/airbill to the back of this form. 6. Do tedlar bags show condensation? Describe below if yes. 7. Are 25.1 condensatè traps immersed in dry ice? 8. Are 25.1 sampling trains intact? 9. Are 25.3 condensate vials still attached to the sampling train? 10. Are 25.3 condensate vials on wet ice? NA No No 4,0 No °C NA NA NA NA NA Section C: Additional Comments 02/16/01 11:36:26 Generated in LlMS R.tinq~ ~ \Û~-::. y.UOW and Pink to CII.nl. ~~~ Dot.: '2.. \ ' \o~J ~~'.~~ 'iõiñiõõ"R:'vtslon ReceIv.d by. (Signal....) Tlmo: Field Sample Identification ~,¡ q I'ò, " ( 2/15/01 2/15/01 2/15/01 2/15/01 2/15/01 2/15/01 2/15/01 2/15/01 2/15/01 SAMPLING DATE I TIME 1525 1430 1345 1425 1410 1300 1440 1005 1420 R.ceiv.d by. (Signature) 1 1 1 1 1 1 1 1 .1 1 R.celv.d by: (Sig;;'.t...) MATRIX NO. OF CONT. Ê II> ... o !!? .. :¡; .. .. '" = Q. , ::J: a.. I- ...,; X X X X X X X X X X X \ tt:::::- Ê 10 ... o !!? .. :¡; ¡¡ u ~ x iii , ::J: Q. I- X X X X X íi ... N o !!? iii III I- :E - >< iii I- III X íi o '" '" !!? .. ! .. c Q '" >- " o + iii III I- :E - >< iii I- III X x x I o LA - RWQCB REPORT FORMD UST AGENCY: GClMS MTBE CONFIRMATION: HIGHEST_ SPECIAL INSTRUCTIONS OR NOTES: HIGHEST per BORING _ ALL_ TEMPERATURE ON RECEIPT C' r íi o '" N !!? .. ! .. c Q '" >- " o + .. .. :¡ "5 II. .. U o > X X X X X X X X X ~ .. ~ .. õ > ~ .2 c o :e ~ " iii 10 I') o 10 oct a.. iii õ z Q .. I/) ë .2 ~ E æ c o u íi o ... N !!? iii III I- :E X íi ... N o !!? ~ .. E o ~ "CI ! .. c .. '" o ¡¡; ::J: .. U o > m '" .. o !!? Õ c .. oS Q :!: Õ c .. .:: Iii ~ u Q &:I. !!!. .. ¡¡; t :E ... ~ ~ ::J: a.. II: I- iõ ... Ò t:- iii III I- :E >< iii I- III .. U o > Õ &:I. .. > Dol.: Dol.: iõ ... Ò - I- E - ... .. ... :S ~ = :E ::I l- II. I/) oct .. - U ::J: o a.. > I- o (; &:I. &:I. .. .. > > 1/r~1 0 ô '"t III ... ¡¡; .. o c. .. is ~ .a .. .. Q I- ii" .. en C :E l- I/) $ .. .. .. .. C "CI .. " ¡¡: Õ &:I. .. > ¡ ... N ~ " .. .!! ¡; o >- õ CD c !!? .. ill u "- TIm.: O~ :crv TiiñÕ: Container/Preservative or PID Readings or Laboratory Notes FIELD NOTES 626-304-1500 C 626-535-9076 TURNAROUND TIME (BUSINESS DAYS): o 10 DAY!!] S DAYS 0 72 HOUR:(J 48 HOURS ~ 24 HDURS E-MAIL: o LESS THAN 24 HOURS REQUESTED ANALYSIS CITY: 1 IT Corporation 3452 E. Foothill Boulevard, 9th floor Pasadena, CA 91107 ADDRESS: (714) 895-5494 CONSULTANT COMPANY: Garden Grove, CA 92841-7501 (714) 894-7501 fax Equiva Project I'c' .................... : .. $q~Ñ~:~:~~~ l:elT~CA:6.iiM#~::::::~ 't):cRl¥:ff.~~Q~ : Mark Passarini - Tech Services Ed Paden -Environmental Engineer SITE ADDRESS (streot and CIty): 101 South Union Avenue. Bakersfield, CA 93307 PROJECT CONTACT (Ropott ID : Pat McCullough SAMPLER HAME{S) (Print): Lowell Kessel 1 CONSULTANT PROJECT NO.: 822407 :-~~/$~ ~ I~ i~ ~i ~II'II! ~ ~ ; : ~ DATE: PAGE: ;;¿jJJ'!!/ { of ( 7440 Lincoln Way ----- -CAL~NClIMIRO~TAL- - - LABORATORIES,INC Manager to be invoiced mul~e.llJ!esm: c!9!Iin Mark Pas ePtullØdy.oP - - -. I I I I I I I I I I I I I I I I I iíË _a/science - Environmental Laboratories, Inc. February 22,2001 Pat McCullough IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Subject: Calscience Work Order No.: Client Reference: 01-02-0745 101 South Union, Bakersfield, CA Dear Client: Enclosed is an analytical report for the above-referenced project. The samples included in this report were received 2/16/01 and analyzed in accordance with the attached chain-of-custody. The results in this analytical report are limited to the samples tested and any reproduction of this report must be made in its entirety. If you have any questions regarding this report, require sampling supplies or field services, or information on our analytical services, please feel free to call me at (714) 895-5494. Wilram H. C Istensen Quality Assurance Manager 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 I I I I I I I I I I I I I I I I I E _a/science -. pvironmental Laboratories, Inc. Analytical Report Page 1 of 2 LABORATORY ID: 01-02-0745 Method: EPA 418.1 M TRPH Matrix: Soil/Solid CLIENT: PROJECT: IT Corporation 101 South Union, Bakersfield, CA Results Sample ID TRPH Dilution Date Date (mg/kg) Factor Extracted Analyzed H-1-10 ND 1 02116/01 02116/01 SP-3 ND 1 02116/01 02116/01 Method Blank ND 1 02116/01 02116/01 Reporting Limit: 10 Quality Assurance and Control Information Matrix Spike Sample ID: 01-02-0740-6 Batch ID: 02160101 Spike Cone. ppm RPD Control Limits TRPH 200 0-30 Ke: Rec=Recove ND=Not Detected at the re ortin level 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 ¡¡ a/science I:, nvironmental Laboratories, Inc. Analytical Report Page 2 of 2 I I LABORATORY ID: 01-02-0745 Method: EPA 7421 Total Lead Matrix: Solid/Soil IT Corporation 101 South Union, Bakersfield, CA B-G-4 Method Blank 0.27 NO 1 1 02116/01 02116/01 Reporting limit: 0.25 Matrix Spike Sample 10: Batch 10: 0102161 B-G-4 Spike Cone. ppm LCS Result ppm Total Lead 0.025 0.0271 · The MS/MSD associated with this batch of samples was out of control due to a matrix interference effect. The associated batch LCS/LCSD was ¡ncontrol and, hence, the associated sample data was reported with no further corrective action required, Ke: Rec=Recove ND=Not Detected at the re ortin level 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 I I I I I I I I I I I I I I I I I jf a/science ::: nvironmental I. aboratories, Inc. Analytical Report Page 3 of 4 LABORATORY ID: 01-02-0745 Method: Acute Aquatic Bioassay Matrix: Soil/Solid CLIENT: PROJECT: IT Corporation 101 South Union, Bakersfield, CA Results Test Species: Mean Length: Mean Weight: T est Period: Note: Fathead minnows (Pimephales promelas) 39mm 0.41 gm 02/16/01 - 02/20/01 All results represent percent mortality after 96 hours. Sample ID 750 mglL 250 mglL SP-3 0% 0% Laboratory Notes 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 il =alSCience - Environmental Laboratories, Inc. Analytical Report Page 4 of 4 ,II . I I lABORATORY ID: 01-02-0745 ~ Method: Inorganic Constituents Matrix: Soil/Solids IT Corporation 101 South Union, Bakersfield, CA SP-3 Method Blank ND ND ND ND 8.50 NA 1 1 I EPA Method: Date Analyzed: Reporting Limit: SW-846 Chapter 7 02119/01 0.5 SW-846 Chapter 7 02119/01 0.5 . Laborato Control Sample/Laborato Control Sample Duplicate Reactive Cyanide Du licate Sample ID: SP-3 Reactive Sulfide Duplicate Sample ID: 01-02-0751-1 pH Ke: ND=Not Detected at the re ortin level NA=Not a licable 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 I I E _a/science 't:: nvironmental Laboratories, Inc. ANALYTICAL REPORT I IT Corporation .452 East Foothill Blvd., 9th Floor ~asadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0745 Total Digestion EPA 6010B / EPA 7471A Iroject: 101 South Union, Bakersfield, CA Page 1 of 2 Client Sample Number: Lab Sample Date Date Date Number: Collected: Matrix: Prepared: Analyzed: QC Batch ID: ,·tlf':~1!:::::::::'::·'::,:::,:::::::::::::::::::::::,: ":::::::'::::::::::'::::::::::::::::':::::::::,:::::::::::::::::::::::':::::::::::::::,91Â~3i?¡*1.:::::::::::':::::::'::::::'·9ìt1~ì9,1::::::::::::::·:-::~M\~::':·:::::'::::"9Y1~ì9,':::::::::::::::::::9Y:1iì~~:::::::::::::::!19~:j'~J~P:::::::::::::::::::::::;::::::: Mercury was analyzed on 2/19/01 10:43:24 AM with batch 01 02161cs3 Result RL DF Qual Units Parameter Result RL DF Qual Units I Comment(s): arameter Antimony _rsenic arium eryllium Cadmium íhromium (Total) obalt opper Lead 1.22 0.75 mglkg Mercury ND 0.0835 1 mglkg 10.6 0.7 mglkg Molybdenum ND 0.250 1 mglkg 157 0.500 mglkg Nickel 12.2 0.2 1 mglkg 0.406 0.250 mglkg Selenium ND 0.750 1 mglkg ND 0.500 mglkg Silver ND 0.250 1 mglkg 19.4 0.2 mglkg Thallium ND 0.750 1 mglkg 10.1 0.2 mglkg Vanadium 51.7 0.2 1 mglkg 15.1 0.5 mglkg Zinc 60.0 1.0 1 mglkg 5.21 0.50 mglkg ;~g*:':';:::::':::'i':'::':::"::':'::'::::::'::::::'i::::::.::::::::.::.:::.:.:::,::':.:;::':.:':':.::.:::::::::.:·::·:::::·:·:·:::·:·:·:·:::·:::::.::::91m~&!~¡~:.:·:::·::(:·::¡:::::·:::::PY1~f:~1.::::':·:::·:::::::§:~i¡~::·:::.::::::::::PY·1~f:~î:;::·:.:·::::::~i!1!&':::::::;::::~·~9~l~·i~!@:::::·:::::::·::\::\:::;:: Comment(s): Mercury was analyzed on 2/19/01 10:46:36 AM with batch 01 02161cs3 arameter Result RL DF Qual Units Parameter Result RL DF Qual Units nt¡mony ND 0.750 mglkg Mercury ND 0.0835 1 mglkg Arsenic 7.42 0.75 mg/kg Molybdenum ND 0.250 1 mglkg ,arium 123 0.500 mglkg Nickel 9.15 0.25 1 mglkg eryllium 0.328 0.250 mglkg Selenium ND 0.750 1 mglkg admium ND 0.500 mglkg Silver ND 0.250 1 mglkg Chromium (Total) 15.0 0.2 mglkg Thallium ND 0.750 1 mglkg íObalt 8.16 0.25 mglkg Vanadium 39.7 0.2 1 mglkg opper 12.8 0.5 mglkg Zinc 48.2 1.0 1 mglkg ead 4.71 0.50 mglkg :::M~y.Æ~:it~~~::::::::::::,::::::::::::::::::::::::::::¡::::::::::::::::::::::::::::::::::::::::::::::::::::::::::¡:::::¡:::::::::::::::::::::::::::::::p~~ffi!æ91.~Ì!~::::::::::::::::::::::::':::::::;@i:::::::·:::::::::::::::::::::"~'m!j:::::,::::::::::::':'9#'{1~m'::::::::::::tt¡~P1!(!~::::i::::::::::!1P~1~í~~!:::::::::::::::¡:¡:::::::::':::: Parameter tercury Result RL DF Qual Units ND 0.0835 mglkg I I RL - Reporting Limit. DF - Dilution Factor, Qual - Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 Project: 101 South Union, Bakersfield, CA Page 2 of 2 I I I I I I I I I I I I, I I I I I I I S _a/SCience ä::En vironmen tal Laboratories, Inc. ANALYTICAL REPORT IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0745 Total Digestion EPA 60108 / EPA 7471A Client Sample Number: Lab Sample Number: Date Collected: Matrix: Date Date Prepared: Analyzed: QC Batch 10: ;:::M~m#.~::~i~h!::::::::::::i::::::::::::::::::::::::¡=::::::::::::i.:::::::Ii:i::i:=:ii:::::i¡¡II:::::::::¡:::::::::¡i:i::i::::::::¡:::·~~Íæ:1·&9.~~~;:@~=::::¡'¡::::::::::,:,:':::::~~i:i¡:::::¡::::i::i:::::::::::¡:~:þ"~::::::::':::i::::::;;9.&1~î9,':::::::i::::::¡::::::=~lil:~~::::::¡:::::::::!l~~:í~!~i::::::::::::::::::::¡:i:¡::::¡: Parameter Result RL OF Qual Units Parameter Result RL OF Qual Units Antimony NO 0.750 mglkg Molybdenum NO 0.250 1 mglkg Arsenic NO 0.750 mglkg Nickel NO 0.250 1 mglkg Barium NO 0.500 mglkg Selenium NO 0.750 1 mglkg Beryllium NO 0.250 mglkg Silver NO 0.250 1 mglkg Cadmium NO 0.500 mglkg Thallium NO 0.750 1 mglkg Chromium (Total) NO 0.250 mglkg Vanadium NO 0,250 1 mglkg Cobalt ND 0.250 mglkg Zinc ND 1.00 1 mglkg Copper NO 0.500 mglkg Lead ND 0.500 1 mglkg RL - Reporting Limit. DF - Dilution Factor. Qual - Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 . TEL: (714) 895-5494 · FAX: (714) 894-7501 I I . -a/science I:; nvironmental Laboratories, Inc. ANALYTICAL REPORT I IT Corporation .,452 East Foothill Blvd., 9th Floor lJ'asadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0745 EPA 50308 EPA 80218 JrOject: 101 South Union, Bakersfield, CA Page 1 of 1 Client Sample Number: Lab Sample Number: Date Collected: Matrix: Date Prepared: Date Analyzed: QC Batch ID: .;HSÙ~~W::::i::::::::::{:::,:::i·:·::::::::::,::,:i..:::,,:;::::;:":,,::::,;:;::':::,':, ,,::,,:;::,:,:;?:::?: :::;:¡:::::·p'.ffi~æli~t?'Hi::::;;,::,::';;p.Y1:~&'::'::::;:::::::,:~·Þ!¡~::':::;'::::·:::::·.·NÎ,~;:::'i:J::::':::::~P:'ì!~1.::::::::::::::~1~~:î~'~j:::::::':::\::::::\::\\i::::: 'arameter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 mglkg Xylenes (total) ND 0.010 mg!kg Toluene ND 0.0050 mglkg Methyl-tert-Butyl Ether ND 0.025 mglkg IthYlbenzene ND 0.0050 mglkg Surroç¡ates: REC (%) Control limits Qual ,4-Bromof1uorobenzene 94 47-137 . B;G~.:: :;:i :.::;:::.: i::' i: i :·i::: i·i·: i:::.::: ::.·i: . i :·i:::: i i i:: :.:::::< :.';:: '.: i': :.:·i.;:::i·:.::·:::· . '01 ~2~i:4~~2i·:.:'·'::::::::::;::.· o2i1~tèij: :t;:.:.. i:· .~·9Iiø;:: i:::·:::·:..:· ·fiuA·i:::i :::::::'::P~17J~~:;:::i:::':::~1Ô21~i;;;;:\:::i:;:i:::::;::r tara meter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 10luene ND 0.0050 , thylbenzene ND 0.0050 Surroç¡ates: REC (%) Control limits 1.4-BrOm0f1UOrobenzene 87 47-137 i'M~I:It~~:;::;::::::":::::'::::::::';:'::::::::::i:::i::::::i':::i:::i,:::,::::,::·::::::,::::':;:i::::::;:i:::'::::·:::;::::;;:'.#~i1H&9~i~~~M:::'·:::;::::;;;;':::::·~I,Ã::':::'::::':::::·':::::.··~.~i¡i:::::;::::::":::i:::.:~I,Â'::::::':::::::;:;:::::~iðY~':;i::ii::::i:iii"R#.:@i1iii::::ii:ii:ii:i:¡¡::i::i\¡i:: mg!kg mg!kg mg!kg Xylenes (total) Methyl-tert-Butyl Ether ND ND 0.010 0.025 1 1 mg/kg mglkg Qual arameter Result RL DF Qual Units Parameter Result RL DF Qual Units ,enzene ND 0.0050 mg!kg Xylenes (total) ND 0.010 1 mg!kg oluene ND 0.0050 mglkg Methyl-tert-Butyl Ether ND 0.025 1 mg!kg thylbenzene ND 0.0050 mg!kg REC (%) Control limits Qual 102 47-137 I I RL - Reporting Limit, DF - Dilution Factor. Qual - Qualifiers 7440 Lincoln Way, Garden Grove. CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0745 EP A 5030B EPA 8021B I I I I I I =alscience If:. nvironmental Laboratories, Inc. ANALYTICAL REPORT Project: 101 South Union, Bakersfield, CA Page 1 of 1 I I I I I Client Sample Number: Lab Sample Date Date Date Number: Collected: Matrix: Prepared: Analyzed: QC Batch ID: ::::§Rii::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::,::::::::::::::::::::::::::::::::::.:':::::::::::::::::::i::::::::::i::::::::::::::i:::::::i:;P.1:æ:~&?~~:::::::i:i::::t:::::::::i·::9~1~r9~::::::::':::::::¡;::'~:þ=¡¡~:i¡:::t;i¡::;:::::i::¡:::;:~i,~;::::::::::;t:::::::::::¡Y1ì{i,::::::::::::::::¡,y~:iAA1~i.::¡:::::::::::::::¡:::::¡::;: Parameter Result RL DF Oual Units Parameter Result RL DF Oual Units Benzene ND 0,0050 mg!kg Ethylbenzene ND 0.0050 mg!kg Toluene ND 0.0050 mg!kg Xylenes (totaQ 0.044 0.010 mg!kg SurroQates: REC(%) Control Limits Qual 1,4-Bromofluorobenzene 95 47-137 :i:M~~Þ.§~;~!~h~l:':::::i:i::.:::::i:::i:¡i,:ii:i:;::i:,i.i;:;.::':·::;::':.i::'i,:i'::::;:.:i:;:::::;:::;i,::i,:::;:¡':·i:::::i·::;:·:·:·::;·::P~!$1:P~i.f~~~~~:·::::':::;:::i::·:':';:::Nr.~·'·¡:,i':::i·ii·::;::::::¡~~¡¡ßt,::::::i::,:::::::ii:::;:::':N!~::;:'::::,i:::i::':::;::::::911!W,::i:::::::::¡~1P~i~P1~i:;::i::':¡'::;¡;::::::¡::,::: I I II II II I Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 mg!kg Ethylbenzene ND 0.0050 mg!kg Toluene ND 0.0050 mg!kg Xylenes (total) ND 0.010 mg!kg SurroQates: REC C%) Control Limits Qual 1,4-Bromofluorobenzene 102 47-137 I II RL - Reporting Limit, DF· Dilution Factor, Qual - Qualifiers I I 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 I I s _a/science - ~nvironmenta/ '- aboratories, Inc. ANALYTICAL REPORT I IT Corporation .452 East Foothill Blvd., 9th Floor lI>asadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0745 EPA 3550A EP A 8082 Iroject: 101 South Union, Bakersfield, CA Page 1 of 1 Client Sample Number: lab Sample Number: Date Collected: Matrix: Date Prepared: Date Analyzed: ac Batch 10: :Jæ~:::::::::::.::::::::::::::::::·::·:·:::::::::·:::::::::::::::::::::::::(:::::::::::::::::·:::::>::::91.~~P!~~:::::::::::::::::::::::::::øÐ.1~iM:t:::::::·:~·~i.!~::::::·:::"'9Y1~P'::::::::::::9,¡;(~1::::::::::::::::919~:@:1~::::::::::::::t:::::::::::::::::: larameter Result RL OF Qual Units Parameter Aroclor-1016 NO 50 uglkg Aroclor -1248 ¡rOCIOr-1221 NO 50 uglkg Aroclor-1254 roclor-1232 NO 50 uglkg Aroclor-1260 roclor-1242 NO 50 uglkg Aroclor-1262 REC (%) Control Limits Qual SurroQates: 128 50-130 2,4,5,6- T etrachloro-m-Xylene Result RL OF Qual Units NO 50 1 uglkg NO 50 1 uglkg NO 50 1 uglkg NO 50 1 uglkg REC (%) Control Limits Qual 89 50-130 :.M~~ij§~:@j~~~:::::::::::::::::::::::::;:::·:::::::::::::::::::::::::::::::::::::':::::':::::::::::;::::::::::::::::::'::::'9~æ'1æ:1~S~~!~::::;:;;:::::::::::::::':W~::::::·::::::::::::::::::::·~~i¡~:::::::::::::::9~j1~~1::::::::::::::9.i.~~~':::::::::::::~19~·1:~1¡':::::::::::::::::::::::.::::::::::: Iroclor-1016 roclor-1221 roc lor -1232 Aroclor-1242 lurroç¡ates: Oecachlorobiphenyl Result RL OF Qual Units Parameter NO 50 uglkg Aroclor-1248 NO 50 uglkg Aroclor-1254 NO 50 ug/kg Aroclor-1260 NO 50 uglkg Aroclor-1262 REè(%) Control Limits Qual Surroç¡ates: 112 50-130 2,4,5,6- T etrachloro-m-Xylene Result RL OF Qual Units NO 50 1 uglkg NO 50 1 uglkg NO 50 1 uglkg ND 50 1 uglkg REC(%) Control Limits Oual 79 50-130 I I I I I RL - Reporting Limit, DF - Dilution Factor, Qual- Qualifiers 7440 Lincoln Way, Garden Grove. CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501 IE _a/science - Environmental Ii ' .. aboratories, Inc. ANALYTICAL REPORT IT Corporation 3452 East Foothill Blvd" 9th Floor Pasadena, CA 91107 02/16/01 01-02-0745 TCLP EPA 8260B Date Received: Work Order No: Preparation: Method: Project: 101 South Union, Bakersfield, CA Page 1 of 2 I I I I I Client Sample Number: Lab Sample Date Date Date Number: Collected: Matrix: Prepared: Analyzed: ac Batch ID: I :j:§Re:::::::jj::::::::::::::::I:::::::j::::::::::::::::::::::::':j::::::::::::::::::::::::::::::::::j::::::::·::::::::::::::::j::::::::::::::·:::::::::::jp1·&~&i~~:::::::::::::::::::::::::::::::··:.:9?d1~t#:':::::::::::j:::';§:~"~':j::::::::::::::::j::::9P1it#:,j:::::::j:j:::::j:j:j9~~~::::::::::::::j:i1g~lrrç::::::::j:::::::::j:j:j::I::::!:: Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units Acetone ND 1000 1 uglL 1 ,3-Dichloropropane ND 100 1 ug/L Benzene ND 50 1 uglL 2,2-Dichloropropane ND 100 1 uglL Bromobenzene ND 100 1 uglL 1,1-Dichloropropene ND 100 1 uglL Bromochloromethane ND 100 1 ugIL c-1,3-Dichloropropene ND 50 1 uglL Bromodichloromethane ND 100 1 uglL t-1,3-Dichloropropene ND 50 1 uglL Bromoform ND 100 1 uglL Ethytbenzene ND 100 1 uglL Bromomethane ND 100 1 uglL 2-Hexanone ND 1000 1 uglL 2-Butanone ND 1000 1 uglL Isopropytbenzene ND 100 1 uglL n-Butylbenzene ND 100 1 uglL p-Isopropyltoluene ND 100 1 uglL sec-Butylbenzene ND 100 1 ug/L Methytene Chloride ND 1000 1 uglL tert-Butylbenzene ND 100 1 uglL 4-Methyt-2-Pentanone ND 1000 1 uglL Carbon Disulfide ND 1000 1 uglL Naphthalene ND 1000 1 ug/L Carbon Tetrachloride ND 50 1 ug/L n-Propytbenzene ND 100 1 ug/L Chlorobenzene ND 100 1 uglL Styrene ND 100 1 uglL Chloroethane ND 100 1 uglL 1,1 ,1 ,2-Tetrachloroethane ND 100 1 uglL Chloroform ND 100 1 uglL 1,1,2,2- Tetrachloroethane ND 100 1 uglL Chloromethane ND 100 1 uglL T etrachloroethene ND 100 1 ugIL 2-Chlorotoluene ND 100 1 uglL Toluene ND 100 1 uglL. 4-Chlorotoluene ND 100 1 ug/L 1,2,3- Trichlorobenzene ND 100 1 ugIL Dibromochloromethane ND 100 1 uglL 1,2,4- Trichlorobenzene ND 100 1 uglL 1,2-Dibromo-3-Chloropropane ND 500 1 uglL 1,1,1- Trichloroethane ND 100 1 uglL 1,2-Dibromoethane ND 100 1 uglL 1,1,2- Trichloroethane ND 100 1 ugIL Dibromomethane ND 100 1 uglL Trichloroethene ND 100 1 uglL 1,2-Dichlorobenzene ND 100 1 ug/L Trichlorofluoromethane ND 1000 1 uglL 1 ,3-Dichlorobenzene ND 100 1 ug/L 1,2,3- Trichloropropane ND 100 1 uglL 1,4-Dichlorobenzene ND 100 1 ug/L 1,2,4- Trimethylbenzene ND 100 1 uglL Dichlorodifluoromethane ND 100 1 uglL 1,3,5- Trimethytbenzene ND 100 1 uglL 1 ,1-Dichloroethane ND 100 1 ug/L Vinyt Acetate ND 1000 1 uglL 1,2-Dichloroethane ND 50 1 uglL Vinyt Chloride ND 50 1 uglL 1,1-Dichloroethene ND 100 1 uglL p/m-Xylene ND 100 1 uglL c-1,2-Dichloroethene ND 100 1 ug/L o-Xylene ND 100 1 uglL t-1,2-Dichloroethene ND 100 1 ug/L Methyl-tert-ButyI Ether ND 100 1 uglL 1 ,2-Dichloropropane ND 100 1 uglL Surroç¡ates: REC (%) Control Limits Qual Surroç¡ates: REC (%) Control Limits Qual Dibromofluoromethane 99 86-118 Toluene-d8 98 88-110 1,4-Bromofluorobenzene 109 86-115 Rl- Reporting limit. DF - Dilution Factor , Qual - Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) B95-5494 · FAX: (714) 894-7501 II I I I I I I I I I I I I I ii = a/science - §nvironmental I aboratories, Inc. ANALYTICAL REPORT I IT Corporation .452 East Foothill Blvd., 9th Floor lJ>asadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0745 TCLP EP A 8260B Iroject: 101 South Union, Bakersfield, CA Page 2 of 2 Client Sample Number: Lab Sample Number: Date Collected: Matrix: Date Prepared: Date Analyzed: ac Batch ID: -:M~'~~~:~¡~~~::::::·:::::::;:::::::::::;:·::::::::::::if:::::;::;::::::::::::::::::;:::::::::::::::::::::::;::··£~~S1"æAAS1~~.~~:::::::::::::::::::·"·N"i:::::¡::::::·::Â~~!§9.~::::::i9P17!.M:::::::¡:¡:¡~~~t:9ì¡::¡¡:::::¡;:¡~19~:~:ªi:::::¡:::¡:::::::::I:::::¡:::: larameter Result RL OF Oual Units Parameter Result RL OF Qual Units Acetone NO 1000 1 uglL 1 ,3-Dichloropropane NO 100 1 ug/L Benzene NO 50 1 uglL 2,2-Dichloropropane NO 100 1 ug/L Iromobenzene ND 100 1 uglL 1,1-Dichloropropene ND 100 1 uglL romochloromethane ND 100 1 uglL c-1,3-Dichloropropene NO 50 1 uglL Bromodichloromethane ND 100 1 uglL t-1,3-Dichloropropene NO 50 1 uglL Bromoform NO 100 1 ug/L Ethylbenzene NO 100 1 uglL Iromomethane NO 100 1 uglL 2-Hexanone NO 1000 1 uglL -Butanone NO 1000 1 ug/L Isopropylbenzene NO 100 1 uglL n-Butylbenzene NO 100 1 uglL p-Isopropyltoluene NO 100 1 uglL sec-Butylbenzene NO 100 1 uglL Methylene Chloride ND 1000 1 uglL ,rt-Butylbenzene ND 100 1 uglL 4-Methyl-2-Pentanone NO 1000 1 uglL arbon Disulfide NO 1000 1 uglL Naphthalene NO 1000 1 uglL arbon Tetrachloride NO 50 1 uglL n-Propylbenzene NO 100 1 uglL Chlorobenzene ND 100 1 uglL Styrene NO 100 1 ug/L _hloroethane NO 100 1 uglL 1,1,1,2- Tetrachloroethane NO 100 1 uglL hloroform ND 100 1 uglL 1 ,1,2,2- Tetrachloroethane NO 100 1 uglL . hloromethane ND 100 1 uglL T etrachloroethene NO 100 1 uglL 2-Chlorotoluene NO 100 1 uglL Toluene NO 100 1 uglL IChlorotoluene NO 100 1 uglL 1.2,3- Trichlorobenzene NO 100 1 uglL ibromochloromethane ND 100 1 uglL 1,2,4- Trichlorobenzene NO 100 1 uglL ,2-Dibromo-3-Chloropropane NO 500 1 uglL 1,1,1- Trichloroethane NO 100 1 uglL 1 ,2-Dibromoethane NO 100 1 uglL 1,1,2- Trichloroethane ND 100 1 uglL libromomethane NO 100 1 ug/L Trichloroethene NO 100 1 uglL ,2-Dichlorobenzene NO 100 1 uglL Trichlorofluoromethane NO 1000 1 uglL ,3-0ichlorobenzene NO 100 1 ug/L 1,2,3- Trichloropropane NO 100 1 ug/L 1,4-0ichlorobenzene NO 100 1 ug/L 1,2,4- Trimethylbenzene NO 100 1 ug/L lichlorodifluoromethane NO 100 1 uglL 1,3,5- Trimethylbenzene NO 100 1 uglL ,1-Dichloroethane NO 100 1 ug/L Vinyl Acetate ND 1000 1 uglL ,2-0ichloroethane NO 50 1 uglL Vinyl Chloride NO 50 1 ug/L 1,1-0ichloroethene NO 100 1 uglL p/m-Xylene NO 100 1 uglL 1-1,2-Dichloroethene NO 100 1 uglL o-Xylene NO 100 1 uglL 1 ,2-0ichloroethene NO 100 1 uglL Methyl-tert-Butyl Ether NO 100 1 uglL ,2-0ichloropropane NO 100 1 uglL urro ates: REC (%) Control Limits Qual Surroç¡ates: REC(%) Control Limits Qual ibromofluoromethane 96 86-118 T oluene-d8 97 88-110 1,4-Bromofluorobenzene 111 86-115 I RL - Reporting limit . OF - Dilution Factor, Qual - Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 !fl a/science ::: ggnvironmenta/ Laboratories, Inc. I ANALYTICAL REPORT I Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0745 TCLP EPA 8270C I IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Project: 101 South Union, Bakersfield, CA ;1 Page 1 of 2 II I Client Sample Number: lab Sample Date Date Date Number: Collected: Matrix: Prepared: Analyzed: QC Batch 10: ::¡§R~:=:::::::i::::::::::::::i::::i::::=::::::::='==:::i=j=::::::j:':¡:::=::::::',::'::=::':::':::::::=::::::::=,::::=:::=:;::::::=:=j:j::j=j::j=:i=:':~1'lli~æi;m~:::::=::::::':j::::::·:j:::=:=::9.&1~m':::::=:¡'::::¡i::,::·§:~¡!~'=::::=:::j::';'::··.9.&1~r,~,:::'¡::::':=:::¡:¡:¡'9Y1i~~1:::::::::::::¡:91~~:îMI:::::::i:::::i:::::::::i::::::¡:::: Parameter Result Rl ND 250 ND 250 ND 250 ND 250 ND 250 ND 250 ND 250 ND 250 ND 250 ND 250 ND 250 ND 250 ND 250 ND 250 ND 250 ND 250 ND 250 ND 250 ND 250 ND 500 ND 250 ND 250 ND 250 ND 250 ND 500 ND 250 ND 250 ND 250 ND 2500 ND 250 ND 250 ND 250 ND 250 ND 250 ND 250 N-Nitrosodimethylamine Aniline Phenol Pyridine 8is(2-Chloroethyl) Ether 2-Chlorophenol 1,3-Dichlorobenzene 1,4-Dichlorobenzene 8enzyl Alcohol 1,2-Dichlorobenzene 2-Methylphenol 8is(2-Chloroisopropyl) Ether 3/4-Methylphenol N-Nitroso-di-n-propylamine Hexachloroethane Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol Benzoic Acid 8is(2-Chloroethoxy) Methane 2,4-Dichlorophenol 1,2,4- Trichlorobenzene Naphthalene 4-Chloroaniline Hexachloro-1,3-Butadiene 4-Chloro-3-Methylphenol 2-Methylnaphthalene Hexachlorocyclopentadiene 2,4,6- Trichlorophenol 2,4,5- Trichlorophenol 2-Chloronaphthalene 2-Nitroaniline Dimethyl Phthalate Acenaphthylene DF Qual Units 1 uglL 1 uglL 1 uglL 1 uglL 1 uglL 1 uglL 1 uglL 1 ugll 1 uglL 1 uglL 1 ugll 1 uglL 1 uglL 1 uglL 1 uglL 1 uglL 1 uglL 1 uglL 1 uglL 1 uglL 1 uglL 1 uglL 1 uglL 1 uglL 1 uglL 1 uglL 1 uglL 1 uglL 1 uglL 1 ugll 1 ugll 1 uglL 1 ugll 1 uglL 1 uglL Surroç¡ates: REC (%) Control Limits Qual 2-Fluorophenol Nitrobenzene-d5 2,4,6- Tribromophenol 56 21-100 79 35-114 67 10-123 Rl - Reporting limit , DF - Dilution Factor . 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 Qual - Qualifiers Parameter Result RL DF Qual Units 3-Nitroaniline ND 250 1 uglL Acenaphthene ND 250 1 uglL 2,4-Dinitrophenol ND 500 1 uglL 4-Nitrophenol ND 500 1 uglL Dibenzofuran ND 250 1 uglL 2,4-Dinitrotoluene ND 130 1 uglL 2,6-Dinitrotoluene ND 250 1 uglL Diethyl Phthalate ND 250 1 uglL 4-Chlorophenyl-Phenyl Ether ND 250 1 uglL Fluorene ND 250 1 uglL 4-Nitroaniline ND 250 1 uglL Azobenzene ND 250 1 uglL 4,6-Dinitro-2-Methylphenol ND 500 1 uglL N-Nitrosodiphenylamine ND 250 1 uglL 4-Bromophenyl-Phenyl Ether ND 250 1 uglL Hexachlorobenzene ND 130 1 uglL Pentachlorophenol ND 500 1 uglL Phenanthrene ND 250 1 uglL Anthracene ND 250 1 uglL Di-n-Butyl Phthalate ND 250 1 uglL Fluoranthene ND 250 1 uglL Benzidine ND 500 1 uglL Pyrene ND 250 1 uglL Butyl 8enzyl Phthalate ND 250 1 uglL 3,3' -Dichlorobenzidine ND 250 1 uglL Benzo (a) Anthracene ND 250 1 uglL 8is(2-Ethylhexyl) Phthalate ND 250 1 uglL Chrysene ND 250 1 uglL Di-n-Octyl Phthalate ND 250 1 uglL 8enzo (k) Fluoranthene ND 250 1 ugll Benzo (b) Fluoranthene ND 250 1 ugll Benzo (a) Pyrene ND 250 1 uglL Indeno (1 ,2,3-c,d) Pyrene ND 250 1 ugll Dibenz (a, h) Anthracene ND 250 1 ugll Benzo (g,h,i) Perylene ND 250 1 ugll Surroç¡ates: REC (%) Control Limits Qual Phenol-d6 39 10-94 2-Fluorobiphenyl 69 43-116 p-Terphenyl-d14 95 33-141 I I I I I I I I I I I I I I i. a/science :: ggnvironmental 5 . ... aboratones, Inc. ANALYTICAL REPORT I IT Corporation 1452 East Foothill Blvd., 9th Floor asadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0745 TCLP EPA 8270C Iroject: 101 South Union, Bakersfield, CA Page 2 of 2 Client Sample Number: Lab Sample Number: Date Collected: Matrix: Date Prepared: Date Analyzed: QC Batch ID: ::M~j~~~'~!~~~::::::::;:::::::::::::::::::::::::::::::::::::::::;::::::::·::::::::.::::::::::·::::::¡::::·9~~æ~æ9.Í#.~~:::::·:::::::::::;.·.·~"A::::::::::::.::·A~~~~9~:::::·::Y~1~ì!~::::::::::·:::gY.1!{9ì:::::¡:::::::::P19~ll:::::::::::::¡¡::¡::::¡:::::::::::::¡:::: lara meter Result RL DF Oual Units Parameter Result RL DF Qual Units N-Nitrosodimethylamine ND 250 1 uglL 3-Nitroaniline ND 250 1 uglL Aniline ND 250 1 ug/L Acenaphthene ND 250 1 ugll ,yridine ND 250 1 ugll 2,4-Dinitrophenol ND 500 1 ugll henol ND 250 1 ugll 4-Nitrophenol ND 500 1 ugll is(2-Chloroethyl) Ether ND 250 1 ugll Dibenzofuran ND 250 1 ugll 2-Chlorophenol ND 250 1 ugll 2,4-Dinitrotoluene ND 130 1 ugll ,3-Dichlorobenzene ND 250 1 ugll 2,6-Dinitrotoluene ND 250 1 ugll 4-Dichlorobenzene ND 250 1 ugll Diethyl Phthalate ND 250 1 ugll enzyl Alcohol ND 250 1 ugll 4-Chlorophenyl-Phenyl Ether ND 250 1 ug/l 1,2-Dichlorobenzene ND 250 1 ugll Fluorene ND 250 1 ug/l IMethYIPhenol ND 250 1 ugll 4-Nitroaniline ND 250 1 ug/l is(2-Chloroisopropyl) Ether ND 250 1 ugll Azobenzene ND 250 1 ugll r4-Methylphenol ND 250 1 ug/l 4,6-Dinitro-2-Methylphenol ND 500 1 ugll N-Nitroso-di-n-propylamine ND 250 1 ug/l N-Nitrosodiphenylamine ND 250 1 ugll lexachloroethane ND 250 1 uglL 4-Bromophenyl-Phenyl Ether ND 250 1 ugll itrobenzene ND 250 1 uglL Hexachlorobenzene ND 130 1 ug/l ophorone ND 250 1 uglL Pentachlorophenol ND 500 1 ugll 2-Nitrophenol ND 250 1 ugll Phenanthrene ND 250 1 ugll I4-DimethYIPhenol ND 250 1 ugll Anthracene ND 250 1 ugll enzoic Acid ND 500 1 ug/l Di-n-Butyl Phthalate ND 250 1 ug/l is(2-Chloroethoxy) Methane ND 250 1 ugll Fluoranthene ND 250 1 ugll 2,4-Dichlorophenol ND 250 1 ugll Benzidine ND 500 1 ugll 1,4- Trichlorobenzene ND 250 1 ug/l Pyrene ND 250 1 ugll phthalene ND 250 1 ugll Butyl Benzyl Phthalate ND 250 1 ugll Chloroaniline ND 500 1 ugll 3,3'-Dichlorobenzidine ND 250 1 ugll Hexachloro-1,3-Butadiene ND 250 1 ugll Benzo (a) Anthracene ND 250 1 ugll IthlorO-3-MethYIPhenOI ND 250 1 ugll Bis(2-Ethylhexyl) Phthalate ND 250 1 ug/l Methylnaphthalene ND 250 1 ugll Chrysene NO 250 1 ugll xachlorocyclopentadiene ND 2500 1 ugll Di-n-Octyl Phthalate NO 250 1 ugll 2,4,6- Trichlorophenol ND 250 1 ug/l Benzo (k) Fluoranthene NO 250 1 ug/l 1,5- Trichlorophenol ND 250 1 ugll Senzo (b) Fluoranthene NO 250 1 ug/l Chloronaphthalene ND 250 1 ugll Senzo (a) Pyrene ND 250 1 ugll Nitroaniline ND 250 1 ug/L Dibenz (a,h) Anthracene ND 250 1 ugll Dimethyl Phthalate ND 250 1 uglL Indeno (1,2,3-c,d) Pyrene ND 250 1 uglL enaphthylene ND 250 1 ugll Senzo (g,h,i) Perylene NO 250 1 uglL rro ates: REC (%) Control Limits Qual SurroQates: REC(%) Control Limits Qual f,uoroPheno, 56 21-100 Phenol-e 6 68 10-94 trobenzene-d5 86 35-114 2-Fluorobiphenyl 80 43-116 ,6- Tribromophenol 40 10-123 p- T erphenyl-d14 105 33-141 RL - Reporting Limit, DF - Dilution Factor. Qual - Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 æ _a/science - nvironmenta/ · aboratories, Inc. Quality Control - Spike/Spike Duplicate I I I I Date Spiked Sample ID Matrix Instrument Prepared m'AHNé}::::::¡:::::·'·:::::¡::·)·:;:¡:.¡·:·¡::::::::::::::::::¡:¡::::::::::.:::):::::::¡:::::::.::.:::¡::::)j:::j:::}:::r::)::::)y's6im:::::::::m::r:::(::r::·::::iB#:~ióM:::::::::::·::"::::::::'·:¡¡iAifò~::::::::::::·::¡::·¡:)·:):¡·::¡:':óij~J.~::::¡:::¡::¡::)::·:::·¡::·:::::::ó:i~i¡ig;ij::::::¡·:::1 I I I I I I I I I I I IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: Project: 101 South Union, Bakersfield, CA Date Analyzed Parameter MS %REC MSD %REC %REC CL RPD RPD CL Antimony 58 59 50-115 2 0-20 Arsenic 85 B4 75-125 1 0-20 Barium 6 3 75-125 1 0-20 Beryllium 88 87 75-125 1 0-20 Cadmium 90 89 75-125 2 0-20 Chromium (Total) 85 82 75-125 3 0-20 Cobalt 86 B4 75-125 1 0-20 Copper 85 B4 75-125 0 0-20 Lead 82 82 75-125 1 0-20 Molybdenum 81 81 75-125 0 0-20 Nickel 79 77 75-125 1 0-20 Selenium 87 88 75-125 1 0-20 Silver 95 88 75-125 7 0-20 Thallium 64 65 75-125 1 0-20 Vanadium 61 57 75-125 2 0-20 Zinc 94 65 75-125 14 0-20 02/16/01 I 01-02-0745 Total Digestion I EPA 60108 MS/MSD Batch Number Qualifiers 3 3 3 3 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 I I I I I I I I I I I I I I I I I I Ii _a/science - l1vironmenta/· Quality Control - Laboratory Control Sample Laboratories, Inc. IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0745 Total Digestion EPA 60108 Project: 101 South Union, Bakersfield, CA LCS Sample Number Matrix Instrument Date Analyzed Lab File 10 LCS Batch Number ·::9~Ìæ1æ~~:t~i1;~!::·:::·¡:::::·:::·::::::::::::¡:.::::::::·::·:::~~Î!~:::'·:·::.::·:::,::··:·'·"-:':'·:,:,:::·:·:::::·:.:::;,·::!šß::~~iffl:·:::·:·:·:·:::·::·':::::.:·:'¡:::·;:~3!'1~íR1·:::':·:·::::':::':·::::·;::··:~~·~31!~::::':,::::':::::':::::::':::::,:::::::::::':::::::::~1g~~~i;!:::::::::::¡:::,; Parameter Cone Added Conc Recovered Ok Ree %Ree Cl Qualifiers Antimony 50 45.6 91 80-120 Arsenic 50 44.2 88 80-120 Barium 50 51.2 102 80-120 Beryllium 50 50.8 102 80-120 Cadmium 50 53.1 106 80-120 Chromium (Total) 50 52.7 105 80-120 Cobalt 50 53.6 107 80-120 Copper 50 50.4 101 80-120 Lead 50 49.9 100 80-120 Molybdenum 50 50.5 101 80-120 Nickel 50 53.1 106 80-120 Selenium 50 49.2 98 80-120 Silver 25 25.2 101 80-120 Thallium 50 48.7 97 80-120 Vanadium 50 50.3 101 80-120 Zinc 50 55.3 110 80-120 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 MSD %REC %REC CL RPD RPD CL Qualifiers I I I I I I I I I I I I I I I ! I I I ~ =alSCienCe íL nvironmental Laboratories, Inc. Quality Control - Spike/Spike Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0745 Total Digestion EPA 7471A Project: 101 South Union, Bakersfield, CA Date Spiked Sample ID Matrix Instrument Prepared :!::·¿;$iŒ¡;~'tj:::::::·:::::'::¡:!::¡:¡':·¡::::·!::::::·::::::¡:¡':¡:'¡:::¡'::-¡·¡:'¡:¡:·:::'i::·¡·:.¡·:'¡:::';:':':::::::!:¡:'¡::'¡':::'::¡:'::îtiwf:¡':'::::¡:,!::·¡:::;:¡·:;:'¡:t::::::·'MWJii::'::::::(':::::";¡::::::::i:::'~iAilðj::::::::::::::::::::::::::::~iAti~~¡:::j¡:::::::¡::::¡:::::¡::iij:i~í':;~à.::::¡::¡¡:: Date Analyzed MSIMSD Batch Number Parameter MS %REC Mercury 102 96 76-136 5 0-16 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 I I I I I I I I I I I I I I I I I ã _a/science - l'vironmental Quality Control - Laboratory Control Sample Laboratories, Inc. IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0745 Total Digestion EPA 7471A Project: 101 South Union, Bakersfield, CA LCS Sample Number Matrix Instrument Lab File ID LCS Bateh Number Date Analyzed :.:p,~!li~li~!tÎ~Ì:'·::;::::::·'·::::,:·:.:·:::;:·:·::::::":::·:·:;:.::§11,~g:·:·::::::::':::::·::'::::·:':::::'·:·:·:·:':':::;:M~r~~ti:::':::.::::':::'.:·:::::::·:·::··'~3{1~('~J,:::·:::::.:::·::·':::;:··::,::P,1~.3~~:~·:;::::::::::::,:::::::::::::::::::·:::::::::·:·:::;~1~~·1~!~~:::::::::::;::::::: Parameter Cone Added Cone Recovered °Æ>Rec 98 °Æ>Ree CL ~ Mercury 0.835 0.822 82-124 7440 lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 S -a/science ... nvironmenta/ Laboratories, Inc. Quality Control - Spike/Spike Duplicate 02/16/01 01-02-0745 TCLP EPA 60108 I I I I I I I ¡ I I I I I I I I I I I Date Spiked Sample ID Matrix Instrument Prepared ':::~i:š::¡~~::':::':::':':::::':::::::'::::'~':::.:':.:i·:::::::::·::::::::~:·:::::·::·::·::::;::·::::::·::':::':::@::::::::::::::::.:.:::.:::::::::::::::::::::~gMm:::::':':'i::'::::::::::::::::::':':::::MÞ:~;:6M::~:·:::':::':':'::::::::::':'::::::6iAî¡J~::'::::::::::::::::::::':::':':::'¡i~~WJ~:::::::::::::::~:::::::':::::::::6:~;¡ii;m~::::::::::: IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: Project: 101 South Union, Bakersfield, CA Date Analyzed MS/MSD Batch Number Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers Arsenic 83 87 75-125 5 0-20 Barium 75 80 75-125 6 0-20 Cadmium 83 86 75-125 4 0-20 Chromium (Total) 87 89 75-125 3 0-20 Lead 77 81 75-125 4 0-20 Selenium 83 87 75-125 5 0-20 Silver 80 85 75-125 6 0-20 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501 I. I I I I I I I I I I II I I I I I I I æ _a/science - ggnvironmental Quality Control - laboratory Control Sample Laboratories, Inc. IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0745 TCLP EPA 6010B Project: 101 South Union, Bakersfield, CA LCS Sample Number Matrix Instrument Date Analyzed Lab File ID LCS Batch Number :·:p~ìm~æH:1.~Jit!~::::::::::·::·:::::::·:::·:::::·::::::::.~~J,i~:::::·::.:.::::·::::.::::::::·::::::::::.::::::::::::m~¡~~m·:::·::::::·:::;:·;:·:::::::..~3rí~{~1:::::;:::::::::::·:¡:.~~~ì1!~:::::::·:::::·:·:::::::::¡·¡:¡':-:;::::::i::¡::.:;P,1¡3~~:i~~::::::·:::::::::· Pa fa meter Cone Added Cone Recovered 0A, Ree %Ree CL Qualifiers Arsenic 10 9.26 93 80-120 Barium 10 9.75 98 80-120 Cadmium 10 10.2 102 80-120 Chromium (Total) 10 10.5 105 80-120 Lead 10 9.80 98 80-120 Selenium 10 9.74 97 80-120 Silver 5.00 4.87 97 80-120 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501 Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers I I I I I I II I I I I I I I I I I I I I S -a/science I::, nvironmental I aboratories, Inc. Quality Control - Spike/Spike Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0745 TCLP EPA 7471A Project: 101 South Union, Bakersfield, CA Date Spiked Sample ID Matrix Instrument Prepared :::ö:j~i$ìti.lî:!:¡':::·¡::¡::¡'::¡::¡::·::·¡:::¡'::::::.;¡:::¡:!::::.¡::::::¡.:.::.¡::.:::::,):¡::'::!,:!:¡::¡:::·:·¡·::¡·:·¡::¡·:·:::::,::::¡:·¡:::¡:·:::%Mm¡:::¡·::¡:!·!:::!:·:·::::!·::::::::·¡:¡¡·:::·:·:AA@~t:t:.\.:::::·:!::::,:·::::!::::::::::::·ijiAiìój!·!::::\::::!·:·::::::::::·:::·::!:~i¡~mój::::::!¡::::::\:::t!:::\::::::iji~~¡:i.:!:::::::: Date Analyzed MS/MSD Batch Number Mercury 100 97 71-134 3 0-14 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) B95-5494 · FAX: (714) 894-7501 I I I I I I I I I I I I I I I I I !Ë _a/science n-~iiPvironmenta/ Quality Control - Laboratory Control Sample Laboratories, Inc. IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0745 TCLP EPA 7471A Project: 101 South Union, Bakersfield, CA LCS Sample Number Matrix Instrument Date Analyzed Lab File ID LCS Batch Number Parameter Mercury Cone Added Cone Recovered 0A, Ree %Ree CL Qualifiers 0.0500 0.0522 104 90-122 7440 Lincoln Way, Garden Grove, CA 92841-1432 . TEL: (714) B95-5494 . FAX: (714) 894-7501 Date Spiked Sample ID· Matrix Instrument Prepared :'::ó:i%imiû@::'¡:::¡.::¡::,¡'::¡":¡I::::':::,:::::::::::::,¡,:,:::,:::¡::::¡::,¡.:::,:.::.:,:::,:,¡:¡,::.:.¡.¡.:':·:::·:¡·::¡:'::·:¡:.¡::::::¡·:·¡::¡::·¡':·:1Miß:::·¡::¡:::¡':::::::·::¡:::¡:¡.::'·¡::::':¡:'i::¡::·'&ê:'~M:::::':·¡':::·::::::¡::.¡::::::·¡:,¡:::¡::::·¡::·:·ij·1i:::·¡':::::::::::::::::::::':::::¡::¡::::::::6i~~ìÎ.ð~¡:\'¡,¡:¡\::::::¡::::::::::::'¡'~'öij¡ö~iI:¡:::::: Date Analyzed MSIMSD Batch Number I I I I I I I I I I I I I I I I I I La/science :: pvironmenta/ I aboratories, Inc. Quality Control - Spike/Spike Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0745 EPA 50308 EPA 8021B Project: 101 South Union, Bakersfield, CA Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers Benzene 95 95 46-136 0 0-15 Toluene 92 92 45-138 0 0-18 Ethylbenzene 94 94 62-121 1 0-17 p/m-Xylene 94 95 53-130 1 0-17 o-Xylene 95 96 64-120 1 0-13 Methyl-tert-Butyl Ether 88 90 24-144 2 0-23 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-750 I I I I I I I I I I I I I I I I I !Ë _a/SCience - nvironmenta/ I aboratories, Inc. Quality Control - LCS/LCS Duplicàte IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0745 EPA 5030B EPA 8021B Project: 101 South Union, Bakersfield, CA Date Date lCSILCSD Batch lCS Sample Number Matrix Instrument Prepared Analyzed Number :@~i1H&9~8~;~I::~:::::::::::::::::::::::::::::::::::::if::::::::::::::::::::::::::::::::::::::::::::::::::::~þ¡gÚ:::::::::::I::::::::::::::::::::gç':~:,::::::::::::::::::::::::::::::':::::::::Nl¥::::::::::::::::::t:::::::::::·9~1.'~t#i::::¡::::::::::::::::::::::::::::::::::::;¡M9.~1.:~p.~~~:::::::::::::::::::::~:::¡:::¡:::¡:::::::¡::::::: Parameter LCS %REC LCSD %REC %REC Cl RPD RPD Cl Qualifiers Benzene 96 97 81-111 1 0-17 Toluene 93 94 81-111 1 0-16 Ethylbenzene 94 96 78-113 1 0-17 p/m-Xy1ene 95 96 70-118 1 0-18 o-Xylene 96 97 77-114 1 0-17 Methyl-tert-ButyI Ether 100 98 65-126 1 0-27 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501 iË a/science ::: ænvironmental Laboratories, Inc. Quality Control - Spike/Spike Duplicate 02/16/01 01-02-0745 TCLP EPA 82608 I II I I I I I I I I I I I I I I I I I Date Spiked Sample ID Matrix Instrument Prepared ::ó'j~i$ii~'ti:¡,:::::t:::::::::¡:::,::'::::::::r::::@::::::::',:·'·'::I::·:':·:::::'¡:::::':¡:¡:::::::¡:¡:':':::::::'::@Mkë::::¡::::¡';:::':·:·:::i:·:·:::·'::·:ÕßJM~'d'::¡':':':':':::::::':'::::::::::":¡¡2AÚð1::::t::::':,¡:¡·:,¡·:::¡::¡':'¡i1žijìJ.l'::¡::::::::::¡:::'¡I:::;:~'~~·~U$iÖ.1::'::t: IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: Project: 101 South Union, Bakersfield, CA Date Analyzed MSIMSD Batch Number Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers Benzene 104 101 72-127 3 0-25 Carbon Tetrachloride 97 93 70-130 3 0-25 Chlorobenzene 103 102 72-131 0 0-25 1 ,2-Dichlorobenzene 102 99 70-130 2 0-25 1,1-Dichloroethene 104 99 69-127 5 0-25 Toluene 103 100 75-124 3 0-25 Trichloroethene 103 100 60-137 3 0-25 ' Vinyl Chloride 115 109 70-130 5 0-25 Methyl-tert-ButyI Ether 95 93 80-120 2 0-25 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 I I I I I I I I I I I II I I I I I ã = a/science - nvironmental Laboratories, Inc. Quality Control - LCS/LCS Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0745 TCLP EPA 8260B Project: 101 South Union, Bakersfield, CA Date Date LCSILCSD Batch LCS Sample Number Matrix Instrument Prepared Analyzed Number I:P~~b19~¡mi1;~~~·;::;::::::::::::::::::::::::::::::.::::·:::::::::::::::;:::::::·Â~ª@º~::::::::::::::::·~Ç!M~·ç:::::::::::::::::::~Y17mj:I::::::::·::::::::::·¡)#í.î9.r91::::::::::::::::;:::::t::::::::::::::P.1~~11~::::t:::::::::::::::::::::::::::::::':::::::::::::1 Parameter LCS %REC LCSD %REC %REC CL RPD RPD CL Qualifiers Benzene 102 102 72-127 0 0-25 Carbon Tetrachloride 89 94 70-130 5 0-25 Chlorobenzene 102 103 72-131 1 0-25 1 ,2-Dichlorobenzene 99 101 70-130 1 0-25 1,1-Dichloroethene 100 101 69-127 1 0-25 Toluene 99 101 75-124 3 0-25 Trichloroethene 100 102 60-137 1 0-25 Vinyl Chloride 105 108 79-118 3 0-25 Methyl-tert-Butyl Ether 96 94 80-120 3 0-25 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 Parameter I I I -I I I I I I I I I I I I I I I I æ _a/SCienCe - ¿g¡nvironmental Laboratories, Inc. Quality Control - LCS/LCS Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0745 EPA 3550A EPA 8082 Project: 101 South Union, Bakersfield, CA Date Date LCSILCSD Batch LCS Sample Number Matrix Instrument Prepared Analyzed Number :~~~&'&1i;~~y.i::¡::.:¡:::::::::::::::::::::::·:::::::::::::¡:::::::·:.:::::::::::;(:§~'At::::::::::::::::::::::::::::::::#Ç:1~:::::'::::::::::::::::::::::::9Y1~@':::::::::::::':::::::::'Þ~}îÞm1::::::::::::::::::::::::::::::::::::::::::::¡::9:':9ì.j~:'¡:::::::::::::::::::::::::::I:::::::::::}:::::::: Aroclor-1260 LCS %REC 100 LCSD %REC 100 %REC CL RPD RPD CL Qualifiers 50-135 0-25 7440 Lincoln Way, Garden Grove. CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 II I I I I I I I I I I I I I I I I ã _a/science - i¥nvironmenta/ I- aboratories, Inc. Quality Control - Spike/Spike Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: Project: 101 South Union. Bakersfield, CA Instrument Date Prepared Date Analyzed Spiked Sample 10 Matrix 02/16/01 01-02-0745 TCLP EPA 8270C MS/MSD Batch Number Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers Phenol 49 38 20-120 26 0-42 2-Chlorophenol 87 82 23-134 6 0-40 1,4-Dichlorobenzene 79 84 20-124 6 0-28 N-Nitroso-di-n-propylamine 91 97 0-230 6 0-38 1,2,4- Trichlorobenzene 84 90 44-142 7 0-28 Acenaphthene 94 102 47-145 8 0-31 2,4-Dinitrotoluene 91 98 39-139 8 0-38 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501 IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 02/16/01 01-02-0745 TCLP EPA 8270C I I I I I I I I : I I I I I I I I I I I I :.. a/science - Environmental Laboratories, Inc. Quality Control - LCS/LCS Duplicate Project: 101 South Union, Bakersfield, CA Date Date LCSILCSD Batch LCS Sample Number Matrix Instrument Prepared Analyzed Number l:çªi&i&ºì~~~:'I:::::::::::::::::::·:::'::::::::::::::':::::::·':'·::::::'::·Aij4i&º~:::·:::::::::::::@:::::·:§ç¡Mª:4:::::::::::::::':::::::::ºY.1~1'H::::::::::::::::::::::::º~H~m,\:::\::::IIII'::::\I:':::¡¡::::¡:9:@~1!í\:::::::::::¡::¡::::::::::'¡::¡:\::::::::::::::::::::¡~ Parameter LCS %REC LCSD %REC %REC CL RPD RPD CL Qualifiers Phenol 57 64 20-120 13 0-42 2-Chlorophenol 71 76 23-134 7 0-40 1,4-Dichlorobenzene 72 75 20-124 4 0-28 N-Nitroso-di-n-propylamine 83 85 0-230 2 0-38 1,2,4- Trichlorobenzene 79 80 44-142 1 0-28 Acenaphthene 76 83 47-145 9 0-31 2,4-Dinitrotoluene 88 91 39-139 3 0-38 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 I I. I I I I I I I I I I I I I I I &.._alSCience GLOSSARY OF TERMS AND QUALIFIERS ~J1vironmental . '- aboratories, Inc. Work Order Number: 01-02-0745 Qualifier Definition NO Not detected at indicated reporting limit. 7440 Lincoln Way, Gàrden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 Comments I I I I I I I I I I I I I I I I I I Generated in LlMS I 02/16/01 02/16/01 JP SAMPLE RECEIPT FORM Work Order Number: Delivery Container Type: Client Project 10: 01·02-0745 Cooler 101 South Union, Bakersfield, CA Date Received: Date Opened: Opened By: Section A: Pass/Fail Criteria 1. Chain of custody document(s) received with samples, 2. Sample container label(s) consistent with custody papers. 3. Sample container label(s) complete (10, date, time, taken by). 4. Sample container(s) intact and in good condition, 5. If applicable, proper preservation noted on sample label(s), 6, Sufficient sample volume received for analyses requested. 7, Correct containers used for analyses requested, 8. If applicable, VOA vials free of heads pace. Yes Yes Yes Yes NA Yes Yes NA Section B: Additional Observations 1, Describe packing materials used in container. 2. Was sample container('s) sealed with custody seals? 3. Were all samples sealed in separate plastic bags? 4. Measured temperature inside delivery container when opened, 5. If delivery container shipped by third-party carrier, did container come with shipping slip, airbill, etc.? If YES, attach copy of shipping slip/airbill to the back of this form. 6. Do tedlar bags show condensation? Describe below if yes. 7, Are 25,1 condensate traps immersed in dry ice? 8. Are 25,1 sampling trains intact? 9. Are 25.3 condensate vials still attached to the sampling train? 10, Are 25.3 condensate vials on wet ice? NA No No 5.0 No °C NA NA NA NA NA Section C: Additional Comments 02/16/01 11 :42:48 ~~'l DI ·v,o .vvv ùUIU . - -- - -- I I I I II I I I I I I I I II I I ,I I I I I I I WASTE MANAGEMENT PROCEDURES P.~ 48-10 ISSUED DATE: 05/'23/97 CANCELS ISSUE: 03/05/97 ISSUED BY: RLG MATERIAL: SOIL CONTAMINATED WITH HYDRAULIC FLUID USE FOR ARIZONA, CALIFORNIA AND NEVADA WASTE ONLY!!! MINIMUM REOUIRED TESTING TRPH = TOTAL RECOVERABLE PETROLEUM HYDROCARBONS = EP A 418.1 BTXE = EP A 8020 CAM METALS = TTLC ALL: STLC ON ALL TTLC METALS lOX STLC MAXIMUM: TTLC LEAD => 13 MGIKG REQUIRES ORGAN1C ANALYSIS TCLP EXTRACTION = EPA 1311 AND VOC ON EXTRACT = EP A 8240 SVOC ON EXTRACT = EP A 8270 MET ALS ON EXTRACT = EPA 6010, (USE 7470 FOR Hg) NOTE: IF PESTICIDES = EPA 8080 (ON EXTRACT) IF HERBICIDES = EPA 8150 (ON EXTRACT) PCBs = EP A METHOD 8080 (NOT ON EXTRACT) HYDROGEN SULFIDE = SW~846 (7.3.4.2) (REACTI'V1TY) HYDROGEN CYANIDE = SW-846 (7.3.3.2) (REACTIVITY) pH (CORROSIV1TY) AQUATIC BIOASSAY (FISH TOX) = PART 800 OF "STANDARD METHODS FOR THE EXAMINATION OF WATER AND WASTEWATER (1 5TH EDITION)" LABORA TOR\' INSTRi!Cïiû~S (MIN¡¡,jUMGüíüELiNES ONLY; _ TRPH REQUIRED FOR ALL SAMPLES. ' _ ALL 011ŒR TESTS REQUIRED TO BE RUN ON COMPOSrrE{S). MAXIMUM 4 SAMPLES pER COMPOSITE. _ SILC REQUlRED FOR METALS WITH TTLC VALUE lOX STLC MAXIMUM. _ ORGANIC ANALYSIS REQUIRED FORTTLC LEAD OF 13 MGIKG OR GREATER. _ LABORATORY IS TO SUPPLY QNQC INrORMATION WlTH ALL ANALYTICAL REPORTS. _ MAIL OR FAX ALL ANALYSIS TO PERSON REQUESTING ANALYSIS. PROCEDURE ORIGINAL DATE: 07/10190 PROCEDURE JŒV1SED DATI: OJ/OSf')' ;;).((5"70 f t of f EQUIVA Services LLC Chain Of Custody Record OATE: PAGE: ¡i;iii!t1!~!g~;~~I~~;M~~~':(~¡'~i;9~~)t~i;~ none ~ ~ ~ i ~ ~ 1 350 7 4 --- CAL SCIENCE ENVIRONMENTAL LABORATORIES, INC. Equlva Project Manager to be Invoiced: Mark Passa 7440 Lincoln Way l:ø~~!~~:~:ß.!¢~~E~~1 Mark Passarini . Tech Services Garden Grove, CA 92841-7501 IliII········ ............ Ed Paden -Environmental Engineer . . . .1.E~~~~~:5~~E~' (714) 895-5494 (714) 894-7501 fax I:~.~~~:~~~:: SITE ADDRESS (Stre.. and Clly): CONSlL rANT COMPANY: 101 South Union Avenue. Bakersfield. CA 93307 PROJECT CONTACT (Report 10): IT Corporation ADDRESS: ëñY: 822407 r CONSUlTANT PROJECT NO. 3452 E. Foothill Boulevard, 9th floor Pat McCullough SAMPlER IIAUE(S) (PoH): Pasadena, CA 91107 Lowell Kessel T &MAL: =;-304_1500 r:: 626-535-9076 TURNAROUND TIME (BUSINESS DAYS): [J 10 DAY![J 5 DAYS e 72 HOUR!C 48 HOURS Ii!I REQUESTED ANALYSIS FIELD NOTES: Contain er/Preservatlve or PID Readings or Laboratory Notes Soil with Hvdraulic Fluid Back Ground Sample .x.. please refer to attached sheet 6-20 ~i ~l ð2.{lfø(ol Sf)þtt¡ 'Tiff TIme: o g : c;rC) ;;; ~ ii ~ ::. ::. 0{ IoL X õ ., o !!!. ~ in u ... ;:; ... t:. " ~ .! ii Õ .. -..1 Oate: z..{/(P{a/ ¡;;¡;: X ¡;;- N I m ~ ;;; 1/1 o a. II' i5 ... .E êií II I- éò " 0'1 Õ ::;¡ I- C/ ~ 1/1 II 1/1 to o " II )( ¡¡: ... o a. to > l Ê '" ::; '" ::;¡ I- C/ ~ :J: IL I- ... o a. to > ~ Ó !:. - 1/1 :¡ :; IL II' o o > .. o a. to > iñ - Ó !:. w m I- ::;¡ >< w I- m II' o o > ... o a. to > <15 - :!. :J: IL II:: l- X ~ 'ü II a. !!!. II' ~ II ::;¡ íD In - o !E- Õ C to .s II ::;¡ Õ C to .c ùí íD - N o !E- .':: to E o < :t; :1 to C II '" o ;;; :J: .. o o > II' :S to Õ > ... .E c ~ U to ~ W In '" o In c( IL W f;;ù II Õ Z II II C/ é ~ to E ,¡: c o o íD o CD N !E- w m I- ::;¡ C LESS THAN 24 HOURS 24 HOURS íD o '" N !E- li' :1 to C II '" ~ o + - 1/1 ::::¡ :; IL .. o o > íD o '" N !E- .. :1 to C II '" ~ o + w m I- ::;¡ - >< w I- m HIGHEST per BORING _ ALL_ TEMPERATURE ON RECEIPT C'r [J LA - RWQCB REPORT FORMe UST AGENCY: GClMS MTBE CONFIRMATION: HIGHEST _ SPECIAL INSTRUCTIONS OR NOTES: íD - N o !E- w m I- ::;¡ - >< w I- m X v 1. X Ê In .. o !E- li :E J! u to ~ W , :J: IL I- Received by: (Slgnatln) vr'. ~V1 Ê In Õ !E- li :E to .. e' ::I IL , :J: IL I- NO. OF CONT. 1 1 1 MATRIX SAMPLING TIME 2/15/01 2115101 2115/01 DATE 'kJ' fr \" Field Sample Identification - - ()5" ...evtsto~ , (j~ Time: - tol.£i - I - Date: "2.\ - - - Received by: (Slgn.tIn) Recelved=tlnQ¡~ - -- - ~~ ~ _Bun ftnal ::-~ndPl~ I I I I I I I I I I I I I I I I I IE =alSCienCe L nvironmental Laboratories, Inc. March 07, 2001 Pat McCullough IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Subject: Calscience Work Order No.: Client Reference: 01-03-0160 101 South Union Avenue, Bakersfield, CA Dear Client: Enclosed is an analytical report for the above-referenced project. The samples included in this report were received 3/5/01 and analyzed in accordance with the attached chain-of-custody. The results in this analytical report are limited to the samples tested and any reproduction of this report must be made in its entirety. If you have any questions regarding this report, require sampling supplies or field services, or information on our analytical services, please feel free to call me at (714) 895-5494. Sincerely, C WI iam H. Christensen Quality Assurance Manager 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501 I I I I I I I I I I I I I I I I I E _a/science - Environmental Laboratories, Inc. Analytical Report Page 1 of 1 LABORATORY ID: 01-03-0160 Method: DOHS LUFT Organic Lead Matrix: Soil/Solid Results CLIENT: IT Corporation PROJECT: 101 South Union Avenue, Bakersfield, CA Sample ID Organic Lead Dilution Date Date (mg/kg) Factor Extracted Analyzed Composite SP-1-1 ,2,3,4 NO 1 03/07/01 03/07/01 Method Blank NO 1 03/07/01 03/07/01 Reporting Limit: 1,0 Quality Assurance and Control Information Matrix Sample Spike 10: 01-03-0159-1 Batch 10: Spike LCS RPD 010307 Conc. Result Control ppm ppm Limits Organic Lead 25.0 21,4 0-20 Ke: Rec=Recove NO=Not Detected at the re ortin level 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501 La/science :: J'vironmental Laboratories, Inc. ANALYTICAL REPORT I I I I I I I I I I I I I I I I I I I IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 03/05/01 01-03-0160 Total Digestion EPA 60108 Client Sample Number: Project: 101 South Union Avenue, Bakersfield, CA Page 1 of 1 Lab Sample Number: Date Date Date Matrix: Collected: Prepared: Analyzed: QC Batch ID: ...................... ......... .... .... ..... ..... ................ .. . . ··.·šòìid::\/:· >ii3jÖ2i~':::::?:::P:~~~~!:M::::::::::::::P:~!:g~~ª~::::j::::::::::::::::~j,~M!!f~;:::::::::::::::::::::::::::::: ..........,....... .............................. ......................................... ................... ............................... ... .. .. ................" .. .... ... ...,. :j::JtRmM~~!:.~ff,~f1,;,~~f;~:\::·::::::::::::m::\)::)mi:::::::\:::::.:.:..:::~~~~3!1~~f.1.~:::'i(//..... Parameter Result Lead 4,19 . .... . --. ".. . . . . . . . . . :::jf8\mêg#:~#:~f~~~~~iìi!::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::: ....... Parameter Result Lead 5.33 RL 0.50 DF Qual Units mglkg ............ ........".............,. ............................. ............................. ~Œ9.?:3ØMt,1IL.:.: ::...:~~!i~:::::::::..:9.~!ø#:(q,j::.·.··~~~~~{~!::::::::::~WM'=!1:::::::::.··:,·.q:'~~q!i,f~f:jj¡:::j¡::::::::::::::¡:::¡:: RL 0.50 DF Qual Units mglkg ::i·:~gmêê~~,·~fjJt1.~3~i1·:::::::::·::::·::::::·':i:::::::.::::.:::.:jj::::::::::::.:"j:::::::::::.:.j:::::·:.:":.·~1æ~æ1~gj1:!·:::::::····j::::::::::::··:::·:::::::·:::·..·~r~¡~::::::::::·::.::~~(9~('~.:::·:::::::··R~(#:~{"1:::·:..·:·.:·~~(~~('~::::::::::::::·::·:::~·1~~g!'f~J,:::::::::::::::::::::::::::::. Parameter Result Lead 20.5 ............................ ::::·M~t~~ij¡i!~r~;:::::::·:.:.· . RL 0.5 DF Qual Units mglkg .. :::::::::::::···::Ø~i~1~Qi.~~Hii\:(:::::::::..::.:.::.....::.:::...::.......$.......þ.·:.'.·..i.~.:.·...:.:.::.:.:.:.:.:..!.:.:.::.:.:..:..................................... Nl...·..·.....·~.:....·.:..·..:..:.:..:.:..:.:.'..:...............:..·....O.........~......!.OJiiØ~!:::?(Q.·:.~.::·.l.:P. J!ô;.~.:..:.:.:.::}}:::!:!]Hø~.D.:.::.:.~.:...··.·.,.:.Cs.:.:..··....:..:..:.:.J.:..:.:.:.:.:.:..:.::.::..:.:.::.:.::.;.:.:'.:.:.:,:,!:.,::.:,.:,::.:.:.::.;.: ..................................................:.........;.:...;.;.;.;.;.:...;.:.:.:.:.;.:-:.:.:.;.:.;.;.:-:.;.:.:-:-:-:.:-:.;.:.:.;.:.:.:.:-:- ................ ......... ... ................. .... .... ....... Parameter Result Qual Units Lead ND RL DF 0.500 mglkg RL - Reporting Limit. DF - Dilution Factor. Qual- Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501 I I Ë _a/science - nvironmental £. aboratories, Inc. ~T Corporation .452 East Foothill Blvd., 9th Floor I'asadena, CA 91107 ANALYTICAL REPORT Date Received: Work Order No: Preparation: Method: 03/05/01 01-03-0160 EPA 5030B EPA 8015M/8021B roject: 101 South Union Avenue, Bakersfield, CA Page 1 of5 Client Sample Number: Lab Sample Number: Date Collected: Matrix: Date Prepared: Date Analyzed: QC Batch ID: .·§R~~~î::::::·:::::::::::::.::::::::::::::::::::::·:::;::::::::.:::::.:::.:::::::::::::::::::::::::::::::::::::::::::::.::::::.·9'.m~iPJ~9~1·::::::::·::::::::::::::9~!~i.(9~:::::::::::::::·§·Ãi.¡~::·:::::::::::::::··NtÃ:::::::::::::::::.:~~!~§'!9?¡::::·::::::jø.1~~~~9:1.~i:::::::::{{:::::::{ Itarameter ~enzene Toluene IthYlbenzene urroQates: Result RL DF Qual Units Parameter Result ND 0.0050 mg/kg Xylenes (total) ND ND 0.0050 mg/kg TPH for Gasoline ND ND 0.0050 mglkg RL DF Qual Units 0.010 mglkg 0.50 mglkg REC (%) Control limits Qual Surroç¡ates: REC (%) Control limits Qual ,4-Bromofluorobenzene 67 47-137 1,4-Bromofluorobenzene - FID 65 34-141 :·§Ri~~~:::::::::::::::·::¡::::·::·:.::::::::¡::¡:::::::::::::¡¡::::::::::¡::::::::::::::':::':.:::::::::::.:::::::::::':::¡:::':::::::'::::P1'w~'pl¡¡Pi~'::::¡::::::::::¡:::::·.9i{~~œ~:::¡:::::·:::::§.~m~::::::::::·::::·:·Nt.~::::::::;::::::::::#'~!9~1:~1::r:::::P1~~*~#1~~:¡:::¡:::::':¡::II:: 'ara meter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 mglkg Xylenes (total) ND 0.010 mglkg ìo,uene ND 0.0050 mg/kg TPH for Gasoline ND 0.50 mglkg thy1benzene ND 0.0050 mglkg Surroç¡ates: REC (%) Control limits Qual Surroç¡ates: REC(%) Control limits Qual ,4-Bromofluorobenzene 84 47-137 1,4-Bromofluorobenzene - FID 80 34-141 ':§R~!r!¡:':::¡¡¡:¡:::::::::¡¡::::::::::::¡:¡::::::@·::::::':::::::::::::¡¡:::::':::¡::::::¡::::::¡:::¡:::::¡::::::¡::::::::::¡¡:¡:::::::':::::::::':#1'm~:p'1iffi$::::::¡::::::::¡::::::¡:::::··:9Y~~œ,:::::::¡::::::::::#.·þí.¡!::¡:::::¡:¡::::·:::::::Nt.~:¡:::::::::::¡:::¡:¡::::::M:!9!t!t:::¡::::¡::i1¡~9,~#,~i¡¡¡:::::¡:¡:¡::¡¡:::¡::¡¡:¡: larameter Benzene 10luene thy1benzene Result RL DF Qual Units Parameter ND 0.0050 mglkg Xylenes (total) ND 0.0050 mglkg TPH for Gasoline ND 0.0050 mglkg Result RL DF Qual Units ND ND 0,010 mglkg 0.50 mglkg Surroç¡ates: I4-BrOmOfluorobenzene REC (%) Control limits Qual Surroç¡ates: REC (%) Control limits Qual 80 47-137 1,4-Bromofluorobenzene - FID 78 34-141 I I RL - Reporting Limit. DF - Dilution Factor, Qual- Qualifiers 7440 Lincoln Way, Garden Grove. CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 E _a/science __ nvironmenta/ '- aboratories, Inc. ANALYTICAL REPORT IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 03/05/01 01-03-0160 EPA 5030B EPA 8015M/8021B Project: 101 South Union Avenue, Bakersfield, CA Page 2 of5 I I I I I Client Sample Number: Lab Sample Date Date Date Number: Collected: Matrix: Prepared: Analyzed: ac Batch ID: [;§JEî@::::::::::[:::¡::[:::::::::::::::::::::::::::'::::":::::::':::::::::'::::::::::'::::::::::::::'::::':::::::,::::':::::::::::::::::::::::::::::::::::::::::::';'9'1'æ~æ:1~pâ:::::::'::':::::::::::::::::::::::'q~gi.r~':::::::::::::::::::':[·~:¡¡~:::::::::::::::·::::::::::'::··~[i:::::::::::::::::::::::::::~~!9.i(!i::::::::::::::::!1g~~~1¡¡:::::::::::::::::::,:::::::::1 Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene NO 0.0050 mglkg Xylenes (total) NO 0.010 mglkg Toluene NO 0.0050 mg/kg TPH for Gasoline NO 0.50 mglkg Ethylbenzene NO 0.0050 mg/kg Surroç ates: REC (%) Control limits Qual Surroç ates: REC (%) Control limits Qual 1,4-Bromof1uorobenzene 71 47-137 1,4-Bromof1uorobenzene - FIO 74 34-141 I I !m¡¡&1:II..m_81011i!!;:i#:~¡JiJ0.!i!ilg#œI1mlm'~B.¡0_...I¡¡T_._ I Parameter Result RL OF Qual Units Parameter Result RL OF Qual Units Benzene NO 0.0050 mglkg Xylenes (total) NO 0.010 mglkg Toluene NO 0.0050 mg/kg TPH for Gasoline NO 0.50 mglkg Ethylbenzene NO 0.0050 mg/kg Surroç ates: REC (%) Control limits Qual Surroç ates: REC (%) Control Limits Qual 1,4-Bromof1uorobenzene 67 47-137 1,4-Bromof1uorobenzene - FIO 65 34-141 I I I Parameter Result RL OF Qual Units Parameter Result RL OF Qual Units Benzene NO 0.0050 mg/kg Xylenes (total) NO 0.010 mglkg Toluene NO 0.0050 mglkg TPH for Gasoline NO 0.50 mglkg Ethylbenzene NO 0.0050 mglkg Surrogates: REC (%) Control Limits Qual Surrogates: REC (%) Control Limits Qual 1,4-Bromof1uorobenzene 82 47-137 1,4-Bromof1uorobenzene - FIO 79 34-141 RL . Reporting Limit, OF· Dilution Factor, Qual- Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-750 I I I I I II I I ~ a/science ;=- nvironmental ... aboratories, Inc. ANALYTICAL REPORT I IT Corporation 1f452 East Foothill Blvd., 9th Floor ~asadena, CA 91107 Date Received: Work Order No: Preparation: Method: 03/05/01 01-03-0160 EPA 5030B EPA 8015M/80218 IrOject: 101 South Union Avenue, Bakersfield, CA Page 3 of5 Client Sample Number: Lab Sample Date Date Date Number: Collected: Matrix: Prepared: Analyzed: ac Batch ID: :,§r~¥:~f::::::!:::'::':::"!':::':::::':·.:::::::::':':'.:,:!,:!,,::,!,::::,:,!:,:::'::::::::!!::::::::::::!:,:::,,:::::::·:'.:P:1·W~P1~P~!::·:!::::,::::,,',:'::::·.9.~!~~(9,~:::'!:::::;:::'·~·~¡¡~::::"::::;:·':':':·:Ñ(#:::·::,:":·::::":::::~~!9!(q"::::::¡::¡:P:1P~pI1#i\::::::::::!:!::\::\:!::\::' arameter ~ RL DF Qual Units Parameter enzene ND 0.0050 mg/kg Xylenes (total) Toluene ND 0.0050 mglkg TPH for Gasoline _thylbenzene ND 0.0050 mglkg urroQates: REC (%) Control Limits Qual SurroQates: ,4-Bromofluorobenzene 67 47-137 1 ,4-Bromofluorobenzene - FID Result RL DF Qual Units ND 0.010 mglkg 4.3 0,5 mg/kg REC (%) Control Limits Qual 65 34-141 )~r~ì~·::"::'::::::'::!:'::::::!,:,:::::·,:::::,:::::":::!::::::::.:::::::,:::'::::'::!:::::':'::!'::::::::::::':::·:::::I::::':::::::·':::9"W~P1~i~!:::::·:'·:::::::!:·::::'·.pæ#~p'::::':::::::::::·§Þi!~::::::::::::::::::':N':~::::::::":::::!::pi!9!(~1::!::,:!::::::9,1P~9~P1~M::::¡:¡::::::¡::::¡:::: 'arameter Result RL DF Qual Units Parameter Benzene ND 0.0050 mglkg Xylenes (total) fOluene ND 0.0050 mglkg TPH for Gasoline thylbenzene ND 0.0050 mg/kg SurroQates: REC (%) Control Limits Qual SurroQates: ,4-Bromofluorobenzene 85 47-137 1 ,4-Bromofluorobenzene - FID Result RL DF Qual Units NO 0.010 mglkg ND 0.50 mg/kg REC (%) Control Limits Qual 82 34-141 .··§r~1·~':!:::::::!:::':::::::::::::::::'::'::':!::::':::'.:':'::':!::::j"":':¡:'.:!::'::::::,::::::::::::!!:::::::!:!:!:::·::::::':::¡::·.91W~·P1AAii::::':::¡:::::::::·::··9æ~~p'::::::¡::::¡::·.·§.~i!~:::::::::!:::'::::¡:'@l,i::!:':::::::¡:¡:¡:::¡::"~~!I(~1::::¡::::¡:::':9,1P~9~91~!::!::::::::::::::::::::::: larameter Result RL DF Qual Units Parameter Result 'RL DF Qual Units Benzene IOluene thylbenzene ND 0.0050 mg/kg Xylenes (total) NO 0.010 mg/kg ND 0.0050 mg/kg TPH for Gasoline ND 0.50 mg/kg NO 0.0050 mg/kg REC (%) Control Limits Qual SurroQates: REC(%) Control Limits Qual 81 47-137 1,4-Bromofluorobenzene - FIO 78 34-141 SurroQates: 1,4-BrOmOfluorobenzene I I RL - Reporting Limit, DF - Dilution Factor. Qual- Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 iË _a/SCience ... nvironmental Laboratories, Inc. ANALYTICAL REPORT IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 03/05/01 01-03-0160 EPA 5030B EPA 8015M/8021B Project: 101 South Union Avenue, Bakersfield, CA Page 4 of 5 I I 1 I I Client Sample Number: Lab Sample Date Date Date Number: Collected: Matrix: Prepared: Analyzed: QC Batch ID: :'§R~1;~::::::::::::::::::I¡::::::::::::::¡:::::::':::::::::::::::::::::::::::::::::::::::::::.::::::::::::::::::::::::::::::¡::::::::::::::::::::::::::::·.p·iæ~3i·1:§RS~!:¡:::::::::::::::::::;·9.~~~Î,~1:::::::·::·::::::::.§:~¡¡~::::::::::::::::::::::::.,~!~:::::::::::::::::¡:::::':¡::~~i9.!î~~¡:I::'¡I:¡91~~9,~'~!¡I:I:::::::::::::::::::1 Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 mglkg Xylenes (total) ND 0.010 mglkg Toluene ND 0.0050 mg/kg TPH for Gasoline ND 0.50 mg/kg Ethylbenzene ND 0.0050 mglkg SurroQates: REC (%) Control Limits Qual SurroQates: REC (%) Control Limits Qual 1.4-Bromofluorobenzene 78 47-137 1.4-Bromofluorobenzene - FID 76 34-141 I I Jj\'!::.oI..liáillí¡;.f_¡;;_1{¡¡iMlí:¡l:~tl.í.¡;m!IÆAmlJj¡~¡¡i!~[íÌ{¡¡1I1¡¡¡¡.¡i&í'¡m:.li~i~!iij!,..¡¡¡1 Parameter Result RL DF Qual Units Parameter Result RL DF Qual Units Benzene ND 0.0050 mg/kg Xylenes (total) ND 0.010 mg/kg Toluene ND 0.0050 mg/kg TPH for Gasoline ND 0.50 mg/kg Ethylbenzene ND 0.0050 mglkg S urroQates: REC (%) Control Limits Qual SurroQates: REC(%) Control Limits Qual 1.4-Bromofluorobenzene 76 47-137 1,4-Bromof1uorobenzene - FID 74 34-141 i:!'RH~i::i:::I:i:l:i::::::::i::::::::i;i::i:::;::::I:::::::::::::,::::::::;:;1:::::::::;::::;::::,::;::::·:::::::::::;;::1:::::::;::::::1::::;::::::::::::::::::::::;:p~·æ~3i1§9a!:::::::::':::¡::·:::::::::9.~~~œ1::::::::::::¡:::::¡'§·~¡¡~:¡:::::::'::::::::::::'::·.·m~::::::::::::::::::::::¡::::~!~îq,1::¡:::::::¡:::::919~9,~'~!¡¡¡:¡:::¡¡::¡::¡::¡i::'¡:¡:: Parameter Result RL DF Qual Units Parameter Result Rl DF Qual Units Benzene ND 0.0050 mg/kg Xylenes (total) ND 0.010 mg/kg Toluene ND 0.0050 mg/kg TPH for Gasoline . ND 0.50 mg/kg Ethylbenzene ND 0.0050 mg/kg SurroQates: REC (%) Control Limits Qual Surrogates: REC (%) Control Limits ~ 1.4-Bromofluorobenzene 78 47-137 1.4-Bromofluorobenzene - FID 76 34-141 RL - Reporting Limit. DF - Dilution Factor. Qual - Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-750 1 I . I I I I I I I I I I I IT Corporation .452 East Foothill Blvd., 9th Floor "asadena, CA 91107 æ _a/science - Environmental I- aboratories, Inc. ANALYTICAL REPORT Date Received: Work Order No: Preparation: Method: 03/05/01 01-03-0160 EP A 5030B EPA 8015M/8021B Iroject: 101 South Union Avenue, Bakersfield, CA Page 5 of 5 Client Sample Number: Lab Sample Date Date· Date Number: Collected: Matrix: Prepared: Analyzed: QC Batch ID: :;M~~ij~~·¡!~~k:::::::;:.:::::::·:::::::::::.·::;::::::::::::::::::::::::::::::::::::::::::::::.::::::.::::::::::·::·:p~!1H&9.¥~~~~~!;:::::::::::::::···~(~:::::::::::::::::::'::'~Þi¡4;:::::::::::::;::::::::"@~:::::::::::::::::I:9~!AA(q~:::I:::::::.~1Y~P~9'~!::::::::::¡::::::::::::::¡.: _arameter enzene Toluene .thYlbenzene ~urroç¡ates: Result RL DF Qual Units Parameter Result RL DF Qual Units ND 0.0050 mg/kg Xylenes (total) ND 0.010 mglkg ND 0.0050 mglkg TPH for Gasoline ND 0.50 mglkg ND 0.0050 mglkg REC (%) Control Limits Qual Surroç¡ates: REC (%) Control Limits Qual 87 47-137 1,4-Bromof1uorobenzene - FID 84 34-141 1,4-BrOm0f1UOrObenzene I I I ' , I I I I I I RL - Reporting Limit. DF - Dilution Factor, Qual- Qualifiers 7440 Lincoln Way, Garden Grove, CA 92841-1432 '. TEL: (714) 895-5494 · FAX: (714) 894-7501 Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers I II II I I I I II I I II II I I I I I I Ii -a/science I:. nvironmenta/ Laboratories, Inc. Quality Control - Spike/Spike Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 03/05/01 01-03-0160 Total Digestion EPA 6010B Project: 101 South Union Avenue, Bakersfield, CA Date Spiked Sample ID Matrix Instrument Prepared ¡:ó:1:ili~:iØ~j~:!~1¡::):::::::::):l::::::::::t::::::::::::t:::::::::::¡:::{:::·::::::::::::¡:::·::·¡:,::::::::@giid:::::::::::::::::::::::::::::::::I::::::::iB~:~l¡¡ijm:I::·:::¡::::::::::::::·:::~š:;6i¡Ó~::;:::::::::::::::¡·¡·:::·:·:·:tjiði)6~:::I::::::·::::t:::::.¡:::ijilij:~M;î:::I::: Date Analyzed MSIMSD Batch Number Lead 93 92 75-125 0-20 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 I I I I I I I I I I I I I I II I I !Ë _a/science ~ ~Environmenta/ Quality Control - Laboratory Control Sample Laboratories, Inc. IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: 03/05/01 01-03-0160 Total Digestion EPA 6010B Project: 101 South Union Avenue, Bakersfield, CA lCS Sample Number Matrix Instrument Date Analyzed lab File ID lCS Batch Number ····~~îw1æij~:t3;1:r!:::·::·:·::::·:::·:::·:·:·:::::::·:::·:i:::::::~~1i~:::::::·::::::,:·:,::::::::,:':::::'::·:·:·:::::::·::·.··!Šg·~~!W::::::::;::::.::::·:·:.::·::::.:9~l,g~r~1··::·::::::·::::·::··:::··:·.·9~ij~~~d;:·;::::·:::::\::·:·::::::::·::::::::.::::::¡1~¡ij~¡~!::::::::::j:\.::\.: 50 51.7 %Rec 103 O'('Rec CL Oualifiers Parameter Cone Added Cone Recovered Lead 80-120 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 Date Spiked Sample ID Matrix Instrument Prepared Date Analyzed I I I 03/05/01 I 01-03-0160 EPA 50308 I EPA 8015M/8021B I I I I I I I I I I I I I MS/MSD Batch Number Ë _alscience - Environmental Laboratories, Inc. Quality Control - Spike/Spike Duplicate IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Received: Work Order No: Preparation: Method: Project: 101 South Union Avenue, Bakersfield, CA Parameter MS %REC MSD %REC %REC CL RPD RPD CL Qualifiers Benzene 86 93 46-136 8 0-15 Toluene 81 88 45-138 9 0-18 Ethylbenzene 76 86 62-121 12 0-17 p/m-Xylene 72 82 53-130 13 0-17 o-Xylene 79 88 64-120 11 0-13 TPH for Gasoline 88 83 44-122 7 0-30 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-750 II I I I I I I I I I I I I I I I I S _a/SCience - Environmental Laboratories, Inc. Quality Control - LCS/LCS Duplicate Project: Date Received: Work Order No: Preparation: Method: 101 South Union Avenue, Bakersfield, CA 03/05/01 01-03-0160 EPA 5030B EPA 8015M/8021B IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, CA 91107 Date Date lCSILCSD Batch LCS Sample Number Matrix Instrument Prepared Analyzed Number ::Ä~M¡H¥º~S~~~~!:.::·:::::::::::::::::::::::::::::::·:':':::::'::::::'::::::::::::::'::::.:::~þ¡@:,:,:::::::::::::::::::::::::::::·::§9~:1::.:::::::::::::·:.::::::::::::N!¥:::::::::::::::::::::':::::::'º~(9~m1:::::::::::::::::::::::::::::::::::t:::~1~¡~º,!~f.:::::::::::::::::::::::1::::::::::::::::::::: Benzene Toluene Ethylbenzene p/m-Xylene a-Xylene TPH for Gasoline LCS %REC LCSD %REC %REC Cl RPD RPD Cl Qualifiers 98 96 81-111 2 0-17 95 93 81-111 2 0-16 97 95 78-113 2 0-17 98 96 70-118 2 0-18 98 95 77-114 3 0-17 110 108 57-132 2 0-13 Parameter 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 Qualifier Definition I I I I I I I, I I I I II I I I II II I "=alscience GLOSSARY OF TERMS AND QUALIFIERS - nvironmental I.. aboratories, Inc. Work Order Number: 01-03-0160 NO Not detected at indicated reporting limit. 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) B94-750 I I I I I I I I I I II I II I I I I I I I SAMPLE RECEIPT FORM Work Order Number: Delivery Container Type: Client Project ID: 01-03·0160 Cooler 101 South Union Avenue, Bakersfield, CA Date Received: Date Opened: Opened By: 03/05/01 03/05/01 JP Section A: Pass/Fail Criteria Comments 1. Chain of custody document(s) received with samples. 2. Sample container label(s) consistent with custody papers. 3, Sample container label(s) complete (10, date, time, taken by), 4. Sample container(s) intact and in good condition. 5. If applicable, proper preservation noted on sample label(s). 6. Sufficient sample volume received for analyses requested. 7. Correct containers used for analyses requested. 8. If applicable, VOA vials free of headspace, Yes Yes Yes Yes NA Yes Yes NA Section B: Additional Observations 1. Describe packing materials used in container. 2. Was sample container('s) sealed with custody seals? 3, Were all samples sealed in separate plastic bags? 4, Measured temperature inside delivery container when opened. 5. If delivery container shipped by third-party carrier, did container come with shipping slip, airbill, etc.? If YES, attach copy of shipping slip/airbill to the back of this form. 6. Do tedlar bags show condensation? Describe below if yes. 7, Are 25.1 condensate traps immersed in dry ice? 8. Are 25.1 sampling trains intact? 9. Are 25.3 condensate vials still attached to the sampling train? 10. Are 25.3 condensate vials on wet ice? NA No No 0.0 No °C NA NA NA NA NA Section C: Additional Comments 03/05/01 13:00:16 Generated in LlMS EQUIVA Services LLC Chain Of Custody Record Manager to be Invoiced ~~~':p,~~~!i~~¡~~~~'~~!~¡i¡~~J,tQ, - - - - - ,-, :.:.: :'.::: :::.'; ~ ~ ~ ~ ~ 13507 Marc!l2....2Q01 _2_ of _1_ DATE: PAGE: Mark Passarini- tech services Equlva Project :O~q~~q;~;~~~~~~ :r~ ;i#¥i4.~:#~~~:):::' :lti~~Mi~ij9~: CALSCIENCE ENVIRONMENTAL LABORATORIES,INC 7440 Lincoln Way Garden Grove, CA 92841-1432 (714) 894-7501 fax (714) 895-5494 CONSUlTANT COMPANY: Edward Paden- Environmental Engineer SITE ADDRESS (Street and CIIy): IT Corporation I CONSUlTANT PROJECT NO.~B.a Bakersfield. CA 101 S. Union @BrundageAvenues PROJECT CONTACT (A_ta): 3452 East Foothill Blvd, 9th floor g-2.:2.- ~o 7 Patrick McCullough SAMPLER NAME(S) (PrinI): Lowell Kessel CA 91107 CITY: Pasadena, TELEPHONE: I FAX:----= 626-304-1500 ~6.s35.g076 TURNAROUND TIME (BUSINESS DAYS): [J 10 DAYS [J 5 DAYS [J 72 HDURS [J T E-MAIL: REQUESTED ANALYSIS FIELD NOTES Container/Preservative or PID Readings or Laboratory Notes .J N I CD .. ¡; II! o a. II! i3 .2 .. II! '" l- X íjj .. en éi :E l- I/) 5- II! '" II! .. CJ " '" )( ¡¡: o a. .. > Ë II) :; .., :E l- I/) 5- J: A. I- o a. .. > iñ - o '=- .. II! :J -= U. II! o o > o a. .. > íiì ~ 6 t. w CD I- :; >< W I- CD II! o o > o a. .. > - ... - :!. J: A. II:: I- m- Il> Õ e. õ c: .. ... ãí :æ õ c: .. ... ûi ~ ïj .. a. !!!. II! B '" :æ m- N o e. u ;::: .. E e ~ " l!. .. c: '" 01 o ¡; :r II! o g II! :S .. õ > ~ .2 c: .~ Ü ~ ~ W II> .., e II> ct A. W õ z '" '" I/) ¿ ~ .. E C c: o o m- e II) N e. w m I- :æ m- e II) N e. II! l!. .. c: '" 01 '" )( o + .... II! :J -= U. II! o o > m- e II) N e. II! .. ... c: .. 01 '" )( o + W m I- :æ >< w I- m m- .. N e e. w CD I- :æ >< w I- m Ë II> Õ e. '" :is 13 u ~ ~ w , J: A. I- Ë II> Õ e. '" :is .. '" 01 ; A. , :r A. I- THAN 24 HOURS 24 HOURS ~ LESS 48 HOURS [J [J LA - RWQCB REPORT FORMAT [J UST AGENCY: GClMS MTBE CONFIRMATION: HIGHEST _ SPECIAL INSTRUCTIONS OR NOTES: HIGHEST per BORING _ ALL_ TEMPERATURE ON RECEIPT C'r composíte samples 1 through 4 together composite samples 5 through 8 together Field Sample Identification NO. OF CONT. SAMPLING DATE I TIME MATRIX 1 1200 3/2/00 X 1 1200 3/2100 sp-2-2 X 1 1200 3/2100 X X X X X 1 1 1215 1215 3/2100 3/2100 sp-2-1 sp-2-3 sp-2-4 sp-2-S sp-2-6 sp-2-7 sp-2-8 1 1 1 1200 1215 1215 3/2100 3/2100 3/2100 ~ . TIme: o~ :¡:¡¡¡;;: <:f\ \ '5 ) Doto: "'3 ii8ië: ~ Received by: (SI""""~ \í RocoIved by: (81"""") ~J/%"p1 R shed by: (SIgnalln) - - Time: ~O¡'.~ 10/23JOO RovIslon - - sl~\ - 1 - Dolo: ~ - - - ~ - - R_d by: (SIgnat1.n) - - - ¿,"A"~ or _IBUTIC¡¡¡ wI1II II_Groen 10 Filo, Volow ond PlnktQ ClenI. ReI~shedbyh CALSCIENCE ENVIRONMENTAL _ _BOI dE"-_ Equiva Project Manager to be invoiced: ij:j¡¡,::~~t!;\~N~j¡~~M~~~i~~I~,j~~~fØl¡¡¡iiii¡ 7440 Lincoln Way rtr" ............ .......... "1 ~ : <$q~~ÇE:~:~t:iJ:~!1!-!~ DATE: March 2. 2001 Garden Grove, CA 92841-1432 rraT:~@ì4.~:~~R1i.ç~;::::::1 Mark Passarini- tech services (714) 895-5494 l]a~~~)f9Ç~~~:????1 PAGE: _2_ of _2_ (714) 894-7501 fax Edward Paden- Environmental Engineer CONSULTANT COMPANY: SITE ADDRESS (street and Clly : I IT Corporation ADDRESS: 101 S. Union (!i! Brundaae Avenues Bakersfield, CA I 3452 East Foothill Blvd, 9th floor PROJECT CONTACT (Rop"''''): CONSULTANTPROJECTNO.:8i1~ 10 CITY: Patrick McCullough -'- 8'2..2. C{ 0 '7 I Pasadena, CA 91107 SAMPLER NAME{S) (PrtnI): - TELEPHONE: I FAX: E-MAIL: I 626-304-1500 626-535-9076 Lowell Kessel I TURNAROUND TIME (BUSINESS DAYS): 0110 DAYS 0 5 DAYS 0 72 HOURS 0 48 HDURS o 24 HOURS ~ LESS THAN 24 HOURS REQUESTED ANALYSIS o ILA - RWQCB REPORT FORMAT o UST AGENCY: ãì ãì Õ ãì - 0 0 z N iñ iD J I U> .. .. - GCfMS MTBE CONFIRMATION: HIGHEST HIGHEST per BORING U> N .. ~ 0 0 ... ALL N e e en FIELD NOTES: e u I=- iñ C SPECIAL INSTRUCTIONS OR NOTES: .. ë .. ~ - TEMPERATURE ON RECEIPT CO .. Õ N Ê ell .. 0 IIJ 0 :!E I Ê ';;j ';;j :; > .. ãì m Ê Container/Preservative 11\ e .. E 11\ l=- I- e I- 11\ c; .. .. Ë 2 0 c; :E U> (I , or PID Readings 0 m '" < - ; 5- ~ '" >- e ~ .. m e N >- )( J:: :8 =õ - :::; '" ... or Laboratory Notes )( 0 c Õ )( 1/1 - .. 0 0 0 .. w :E .. .. :E ~ + 0 u - e ~ I- :; I- .. iõ :E + ~ .. .. IL .. 1/1 cpmposite samples 1 through 4 together .. - ãì c m (I CI .. Ü w W 1/1 ';( .. :5 ü 5- 0 .. m m :::; 0 '" .. .. - 1/1 .. .., 0. I .. W 1/1 ~ ~ l- I- U> 0 :E 0. cò 0 0 :J: .. :J :E :E '3 N 11\ iõ ~ ~ 0 0 IL )( Õ e '" ¡¡: IL W - - IL 0 :J: Õ > > I- .. .. 2 SAMPLING , )( )( .. W 11\ .. C ¡;; :J: .. (; (; (; Field Sample Identification NO. OF :J: :J: W W 0 m ct 0 .. IL 0 .. MATRIX I- J: 4í 0. 0. 0. 0. .. DATE TIME CONT. IL IL l- I- g :E IL 0 W :E II: .. .. .. .. .. l- I- m m w > I- > > > > I- sp-1-1 3/2/00 1230 1 X sp-1-2 3/2100 1230 1 X sp-1-3 3/2/00 1230 1 X sp-1-4 3/2100 1230 1 X A Rrr;~by.(S~Y jI r)f X Received by. (Sp~ - Det;. ~ 5" ( Time: I ./""" 'n.¿Jo c.. ."\\ ^ .. _\~ ~ °1 Gð: ~ RiI~shod by. (Sgnature) , Received by. (Spttre) Dete: Time: I \ .. Relnqlished by. (S~lIre) ,~ ~ . -. Rocelvedby. (S~ttre) ~'"'-- Dete: Time: I ,',,-- .~ ..-. -!/ 3 \ S-\ 0' (,)9~ c:::ro J Y DISTRIBUTION: WhIte with ftnel report, Groen to Fllo, YoIow end Pink to Clonl. -----------. 10/23/00 Revtston - - IiiUI~elllife5illllC iilin 6MIC"dYlilcollill - - - ,../ ;- ~ CITY OF BAKERSFIELD CLAIM VOUCHER CC(Q)~y Vendor No. I certify that this claim is correct and valid, and is a proper charge against the City Agency and account indicated. CLAlMANT'S NAME AND ADDRESS: Equilon Enterprises LLC 2255 N Ontario Street RM 208A Attn: Feryal Sarratian Burbank. CA 91504 (AUTHORIZED SIGNATURE OF CITY AGENCY) Date: 01/23/02 Initials of PreDarer : BA W CITY DEPARTMENT: PLEASE PROVIDE SHORT EXPLANATION OF PAYMENT: Fire Prevention (Including Contract Number if Applicable) The business made a duplicate payment of $160,00, We need to refund this credit and send it attention Feryal Sarratian Fund Dept. 11 0000 Base Ell Obit Proiect # 123 7900 Invoice # Amount Comments on check stub $160,00 VOUCHER TOTAL $160.00 SECTION 72, PENAL CODE Section 72, Presenting False Claims. Every person who with intent to defraud, presents for allowance or for payment to any state board or officer, or any county, town, city district. ward or village board or officer. authorized to allow or pay the same if genuine, any false or fraudulent claim, bill, account, voucher, or writing, is guilty of a felonv. FINANCE DEPT. USE ONLY o Examined & Approved for Payment Amount ..... ",,'- "'.~ ;,0;1 .' STATEMENT OF ACCOUNT PAGE 1 CITY OF BAKERSFIELD POBOX 2057 BAKERSFIELD, CA 93303-2057 (661j 326~3979 ',',).. ,"-' .- ~ DATE: 1/15/02 TO: EGUILON ENTERPRISES-LLC 2255 N ONTARIO 5T RM 20eA'~ ATTN: FERYAL 5ARRAFIAN BURBAN~, CA 91504 -~~_¥ ~.(. ~ ~\ '-""~'('~'<'::l:vry""" ¥', .X· ;". <,e' ::' ."-,""--:--: . .".1 r.,J :.., :' ~ ...... >< .\ 'A "h", ",,-~,_ \ CUSTOMER NO: 3800 CUSTOMER TYPE: FD/ 30466 ------------------------------------------------------------~--------------- CHAR:~E DATE DESCRIPTION' h" _ ¡': : R~f~~UM~ER PUE'riAT,~ TOTAL AMOUNT ------ -------- -~--------------------.;:_:_, ,~_:_~,~----~~- ------::--:.7 -------------- - .' 12/15;01 BEGINNING BALANCE 160. 00- " , ,......, FOR QUESTIONS OR CHANGES TO~YOUR ACCOUNT PLEASE CALL THE NUMBER AT THE TOP OF THIS 5TATMENT, -------------- -------------- -------------- -------------- CURRENT OVER 30 OVER 60 OVER 90 -------------- -------------- -------------- -------------- DUE DATE: 2/04/02 PAYMENT DUE: TOTAL DUE: 160.00- $160.00- , . , - ¡:~'" > . ' . '-- ,.,.,~. , GROUP, INC. . , ~'. .1 AN m COMPANY' "', December 30, 1999 Project 705-131.ÍB Mr. Ralph E. Huey, Director , Office of Environmental Services Bakersfield Fire Department I· 1715 Chester Avenue Bakersfield, Californiå 93301 Re: Subsurface Soil Assessment Former Shell-:Branded Service Station 101 South Union A venue at Brundage Lane " Bakersfield, California ' , . Dear Mr. Huey: Pacific Environmental Group (PEG), on behalf of Equiva Services, LLC (Equiva), is pleased to submit this site assessment report for the site referenced above. This report was prepared in response to a letter dated March 16, 1999, from the Bakersfield Fire . Department, Office of Environmental Services1 arid in accordance with our app~oved 'WorkplanforAdditional Site Assessment, dated May 03, 1999, PEG performed this work to further evaluate soil conditions near the fuel dispensers. , . / In July 1999, excavation activities related to a municipal water supply pipeline installation along Brundage Lane encountered hydrocarbon-impacted soil. Based on results of additional drilling and laboratory analytical results, PEG determined that the ' hydrocarbons discovered in the street did not originate from service station oper~tions. BACKGROUND " Site Description The subject site (Site) is located at 101 South Union Avenue, at the intersection of Brundage Lane, in Bakersfield, California (Figure 1). The Site is inactive and formerly, operated as a Shell-branded service station. The Site is occupied by a station building, including car wash, three dispenser islands, and three 10,000-gallon underground storage tanks (USTs) which' store gasoline fuel (Figure 2). ' N:\data\PROJEClì705-eauiva\Union-131\131 Renort doc 650 Sierra i\1adre Villa, Suite 204· Pasadena, California 91107-2013 (626) 351:4814 FAX (626) 351-4822 ~ J- December 30,1999 Page 2 According to a Phase I Environmental Site Assessment prepared during October 1999 by Artemis Environmental ,Consulting, Inc,: . , , , - , According to historic sources, the subject site was operated as a Wilshire Oil gasoline station in 1960. Shell Oil constructed the current station in 1965, and , began operating in 1966, with one 8,000-gallon product UST, two 5,000-gallon product USTs, and one S50-gallon waste oil UST. A second 8,000-gallon UST was installed in 1970. These USTs were apparently removed in 1987, and replaced with the current on-site ÚSTs. The waste oil UST was apparently not replaced. " Previous Assessment On July 10, 1998, Cambria Environmental Teéhnology, Inc. (Cambria) observed upgrade activities at the Site, including installation of secondary containment to the existing dispensers and gasoline turbines. I Cambria subsequently collected ,soil samples from beneath all dispensers. Among these samples, tQe highest detected hydrocarbon concentrations occurred at 2, feet beneath the north dispenser at the island located alongside Union Avenue, identÌfied by Cambria as D-4 (2'). Reported analytical results were 2,600 milligrams per kilogram (mg/kg) total petroleùm hydroèarbons as gasoline (TPH-g). Table 1 summarizes analytical, results frQm Cambria's July 1998 assessment. FIELD I,NVESTIGA T'¡ON Pre-field Activities PEG visited the Site to mark boring locations for the June 1999 soil sampling event and contacted Underground Service Alert more than 48 hours before drilling, arranged the drilling schedule, and mobilized drilling equipment a~d materials. PEG prepared a site- specific health and safety plan before initiating any field activities. June 1999 Drilling and Subsurface Soil Sample Collection On June 15, 1999, PEG supervised the drilling of two exploratory soil borings (B-1 and B-2) using a direct-push technology (DPT)rig (Figure 2), Soil boring B~l was drilled to an approximate depth of 25-feet below g~ound surface (bgs) and boring B-2 was drilled to approximately 20-feet,bgs. PEG monitored total volatile organic compounds (VOCs) during drilling and recorded results of soil headspace analyses on the exploratory boring ,logs, 'Boring logs are included in Appendix A. Field procedures are summarized in Appendix B. PEG supervised the collection of soil samples for logging and analytical testing at 5-foot intervals using a direct-push sampler. PEG staff retained the samples in I-inch diameter stainless steel rings, sealed the rings at each end with a Teflon®-liner and plastic end caps, labeled the sampl~s, and stored them on' ice for transpórt to a state certified ,\\P ASAFP 1 \COMMON\data\PROJECT\ 705-equiva\Union-131 \131 Report.doc "'" .~ December 30,1999 Page 3 analytical laboratory. A courier transported the soil samplês under chain of custody documentation to Calscience Environmental Laboratories (Calscience) in Garden Grove, California. Soil samples were analyzed soil for methyl tert-butyl ether (MtBE) and benzene, toluene, ethylbenzene, total xylenes (BTEX) using EPA Method 8021B and TPH-g using Method 8015 modified. Soil Stockpile Sample Collection - July 1999 Brundage Lane Field Investigation W.M. Lyles' Co., a pipeline ·còntractor working for Califorpia Water, encountered impacted soil adjacent to the Site while performing horizontal drilling along Brundage Lane and beneath th~ intersection with Union Avenue. A PEG geologist met with Steve Yoder, site foreman for W.M. Lylt(s, and collected samples from W.M. Lyles' . soil stockpilès on July 21, 1999. According to Mr. Yoder, W.M. Lyles performed horizontal drilling to install an 18.,.inch diameter steel pipeline beneath the intersection, Drilling proceeded from east to west across Union Avenue. Reportedly, the first 200 feet of the 225-feet long boring produced . soil cuttings that appeared "èlean" and the last 25 feet produced cuttings ·that smelled strongly of hydrocarbons. Based on Mr. Yoder's descriþtion of the underground boring location, W.M. Lylès encountered the impacted soils along Brundage Lane at approximately 5-feet north of the Site's. northern border and from approximately 15- to 40-feet west of the Site's eastern border. ·Mr. Yoder reportedly directed his crew to stockpile separately the "clean" soil and impacted soil. A PEG geologist obtained sample SP-2-1 from the repprtedly ¡'clean" stockpile and samples SP-l-l, SP-I-2, and SP-I-3 from the impacted stockpile~ Sample SP-l-l was collected from the stockpile's surface and samples SP-l..2 and SP-I-3 were collected . from approximately 20-inches below the surface. PEG staff retained the samples in sealed glass jars, labeled the jars, and stored them on ice for transport to Calscience. . A courier transported the soil samples under chain of cùstody to Calscience. Calscience analyzed soil samples from the June 1999 phase of work for methyl tert-butyl ether (MtBE) and benzene, toluene, ethylbenzene, total xylenes (BTEX) using EP A Method 802lB and TPH-g and total extractable petroleum hydrocarbons (TPH-e) using Method 801.5 modified. Due to the unusual chemical characteristics identified in the stockpile samples as reported . " by Calscience, PEG directed Calscience to 'send the stoGkpile samples, which contained, detectable concentrations of TPH-g and TPH-e, to Global/Zymax for a more-detailed hydrocarbon characterization, \\P ASAFP 1 \COMMON\data\PROJEC1ì 705-equiva\Union-131 \131 Reportdoc ~. December 30, 1999 Page 4 Drilling and Sampling Collection - July 1999 Brundage Lane Field Investigation On July 22, 1999, PEG supervised the drilling of three exploratory soil borings (B-3? B-4, . and B-5) using a hollow-stem auger drill rig (Figure 2). The borings were drilled to confirm that impacted soil encountered during the Brundage Lane excavation work was not related to service station operations. Soil borings B-3, B-4, and B-5 were drilled to .approximate depths of 25-, 40-, and 25-feet bgs, respectively. PEG monitored total volatile organic compounds (VOCs) during drilling and recorded results of soil headspace analyses on the exploratory boring logs. Boring logs are included in Appendix A. Field procedures are summarized in Appendix B. PEG supervised the collection-of soil-samples for logging and analytical tèsting at 5-foot intervals using a modified California split~spoon sampler. PEG staff retained the samples in 2-inch diameter brass or stainless steel rings, sealed ,the rings at each end with a Tef1on~:-liner and plastic end caps, labeled the samples, and stored them on ice for transport to Calscience. A courier transported the soil samplès under chain of èustody to Calsciencé. I , I Soil samples from borings B-3,B-4, and B-5 were analyzed for methyl tert-;-butyl ether (MtBE) and benzene, toluene; ethylbenzene, total xylenes (BTEX) using EP A Method 8021B and TPH-g and total petroleum hydrocarbons as diesel (TPH-d) using Method 8015 modified.· , FINDINGS Subsurface Conditions Soil encountered during drilling activities 'consisted of sands, sandy silts, and clayey silts. The soils above approximately 20- t9 25-feet bgs generally consisted of silts, including sandy silt and clayey silt. This unit was directly underlain by poorly sorted sands with varying amounts of silt and fine gravel. Groundwater was not encountered during drilling . operations. Soil Analytical Results - Soil Borings TPH-g, BTEX, and MtBE were not detected above laboratory reporting llmits in any of the samples analyzed from borings B-1, ß:-2, B-3, B-4, and B-5.. Similarly, no TPH-d was detected above laboratory reporting limits in any of the samples. Soil analytical results are summarized in Table 2.· Certified analytical reports and chain of custody documentation are included in Appendix C. Soil Stockpile Analytical Results - Brundage Lane Excavation TPH-g and TPH-e were detected in all three samples collected from the impacted sòil stockpile (Brundage Lane excavation), at levels up to 39 rrig/kgand 180 mg/kg, respectively. Calscience reported no tPH-g . above laboratory reporting limits in the ~\P ASAFPI \COMMON\data\PROJEC1ì 705-equiva\Union-131 \131 Report.doc ~ December 30,1999 Page 5 sample collected from the reportedly "clean" soil stockpile. No MtBE or BTEX constituents were reported àbove laboratory reporting limits in any of the samples analyzed from the soil stockpiles. Cert~fied analytical reports and chain of custody documenfation are included in Appendix C. Based on the results of the simulated distillation and gas chromatography/mass spectrometry analyses; Global/Zymax concluded that "stoddard solvent is the dominant type of hydrocarbon" among the three samples. Additionally, Global/Zymax determined that a significant amount of waste oil (heating oil #6) wàs present in the two samples collected from deeper within the soil stockpile. Global/Zymax's full interpretive report and supporting laboratory data are included as Appendix D. CONCLUSIONS Based on the results of this investigation, PEG concludes the following: · Hydrocarbon-impacted soils encountered during the July 1998 di~penser upgrade 'and sampling event appear limited in lateral and vertical extent. · Laboratory analyses and hydrocarbon characterization sugg~sts that hydrocarbon impact to soils found along Brundage Lane does not originate from the Site.. · The possible limited hydrocarbòn inípactto soil observed in the field at boring B-4 appears to originate from the direction of Brundage Lane, based on reported depths of occurrence. · Site conditions warrant no further work at this time. On behalf of Equiva Services LLC, PEG requests that case closure be granted for the Site. I \\P ASAFPI \COMMON\data\PROJECT\ 705-equiva\Union-131 \ 131 Report.doc ~ TABLES j ;'. December 30,1999 Page 6 Should you have questions or need further assistance, please call me at (626) 351-4814, Sincerely, , Pacific Environmental Group p~ Gary P. estana, R. G, Senior Geologist . Attachments: Table 1 Table 2 I cc: Mr. Edward Paden - Equiva Services LLC \\P ASAFP 1 \COMMON\data\PROJEC1ì 705-equiva\Union-131 \131 Report.doc , '." 8M 49~ ~9~U¡=¡N[:;:J¡;b~ .II ~~ Jf9~ ~.."O ...... } I eNblø:;;~ A ~ ¡', - ~',..- ~'O/M0~ ~~~~ I 7~ :¡ .. ';F - t' 8M Dl 39~~: ~' ":,' ',,- 00 M'~~~ 'II ,1Qt-~ 15 N \.,' ~--~- " II U '¡&fo~' mac Ii c' ' .".' :-----,------'. ..-' , ~:~e pan,.uL, C_·~=-- gZ . \ :.82 t ... ~-~.-:. -~ ':,1 I '/' i . .: .' _' I Ii'2!d! ~ ~ '> ! ¡ t A1~ ~ ~ ~ .:: . "~.(¡),. lJl :1 ~ ~ .,. /"., 8 ~"''-' _ ="" U ., '. \ I .r -=- _ '~..NdJlM._ .j:. _ {. . .. _ 'Di~ [1_ _ 'i : ':A~~ 8M 3'93' :. ~. :. ___:JII .. J~i'(l" .> 0 -5 . 388 _~ _ "., -, 1¡¡¡¡].'.,.Res I ,. .. ===),hC=====: ---1 ========== ,........ Y:¡¡: !-----*~i;:: ~¡ lie=!. Q ..).r..,«-~.:>:.>",. '-----'-I f rIh. ,-. __ ,= þ== ...;-"/ II .-'CJ ........::~> :¡;;J'S5~', { ~"~, W ~ rl·G!I~~er \.. '\ îr /t ~ I ~-d;---": "'~'>;¡;.. .~. . 5;'-', Jl' ayan:J8ee J /' /1\-' ---- II: \ !jl;-·~h . ,'. ~'~~~~~,. .: /~ .' ¡l~RAë~1;-~oo",-..:~~~~, "''o''>~~'<~~_5. I"-;~~_ " \~" ~ 1.,\ ~:\:.>"'< I\",~_==·=~., - .~'~~'~ ~,\\~UNïY 111:, '''~'~;'''':~~~ - . .:" .. . == = 1 ~(.",\-;I) .;' "-" !~:JI !)¡"""..--u. ./ "";, , ',0':"'",,,..- . 1 I,.,» -g " ". 1 III \\:" I.- 'Fli! ~ FA!. NDS ".:.~ ':-,,!};:, "- "0 : V \~. '. /'. '\ '':\,\\".,.....,r. '-"'" '~ ~) . . _ I'" _,...~ -. ~~"I . '~:.~.. " ...~\-' ~_:õ :~ OMA f-. . ':, : ·Q~k,)~ -/ Casa, LO~h.~_d~~' '. m. ! ~.: ~::; .--- . ...~.. ~ II L Y - - . :.. Rese,vo¡r'..~&~ ~."." ,:. .. ., -- - 01 Æ' Rese,vol'co: .' = . . c:9 ' . :"":.t:~ ~ ".-, ',..... .,.' . ":". ~ I -.. _. .. . . O! .~, 'Ii: ~ ,). :". '.~"" ".""""n T.T<01""," . .... . _. g g../·<;·:,II """·':6 II~OIi~. ;;; -" - 11'-\ f.!...... ~ i~!SC~ , <' RN/ f. ~ 1'.11 ' '.' .' III .; II '" ~. ::!~í' D~ '. II', = 6~~ '. 7 = \!J ev t , " :. /-' -....SR N~¡:-"'" ':: '-1/ ")/I,Q) (J " ..." 1111 I '.' ". Iln381'i ~ F== I- == == ~_I_. ~ ..:¡":',' ~ ~., :;. ~ QUADRANGLE LOCATION v .. ~= ,--., - ()~¡; -. ",--_... ... ,.. - SITE LOCATION " .... I~ 01· "'i /'11 'V ! U, ......i REFERENCES: USGS 7.5 MIN. TOPOGRAPHIC MAP TITLED: GOSFORD, CALIFORNIA; LAMONT, CALIFORNIA DATED: 1954 REVISED: 1973 ~ SCALE IN FEET I o I 2000 PACIFIC ENVIRONMENTAL GROUP, INC. I 2000 SHELL SERVICE STATION 101 South Union Avenue Bakersfield, California FIGURE: 1 PROJECT: 705-131.1B SITE LOCATION MAP ;:< BRUNDAGE L~~E I .----- ------ , B-5 I UNDERGROUND , STORAGE 1 TANKS ¡ /-__1 ___ I { t \ 1 ...._______J /------- , ! \ 1 ....-------/ /------- I I \ I ....-------/ , I I IWJ h Z S ,-1 I;.. Z,..... h ~ -0:: I WJ U c.. <r' 19 ;> -- , "'- I I I , I I I , I I I I I I I I I I ------------------------------------1 ------- --- B-4 " '", .. \ , \ \ \ I I I..... U '-0:: I~ "'- 1"'- 1-0:: I;,¿ 1-1 1-0:: :::: 115 1C/1 r -. I D-I ! . I I I 4( ! I I B-3 DISPENSER ISLAND .-- ..-- 0_- D DISPENSER ISLANDS B-I\ D-4 · .'. \ I I ,< HIGH'VAY 58 LEGEND Co (Q :2 21 ~ M ... iñ o ,... éi5 (9 z ~ o ¡::::: () UJ ...., o a:: a. B-1. SOIL BORING'LOCATION AND DESIGNATION D-I. 1998 DISPENSER SOIL SAMPLE LOCATION AND DESIGNATION APPROXIMATE SCALE I 30 I o ~ SHELL SERVICE STATION 101 South Union Avenue Bakersfield, California FIGURE: 2 PROJECT: 705-131.1 B PACIFIC ENVIRONMENTAL GROUP. INC. SITE MAP N ¡;.;: -- ""'" ~ ~ > < ~ o - z ;::; c -< o x "'- c.. I 60 FEET <.- Table 2 Soil Analytical Results Summary Former Shell-Branded Service Station WIC No. 204-4262-2100 101 South Union Avenue Bakersfield, California B-I-5 06/1 5/99 5 ND«0.5) NA ND«0.005) . ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) B-l-IO 06/15/99 10 ND«O.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) B-I-]5 06/15/99 15 ND«O.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) B-I-20 06/1 5/99 20 ND«O.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) B-I-25 06/1 5/99 25 ND«O.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) B-2-5 06/15/99 5 ND«O.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) B-2-10 06/15/99 10 ND«0.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) B-2-15 06/15/99 15 ND«O.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) B-2-20 06/15/99 20 ND«O.5) NA ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) B-3-5 07/22/99 5 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«O.025) B-3-10 07/22/99 10 ND«O.5) ND«5) ND«O.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) B-3-15 07/22/99 15 ND«0.5) ND«5) ND«0.OO5) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) B-3-20 07/22/99 20 ND«O.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«0.010) ND«0.025) B-3-25 07/22/99 25 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) B-4-5 07/22/99 5 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O,OIO) ND«0.025) B-4-1O 07/22/99 10 ND«O.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«O.025) B-4-15 07/22/99 15 ND«O.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) B-4-20 07/22/99 20 ND«O.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) B-4-25 07/22/99 25 ND«O.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) B-4-30 07/22/99 30 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) B-4-35 07/22/99 35 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) B-4-40 07/22/99 40 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND( <0.0] 0) ND«0.025) B-5-5 07/22/99 5 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) B-5-10 07/22/99 10 ND«O.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«0.025) B-5-15 07/22/99 15 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.O] 0) ND«0.025) B-5-20 07/22/99 20 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«O.OIO) ND«O.025) B-5-25 07/22/99 25 ND«0.5) ND«5) ND«0.005) ND«0.005) ND«0.005) ND«0.010) ND«0.025) Notes: mglkg = Milligrams per kilogram ND = Not detected NA = Not analyzed TPH-g = Total petroleum hydrocarbons as gasoline MtBE = Methyl tert- butyl ether '\. " CAMBRIA ~~.:" Table 1. Dispenser Sample Analytical Data - Shell-branded Service Station - WIC 11204-0462-2100, 101 S. Union Avenue, Bakersfield, California Date Sample ID Depth TPHg MTBE Benzene Tolu~nc Ethylbenzene Xylenes (feet) . (Concentrations reported in milligrams per kilogram) þo 7/10/98 D-1 (2') 2.0 <20 30( 19) <0.1 <0.1 <0.1 <0.1 7/10/98 D-2(2') 2.0 <1.0 0.21 <0.0050 <0.0050 <0.0050 <0.0050 7110/98 D-4(2') 2.0 .2,600 <6.2 <1.2 2.3 1.3 70 7/10/98 D-5(2') 2.0 '58 3.2 <0.050 <0.050 <0.050 1.4 Ahhrevlallons and Noles: TPHg = Total petroleum hydrocarbons as gasoline by modified I!PA Method 8015. MTBl! = Methyl tert-butyl elher by EPA Method 8020. Result in p:II'entheses represents MTDI! by I!PA Method 8260, ßenzene, ethylbenzene. toluene, and total xylenes by I!PA Method 8020. <n= Below detection limit of n milligrams per kilograms . . ~ ~ FIGURES· " APPENDIX A EXPLORATORY BORING LOGS I . \ I I I LOCATioN MAP " / , / \ ~/ /', "</ ", , , , , "" ,/-:/ ~\, (/ HIGHWAY 58 .. ,', ". ", ,-' ::' ~ PACIFIC ENVIRONMENTAL GROUP, INC. BORING NO. B-1 'I PAGE 1 OF 1 w N PROJECT NO. 705-131,1B CLIENT: EQUIVÄ ::J I LOGGED BY: P. TEENSMA DATE DRILLED: 6-15-99 z w DRILLER: BC2 ENVIRONMENTAL LOCATION: 101 S. UNION AT HIGHWAY 58, ~ DRILLING METHOD: DIRECT PUSH BAKERSFIELD ð SAMPLING METHOD: PROPRIETARY HOLE DIAMETER: 2" z SAMPLER HOLE DEPTH: 26' ::J CASING TYPE: NA WELL DIAMETER: NA SLOT SIZE: NA WELL DEPTH: NA GRAVEL PACK: NA CASING STICKUP: NA EH '. z 0..-. -' BOREHOLE w~ -~ ~ w LITHOLOGY/REMARKS ~~ C<: BACKFILL a:::z Ê w a. >- - ç =>w a. :r:..-. C<: :!; ~~ ~ ~:š: ~~ w w ~z Wo a.w > -' ....J o a. Ô 00 0 z....J WW u ::; ~ü ã: wlJ) o!:S w « CI) a.~ C<: (J CONCRETE: 4" Dp 190.5 Dp 77.4 Dp 45.3 Dp 14.1 Dp 1.2 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 ML SILT: (Alluvium); clayey; medium-dark olive brown; low to moderate plasticity; trace clay; faint hydrocarbon odor. @ 10': as above; some clay. @ 15': as above; trace very fine to very coarse grained sand; no hydrocarbon odor. CLAYEY SILT: (Alluvium); orangish olive brown; low to moderate plasticity; with clay; no hdyrocarbon odor. SP SAND: (Alluvium); gravelly; light brownish gray; medium texture; fine to coarse grained sand; trace fine gravel; poorly sorted; poorly graded; subangular; no hydrocarbon odor. BOTTOM OF BORING 26' LOCATION MAP i PACIFIC ENVIRONMENTAL GROUP, INC. BORING NO. B-2 'I PAGE 1 OF 1 W N PROJECT NO. 705-131.1B CLIENT: EQUIVÄ ::> I LOGGED BY: P. TEENSMA DATE DRILLED: 6-15-99 z W DRILLER: BC2 ENVIRONMENTAL LOCATION: 101 S. UNION AT HIGHWAY 58, ~ DRILLING METHOD: DIRECT PUSH BAKERSFIELD ð SAMPLING METHOD: PROPRIETARY HOLE DIAMETER: 2" z SAMPLER HOLE DEPTH: 21' :J CASING TYPE: NA WELL DIAMETER: NA SLOT SIZE: NA WELL DEPTH: NA GRAVEL PACK: NA CASING STICKUP: NA .. , ' , , , ~ ' " #/ " '( " ... "~,{;# HIGHWAY 58 z 0- -' BOREHOLE « wI-- -I-- 6: W LITHOLOGY/REMARKS BACKFILL C:::z Ê ~~ w ~ 0.. >- f- ç :Jw 0. I- 0:: ~ I 1--1-- ~ I--~ 1--1-- w w 0.. ~z Wo o..W > -' ~ ....I 0 o a. ë5 00 Z....l wW U ::;: :2ü ã: WeD o!:S w « C.9 Cf) 0......- 0:: tJ) CONCRETE: 4" Dp 372 Dp 33.9 Dp 50.1 Dp 3.2 2 4 6 ML 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 SILT: (Alluvium); clayey; medium-dark olive brown; low to moderate plasticity; some clay; moderate hydrocarbon odor. CLAYEY SILT: (Alluvium); sandy; olive brown; low to moderate plasticity; with clay; trace very fine to very coarse grained sand; poorly sorted; poorly graded; no hydrocarbon odor. SANDY SILT: (Alluvium); clayey; olive brown; with very fine to fine grained sand; trace clay; poorly sorted; poorly graded; no hydrocarbon odor. CLAYEY SILT: (Alluvium); sandy; olive brown; low to moderate plasticity; with clay; trace very fine to very coarse grained sand; poorly sorted; poorly graded; no hydrocarbon odor. BOTTOM OF BORING 21' LOCA TfoN MAP BRUNDAGE . . -'.- ~ -- , " <,,:,/~ "', , , '.. ,/ , / '~";:) · . · . . · , : "---~----~---~'-'--------_.~-----,--' . ;..:.:< ---'-'-'---.---.-----.-.-.---.- A N PROJECT NO. 705-131.1B I LOGGED BY: P. TEENSMA DRILLER: GREGG DRILLING DRILLING METHOD: HSA SAMPLING METHOD: CA S.SPOON CASING TYPE: NA SLOT SIZE: NA GRAVEL PACK: NA PACIFIC ENVIRONMENTAL GROUP, INC. BORING NO. B-3 PAGE 1 OF 1 CLIENT: EQUIVA DATE DRILLED: 7-22-99 LOCATION: 101 S. UNION AT BRUNDAGE, BAKERSFIELD HOLE DIAMETER: 8" HOLE DEPTH: 25' WELL DIAMETER: NA WELL DEPTH: NA CASING STICKUP: NA z 0- -' BOREHOLE UJI- -I- ~ UJ LITHOLOGY/REMARKS BACKFILL a:z Ê !;¡:u. w º a. a:Cñ > ~ ç =>UJ 0- J:- a:: ~ J: 1-1- S I-~ 1-1- w w a... ~z UJo a...UJ > -' C2 ..J 0 o D- O 00 z..J UJUJ u ::;¡ ~o ã: UJoo o!:!:. w « ø (/) a...~ a:: (J) ASPHAL T: 4" _i_ _ _ L _ _ _ \; <:::~~." '-. B-3 e\ \,\ ~ "'-': z " UJ ,I ~ '-" z o Z H => Dp 0 Dp 0 Dp 0 Dp 0 Dp 0 2 4 10 6 8 14 10 12 14 22 16 18 34 20 22 24 34 26 28 30 32 34 36 38 40 42 44 ML SILT: (Alluvium); clayey; medium olive brown; low to moderate plasticity; some clay; no hydrocarbon odor. CLAYEY SILT: (Alluvium); medium dark olive brown; low to moderate plasticity; with clay; no hydrocarbon odor. SILT: (Alluvium); clayey; medium olive brown; low to moderate plasticity; some clay; no hydrocarbon odor. SANDY SILT: (Alluvium); clayey; medium olive brown; low to moderate plasticity; with very fine to medium grained sand; trace clay; no hydrocarbon odor. SP SAND: (Alluvium); light brownish gray; medium texture; fine to very coarse grained sand; poorly sorted; poorly graded; very faint hydrocarbon odor. BOTTOM OF BORING 25' /' LOCA ION MAP BRUNDAGE .. -'- - - -',- - - -it- - --, ~---' " B-4' " --- / . / /' < / . '.¿' ", " " . / "~,{; A w N PROJECT NO. 705-131.1B :J I LOGGED BY: P. TEENSMA as DRILLER: GREGG DRILLING ~ DRILLING METHOD: HSA z SAMPLING METHOD: CA S.SPOON o z CASING TYPE: NA :J SLOT SIZE: NA GRAVEL PACK: NA BORING NO. B-4 PAGE 1 OF 1 CLIENT: EQUIVÄ DATE DRILLED: 7-22-99 LOCATION: 101 S. UNION AT BRUNDAGE, BAKERSFIELD HOLE DIAMETER: 8" HOLE DEPTH: 40' WELL DIAMETER: NA WELL DEPTH: NA CASING STICKUP: NA PACIFIC ENVIRONMENTAL GROUP, INC. z o~ ..J BOREHOLE wI-- -I-- ~ W LITHOLOGY/REMARKS BACKFILL C:::z Ê ~~ w ~ a. >- I- ç :Jw a. ::r:~ II:: ~ ::r: 1--1-- .e: I--s: 1--1-- w w a. ~z Wo a.w > ..J ~ ...J 0 o a. Õ 00 z...J WW u :::;¡ ~ü ã:: WCD o!:s w <:: (!) CJ) a. ~ II:: VJ ASPHAL T: 3" Dp 0 Dp 0 Dp 0 Dp 0 2 4 10 6 ML 8 13 10 12 14 24 16 18 20 20 22 24 Dp 42,7 26 26 28 Dp 25.3 30 30 32 34 Dp 10.7 26 36 38 Dp 1.0 30 40 42 44 ........ SILT: (Alluvium); clayey; medium dark olive brown; low to moderate plasticity; trace clay; no hydrocarbon odor. @ 15': as above; some clay; trace medium grained sand. @ 20': as above. @ 25': as above; grayish olive; some fine to coarse grained sand; stained; moderate hydrocarbon odor. SP SAND: (Alluvium); brownish gray; fine texture; fine to coarse grained sand; poorly sorted; poorly graded; angular to subangular; faint hydrocarbon odor. @ 35': as above; gravelly; subangular; very faint hydrocarbon odor. @ 40': as above. BOTTOM OF BORING 40' LOCATION MAP BRUNDAGE ~ Z 0...... ...J BOREHOLE wI- -I- ~ w LITHOLOGY/REMARKS BACKFILL D:::z Ê ~~ w 0 a. =:Iw > I- ç Co :r:...... cr: ;¡; :r: 1-1- .9: I-~ 1-1- w w a. ÇQz Wo a.LU > ...J ~ -J 0 o C- O 00 z-J WW u ;:¡ :2:0 ë: weD o!:S w « (!) C/) a._ cr: (J) ASPHAL T: 4" 2 4 Dp 0 12 6 ML SILT: (Alluvium); sandy; medium olive brown; low plasticity; some very fine grained sand; no hydrocarbon odor. 8 Dp 0 21 10 @ 10': as above; clayey; some clay; trace very fine to very coarse grained sand. 12 14 Dp 0 31 @ 15': as above. 16 //' , , ,- < ,,// "', , , , , , , , , . , . / ~>:/ Dp 0 Dp 0 ~ w N PROJECT NO. 705-131.1B =:I I LOGGED BY: P. TEEN SMA z w DRILLER: GREGG DRILLING ~ DRILLING METHOD: HSA ð SAMPLING METHOD: CA S.SPOON z CASING TYPE: NA =:I SLOT SIZE: NA GRAVEL PACK: NA BORiNG NO. 8-5 PAGE 1 OF 1 CLIENT: EQUIVÄ DATE DRILLED: 7-22-99 LOCATION: 101 S. UNION AT BRUNDAGE, BAKERSFIELD HOLE DIAMETER: 8" HOLE DEPTH: 25' WELL DIAMETER: NA WELL DEPTH: NA CASING STICKUP: NA PACIFIC ENVIRONMENTAL GROUP; INC. 18 35 20 22 24 SM 19 26 28 30 32 34 36 38 40 42 44 SANDY SILT: (Alluvium); clayey; medium olive brown; low plasticity; with very fine to fine grained sand; trace clay; no hydrocarbon odor. SILTY SAND: (Alluvium); medium texture; fine to very coarse grained sand; with silt; poorly sorted; slightly graded; subrounded to subangular; no hydrocarbon odor. BOTTOM OF BORING 25' · i:' APPENDIX B FIELD PROCEDURES .' FIELD PROCEDURES DPT Drilling and Soil Sampling Procedures. Each boring location was cleared of underground structures by notifying Underground Service Alert and hand digging the upper portion ofthe borehole using a hand auger. All soil borings were then drilled using a DPT hydraulic push rig with a I-inch diameter sampler. Upon reaching the desired sampling interval, the driller opened the sampler and advanced the assembly an additional 24 inches. Soil samples for chemical analysis were retained in stainless steel liners, capped with Teflon™ and plastic end caps, labeled, and sealed in ZipLock™ bags. The samples were placed on ice for transport to the analytical laboratory and accompanied by chain-of-custody documentation, A PEG geologist logged the boring samples using the Unified Soil Classification System. BC2 washed all down-hole sampling equipment between samples in a non-phosphate detergent and rinsed them successively with potable and distilled water. Upon completion, each DPT boring was backfilled with bentonite clay chips and the pavement restored. HSA Drilling and Soil Sampling Procedures. Each boring location was cleared of underground structures by notifying Underground Service Alert and hand digging the upper portion of the borehole using a hand auger. All soil borings were then drilled using a HSA rig, Upon reaching the desired sampling interval, the driller advanced a 2-inch inside diameter California modified split spoon sampler an additional 18 inches. Soil samples for chemical analysis were retained in brass or stainless steel liners, capped with Teflon™ and plastic end caps, labeled, and sealed in ZipLock™ bags. The samples were placed on ice for transport to the analytical laboratory and accompanied by chain-of- custody documentation. A PEG geologist logged the boring samples using the Unified Soil Classification System. All down-hole sampling equipment was washed between samples in a non-phosphate detergent and rinsed them successively with potable and distilled water. Upon completion, each boring was backfilled and the pavement restored. Organic Vapor Analysis Procedures. Soil samples collected in the field were analyzed using a RAE Systems MiniRAE photo-ionization detector (PID), The PID was calibrated using an isobutylene standard of 98 parts per million by volume (ppmv). The test procedure involved placing approximately 30 grams from a soil sample into a new ZipLock™ bag, The bag was sealed and allowed to warm to ambient temperature. The bag was then pierced and the headspace tested for total organic vapor, measured in parts per million (ppm) as isobutylene. PEG staff recorded the headspace readings on the boring logs included in these appendices. - . .' APPENDIX C CERTIFIED ANALYTICAL REPORT AND CHAIN-OF-CUSTODY DOCUMENTATION · if =a/SCienCe ~§nVironmental Ii aboratories, Inc. June 23, 1999 Pat McCullough Pacific Environmental Group, Inc. 650 Sierra Madre Villa, Suite 204 Pasadena, CA 91107 Subject: Calscience Work Order No.: Client Reference: 99-06-0438 101 South Union Avenue, Bakersfield, CA Dear Client: Enclosed is an analytical report for the above-referenced project. The samples included in this report were received 06/17/99 and analyzed in accordance with the attached chain-of-custody. The results in this analytical report are limited to the samples tested and any reproduction of this report must be made in its entirety. If you have any questions regarding this report, require sampling supplies or field services, or information on our analytical services, please feel free to call me at (714) 895-5494. Sincerely, ca~ Env~ Laboratoriés, Inc. Don Burley Project Manager 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 >< III _ a/science - nvironmenta/ S aboratories, Inc. Analytical Report Page 1 of 1 LABORATORY ID: 99-06-0438 Method: EPA 8015M/8021B TPH(g)/BTEXlMTBE Matrix: Soil/Solid CLIENT: PROJECT: Pacific Environmental Group, Inc. 101 South Union Avenue, Bakersfield, CA Results Sample ID Benz Tol EtB Xyls MTBE TPH-G PID Sur Ree FID Sur Ree Dilution Date (mg/kg) (mglkg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) BFB(%) BFB(%) Factor Analyzed B-1-5 ND ND ND ND ND ND 78 86 1 06/19/99 8-1-10 NO NO NO NO ND ND 79 86 1 06/19/99 B-1-15 NO ND NO NO NO NO 78 85 1 06/19/99 B-2-5 ND ND ND ND ND ND 81 88 1 06/19/99 8-2-10 ND NO NO ND NO ND 78 85 1 06/19/99 8-2-15 ND NO NO NO ND ND 89 96 1 06/19/99 B-1-20 ND NO ND ND ND NO 78 85 1 06/19/99 8-1-25 ND ND NO NO ND ND 76 83 1 06/19/99 B-2-20 NO NO NO ND NO NO 83 96 1 06/21/99 Method Blank ND ND ND ND ND ND 74 80 1 06/18/99 Method Blank NO ND ND ND ND ND 81 92 1 06/21/99 Reporting Limit: 0.005 0.005 0.005 0.010 0.025 0.5 47-137 34-141 Quality Assurance and Control Information Matrix Spike Sample 10: 99-06-0477-12 Batch 10: Spike LCS 4~~'·<· RPO 99061801 Cone. Result ·':~Elt; Control ppm ppm .)¡.(%) Limits Benzene 0.100 0.0937 0-15 Toluene 0.100 0.0954 0-18 Ethyl benzene 0.100 0.0996 0-17 p/m-Xylenes 0.200 0.199 0-17 o-Xylene 0.100 0.0982 0-13 MTBE 0.100 0.102 0-23 TPH-Gasoline 2.00 1.86 0-30 Matrix Spike Sample ID: B-2-20 Batch ID: Spike LCS RPD 99062101 Cone. Result Control ppm ppm Limits Benzene 0.100 0.0942 0-15 Toluene 0.100 0.0951 0-18 Ethyl benzene 0.100 0.0981 0-17 p/m-Xylenes 0.200 0.197 0-17 o-Xylene 0.100 0.0971 0-13 MTBE 0.100 0.0968 0-23 TPH-Gasoline 2.00 2.17 0-30 Key: Benz=Benzene, Tol=Toluene, EtB=Ethyl benzene, Xyls=Total Xylenes, MTBE=Methyl t-butyl ether, Sur-Surrogate, Rec=Recovery, BFB=Bromofluorobenzene, FID=Flame Ionization Detector, PID=Photoionization Detector, ND=Not Detected at the re ort;n level 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501 .,. ËQ U, V (\. ~E"\2.\) ìC CS TURN AROUND TIME Select one only o 24 hrs. 0 48 hrs. . 15 days (Normal) 0 Other Analvsis ReQuired I WIIC OR FACILITY ID: "20 t.t - 4- J. (02- 2-\ 00 10\ ~. \)N'or~ Ã\)~. a,"'''E\'ù?rll::1.-I) ~t\"r MCc.u ~oJG. ~ 65t> ~I~A- MAtJ~vlLV. PMAf>n.JÀ (b..M2) ~~I!..1 ' ~ ~A~ I Site Address: ConsultanUContact: ~ddress: ~hone: ~he" Engineer: I Waste Protocol I Number I S~mpled bl UST A~ency: M-~~Hâ'i) Field Sample ID I \3- \ - 5 J - I - 1 0 ¿ - I - \ 5 J- 2 - 5 J-2-'O J- "2-_\ S I ~ I ~fO~r'~V\ . () T r- f\-"\) Ö N I~ I II I Start Time (military) 12-: oC> p \~E"NSM^ r·'\>, I Sample Time ~ gj o a. (military) ~ :2 o 0 () « t\ \ ·Z: 5B \3:ct l 3: oq \ ~: 51t.:> 1 If: 0 ( \ 'f :0 9 \ G. H ~s T wi £>2 Co 0 \...~SMA ~Cé\- !!! Q) c ïii ë 0 'EÆ u 0 ~9 z N N Iii en en Õ ~ -E I- () () · °l " 01 e DI · 01 · 0 I · 0\ Mt~G Fa P- Date: Time: Date: ~ ..- ~ N ..- g~ ~$OWater in ~ ~ .- o ~ '2 8. . Soil ~ 0 ~ ~ 00 x~- EEE o~:::: ~- WXN~LOLO~~IO~R.$8.~ ~ WON 0 0 g ~ N g N I 00 0 ~~~f6~~_~~~~Q.ð~ -.-.x- x-X-øUJ,-ø ~ ~ w X ~ ~ ¥ ~ w UJ u - ~ ~ ± ± I- W ~ ~ ~ ~ I- U 0 ~ ø ~ ~ ~ ~ I- ~ ~ ~ ~ ~ 0 > Q) Q) _ I- I- ~ m I- I- I- I- ~ > en ~ I- 0 · Date: o (p / \ · · · · · r~·tf 7OS- rbl. I 8> CHAIN OF CUSTODY RECORD II 5/~4 -CA- Results to: I) Consult. OShell CLASS TYPEIDET AIL TYPE Select one only o Site Invest (4441) 0 Wtr RemlSys (4453) Page C:> \ of... D 1- o Soil Clas/Disp (4442) . o Wtr Clas/Disp (4443) o Soil/Air Rem/Sys (4452) o GW. Monitor (4461) . Other II'lC. tt q¡ CZ't 51 D7- SAMPLE MATRIX Select one only o Sludge 0 Sediment o Bedrock 0 Other o NAPL o Vapor LAB USE ONLY Lab Tracking No.: ~4 -Cb- (f43~ Sample Condition/Comments C.C>NL~N- B,O [2., · ed~nature): eceived By (signature): re): Cooler Temperature: . aterial Description t-J SOIL- ::Z~ Printed Name: Date:" rh~ Time: o'9,S Date: Printed Name: Time: Date: "4fG'ý [Ç- STODY WITH INVOICE AND RESULTS II II I ~. \:::Qui vA- ~~v\CES OOlJe=r-S COM P ANY re&~ 70Ç -13{, ifS. CHAIN OF CUSTODY RECORD II I WIC OR FACILITY 10: I-z.-Ö t - 4 -z. G 2- - ¿.... I 0 0 \015, UN I O¡..J Þ..Jt'1. çv.~F'eJ'> £&. M€' '- t.:> ","-,-0 l.)~ J:!.. b'P '7I1~ Mko (1e- Vi ~ PIIT/(f)g.J Þr- (c.."1-b) ?t? 1-1.f91 Lf f ¡;;¡) plH)~ I Site Address: ConsultanUContact: ~ddress: fhone: ~hell Engineer: I Waste Protocol I Number I I S~mpled by: I UST A~ency: p .i:i ~ C- 6L Date: b Co / I 5 /49 -c..A: Results to: . Consult. OShell CLASS TYPE/DET AIL TYPE Select one only o Site Invest (4441) 0 Wtr Rem/Sys (4453) Page D 2_of... 0 1- TURN AROUND TIME Select one only o 24 hrs. 0 48 hrs. . 15 days (Normal) 0 Other o Soil Clas/Disp (4442) o Wtr ClaslDisp (4443) o Soil/Air RemlSys (4452) Start Time (military) \ 2.-: DO .,...... G" ~ ~ S 1/\ A I Sample Time ~ ~ ('I't) &. Q. ml I ary E :g o 0 (.) « :~D F.P, l 3 3: '1: 3i "25 2.-~O l I J!! ~$~e; E o (.) 14 I!! Q) e ïii ë 0 ~ (.) E J::. 0 ~ õ z , N N ~ (/) (/) E ... l- e (.) (.) . D/ . 0 l II 0) Analvsis Reauired ~ N ~ o N CO 0 ìñ £e ~ II') o ~ co 0 x!£.- uJ X ~ I- uJ tj ID I- co ~ !!:! ~ Q. Q. ?,5 ± ± I- Q. a. ID I- I- ::2: . SAMPLE MATRIX o Water 0 NAPL . Soil 0 Vapor ~~ ~ 'õ .~ 2l ~E~EÊ g..!!!. nI _It)LOU)-o-o-~~ _......_~-:(DOI'-~a.·- N 0 0 0 co ~ ~ ~ ~ ~ ~ g~~~~~~~2lc a. -CLW)("'-'><-f/)",~.!!.. XI ¥:::r:wø()-.E~ W I ± I Q. I- (.) 0 ~ ø Q) I- a. Q. Q. ~ ID 0 > m ~ 5 ID I- I- I- I- ::2: > (/) ~ I- 0 II o ~~ I II I · · · · · · p~G,~ \ TeaJ~AA Printed Name: Date: o GW. Monitor (4461) . other I Nt ~ C(i qq 5] 02- Select one only o Sludge 0 Sediment o Bedrock 0 Other LAB USE ONLY Lab Tracking No.: 99 -Ob-043~ Sample Condition/Comments Cooler Temperature: . $ c.\ t... Material Description Printed Name: tS STODY WITH INVOICE AND RESULTS Date: II ßA veø?y I eL-1) Fi;eld Sample ID 9- I - ~Ö I ß- , - I cp- I E _alSCience ~ nvironmental .. aboratories, Inc. July 26, 1999 Eva Rogers Pacific Environmental Group, Inc. 650 Sierra Madre Villa, Suite 204 Pasadena, CA 91107 Subject: Calscience Work Order No.: Client Reference: 99-07 -0557 101 South Union Avenue, Bakersfield, CA Dear Client: Enclosed is an analytical report for the above-referenced project. The samples included in this report were received 07/22/99 and analyzed in accordance with the attached chain-of-custody. The results in this analytical report are limited to the samples tested and any reproduction of this report must be made in its entirety. If you have any questions regarding this report, require sampling supplies or field services, or information on our analytical services, please feel free to call me at (714) 895-5494. Sincerely, ~ C cien e Environmental Laboratories, Inc. Larry Lem Project Manager William H. Christensen Quality Assurance Manager 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 å =alSCience - Environmental ø aboratories, Inc. Analytical Report Page 1 of 2 LABORATORY ID: 99-07-0557 Method: EPA 8015M/8021B TPH(g)/BTEXlMTBE Matrix: Soil/Solid CLIENT: PROJECT: Pacific Environmental Group, Inc. 101 South Union Avenue, Bakersfield, CA Results Sample ID Benz Tol EtB Xyls MTSE TPH-G PID Sur Rec FID Sur Rec Dilution Date (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) BFB(%) BFB(%) Factor Analyzed SP-1-1 ND ND 0.018 0.25 ND 39* 90 110 07/23/99 SP-2-1 ND ND ND ND ND ND 74 70 07/23/99 SP-1-3 ND ND 0.046 0.56 ND 20* 93 120 07/23/99 SP-1-2 ND ND ND 0.072 ND 3.7* 85 87 07/23/99 Method Blank ND ND ND ND ND ND 95 91 07/22/99 Reporting Limit: 0.005 0.005 0.005 0.010 0.025 0.5 47-137 34-141 Quality Assurance and Control Information Matrix Spike Sample ID: Batch ID: 99072201 99-07-0511-16 Spike LCS Cone. Result ppm ppm 0.100 0.0886 0.100 0.0903 0.100 0.0889 0.200 0.180 0.100 0.0905 0.100 0.0987 2.00 1.87 RPD Control Limits 0-15 0-18 0-17 0-17 0-13 0-23 0-30 Benzene Toluene Ethyl benzene p/m-Xylenes o-Xylene MTBE TPH-Gasoline * The sample chromatogram does not match that of the gasoline standard. Key: Benz=Benzene, Tol=Toluene, EtB=Ethyl benzene, Xyls=Total Xylenes, MTBE=Methyl t-butyl ether, Sur-Surrogate, Rec=Recovery, BFB=Bromofluorobenzene, FID=Flame Ionization Detector, PID=Photoionization Detector, ND=Not Detected at the re ortin Jevel 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 !Ii _a/science ~nvironmental Laboratories, Inc. Analytical Report Page 2 of2 LABORATORY ID: 99-07-0557 Method: EPA 8015M TPH-Extractable Matrix: Soil/Solid CLIENT: PROJECT: Pacific Environmental Group, Inc. 101 South Union Avenue, Bakersfield, CA Results Sample ID TPH·E FID Sur Rec Dilution Date Date (mg/kg) DCB(%) Factor Extracted Analyzed SP-1-1 180 98 1 07/23/99 07/23/99 SP-1-3 170 96 1 07/23/99 07/23/99 SP-1-2 14 105 1 07/23/99 07/23/99 Method Blank ND 120 1 07/23/99 07/24/99 Quality Assurance and Control Information Reporting limit: 5 52-135 Matrix Spike Sample ID: SP-1-1 Batch ID: Spike LCS RPD 99072303 Conc. Result Control ppm ppm Limits TPH-Extractable 400 399 0-29 The sample chromatograms are similar in appearance to the JP-5 Standard Ke: Rec=Recove FID=Flame Ionization Detector DCB=Decachlorobi hen I ND=Not Detected at the re ortin level 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714)894-7501 Jul 23 SS 04:0Sp Pacific Env. Group - PAS 626-351-4822 p. 1 . PACIFIC ENVIRONMENTAL GROUP. INC. Facsimile Cover Sheet To: Larry Lem Calscience Environmental Laboratories, Inc. Fax (714) 894-7501 Paul Teensma Pacific Environmental Group, Inc. PHONE: 626-351-4814 FAX: 626-351-4822 July 23, 1999 former Shell Service Station 101 S. Union @ Brundage PEGIIT No. 705-131-1B From: Date: RE: No. Sheets: 3 including transmittal sheet Larry, Thanks for yoUr quick turnaround of the sample analyses on this project thus far and your prompt response to my questions. As we discussed, let's run the 80 IS-extractable analyses for samples SP-I-I, SP-I-2, and SP-I-J. Also, in your report(s) please correct the sample designalions (no "foot" marks). Regarding the additional samples that yoúr courier will deliver today, please run the standard 8015 TPH-g and 8021 for MBTEX. ConfIrm the highest MillE per boring using method 8260. Also. analyze the sample with the highest TPH-g per boring for 80 IS-extractable. The first three characters of each Field Sample ID designate the boring location (for example, B-3). There are three borings from this lot (B-3, B-4, and 8-5). Lastly, please note that the sample for disposal characterization should be performed on standard turnaround time. . Let me know if you have any questions or concerns. Thanks, Paul \\PEG-S\DA TA\1'ROJEC1\70S-cqui\1 3 I\F072399.DOC II Chain of Custody Record ('I) -. (\ ( J CI m Il. ... ... t-. .Q o '") v (\ .. o m (]) - (\ N - ('I) o (]) v o I? ll) ('I) (\ 0\ ~ 10 () /!} W H o Z <! U) C) w Il. >- .Q +' C W U) SITE ADDRESS: _, /0 I ú,.;o~ 7).'''__/;;51-- II ., --.-- SITE ID Number: Dale Slarl lime ,mIlitary): '~'o'ý'- 'ýl~l, '.¿I-b_I/lo 0111 [iliJ/rn/EG] CD:DJ ~ [[[] - CD ¡ [[[]] Re$ults to: . Sampler 0 Clienl / ~ ~h~ Name -L'Æ~ I_,_L ç..~.. J ~_"L...:-_2?~:6:~,.~~~.......",T..f . Address ,_~_~~~~~~ _ /"'!~~_,,=-__t'..f~.:-._,_.._u____. City ,a.L.~4~oo;. ..~__.___ Stale C-!f: Zip 1 /~___ Phone ¡t:,l..¿) 1.r/ _ ¢,y/ý Cllenl: Sampled by: o 14 day (sId.) 1?'4'~T/I 'TI~'e-J~IJ ~I~ I I Time: Name: Date: 7í 2. Z. Time: //~ d HIE LA80RATORY MUST PROVIOi Á·COPYOF HilS E E¿.I ;;{ ¿,., - £5 ....,t,.¿; . UST Agency: ..r c 6#]) Field Sample ID I j: . I ..r: ?c. 7,-;e,.. k Printed Name: J ~ I; Coo'nr OJ 0 . lomporatur~ . ~~ 11me: /ÔÇü Dale: II Page EEJ of ... rn ACS TYPEIQ¡:IAIJ...Jì"PE Self/c' one only . SlIe Inve$1 (4441) 0 Wlr Rorn'SV" (-1453) o Söil ClaslOisp (4442) 0 GW. Monitor (4461) TURN AROUND TIM!; Selec;t one only . Other I nC. I ðent o ., 2~ hr. ~ 0 48 hr 0 Wlr Clas/Disp (4443) c-r-TTl o 72 hr. 0 1 day 0 Other 0 SolVAit RemlSvs (4452) ~ ;:- ..... Analvsis ReClUired SAMPLE MATRI~ Select 0118 only ~ (.f rn- - ~ 0 Water 0 NAPL 0 Sludge 0 Sediment ~ ~ ~ ¡ . Soil 0 Vapor 0 Bedrock 0 0Ihør g Ó "I'> & ~ ~ _I B USE ONLY xe.~ ÊÊ~' ~ô~6'Ô -'È: l: LA 'èi (': I ~ 0 ~ ~ ~ ~ ~ ~ ~ ~ ; ~ ~ ~ ~- ~ í i ð i lab Tracking No,; Sample Time .~ ~ - ( z.~ ~ @ x S ~ ~.,. ~ x S '" ,1/1 !'!. '" é õ ~ C}Q-D1--0 r-:t"} ( III' ta) ~ .~ ~ ~ ~ § It q. uJ >< ~ i ~i~ . if ~ ~ g g 'ë i ~; ¡ s;;;-pls Coodi1len/Comments m ry '''........0 ~ælñ~Il.l1.·~a:lIlo» 041 Oil£; ß ~ lj t3 ... ... ~ <11 ... t-!8' t- ~ > <I) ;¡; I.) -I .-: 1- 0 I il1 Mjf ¡®' %¡:.~ ;;~1 ~;!I )jt iP ~*-~ ~ì ~~~ [ ..J .J>. - / - I 0 41.~.,)<·.~.,~:¡o ~,. 0 / .¥.. ° QJO ~¡o ~o y~O 1(;;0 ~~O q~o >" ,f ? - ~. - . /~' . . . 0 10~. 0 I I\~o ~jo a~~o Q~jo ~o '10 1'~0 ~o ,"; I I S ? - / ' Ü t· ~,:iio ¡::o ¡~,o ~o (10 '~1o ð!o I I . . . . - . J, . . , . / .r :~o :,. 0 I ..0 i $ '," ~ iI\ .~ >J , ' ..J J>. - I. - .2' . . . . 1 J : Z- 1~1o ~J. 0 11" 0 d10 Q!O ~o ~o ~;.o ~o ~o I I 1\ g' rœ ;·a r~ .ì j ~ ff. . I . ~o: 0 . ;0 ~10 (5\0 èio YJO q~o ÿJO ,·~o ( I . . . I · '. . ~1~ ~1 ;~ ]!~ t:1 t1~ .~~ Qì!! ~o J. 0 ~ ' I R;IO (f¡o Q-tO yjO 0::,0 9:0 y~O ;.:~o ~~ ,~,:.; ..~! I I . '. ... . . i;!:\1 ¡;~:I~1:) t;:;J iil~. ¡!J. ~:~ :;:lei ~\'<' ~i:¡ M: IE] _ Material Uc!)cnp!l()!I -----. Name: REvI:>EO ð-~8 ~ ã_a/SCience - 1¥nvironmental I- aboratories, Inc. July 26, 1999 Gary Pestana Pacific Environmental Group, Inc. 650 Sierra Madre Villa, Suite 204 Pasadena, CA 91107 Subject: Calscience Work Order No.: Client Reference: 99-07-0651 101 South Union, Bakersfield, CA Dear Client: Enclosed is an analytical report for the above-referenced project. The samples included in this report were received 07/23/99 and analyzed in accordance with the attached chain-of-custody. The results in this analytical report are limited to the samples tested and any reproduction of this report must be made in its entirety. If you have any questions regarding this report, require sampling supplies or field services, or information on our analytical services, please feel free to call me at (714) 895-5494. Sincerely, C scien nvironmental Laboratories, Inc. Larry Lem Project Manager 1/;1 /fzZL William H. Christensen Quality Assurance Manager 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501 Ë -a/science ~ gnvironmenta/ .. aboratories, Inc. Analytical Report Page 1 of 1 LABORATORY ID: 99-07-0651 CLIENT: PROJECT: Method: EPA 8015M/8021 B TPH(g)/BTEXlMTBE Matrix: Soil/Solid Pacific Environmental Group, Inc. 101 South Union, Bakersfield, CA Results Sample ID Benz Tol EtB Xyls MTBE TPH-G PID Sur Rec FID Sur Rec Dilution Date (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) BFB(%) BFB (%) Factor Analyzed B-3-5 ND ND ND ND ND ND 81 80 1 07/24/99 B-3-1 0 ND ND ND ND ND ND 87 88 1 07/24/99 8-3-15 ND ND ND ND ND ND 86 85 1 07/24/99 B-3-20 ND ND ND ND ND ND 88 87 1 07/24/99 B-3-25 ND ND ND ND ND ND 100 98 1 07/24/99 B-4-5 ND ND ND ND ND ND 80 80 1 07/24/99 B-4-10 ND ND ND ND ND ND 84 84 1 07/24/99 B-4-15 ND ND ND ND ND ND 87 87 1 07/24/99 B-4-20 ND ND ND ND ND ND 83 83 1 07/24/99 B-4-25 ND ND ND ND ND ND 85 84 1 07/24/99 B-4-30 ND ND ND ND ND ND 85 84 1 07/24/99 B-4-35 ND ND ND ND ND ND 85 84 1 07/24/99 8-4-40 ND ND ND ND ND ND 90 89 1 07/24/99 B-5-5 ND ND ND ND ND ND 81 82 1 07/24/99 B-5-10 ND ND ND ND ND ND 84 83 1 07/25/99 B-5-15 ND ND ND ND ND ND 83 83 1 07/25/99 B-5-20 ND ND ND ND ND ND 82 82 1 07/25/99 8-5-25 ND ND ND ND ND ND 87 88 1 07/25/99 Method Blank ND ND ND ND ND ND 99 97 1 07/24/99 Reporting Limit: 0.005 0.005 0.005 0.010 0.025 0.5 47-137 34-141 Quality Assurance and Control Information Matrix Spike Sample ID: Batch ID: 99072401 B-3-5 Spike Conc. ppm 0.100 0.100 0.100 0.200 0.100 0.100 2.00 RPD Control Limits 0-15 0-18 0-17 0-17 0-13 0-23 0-30 Benzene Toluene Ethyl benzene p/m-Xylenes o-Xylene MTBE TPH-Gasoline LCS Result ppm 0.0902 0.0924 0.0916 0.185 0.0931 0.104 2.03 Key: Benz=Benzene, Tol=Toluene, EtB=Ethyl benzene, Xyls=Total Xylenes, MTBE=Methyl t-butyl ether, Sur-Surrogate, Rec=Recovery, BFB=Bromof1uorobenzene, FID=Flame Ionization Detector, PID=Photoionization Detector, ND=Not Detected at the re ortin level 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 Jul 23 99 04:09p ?dC ¡F" l C E..,v. Group - PAS 626-351-4822 p. ~ . . PACIFIC . ENVIRONMENTAL GROUP, INC. Facsimile Cover Sheet . ':'~ To: Larry Lern i ': Ca1science Environmental . Laboratories) Inc. ,1 Fax (714) 894-7501 . ., From: Paul Teensma Pacific Environmental Group) Inc. PHONE: 626-351-4814 FAX: 626-351-4822 Date: July 23, 1999 RE: former Shell Service Station 101 S. Union @ Brundage PEG/IT No. 705-13I-IB No. Sheets: 3 including transmittal sheet - - - Larry Thanks for your quick turnaround of the sample analyses on this project thus far and your prompt response to my questions. As we discussed, let's run the 80 IS-extractable analyses for samples SP- 1-1, SP- I -2, and SP-I-J. Also, in your report(s) please correct the sample designalions (no "foot'" marks). Regarding the additional samples that yoUr courier will deliver today, please run the standard 80 IS TPH-g and 8021 for MBTEX. Conftrm the highest MillE per boring using method 8260. Also, analyze the sample with the highest TPH-g per boring for 80 IS-extractable. The first three characters of each Field Sample ID designate the boring location (for example, B-3). There are three borings from this lot (B-3, B-4, and 8-5). Lastly, please note that the sample for disposal characterization should be performed on standard turnaround time. Let me know if you have any questions or concerns. Thanks, Paul \\PEG-S\DA T A\PROJEcn70S-equi\ t J I\F072399.00C . EQu\ v~ ~~ff ,o5-f31. \ B ~ CHAIN OF CUSTODY RECORD II I II I WIC OR FACILITY ID: 11-0 t - t2- ~2-- 2-\ 0 0 ~S.\.NIO,..1& ¡'(Z.<JfoJPltGë: ~ELþ -~~Cq·I'T· ~..¡ - -- (:oS(:) ~~ t-'ffpPE"" \J~~o'J6 ('""')_~ P_A- \:r- p~ I Site Address: ~onsultantlContact: ~ddress: Ifhone: ¡;¡hell Engineer: I Waste Protocol I Number I S~mpled by; I UST A~ency: Start Time (military) p °l T\:: E"" tJ ~ fI\ fT ~J\i!aesF'El..D F. Þ. FU~ld Sample ID ~- ~ - S- J-3>-\ 0 I ß- 3> I s "3 - 2-0 I ~- 3- '2-5 I ~- ~ ~ I ÎþoNrlJL.M o rP0 YL(N Ý ~~ I II FORM BY IMTRAN I 5" (0 t1\d vJ\¡-H Printed Name: ~C.EL esults to: Date: Page 0 I of ... C>.3 °1/1-'2-/'9 . Consult. OShell CLASS TYPE/DET AIL TYPE Select one only o Site Invest (4441) 0 Wtr Rem/Sys (4453) - CA- o Soil ClaslDisp (4442) o Wtr ClaslDisp (4443) o GW, Monitor (4461) . Other 'Nt:. t'f cy~ 'F1 ~I 02. TURN AROUND TIME Select one only . 24 hrs. 0 48 hrs. 0 15 daYs (Norm.l) 0 other o Soil/Air Rem/Sys (4452) Analvsis Reauired .... SAMPLE MATRIX N .... g ~ ~ ~ 0 Water 0 NAPL iìs ~ ~ .- o ~ 'ij¡ 8. . Soil 0 Vapor coo a.( ) - x~- EEE -!l.:::: m_ WI- Wx NO.... ~II) II) ~;:::ß ô12 ~ 8.~ ~ ~ ~ 0 ~ N ~ N .- ø 0 ~:D ~g ~~~~ ~2 ~ 8.0 8- ;;-;;-x~ )(~x~( )( )....f/I ~ ~ w X ~ ~ ~ x w w U - ~ ~ ± ± I- W I I I Q. I- 0 0 ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ õ >c ( ) :¡; c: ïii c: o o ci z ¡;¡ Õ I- X'" )( )( )( " \¡¡ J I ?EYl- 1:'-' Sample Time i ~ (military) ~ ; o 0 o « o q . o í' lO·DD l o· 0 Ð I 0 ~o or> yb 52- ::::- êii E .r:. ~ Õ ___ I N N (/) (/) c: c: o 0 . -r- ~1 ' €:>2-c.o ~3 ~ rz... .J Time: t7~ THE LABORATORY MUST PROVIDE A COPY OF THIS CHAIN OF 52- DI · 0 I · 0 I ·Of . 0' · 0 ( y\t:?1"" h..t:;~~ V1 €"""T H <9 j) Select one only o Sludge 0 Sediment o Bedrock 0 other LAB USE ONLY La~;l~¿o':T -06> I Sample Condition/Comments Cooler Temperature: Material Description 'SOIL- Date: II Date: Time: Date: Time: Date. ~. .p ~ ~ 7~-r~'. /Þ- . CHAIN OF CUSTODY RECORD 1ë:::"Q0 \ v' ~ WIC OR FACILITY ID: þ..O 'f - \.f 2-0 2- - '2--1 0 ð 10\ S UÑI OÑ@ ~.-1Þ1«..e- ~aJ\ .ä /'" .~ \ 1>. Q'...J ,n- or<:. IVI-u _.-7 _I ..... "'7' ~ ~ ~ ~ ,Cð.c:;1:) ',..- ",..JJ.. AI\ \ J.. . A ....... ," {"'2r",~ ~<::: _ ¥~ I'" ""'- _ TURN AROUND TIME Select one only ~.. ... 24 hrs. 0 48 hrs. 0 15 days (Norm.l) 0 other Results to: . Consult. P 0.., f D 3 age t.- 0 H' OShell CLASS TYPE/DET AIL TYPE Select one only o Site Invest (4441) 0 wtr Rem/Sys (4453) o Soil Clas/Disp (4442) 0 G.W. Monitor (4461) o Wtr ClaslDisp (4443) ~ other (~Cff o Soil/Air Rem/Sys (4452) 4'i err 51 ð-Z- Date: / "2-2.. /44' - C-A Dc I Site Address: ctonsultantlContact: ~ddress: p¡hone: ~hell Engineer: I . Waste Protocol I Number I S~mpled by¡ I UST A~ency: ~~FIØ-p Field Sample ID ~- i - l Ð ~-f--l5 ~-'f-7-0 ~- f I ~- t4- I _ ~- i - 30 5~t Analvsis ReQuired Start Time (military) Dc¡': 0 0 SAMPLE MATRIX o Water 0 NAPL . Soil 0 Vapor Select one only o Sludge 0 Sediment o Bedrock 0 other N ;:" g~ ~~ ÌÌì !!:1 ~ .- o ~ 'g 8- coo a.(/) x~~ ~E~EÊ (/)~ wX- IO~Ô~Ô ~ W ~ ~ 10 10 _ = ~g~ m ~ 00 N 0 0 ~ ~ 00 - ~ ~~-~~e.-~-£- a.a.~~a.w~~~;-~ I i ~ ~ ± ± i ~ ~ 0 0 a. a. m ~ a. a. a. ~ m 0 > y~ ::2: m I- I- ~ ~ ::2: > en (/) Q¡ c: ïii ë o u o z -¡¡¡ Õ I- Te::e-Ñ<;.I-1A- sample Time ~ ui o !!! (military) ~ ; o 0 U <C l 1 : 00 I { \ I : ( : "'2- 1-- I . ? IU ~8.~ .- (/) 'õ ~ .- CII a. a a. ~.e~ "'C _ êii IU (/) .c ~ !!. õ LAB USE ONLY Laq~ël~J--OJ 5 L Sample Condition/Comments E Q¡ .c ~ 9 N N en en "E "E u u . . . 4Ø . 4) ~·P. 01 01 °1 01 o \ -{ 0\1 x: X X :0 ð 10 - Þ5 30 ( l . z.-GJ : '3 0 I 1 (/) c: CII E E f~~e- l Cooler Temperature: . o u Material Description L ~~ I II FORM BY IMTRAN I Printed Name: \...- ~ I/l1>r :;;;;;e: Printed Name: Date: Date: Time: Time: Date: Time: THE LABORATORY MUST PROVIDE A COPY OF THIS CHAIN Time: SHELL CHAIN OF REVISED 12197 II ~. EQ0\VI\:- Ç>~ it 7-OS - /3> 1. 1f2. CHAIN OF CUSTODY RECORD II I flC OR FACILITY ID: pO i - 'f 2- b 2-. - 2- \ D ð I I I~ I II FORM BY IMTRAN I IN< Vt-J/OtJ - .- Df=:'f"~ I rr- (". ~ ... _en -¿ o:wJ&A. , ,_ o¡.C. 1 J.<J _ II Pi v.. t::.ß ' (\ .ä RI ...J -'" A- i...... - I ~-~ Start Time (military) D9: cð 1'Gt=N S Vt,4 F,D. I Sample Time ~ gj ('I't) 8. c. ml I ary E :E o 0 U « l'/ :'fþ l '2-: ~ ) I "2-: 3~ \ -z..: ~ 3 "2-: 5 2- "3>:05 ~ -;-C? I I fA-4~ ( ~ Date: c.. EL o 7 / ~ 1-/ '1 c¡ - c::.4 TURN AROUND TIME Select one only "24 hrs. 0 48 hrs. 0 15 days (Normal) 0 other Analvsis ReQuired N ~ !!! 0 N ~~ Q !:e 0 c: IS) !:e ~ '&j ïã 0 IS) :rl a. ë ex) 0 a.UI 0 ~ ex) ÊÊÊ UI ~ .. u x ~ ~~:::o ~ uJ x N ~ IS) IS) IS) E Q .s:: ci I- uJ 0 N 000 cci N g !:::i ~ Õ Z aJ I- ~ Oex)ex)~ ~~~~ I ~ III X ex)~~ Ñ Ñ ñi Q: ~ a. uJ ~ - >< - ø a. uJ ::I: uJ UI U ~ en Õ ± ± >< I I I ë -E l- I- W :I: :I: :I: a. I- U 0 a. a. III I- a. a. a. Ir III 0 > U U l- I- ~ III l- I- l- I- ~ > en " O} " i'1 Ü I .. ., 0/ 4f M 0 I If AM 0 I .., * 0 I A Results to: o Consult. Po 3 f 0 3 age 0 ... OShell CLASS TYPE/DET AIL TYPE Select one only o Site Invest (4441) 0 Wtr Rem/Sys (4453) o Soil ClaslDisp (4442) 0 GW. Monitor (4461) o Wtr ClasJDisp (4443) . other I ~tT o Soil/Air Rem/Sys (4452) qt '11 5/ 02- SAMPLE MATRIX o Water 0 NAPL ø Soil 0 Vapor RI UI ~ ~ 0 ~ ~ a. ._ 1iî .!!1 g a.oa. ~.E~ -g g¡ ~ ~ I- Õ Select one only o Sludge 0 Sediment o Bedrock 0 other LAB USE ONLY Lab Tracking No,: S!~ -01--06 5L Sa p e CondItIon/Comments Cooler Temperature: . Material Description '50\ t..- Date: Time: Date2 Time: Date: ?/ Received Time: ~S- THE LABORATORY MUST PROVIDE A COPY OF THIS CHAIN Printed Name: Date: Time: Date: II I Site Address: Consultant/Contact: Address: ~hone: ~he" Engineer: W~ste Protocol I Number Sah,pled by:~ Þ I UST Agþncy: ß,I\.....""" .... - (t3-D Field Sample ID i - 'f - Lf'D ~- 5,- 5 ~- Ç'-tê) J..- ç,- /S" I ,- S r ~- S"' I ~ I ~ ~ e-lZ o U .. E - a/science ~ª nvironmenta/ .. aboratories, Inc. August 03, 1999 Gary Pestana Pacific Environmental Group, Inc. 650 Sierra Madre Villa, Suite 204 Pasadena, CA 91107 Subject: Calscience Work Order No.: Client Reference: 99-07 -0651 101 South Union, Bakersfield, CA Dear Client: Enclosed is an analytical report for the above-referenced project. The samples included in this report were received 07/23/99 and analyzed in accordance with the attached chain-of-custody. The results in this analytical report are limited to the samples tested and any reproduction of this report must be made in its entirety. If you have any questions regarding this report, require sampling supplies or field services, or information on our analytical services, please feel free to call me at (714) 895-5494. scie e Environmental Laboratories, Inc. Larry Lem Project Manager 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 · FAX: (714) 894-7501 ;' ã -a/science ~ nvironmenta/ Laboratories, Inc. Analytical Report Page 1 of 1 LABORATORY ID: 99-07-0651 Method: EPA 8015M TPH(d) Matrix: Soil/Solid CLIENT: PROJECT: Pacific Environmental Group, Inc. 101 South Union, Bakersfield, CA ' Results Sample ID TPH-D FID Sur Rec Dilution Date Date (mg/kg) DCB(%) Factor Extracted Analyzed 8-3-5 ND 65 1 07/30/99 07/30/99 8-3-10 ND 81 1 07/30/99 07/30/99 8-3-15 ND 78 1 07/30/99 07/31/99 8-3-20 ND 84 1 07/30/99 07/31/99 8-3-25 ND 85 1 07/30/99 07/31/99 8-4-5 ND 78 1 07/30/99 07/31/99 8-4-10 ND 74 1 07/30/99 07/31/99 8-4-15 ND 77 1 07/30/99 07/31/99 8-4-20 ND 76 1 07/30/99 07/31/99 8-4-25 ND 75 1 07/30/99 07/31/99 8-4-30 ND 77 1 07/30/99 07/31/99 8-4-35 ND 89 1 07/30/99 07/31/99 B-4-40 ND 78 1 07/30/99 07/31/99 8-5-5 ND 74 1 07/30/99 07/31/99 B-5-10 ND 75 1 07/30/99 07/31/99 8-5-15 ND 79 1 07/30/99 07/31/99 8-5-20 ND 73 1 07/30/99 07/31/99 8-5-25 ND 79 1 07/30/99 07/31/99 Method Blank ND 87 1 07/30/99 07/30/99 Reporting Limit: 5 52-135 Quality Assurance and Control Information Matrix Spike Sample ID: 8-3-25 Batch ID: Spike LCS RPD 99073004 Cone. Result Control ppm ppm Limits TPH-Diesel Fuel 400 414 0-29 Ke: Rec=Recove FID=Flame Ionization Detector DC8=Decachlorobi hen I ND=Not Detected at the re ortin level 7440 Lincoln Way, Garden Grove, CA 92841-1432 · TEL: (714) 895-5494 . FAX: (714) 894-7501 Ju¡ 30 SS 12:00p Pacific Env. Group - PAS 626-351-4822 p. 1 . PACIFIC ENVIRONMENTAL GROUP, INC. ó' Facsimile Cover Sheet To: Larry Lem Calscience Environmental Laboratories, Inc. Fax (714) 894-7501 Paul Teensma Pacific Environmental Group, Inc. PHONE: 626-351-4814 FAX: 626-351-4822 July 30, 1999 Former Shell Service Station 101 S, Union @ Brundage PEG/IT No. 705-131-1B From: Date: RE: No. Sheets: 4 including transmittal sheet Larry, Thanks again for your help and prompt response to my questions regarding the samples from the site referenced above. Regarding the second set of samples from this site (see attached CaC), please run an 8015 analysis for TPH-d. Please perfom1 this analysis on standard turnaround time. Thanks, Paul p<DO I!v ) /.1[ßø6 1>le~ß ¡þ7 , r \s(f"I) ~~ ~~ fjJ !J tJù(l; r( D tÇvtv ,A0 /)\ ¡( /lIt I I ~~#' vJ1þD II Let me know if you have any questions or concems. \\PEG-S\DA T A\PROJECm05-equi\131 \F073099.DOC c..., c: ..... (¡,) 0 .:..., CD F CD I ", .... (h N I t' .. \.LI 0 'J:' UJ 0 " -' .I. /.oJ .I:. .@- ~~ft ,05-('51.\ ð HAIN OF CUSTODY RECORD II ~u\ \!1\. a: Page 0 f 0':-. 03 0.»: . eor.utt. OShell 01 11--'2.../, 9 '2- 0 \f - 'f 2- ~ '2-- 2- \ 0 0 ~~~)~~ ~~:=? ~~E4> ~~~~~l~'" o """ ~(4453 o G.W. MIIfIJor(44ØI) . 00-. 'lolL If "t'11 f;J 02.. o s.t. "'-1 (444 \) o SolI ClnlCiap (06442) o Wtr CIuI~ (4443) o SGWAlr RemIS)'t (4.452) Site Add~ss: ConaultantlContact: Address:' PhOne: Sl'MItl et1 in.ør: ~c.E"L. - c.. A- T\JAH ~ND 11ME SeNd aM Oft'" . 2.. rn. 0 ... "IlL 0 15 œy. (NIIIIIIII 0 Od1er Analvsis ReQuired W... PratOcioI Num_ 8ùIIt 111M ~ (millIa'Y (/ l : ð" 0 "t Q 0 .... -t) r. .... :[\ 0 r ~ m -. !:p :] n c: rn . ;~ C1 0 , ':.. 0 3 c: C") " 3 -~ "t :D en en N en I (¡,) ..., U1 .... .... .þ. I CD ~. oJ) CD m N ~ N w (T, 1) & t. t..i (T¡ II " N ~ N:::' ~ ~ ..... ~ 0 w.. :¡; l> ~ .- i~ l!·~ -2 ~~~ ..-'" x-- EE~ 6'-F;" 111.- W~Ñ~4t>1tI ;::-1D-.J:t.....8.~· ...... ~--- IÓN . ~fÒ -~ !!~i:;!g.~ ë. I õ J D;- ~:;j ~ Or u." X'~ ';;~ -l! ~ lift; ~*&:x~fDgg i'j £; ~ ~ ~ œ ~ ~ ~ ~ 2 > ~ ~ ~ 0 X ONAPL Os~ O~ o VlflClr 0 Bedrock 0 oa.c LAB USE ONLY Lab Trøcklrtg No.: 6: ( , ~1'-() r -0 ~ Sample Condition/Comments ; j ~ ;1 SimpleS IIy. TC e-t-1 ~ '^ Þr f"'" Sample Time '""'III ! (mUltary) :i « oq:yb o 1 . S7- ¡o-oD i o· 0 8 p c- 1! [q N tJ tii U) OJ) "õ ~ ~ ~ u 0 · D \ · 01,)(" · 0 1 X · 0 I' X . (){ )( · 0 ( i. VST þ.genc'(. J~IEl.P Field Sample ID B' - ~ - S- ß- 3Þ - \ 0 ß- ~ - \ 5" 'F.Þ. B-3-2-0 ~- 3- '2-5 B- '"f - 5' I O:~O ( 0 : S 2- Ic..o N'fl 90 YL{ tJ CooIe4" T cmpenrlUIe; ?e-Y2- \1 \ C. Y\~'? í M,.cJi7'£ ~ ,.t1.. l^l \ -r- r1 V\ €""1- H ð D ð 2- ~ 0 P-N\ C, Malúf Deacrlplløn SOIl- nleó _me: II FORW 8Y UCfIWl t.¡ C I-' W 0 '-< c.o c c.o r I 1\1 I-' iJ\ I I\) ... .. \ÍI 0 1..0 u.' I-' " ... .t'. ,. L.-I l> "'t 01 0 .... "i) (') .... D r 0 ~ rr1 .... m :J ~ c: m . :B c;) 0 , '-< 0 ~ C " =! "'t J) en ... f' ~ tr 7C'5~J~'. ¡e,. II CHAIN OF CUSTODY RECORD tE:Qù\ V ~ Page 02- of... D 3 Da!iI: WIC OR FACILITY ID: '"'2-0 ~ - '-f 2.(9 2.. - ~ I 0 0 . Comull. OSMI 01·/ 7-2 J 44' c..A o WttR~(~) o G.W. ...,ac¡, ("'1) .0fIer[~'" 4r~SJ~ o &Ie InWIII (4441) o SGII a-tDllp (-4442) o WIt CIMfDi. (~443) o SOIIIAlI R~ (446'2) Site Address: Con~ltantlContact: Ac:Idms: Phon.: 5hIJl E fneør: w.te Pr'1*œI" NU'IIINr !c..eL- 'J'UAN ARO'*J mE SelfJct one ØIIlf . 2A hrw. 0 48 ....' 0 15 _y. III......' 0 CIIha, Anslvs;s ReQuired _1t'TInM (miIIIar)'J o q: tJ 0 .... s -;:- ~ Ow.. ~ i ~ t . SOl g~ ~ 1-1 'ä M)(:=~î¡~ ~~~~'~t~ ~~iE2§i.~Iß~~b11 ~£!!)(iiS~~ :!.)(~..!t ,;:~ ~ C1. 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'i .-- it£~~fff~~og!i~ t-t- ""' CDt-1- t-... ~ > II)~'" u 't aut Time (mIIlbu)) 09: oð o NAP!. 0 SfudØI 0 acãfnent 0 o "'" 0 twrïdc 0 Oller LAB USE ONLY f! i Q SIn\PIØ ~; oþ C~~¡.J s }./t,4- ... ~} Sample Time i ~ ~ ~ (military) ~ ~ ~ ~ 00( õo l "t : 'I Þ ~ l '2-: ~ ) I '2-: 3 G::. \~'-I3 / '2-: S 2- ~:o5 A UST Agenq: t50 Field Sample ID ~ - 'f ..- lorD ~- 5- 5 ~- ç-- t ð ~-t;;- ,5 ~- s,. 7rÔ ~,.. 5'- 7-5 1 :ty e-\Z f Þr- ~ ~ (J 01 #f (:) I .. ·0/ "0.1 " Aft 0'/ ., þ 0 .. ~~... ìJ ~ . f\ IS! \II (]'I II ~. L. c: ..... CIJ C <-. tc c r- tc I /II ... (]'I I I\) .' ',D C \Jj U) ~ "'IS ... ~ W VI 'tJ DI 0 .... () -t D .... r 0 (f) i) m - (T1 :J Z n c:: fT'I . :B '" 0 , , I 0 :3: c: Ci :I. " -i "C :D en ,~ APPENDIX.D INTERPRETIVE REPORT BY GLOBAL GEOCHEMISTRY/ZYMAX FORENSICS ( , ~ ~ August 20, 1999 Mr. Paul Teensma Pacific Environmental Group, Inc. 650 N. Sierra Madre Villa, Suite 204 Pasadena, CA 91107 Re: Characterization of Hydrocarbons in Three Soil Samples (PEG/IT 705-131-1B) Dear Mr. Teensma: Three soil samples collected by Pacific Environmental Group, Inc. were submitted to Global Geochemistry Corporation/ZymaX forensics on August 8, 1999 for hydrocarbon characterization. To perform the objectives, the three following analytical procedures were employed: 1. Simulated distillation on portions of the soils extracted with carbon disulfide; 2. Gas chromatography/mass spectrometry of a methylene chloride soil èxtract to characterize different hydrocarbon families, RESULTS The simulated distillation results are plotted on a curve (Figure 1) relating percent recovered for different boiling points. Samples SP-1-2 and SP-1-3 give essentially the identical results with initial boiling points at about.340°F and final boiling points at 565°F. The initial boiling point for sample SP-1-1 is about 20°F higher and slowly approaches the curves of the other two samples after about 30% of the distillation initiation. The explanation for this is loss of the most volatile components by evaporative weathering from this sample. The concentration of the soil extracts are shown in Table 1 and range from 1429 µg/g in sample SP-1-1 to 4940 µg/g in sample SP-1-3. The total ion chromatogram in Figures 2-4 show a pronounced 'hump' and set of peaks in the range of 500-1 000 scan numbers, optimizing at about 800 scan numbers. For samples SP-1-2 and SP-1-3 there is an additional broad 'hump' at a higher molecular weight between 1700-2700 optimizing at about 2150 scan numbers. The first group of peaks represent the boiling range shown in Figure 1. However, the second 'hump' at 2150 scan numbers falls in the region of Bunker C (heating oil #6) or a waste oil. Figures 5-25 describe homologous series of hydrocarbons at the following mass numbers: 1. Alkanes (m/z 85 mass chromatograms); 2. Isoalkanes (m/z 113 mass chromatogram); 3. Alkylcyclohexanes (m/z 83 mass chromatogram); 4. C4-alkylbenzenes (m/z 134 mass chromatogram); www.ZymaXforensics.com E~ E~ ~ ~ ß~ ~ E~ ß~ Evé ß~ Evé ß~ ß~ Evé Evé E~ E~ ßvé ß~ ß~ 6919 Eton Avenue Canoga Pork CA 91303-2194 fox 818.992.8940 818.992.4103 71 Zaca Lone Son Luis Obispo California 93401 fox 805.544.8226 805.544.4696 email: Corensics@ZymaXusa.com ~ ;- 5. 6. 7. Terpanes (m/z 191 mass chromatogram); Steranes (m/z 217 mass chromatogram); Polynuclear aromatic hydrocarbons. The patterns for the three samples look essentially the same for groups 1-4 (Figures 5-16). Groups 5 and 6 (terpanes and steranes, respectively), which are high molecular weight biomarkers (Figures 17-22) are only present in samples SP-1-2 and SP-1-3. Both appear to be the same. Group 7 (Figures 23-25), for aromatic compounds show a two-fold distribution. The first group of peaks at 500-1100 scan numbers are represented by alkylbenzenes and naphthalenes whereas the second group optimizing at 2150 scan numbers contain hydrocarbons from fluorene to mono- and triaromatic steranes. CONCLUSIONS The characterization of the mass chromatograms represented by n-alkanes, iso- alkanes, methylcyclohexanes and alkyl benzenes closely resemble that of a mineral spirit- type solvent, most probably stoddard solvent. There is a possibility for jet fuel (JP-4 or JP-5) being present. However, in JP-4 there should be a gasoline fraction present which is not present as seen from Figure 1. If JP-5 (or Jet A) were present as a dominant fuel, the naphthanene PAHs would be more prominent than seen in Figures 22-25. Based on these arguments, we concluded that stoddard solvent is the dominant type of hydrocarbons "fuel" for three analyzed samples, whereas a significant amount of waste oil (heating oil #6) are also present in samples SP-1-2 and SP-1-3. Please let me know if you have any questions. ~ Sincerely, 9~~ Isaac Kaplan Senior Consultant A4896-report.wpd 6919 Eton Avenue Canoga Park CA 91303-2194 fax 818.992.8940 818.992.4103 71 Zaca Lane San Luis Obispo California 93401 fax 805.544.8226 805.544.4696 email: £orensics@ZymaXusa.com ~ .. ~ TABLES .. Table 1 Concentration of extracts for samples submitted by Pacific Environmental Group Sample ID GGCID Sample Extract Sample Weight for Weight Concentration Extraction ( Jg) ( Jg/g) (g) SP-1-1 4896-1 30.3 1429 47 SP-1-2 4896-2 31.3 3840 123 SP-1-3 4896-3 32.8 4940 151 ß~ .. ~ E~ Table 2 Key to Chromatogram Symbol Identification Symbol i-10 i-15 i-16 Pr Ph Detail Iso-al kane 'with 10 carbon atoms Farnesane (isoprenoid with 15 carbon atoms) Isoprenoid with 16 carbon atoms Pristane (isoprenoid with 19 carbon atoms) Phytane (isoprenoid with 20 carbon atoms) n-Ce normal alkane n-C15 normal alkane 2,5-(2,4 )-Dimethylhexane 2,3,4- Trimethylpentane 2,3-Dimethylhexane Alkylcyclohexane (where n indicates number of carbon atoms in the side chain) nCe nC15 i-8 i-8' i-8" CH-n ~ . ß~ Table 3 Key for C4-Alkylbenzenes (m/z 134 mass chromatograms) # Compound 16 See-Butyl benzene 17 1-Methyl-3-lsopropylbenzene 18 1-Methyl-4-lsopropylbenzene 19 1-Methyl-2-lsopropylbenzene 20 1,3-Diethylbenzene 21 1-Methyl-3-Propylbenzene 22 Butylbenzene 23 1,3-Diemethyl-5-Ethylbenzene 24 1,2-Diethylbenzene 25 1-Methy-2-Propylbenzene 26 1,4-Dimethyl-2-Ethylbenzene 27 1.3-Dimethyl-4-Ethylbenzene 28 ·1,2-Dimethyl-4-Ethylbenzene 29 1,3-Dimethyl-2-Ethylbenzene 30 1,2-Dimethyl-3-Ethylbenzene 31a 1,2,4,5-Tetramethylbenzene 31 1.2,3.5-Tetramethylbenzene 32 1.2,3,4-Tetramethylbenzene Code o 1 2 3 4 5 Z4 6a 6b 7 A B C D E F G H 10a 10b I 11a J 11b K C29Ts C30* L Ma Mb N o 13a 13b P Q R 14a S 14b T U 15a 15b V WS WR 16a 16b XS XR YS YR Table 4 Key for Tricyclic, Tetracyclic, and Pentacyclic Terpanes Identification (m/z 191 mass chromatograms) Identity C2o-Tricyclic Terpane C21-Tricyclic Terpane C22-Tricyclic Terpane C23-Tricyclic Terpane C24-Tricyclic Terpane C2çTricyclic Terpane C24-Tetracyclic Terpane C26-Tricyclic Terpane C26-Tricyclic Terpane C27- Tricyclic Terpane C2B-Tricyclic Terpane #1 C2B-Tricyclic Terpane #2 C29-Tricyclic Terpane #1 C29-Tricyclic Terpane #2 18a-22,29,30- Trisnorneohopane (Ts) 17a-22,29,30-Trisnorhopane (Tm) 17ß-22,29-30- Trisnorhopane 17a-23,28-Bisnorlupane C30-Tricyclic Terpane #1 C30-Tricyclic Terpane #2 17 a-28,30-Bisnorhopane C31-Tricyclic Terpane #1 17 a-25-Norhopane C31-Tricyclic Terpane #2 17a,21 ß-30-Norhopane 18a-30-Norneohopane 17 a-Diahopane 17ß-21 a-30-Normoretane 18a-Oleanane 18ß-Oleanane 17a,21 ß-Hopane 17ß,21 a-Moretane C33-Tricyclic Terpane #1 C33-Tricyclic Terpane #2 22S-17a,21 ß-30-Homohopane 22R-17 a ,21 ß-30-Homohopane Gammacerane C34-Tricyclic Terpane #1 17ß,21 a-Homomoretane C34-Tricyclic Terpane #2 22S-17 a ,21 ß-30-Bishomohopane 22R-17 a,21 ß-30-Bishomohopane C3s-Tricyclic Terpane #1 C3çTricyclic Terpane #2 17ß,21 a-C32-Bishomomoretane 22S-17a,21 ß-30,31,32-Trishomohopane 22R-17a,21 ß-30,31 ,32-Trishomohopane C36-Tricyclic Terpane #1 C36-Tricyclic Terpane #2 22S-17a,21 ß-30,31 ,32,33-Tetrahomohopane 22R-17a,21 ß-30,31 ,32,33-Tetrahomohopane 22S-17a,21 ß-30,31,32,33,34-Pentahomohopane 22R-17a,21 ß-30,31,32,33,34-Pentahomohopane Carbon # 20 21 22 23 24 25 24 26 26 27 28 28 29 29 27 27 27 28 30 30 28 31 29 31 29 29 30 29 30 30 30 30 33 33 31 31 30 34 31 34 32 32 35 35 32 33 33 36 36 34 34 35 35 ~ .. Code 1 2 3 4 5 6 70 7 80 8 9 90 10 11 12 13 140 14 15 16 17 18 19 20 21A 218 22A 228 23A 238 24A 248 Table 5 ~ Key for Steranes Identification (m/z 217 Mass Chromatogram) Identity 13ß,17 a-diacholestane (20S) 13ß,17a-diacholestane (20R) 13a,17ß-diacholestane (20S) 13a,17ß-diacholestane (20R) 24-methyl-13ß,17a-diacholestane (20S) 24-methyl-13ß,17 a-diacholestane (20R) 24-methyl-13a, 17ß-diacholestane (20S) 14a,17a-cholestane (20S) 24-ethyl-13ß,17 a-diacholestane (20S) 14ß, 17ß-cholestane (20R) 14ß, 17ß-cholestane (20S) 24-methyl-13a,17ß-diacholestane (20R) 14a,17a-cholestane (20R) 24-ethyl-13ß,17 a-diacholestane (20R) 24-ethyl-13a, 17ß-diacholestane (20S) 24-methyl-14a,17a-cholestane (20S) 24-ethyl-13a,17ß-diacholestane (20R) 24-methyl-14ß, 17ß-cholestane (20R) 24-methyl-14ß,17ß-cholestane (20S) 24-methyl-14a,17a-cholestane (20R) 24-ethyl-14a-cholestane (20S) 24-ethyl-14ß, 17ß-cholestane (20R) 24-ethyl-14ß, 17ß-cholestane (20S) 24-ethyl-14a,17a-cholestane (20R) 24-n-Propylcholestane (20S) 4-methyl-24-ethylcholestane (20S) 4a-methyl-24-ethyl-14ß,17ß-cholestane(20S) 24-n-propyl-14ß,17ß-cholestane (20S) 4a-methyl-24-ethyl-14ß,17ß-cholestane(20R) 24-n-propyl-14ß,17ß-cholestane (20R) 4a-methyl-24-ethylcholestane(20R) 24-n-propylcholestane (20R) Carbon # 27 27 27 27 28 28 28 27 29 27 27 28 27 29 29 28 29 28 28 28 29 29 29 29 30 30 30 30 30 30 30 30 ß~ Table 6 Key for Aromatic Compounds Identification in Bar Diagram AB: C3-C6 Alkylbenzenes NAPH: CO-C4 Naphthalenes FL: CO-C4 Fluorenes BP: CO-C2 BP Biphenyl/Oibenzofuran PHEN: CO-C4 Phenanthrenes PY: CO-C4 Pyrenes/Fluoranthenes CHR: CO-C4 Chrysenes BT: C1-CS Benzothiophenes OBT: CO-C4 Oibenzothiophenes NBT: CO-C4 Naphthobenzothiophenes MAS: Monoaromatic Steranes TAS: Triaromatic Steranes >' No. 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 28 39 40 41 42 43 44 45 46 47 48 49 50 51 52 Table 7 ~ Key for Identifying Aromatic Hydrocarbons m/z 120 134 148 162 128 142 156 170 184 166 180 194 208 222 154 168 182 178 192 206 220 234 202 216 230 244 258 228 242 256 270 284 148 162 176 190 204 184 198 212 226 240 234 248 262 276 290 253 267 239 231 245 Compound C3-alkylbenzenes C4-alkylbenzenes Cs-alkylbenzenes C6-alkylbenzenes Co-naphthalene C1-naphthalenes C2-naphthalenes C3-naphthalenes C4~naphthalenes Co-fluorene C1-fluorenes C2-fluorenes C3-fluorenes C4-fluorenes Co-biphenyl C1-biphenyls + dibenzofuran C2-biphenyls + C1-dibenzofuran Co-phenanthrene C1-phenanthrenes C2-phenanthrenes C3-phenanthrenes C4-phenanthrenes Co-pyrene/fl uoranthene C1-pyrenes/fl uoranthenes C2-pyrenes/fl uoranthenes C3-pyrenes/fl uoranthenes C 4-pyrenes/fl uoranthenes Co-chrysene C1-chrysenes C2-chrysenes C3-chrysenes C4-chrysenes C1-benzothiophenes C2-benzothiophenes C3-benzothiophenes C4-benzothiophenes Cs-benzothiophenes Co-dibenzothiophene C1-dibenzothiophenes C2-dibenzothiophenes C3-dibenzothiophenes C4-dibenzothiophenes Co-naphthobenzothiophene C1-naphthobenzothiophenes C2-naphthobenzothiophenes C3-naphthobenzothiophenes C4-naphthobenzothiophenes Monoaromatic steranes Monoaromatic steranes Monoaromatic steranes Triaromatic steranes Triaromatic steranes ~ FIGURES - LL 400 . C) Q) "C - Q) 5 300 ... CU ... Q) Co E Q) 200 I- ¡wø1 Figure 1: Simulated Distillation Curves 600 500 100 o o 80 90 100 50 60 70 30 40 10 20 Percent recovery Figure 2 ... RIC DATA: 21055 11 SCANS 200 TO 2600 08/04/99 12:25:00 CALI: 21055 13 SAMPLE: SP-l-1 (A4896-1) SOIL EXT 0.6UL OF 150UL+0.5UL STD COHOS.: TI=40ITI=5.0ITI2=310,T2=25,R=4 RANGE: G 1,2600 LABEL: N 0, 4.0 QUAN: A 0, 1.0 J 0 BASE: U 20, 3 100.0 RIC 500 15: 11 1000 30:21 1500 45:32 31008. 2000 60:43 2500 75:53 SCAN TIME Figure 3 ~. ¡,. r RIC DATA: 21062 #1 SCANS 250 TO 2800 08/06/99 13:41:00 CALI: 21062 #3 SAMPLE: SP-1-2 (A4S96-2) SOIL EXT 1.2UL OF 100UL INJ COHOS.: TI=40,TI=5.0,TI2=310,T2=25,R=4 RANGE: G 1,2800 LABEL: N 0, 4.0 QUAN: A 0, 1.0 J ø BASE: U 20, 3 100.0 73600. RIC 500 15:11 1000 30:21 1500 45:32 2000 60:43 2500 75:53 SCAN TIt1E Figure 4 RIC DATA: 21057 #1 . SCANS 250 TO 2800 08/05/99 11: 23: Ø0 CALI: 21057 13 SAMPLE:SP-1-3 (A4896-3)' SOIL EXT 1.0UL OF 260UL +0.5UL STD CONDS.: TI=40ITI=5.0ITI2=310IT2=25IR=4 RANGE: G 112800 LABEL: N 01 4.0 QUAN: A 01 1.0 J 0 BASE: U 201 3 100.0 RIC 500 15: 11 2000 60:43 2500 75:53 1000 30:21 1500 45:32 .. ¿ 74880. SCAN TIME 100.0 85 Figure 5 MASS CHROMATOGRAM DATA: 21055 11 SCANS 200 TO 2600 98/04/99 12:,~: 00 CALI: 21055 13 SAMPLE: SP-1-1 (A4896-1) SOIL EXT 0.6UL OF 150UL+0.5UL STD CONDS.: TI=40,TI=5.0,TI2=310,T2=25,R=4 RANGE: G 1,2600 LABEL: N 0, 4.0 QUAN: A 0, 1.0 J 0 BASE: U 20, 3 ...... .... \.J ,..¡ ~ \) ~ <) .... \.; ~ ~ ~ ~ & ~ "" \J ~ 500 15: 11 1000 30:21 ~ .... \..J ~ \..J ~ 1500 45:32 2000 60:43 2500 75:53 ~ ,. , 1754. 85.025 t. 8.588 SCAN TIME Figure 6 MASS CHROMATOGRAM DATA: 21062 tU SCANS 200 TO 2800 08/06/99 13:41:00 CALI: 21062 #3 SAMPLE: SP-1-2 (A4896-2) SOIL EXT 1.ZUL OF 100Ul INJ CONDS.: TI=40/TI=5.0/TI2=310/T2=25/R=4 RANGE: G 1/2800 LABEL: N 0, 4.0 QUAN: A 0, 1.0 J 0 BASE: U 20/3 100.0 3716. ~ \J ~ Q \J ~ ...¡ \f ~ ~ ~ 85 I't\ \J ~ ç} ~ 500 15: 11 1000 30:21 1500 45:32 2000 60:43 2500 75:53 85.025 ± 0.500 SCAN TIME 100.0 Figure 7 MASS CHROMATOGRAM DATA: 21057 11 SCANS 200 TO 2800 08/05/99 11:23:00 CALI: 21057 13 SAMPLE: SP-1-3 (A4896-3) SOIL EXT 1.0UL OF 260UL +0.5UL STD COHOS.: TI=40ITI=5.0ITI2=310IT2=25IR=4 RANGE: G 112800 LABEL: N 01 4.0 QUAN: A 01 1.0 J 0 BASE: U 201 3 ...... \} ~ ~ o ~ "" ~ ~ \...J~ ~ 85 \) ~ ^" \J ~ 500 15: 11 1000 30:21 2000 60:43 2500 75:53 1500 45:32 . I 4600. 85.025 :t: 0.500 SCAN TIME Figure 8 MASS CHROMATOGRAM DATA: 21055 #1 SCANS 200 TO 1900 08/04/99 12:25:00 CALI: 21055 #3 SAMPLE: SP-l-l (A4896-1) SOIL £XT 9.6UL OF 159UL+0.5UL STD COHOS.: TI=40,TI=5.0,TI2=310,T2=25,R=4 RANGE: G 1,2600 LABEl: N 0, 4.0 QUAN: A 0, 1.0 J 0 BASE: U 20, 3 100.0 680 939 ~ I f; o .... I H 545 113 601 ~ \ ti 384 200 6:04 400 12:09 600 18:13 "- ... ( t; 788 ~ "- I H 739 1012 N - I H ~ \ \"'\ 800 24:17 1200 36:26 1400 42:30 1000 30:21 1600 48:34 1800 54:38 . I 279. 113.034 ± 0.500 SCAN TIME Figure 9 .. t1ASS CHROMATOGRAM DATA: 21062 #1 SCANS 200 TO 1900 08/06/99 13:41:00 CALI: 21062 #3 SAMPLE: SP-1-2 <A4896-2) SOIL EXT 1.2UL OF 100UL INJ CONOS.: TI=40JTI=5.0JTI2=310JT2=25JR=4 RANGE: G IJ2800 LABEL: N 0J 4.0 QUAH: A 0J 1.0 J 0 BASE: U 20J 3 679 100.0 545 <:) " I Ii ~ I N 761. CV\ - 786 I t; 937 113 113.034 737 :I: 0.500 0....... 60e ~ I " H I N I'J 384 "'- 101e I H 200 6:04 4øe 12:09 600 18:13 800 24: 17 . SCAN TIME 1000 30:21 1200 36:26 1400 42:30 1600 48:34 1800 54:38 Figure 10 .. MASS CHROMATOGRAM DATA: 21057 #1 SCANS 200 TO 1900 08/05/99 11:23:00 CALI: 21057 #3 SAMPLE: SP-1-3 (A4896-3) SOIL EXT 1.0UL OF 260UL +0.5UL STD CONDS.: TI=40/TI=5.0/TI2=310/T2=25/R=4 RANGE: G 1/2800 LABEL: N 01 4.0 QUAN: A 01 1.0 J 0 BASE: U 201 3 680 546 100.0 1011. (;) " \ M ....... .... I \; 787 ()....... I'f'j 1" 113 \ H 113.034 \-I ± 0.500 *- 938 - \ 385 t-\ 602 738 '" 1012 ì N 439 200 6:04 400 12:09 600 18:13 800 24:17 1000 30:21 1200 36:26 1400 42:30 1600 48:34 1800 54:38 SCAN TIME Figure 11 .. MASS CHROMATOGRAM DATA: 21055 11 SCANS 200 TO 1600 08/04/99 12: 25: 00 CALI: 21055 13 SAMPLE: SP-l-1 (A4896-1) SOIL EXT 0.6Ul OF 150Ul+0.5UL STO CONOS.: TI=40,TI=5.0/TI2=310/T2=25/R=4 RANGE: G 1/2600 LABEL: N 0, 4.0 QUAN: A 0, 1.0 J 0 BASE: U 20, 3 772 100.0 506. ~85 ~ ~ ~ ~ \J 830 905 \0 { ~ \j 83 83.025 ~ 619 964 ± 0.509 531 465 <\.. , ~ o ~ ~ ~ 200 6:04 400 12:09 ·600 18: 13 800 24:17 1000 30:21 1200 36:26 1400 42:30 1600 SCAN 48:34 TIME Figure 12 MASS CHROMATOGRAM DATA: 21062 #1 SCANS 200 TO 1600 Ø8106/99 13:41:00 CALI: 21062 13 SAMPLE: SP-1-2 (A4896-2) SOIL EXT 1.2UL OF 100UL INJ CONOS.: TI=40ITI=5.0ITI2=310IT2=25IR=4 RANGE: G 112800 LABEL: N 01 4.0 QUAN: A 01 1.0 J 0 BASE: U 201 3 684 100.0 ~ ð 530 83 O'J ð 464 389 200 6:04 400 12:09 60Ø 18:13 ~ I ~ \) ~ 767 617 900 ~ ~ 962 800 24: 17 1000 30:21 1200 36:26 1400 42:30 .. 1472. 83.025 :I: 0.500 1600 SCAN 48:34 TIME Figure 13 MASS CHROMATOGRAM OATA: 21957 #1 SCANS 200 'To 1699 08/05199 11:23:00 CALI: 21057 #3 SAMPLE: SP-I-3 (A4896-3) SOIL EXT 1.0UL OF 260UL +0.5UL STO COHOS.:. TI=40/TI=5.0/TI2=319/T2=25/R=4 RANGE: G 1/2800 LABEL: N 9, 4.9 QUAM: A 9, 1.9 J 8 BASE: U 20, 3 685 100.8 ~ ~ ~ ~ Ù (] I't\ 829 \ ~ 0 531 769 183 I '" { \.) 618 r-J I ~ Ù 399 984 465 964 571 200 6:84 400 12:89 600 18:13 1008 38:21 se0 24:17 1154 1249 1200 36:26 1364 1400 42:30 1476 1564 ... :< 1968. 83.025 :I: 9.500 1600 SCAN 48:34 TIME Figure 14 MASS CHROMATOGRAM DATA: 21055 #1 SCANS 600 TO 875 08/04/99 12:25:00 CALI: 21055 13 SAMPLE: SP-1-1 (A4896-1) SOIL EXT 0.6UL OF 150UL+0.5UL STD COHDS.: TI=40JTI=5.0JTI2=310JT2=25JR=4 RANGE: G 1J2600 LABEL: N 0J 4.0 QUAN: A 01 1.0 J 0 BASE: U 20J 3 796 100.0 134 ~ 656~ '\0,,- " " 600 18:13 650 19:44 rt. '- Ii It 710 699 ~ 700 21:15 ~738 d ~ ~ ~ 720 "" ri ~ f'(\ 773 750 22:46 In \t- ~ ~ ('(\ 837 S00 24:17 850 25:48 -.. 3116. 134.040 ± 0.500 SCAN TIME Figure 15 MASS CHROMATOGRAM DATA: 21062 #1 SCANS 600 TO 875 08/06/99 13:41:00 CALI: 21062 13 SAMPLE: SP-1-2 (A4896-2) SOIL EXT 1.2UL OF 100UL INJ COHOS.: Tl=40ITl=5.0ITI2=310IT2=25IR=4 RANGE: G 112800 LABEL: N 01 4.0 QUAN: A 01 1.0 J 0 BASE: U 201 3 793 100.0 134 ';\ ~ c\ 698 ~ 611 ''''' .... " 600 18:13 650 19:44 700 21:15 I'C\ ~ 707 ~ '^ 736 ~ 721 ~ 744 C) ~ 771 't' 752 750 22:46 .......... ~ 1(\ "- Ii' 800 24: 17 ~ ((\ 834 850 25:48 .. 4864. 134.040 :t: 0.500 SCAN TIME Figure 16 MASS CHROMATOGRAM DATA: 21057 11 SCANS 600 TO 875 æ/05/99 11: 23: 00 CALI: 21057 13 SAMPLE: SP-1-3 (A4896-3) SOIL EXT 1.0UL OF 260UL +0.5UL STD COHOS.: TI=40ITI=5.0ITI2=310IT2=25IR=4 RANGE: G 112800 LABEL: N 01 4.0 QUAN: A 01 1.0 J 0 BASE: U 201 3 794 100.0 ~34 ..... r& " " 698 ~ ,~ " " 600 18:13 650 19:44 70e 21:15 '¡\ 708 \o'~ ~37 * 716 1) ~ "- IY\ ~ 745 ~ tC\ 835 ~ '<\ 772 ~ 750 22:46 800 24:17 S5e 25:48 6368. 134.040 ± 0.500 SCAN TIME Figure 17 U I MASS CHROMATOGRAM DATA: 21055 11 SCANS 1800 TO 2600 08/04/99 12:25:00 CALI: 21055 13 SAMPLE: SP-1-1 (A4896-1) SOIL EXT 0.6UL OF 150UL+0.5UL STO CONeS.: TI=40ITI=5.0ITI2=310IT2=25IR=4 RANGE: G 112600 LABEL: H 01 4.0 QUAN: A 01 1.0 J 0 BASE: U 201 3 100.0 Ab~ 2334 2357 191 1800 54:38 2000 60:43 2100 63:45 2200 66:47 2300 69:49 1900 57:41 2437 2492 28. 2541 191.057 ± 0.500 2400 72:51 2600 SCAN 78: 56 TIME 2500 75:53 Figure 18 .. MASS CHROMATOGRAM DATA: 21062 11 08/06/99 13: 41: 00 CALI: 21062 13 SAMPLE: SP-1-2 (A4896-2) SOIL EXT 1.2UL. OF 100UL INJ CONDS.: TI=40ITI=5.0ITI2=310IT2=25/R=4 RANGE: G 112800 LABEL: N 0, 4.0 QUAN: A 01 1.0 J SCANS 1800 TO 2800 100. o BASE: U 20, 3 2490 *" t 2436 413. ~ ~ 191 R ~ 2356 ~~ 2558 191.057 ± 0.500 I'i\ 1962 ~ ()- ~~ ~ 2133 2080 ~ ~ct) 2266\1 ~ 2303 .. ~ " '\( ~~ 2619 1800 54: 38 2000 60:43 2200 66:47 2400 72:51 2600 78:56 2800 SCAN 85:00 TIME Figure 19 100.0 MASS CHROMATOGRAM DATA: 21057 11 SCANS 1800 TO 2800 08/05/99 11:23:00 CALI: 21057 13 SAMPLE: SP-I-3 (A4896-3) SOIL EXT 1.0UL OF 260UL +0.5UL STD COHOS.: TI=40,TI=5.0,TI2=310,T2=25,R=4 RANGE: G 1,2800 LABEL: N 0, 4.0 QUAN: A 0, 1.0 J 0 BASE: U 20, 3 2492 ~ * 2438 ~ ,~ 2560 191 1800 54:38 2000 60:43 2600 78:56 2200 66:47 2400 72:51 .. 316. 191.057 ± 0.500 2800 SCAN 85:00 TIME Figure 20 MASS CHROMATOGRAM DATA: 21055 #1 SCANS 2150 TO 2525 08/04/99 12: 25: 00 CALI: 21055 #3 SAMPLE: SP-1-1 (A4896-1) SOIL EXT 0.6UL OF 150UL+0.5UL STO COHOS.: TI=40ITI=5.0ITI2=310IT2=25/R=4 RANGE: G 1/2600 LABEL: N 01 4.0 QUAN: A 01 1.0 J 0 BASE: U 201 3 100.0 Ab~ . 217 2150 65:16 2200 66:47 2250 68:18 23ß0 69:49 2350 71:20 2400 72:51 2450 74:22 2500 75:53 1. 217.065 ± 0.500 SCAN TIME Figure 21 MASS CHROMATOGRAM DATA: 21062 11 SCANS 2150 TO 2525 . 08/06/99 13:41:00 CALI: 21062 13 SAMPlE: SP-1-2 (A4896-2) SOIL EXT 1.2UL OF 100Ul IHJ CONDS.: TI=40,TI=5.0,TI2=310,T2=25,R=4 RANGE: G 1/2800 LABEL: N 01 4.0 WAN: A 01 1.0 J 0 BASE: U 201 3 2317 100.0 217 2172 2150 65:16 ~ "" ~ 2248 " 2194 I'( 2216 \¡ 2266 2200 66:47 2250 68: 18 2292 2390 69:49 ~ .. ~~ ~ ~ 2361 2380 2433 "- ... ~~ 2397' " 2409 ~ "" .... 2334 2350 71:20 2400 72:51 2457 2487 2450 74:22 2500 75:53 163. 217.065 :t 9.59Ø SCAN TIME Figure 22 MASS CHROMATOGRAM DATA: 21057 11 SCANS 2150 TO 2525 08/95/99 11:23:00 CALI: 21057 #3 SAMPLE: SP-1-3 (A4896-3) SOIL EXT 1.0UL OF 260UL +0.5UL STD CONDS.: TI=40ITI=5.0ITI2=310IT2=25IR=4 RANGE: G 112800 LABEL: N 01 4.0 QUAN: A 01 1.0 J 0 BASE: U 201 3 2318 100.0 217 2171 2161 2195 2150 65:16 2200 66:47 2208 2294 2249 2222 2259 2236 j 2250 68: 18 2300 69:49 2382 2410 2350 2363 2398 2335 2350 71: 20 2499 72:51 2434 2450 . 2450 74:22 2476 2500 75:53 73. 217.065 :t e.see SCAN TIME 100 90 80 70 -4-> ~ ;::j 60 0 S ~ Q.) 50 :> '..... ..¡..) cd 40 .-4 (!) ~ 30 20 10 0 Figure 23 Aromatic Hydrocarbon Distribution SP-1-1 I I. ----- ----- ----- ----- AS NAPH FL BP PHEN PY CHR Aromatic Hydrocarbons Global Geochemistry Corporation - - - - - - - - - - - - - - - - - - -- - - BT DBT N3T MAS T AS Sulfur Cmpds Steranes 100 90 80 70 +-> ~ ;j 60 0 S <r: a.> 50 :> '.-4 +-> ~ 40 ....... a.> ~ 30 20 10 0 Figure 24 " Aromatic Hydrocarbon Distribution SP-1-2 I lit.. - . . I _ - - - . . . . . . - - - . . - AS NAPH FL BP PH EN PY CHR Aromatic Hydrocarbons Global Geochemistry Corporation ----- . - - - - BT DBT f\BT MAS T AS ----- Sulfur Cmpds I I _ I I - - Steranes 100 90 80 70 -+-' Q ;:1 60 0 S <r: ( ) 50 ~ ...... -+-' cIj 40 .~ ( ) p:::; 30 20 10 Figure 25 ~ Aromatic Hydrocarbon Distribution SP-1-3 o I ,IlL ----- ----- ----- ----- AS NAPH FL BP PHEN PY CHR Aromatic Hydrocarbons Global Geochemistry Corporation - - - - - - - - - - - - - - - BT DBT (\J3T Sulfur Cmpds . . - I. - - MASTAS Steranes ~ APPENDIX . QA/QC DATA & CHAIN OF CUSTODY m/z 217 26 I m/z 113 Pristane 1 Tricyclic Terpane C4- Alkylbenzenes m/z 134 ©( R m/z 1 91 R R = C4H7 R = H. CH3. C2H5 Monoaromatic Sterane (MAS) T etracyclic T erpane R R " m/z 1 91 . m/z 253 R = H. CH3. C2Hs R = H. CH3. C2Hs Penta cyclic T erpane Triaromatic Steranes (TAS) " m/z 1 91 m/z 231 " R = H. CH3. C2HS Figure: The compound structures of pristane, C4-alkylbenzene, sterane; terpanes; monoaromatic and triaromatic steranes .t1~;; U~ ~~ l~:"Up JUl-26-1999 17:23 Pacific Env. Group - PAS C~LSC:ENCE PROJ MGMT 626-351-4822 714 æe 2035 p.2 .. P.0V0S ~nce &nv;ronmental ~ L abotatories, Inc. Juty 26, 1999 Eva Rogers Pacffic Environmental Group, Inc. 650 Sierra Madre Vilis. Sui1e 204 Pasadena, CA 91107 Subject: Calscience Work Order No.: Client Ref.renca: 99-01..0557 101 South U.,ion Avenue, Bak.r.field, CA Dear Client Enclosed is an analytical report for the above-referenced project. The samples included in this report were received 07122/99 and analyzed in accordance with the attached chain-of..custody. The results in this analytical report are limited to the samples tested and any reproduction of this report must be made In its entirety. If you have any questions regarding this repert. require sampling supplies or field serviœ!t. Of information on our analytical services. please feel free to call me at (714) 895-5494. Sincerely, William H. ristensen Quality Assurance Manager C cien Environmental Laboratorie$. Inc. Larry lem Project Manager 7440Lin~"Way.Garde"Grove.CA92841·1432 · TEl:(714}895-5494 · FAX: (7'4) 894·7ð01 .HU~ O~ 55 1~:41p JUL-2&-~999 17:24 Pacific Env. Group - PAS CAlSC 1ENCE PROJ MGMT 626-351-4822 '714 898 2036 p.3 ~ P. Ø2/05 'Ence nvironmental 1. aboratories, Inc. Analytical Report Page 1 of2 LA80RA TORY 10 9:)-07-0[.57 JIeUIod: EPA 101S111n%18 'TPHCI)lBTUlMTR 1IatrIJC: SOli/loUd SP·1·t sp.2--, SP.1-3 SP·'·2 Method 81'" ND NO NO NO NO NO HO NO NO NC 0.018 NO 0.046 NO NO 0,15 NO 0.56 0.072 NO NO NO ND NO Nt) 39" NO 20" 3,7" NO 90 74 93 85 95 110 7D '20 87 91 1 1 1 1 , 01/23199 01123199 07123118 07/23199 07122199 BtI'lHf\8 toluene Elhy\ benzene pln'!-Xy¡.nes o-XyIene MTie TPH-G,fOIin8 11:'ft !~ ]:~1~Ei;: ~!~ \if.Jii PD (;coiro! limllS 0-15 0·18 1).17 Oot7 0-13 0.23 0.30 . Ths SImple chromatogr8l1'l doK r.ct match '''at of Ute 9~ s~nd.J1: . (&y: ØeI1Z"'Elenzene, ToÞToIuene. Et8;ft11yl bem.ene. X}'IFTolaI Xy¡.n... Mr8E;Metllyl t·butyI.r. SlSl'"'SurrQ9ate. Reç=~~VVf, 8r:B-o~Mof!uonål~ne. Flo-RamtlQftizallon 0tt4ct0t, PIO;PI1OtOionizlticm 0etecI0r. NOaHol Þele.d .t t!\e . n Iøvei 7440 Unooln Way. GerdOn Grøw. CA 92841-1432 . TEL: (114) 89S.5494 · FAX: (714) 894-1501 .n~6 uc ~~ !C;~!P ~aciFic Env. Group - PAS CALSC 1 ENŒ PRO!. 11Gì1T 626-351-4822 714 8ge 2Ø3ó p.4 ~ JUL-26-1399 17:24 P.03/Ø5 ~nce 6-nvlronmental 'Ji!r I. aÞoratorie$, Inc. Analytical Report Page 2 of2 LABORATORY 10' 9~,.,07 lJ~)5ì 1IIdIoð: EPA aÐ1&M '!1'H-ExtrKtab'- llatrf¡c $oiliSolld .1-1 sP·1-3 SP·1-2 Method BlanK 1SO 110 14 NO 98 9i 106 120 C7123iW 01l231n 071231S9 07123/99 01123199 Q7rl3119 07r.&1199 0112"99 rile MftII Ie (;hrom8fQgrimf .r. simiJM In appeerence 10 the JP"¡ Sœnclard FI "'Flame loni¡ation Detect« DeB: 7440 Lincoln Way. Garden Grove. CA 9284 1-1432 · TEl: (11 ") 895-S-4SM · FAX: (714) 8Ø4-7ð01 ,"rG u<:' ...... J.C:;~J.F t-'aClf"ic Env, Group - PAS 626-351-4822 5 p. 714 8ge 2036 P.04/05 ... JUL -ë:-6-1999 17: 24 CALSC ì ENCE PRaJ MGMT .PACIF1C eNVIRONMENTAL. GROUP. INC. Fa~imüe Cover Sheet To: Larry Len\ Calsçjence Environmental Laboratories, Inc. Fax (114) 894-7501 From: Paul TecnmJA Pacific Environmental Group, Inc. PHONE; 626-3S1-4S14 FAX: 626..351-4822 Dott: July 23. 1999 BE: former Shell Serviçe Station 10 J S. Union @ Bnmdagt PEGlIT No. 70S·131-1B Nø. Sleuts:....L includin¡ ttaI'.mútta! sheet Larry, Thank$ fOf your quiçk turnaround ofthc sample analyses an this project thus far and your prQtnpt rcsp01'lSe to my queStions. As we discussed, let's run the S01S-extractable analyses for samples SP-l-I, SP-1-2, and Sp·t-). Also. in your rcport(s) please coneçt the: sa.'tIple de$gn£itiu~ (no "foot" marks). Re¡ardiag the addiûonal samples that yoUr courier wiU deliver :oday, please run the $tandard 801S TPH-g nnd 8021 for MBTEX. Conf1nñ the highest Mill!! p~r boring using method 8260. Also, analyze the sample with the highl:St TPH·g per borin¡ for 80 l5·~xtractAb1e. The first three characters of each Field Sample ID designate the boring . location (for example. 8·3). There are three borings from this lot (B-3, B-4. and 8-S). . Lastly, please note that the sample for disposal characterization should be perlOrmed on standard tumæoW1d timt. Let me know ¡fyou have any question¡ Of concems- Tha.'iks. Paul III'EG-5\D^ T A\I'RQJf,",,?ðX1 V1'\t )11!'O)2)99.D()C '. '1 II Chain of Custody Record SITE ADDRESS: _Lo !-J""';o~ lJ,..~'/-;¡'!L. II r>agc æ of ··m _~Wj; elech... only ..$/1e IntUI (4441) 0 1M! ~(<<5») o SiIi1 CJ:.nIUIIø (<<.21 0 G.,^,. lot....... !~.at) In(løcr)t- . , It... t.: ..s-Irf 0 a.nI , ð fr'hM¿#. H.ne .. '.4':f.I..__L~~.!J.rl~_'!..::_J!.~ :¡/!~..~'.!!.!;"'~-n' ~ '-sO ./....,._~ ~.. /.... v--: ~. -.,,- "~"--- . '-'-- -....--- ..._----~_. --..---..,..- -.....--. Or ~b~-:1~...~,_.__._ ~1aI. C,tf:. ~ U/~7__ I'tøIr 'l. / V ClIft: s.., tIf: ru AA o ~. "ay 1t1tt.) OWl' CIftOi-.¡> (t4U) o 501ft'''' R-.mIS,. (44~) Q c: .. ... .. C1 1'1 J < . C "1 C C " "1: J: ~ IJ. a: I\: a: I c...: U1 ... I ~ (X) N N Ul:T ,.. ... ~~ t' /(C¿;#]) ~ ~ 1j ""'-r. Sampte Time I_ ~q Field Samp1& ID (mlJJtary) ¡- .It ~ t! ~ i ... 00 1> - I- I I .,):o.r 0 ~. 0 I .J .11' -;1. / ~ / . v / - .s. p. -. I .- .J : I ·0 I J J> /-1.' / 0 ·0 I 0 . .. . . 0 0 .. . . . , r.¡~ ~. .... Ji""" me; OeIc;h t!.~ ___.__I~:ff~Ø nlE LAßOI~AroRY MUST PROVtr>E ^ 1:01'.,- OF 'rtf'S C' éç,I' í:2 ~~ - .E, """'~' .. " en - ~ ~- - - --.. - - _. - - .- - -. ....-. . . . -- LABORATORIES, INC. t:JL()'þ/KC--' CI~ - . -. ?~ 1'(): ø~/9 6'f¡)A/ ¡wG , CHAIN OF CUSTODY RECORD dz/9' .' 7440 LINCOLN WAY /f CAIJf)f7A-P,tr~ cA- q/3ò~ Date GARDEN GROVE, CA 92841-1432 .. TEL: (714) 895-5494 . FAX: (714) 894-750 4, ? /6 / / Page of I LABORATORY CLlENT:~ · &..;VI/2ðYJM~/V/A'~ 6~...,p CLIENT PROJECT NAME I NUMBER: P.O. NO.: -:,¡~~ ~/r 7ð5-/5/-/ß - I ADDRESS~ S'~,-2.R4- ~é I/Í /14- I ~u,.,.é 7ot./ P~OJECT CONTACT: IS l' /. ') QUOTE NO.: I CITY /Þ'~~/.L STATé?q- ~P '7 '~L- 7é€A/..,S('r)~ 'f ?- /10 SAMPLER(S): (SIGNATURE) ~~ IT~u,/.3.!;-¡-¥ø/rl b~/a!:'l-ÝbZ2- I E-MAIL: G¢ry Fe 5 s~~~:tr Ji;~ t I TURNAROUND TIME REQUESTED ANALYSES o SAME DAY 0 24 HR o 48 HR o 72 HR o 5 DAYS o 10 DAYS I SPECIAL REQUIREMENTS (ADDITIONAL COSTS MAY APPLY) - CD q- o RWaCS REPORTING 0 ARCHIVE SAMPLES UNTIL _ / _ / _. ~ C> ~ ëiJ ~ 0 0 iñ e ~ SPECIAL INSTRUCTIONS ~"I ,,?G~ æ,é?JT ,p GtPue57 ëiJ ~ ~ S ~ ~ 0 0 N 6 ... ~ ëiJ N !:e- o ~ 0 - 0 '= - V,) !:e- ~ ~ N ~ ~ Lri Lri 0 ..,¡. ..... ... (';(7/ :5 . V7--' Œ ~jJ1ô<tt7e) V,) <I: V,) 0 £::!. £::!. ~ G 0 I-- ..... « \ ~ u.J :2 ëiJ 0 « !£ u.J <I: 0 V,) ce 0 0 ,.... ~ Ñ ::2: I-- S q- ::2: u.J ce c.. u.J ~ mH6/l-~r/&Ø/ CA- 0 I-- e:: co N ce 00 u ::2: ~ 6 :2 V,) ~ N ~ 0 0 ce N C") <I: < ~ ~ ~ N ~ t:. (.!J (.!J (.!J 0 - u CI) 0 I-- V,) I-- X 0 CI) U I-- CI) - Ù ::2: CI) ell - c SAMPLING NO. OF :I: :I: u.J ..... U 0 V,) ce ce c: < u .. u.J ~, SAMPLE ID LOCATION/DESCRIPTION MATRIX c.. c.. I-- <I: 0 >- u.J U 0 <I: S::! ::2: 0 :I: X DATE TIME CONT. I-- I-- ce :I: >- V,) c.. c.. u.J u c.. >- u ü: :5fJ-/-1 %/ /605 5 1 'i ~P-I-:2- / /52.-1 '$ 1 y ~~>;'-··I Sf?, I*' 3 lV 15/3> ~ I ~ liíf~{9:i&¡! Ii'),)·· If , I ~ Relinquished by: (S~ture) A .J/ Received by: (Signatur/-ð''o -6- X Date: Ti~ I ~'7Jð o1J-tJ2~? Relinquished by: (SignaturãJ 'F6o-6)¿ ~;?~ , Date: P9' ;7tJ I { Þ I ~.r-Þvr IJf(O}-- err Relinquished by: (Signature) l1eceivedfor Laboratory by: (Signature) Date: Time: I ~\ ~ ab a- ce ;; & v ;a g. t3 CI ~ CI DISTRIBUTION: White with final report, Green to File, Yellow and Pink to Client. Please note that pages 1 and 2 of 2 of our T/Cs are printed on the reverse side of the Yellow and Pink copies respectively. 02/01/99 Revision j . . / NOTE TO FILE 101 S. Union Ave. Former Shell (Equilon) Service Station 01/08/03 H. Wines, RG 7239 On this date, Ralph Huey informed me that a consultant reviewing the case file for 101 S. Union had alleged a discrepancy exists in the site assessment concerning hydrocarbons detected in the horizontal drilling for a new water main in the street on Brundage Lane adjacent to this site. On 7/15/99 Cal Water notified me that their excavation contractors (W.M. Lyles) had discovered a limited area of soil within their horizontal drilling that was noticeably impacted with a slight petroleum odor. Because the adjacent Equilon site was then subject to corrective action investigation for leaking UST systems, I directed Equilon to further assess this soil where the petroleum was detected by W.M. Lyles. Equilon did assess the area as part of their full site characterization at that time and the results indicated that the petroleum detected by Lyles did not originate at the Equilon site, nor was it apparently extensive in size or concentration. The maximum concentration detected was 151 ppm of an oily substance similar in characteristics to a bunker fuel oil. There were no actionable levels of chemical concern detected. The area involved is effectively capped by asphalt (under the middle of eastbound Brundage Lane) and no threat to groundwater is apparent. Therefore, this area of the investigation is necessarily included in the case closure as having been satisfactorily addressed in Equilon's Subsurface Soil Assessment, dated December 30, 1999, prepared by Pacific Environmental Group as discussed on page 3 and Appendix D therein. FIRE CHIEF RON FRAZE ADMINISTRATIVE SERVICES 2101 MH" Street Bakersfield, CA 93301 VOICE (661) 326-3941 FAX (661) 395-1349 SUPPRESSION SERVICES 2101 "W Street Bakersfield, CA 93301 VOICE (661) 326·3941 FAX (661) 395-1349 PREVENTION SERVICES 1715 Chester Ave. Bakersfield. CA 93301 VOICE (661) 326·3951 FAX (661) 326-0576 ENVIRONMENTAL SERVICES 1715 Chester Ave. Bakersfield. CA 93301 VOICE (661) 326-3979 FAX (661) 326-0576 TRAINING DIVISION 5642 Victor Ave. Bakersfield. CA 93308 VOICE (661) 399-4697 FAX (661) 399-5763 ~ . August 21, 2001 Mr. Gary Pestana, Senior Geologist IT Corporation 3452 East Foothill Blvd., 9th Floor Pasadena, Ca 91107-3159 RE: Fonner Shell-Branded Service Station at 101 South Union Ave in Bakersfield, California Dear Mr. Pestana: This is to infonn you that this department has reviewed the result of the Underground Storage Closure Report dated April 25, 2001 associated with the underground tank removal. Based upon the infonnation provided, this department has detennined that appropriate response actions have been completed, that acceptable remediation practices were implemented, and that, at this time, no further investigation, remedial or removal action or monitoring is required at the above stated address. Nothing in this detennination shall constitute or be construed as a satisfaction or release from liability for any conditions or claims arising as a result of past, current, or future operations at this location. Nothing in this detennination is intended or shall be construed to limit the rights of any parties with respect to claims arising out of or relating to deposit or disposal at any other location of substances removed from the site. Nothing in this detennination is intended or shall be construed to limit or preclude the Regional Water Quality Control Board or any other agency from taking any further enforcement actions. This letter does not relieve the tank owner of any responsibilities mandated under the California Health and Safety Code and California Water Code if existing, additional, or previously unidentified contamination at the site causes or threatens to cause pollution or nuisance or is found to pose a threat to public health or water quality. Changes in land use may require further assessment and mitigation. If you have any questions regarding this matter, please contact me at (661) 326-3979. Sincerely, ~tHLJ--~ Howard H. Wines, ill Hazardous Materials Specialist Registered Geologist No. 7239 Office of Envirorunental Services cc: J, Whiting, RWQCB S:\USTFO~~ST.L8 ('losP~ ~ 'ÒOn~ ~ J/60P6 .o/~ .A ~~,~?.,., Î \.." CITY OF BAKERSFIELD '~ FIRE DEPARTMENT OFFICE OF ENVIRONMENTAL SERVICES 1715 CHESTER AVENUE BAKERSFIELD. CALIFORNIA 93301 . c. ,0 ~ :::::> . d '^- -:;, ""'- ~ Ç) ~ ~ ...J U\ ~ Q -+ \~ Q) ~ ~ ~ ~ I. ~"t. ,;_. , I .":: > '. .; ~ . - . ~ \ , I ~~~"""'.-.--- --- ,~ -ft"".- ./,' I Î '//'(1r (~ ".---- ---,~~r:: r- "', '...' .,·~¡;.:~2Ä(;~~:·i~":~· ;: , ,,,' ~'.:<i~~~~ ·~"~~~·I . ..,~ I ,. !,,: " i," ,. ~,,~L'\'.:' .. ....,J: :,'f("¡.~: ~ .~ , " t 'ç--;-~"" ~i~~,>'~'_.-~~.-oi '. \/,. \, "~. ". '.'. ..... ~",.1. '- ...........~'.. ~> ,.'.' ..', ~ ,~,~:.?,.. .': . . ~ ~..--~¡l '..~. :"">', ", _, '}\..~\r(~ '\..' ,'r'·,":' ~iI..';~¡-~' '. . ,\_.n ..,~ . ,. .':," ':,' ..; :"~~ .. ~ \ JI__ III III /?~:~.- :~ j,~..~ ~~-~ ¡ ,r\.¡" \'_ ~~ ~'J j \\ 'J' \ .,'. ~...' " ~.i -~~:'._~ ___ --; ê;:--: .:~-~">~~'- ~........,. .,.~ --- ¿- -. .,¡. - .- i UNITED STATES POSTAL SERVICE I I ¡ I ¡ i Official Business I _ . . _._. ~ ._. r,--'-" ,., ~..-- - ,. . (-.:...:.:-;.:. : ._".:.. - "-" ~~-~- =--- - -- PENAL TV :a;;;R~V..ût- USE TO AVðIDJ'M~~ OF Pes1í\C3E, ;þ,juO C' ..~' I I j Print your name, address and ZIP Code here ;_ · BAKERSAElD F'RE DEPARTMENT OFFICE OF ENVIRONMENTAL SERVICES 1715 Chester Avenue, Suite 300 Bakersfield, CA 93301 -/1 J 1IIII ¡I, J J J III J II1I ¡ J J I J J II J I J I J III" J , J J II ¡ 11,111111 - --,,~ ::'1 1 J 81 '~I ~ ~~ ~I ~I ~J o Insured ell o COD .~ o Return Receipt for ... Merchandise .. J 7. Date of Delivery .E ! 8. Addressee's Address (Only if requested !I and fee is paid) æl ï=1 I DOMESTIC RETURN RECEIPT I ....' ~ ~1~I~t~¡tems 1 and/or 2 for additional services. Q). plete items 3, and 4a & b. ~ . Print your name and address on the reverse of this form so that we can CD return this card to you. ~ . Attach this form to the front of the mailpiece, or on the back if space .. does not permit. .! . Write "Return Receipt Requested" on the mailpiece below the article number. ... . The Return Receipt will show to whom the article was delivered and the date delivered. 3. Article Addressed to: c o 'C Q) ... ! PAUL SCHOENFELD E EQUIL~N ENTERPRISES LLC 8 8200 STOCKDALE HWY M10 ~ BAKERSFIELD, CA 93311 w - a: c eRE: « ~ 5. Signature (Addressee) :J I- ~ 6. 4a. , I also wish to receive the following services (for an extra fee): 1. 0 Addressee's Address 2. 0 Restricted Delivery Consult po"stmaster for fee. Article Number P 024 368 655 1103 4b. Service Type JJ Registered 11 Certified o Express Mail 101 SOUTH UNION AVE (' P 024 368".~SS ~ Receipt fAl Certified Mail .. . '." NQ..lnsurançe Coverage Provided == Do not use for International Mail (See Reverse) ... en en ... Sen~o PUL SCHOENFELD s~e~td~ No. STOCKDALE HWY MlO PBAIœR5~ CA 93311 Postage $ .32 Certified Fee 1.10 Special Delivery Fe. Restricted Delivery Fee Return Receipt Showing 1.10 to Whom & Date Delivered Return Receipt Showing to Whom, Date. and Addressee's Address TOTAL Postage $ 2.52 & Fees Postmark or Date Q) c: ::J ., Ò o CD ('I) E o u.. C/) Q.. STICt{ POSTAGIE STA¡'jIi'S TO /UITICLIE TO COllIER ~IRST ClASS POSTAGE, CIERTIFIED ¡'jAIL ~EIE. b\lJD CMAIIGIES FOil Am\' SmCTIED OPTlOE!AL SIEIlIfICIES aoo mot!. 1. If you want this receipt postmarked, stick the gummed stub to the right of the return address leaving the receipt attaclftld and present the erticle at a post office service window or hand it to your rural carrier Ino extra charge}. Qì t! ~ ~ ~'" 2. If you do not want this receipt postmarked. stick the gummed stub to the right of the retu address of the article. date. datach and retain the receipt, and mail the article. 3. If you want a return receipt. write the certified meillRlmber and your name and addiëss on a return receipt card. Form 3811. and attach it to tha front of tha article by maans of tho gumlßÐd ends if spaœ parmits. Oth8rwisa. affix to back of articls. Endorse front of articls RIETURN RECEIPT REQUESTED adjacent to the number. .... en en .... 5. Enter fees for the services requested in the appropriate spaces on the front of this récøipt. If return receipt is requested. check the applicable blocks in item 1 of Form 3811. G) c :;] .., Ò Q CO Cf) E .. o u.. !J) Q. 4. If you want delivery restricted to the addressee. or to an authorized agent of the addressee. endorse RESYI'IICYED DELIVERY on the front of th8 article. 6. Save this receipt end present it if you make inquiry. ·102595-93·Z-047a - :1- BAKERSFIELD FIRE DEPARTMJKJ'.,- _. EHVIRONDH'l'AL SDVIa~ 1715 Chester Ave., ,- Bakersfield, CA 93301 (805) 326-3979 TANK RDOVAL INSPEC'l'ION PORM FACILITY~( .t*A}, lJÌ\ g~~~jé_ ~~~~~;~~ LABORATORY :\- TEST METHODOLOGY t , PRELIMANARY ASSESSMENT CO. -cr CO2 RECIEPT _ßf6 "Át 0 ì Ç-O jj ADDRESS If) ~. dhl ()v\ .Avt. PERMIT TO OPERATE' ßR- Ð,;)ì3 CONTACT P,ERSON J...n. r t 'f # OF SAMPLES ~ (P. -, t CON't.ACT PERSON LEL' -& PLOT PLAN ill . r 1)\ sr {\-is yo !:oj /, hi ~~ ~r _ u"~J r-------,- I '{ "/. Y. I r_ _ _ _ _ _ , ~(\\\. Ùt-\. IQ\( r - -- --r- L ~ ~~!_I ~.¿ 'n.!.. ~H'" '1iIL- \I\().I~\ vjVI \ d(\'-1 CONDITION OF TANKS Y'uJ r: "-«I<ðlcr,( fOil' 1- CONDITION OF PIPING SCAlF CONDITION OF \ SOIL NIt} f'Á¡f hAde.. ~/~ú {. COMMENTS~tJIA1 ::or ~t., ;h:IM~ll, (Ji-. ~ /J/-pI.t-.L_ ~ 'I-tf"_ (1+ 6-klJJ¡ln; oJ· t 1M f tf \A ~lr taJAJ\. t- ;)-I-()( DATE .....-.ih..v L ( !JJ('{'tJJI) f)¡( INSPECTORS HAlE L (t,~erkJ SICllATIIII -- -- 12/21/00 0'" 58 - .~ I . u 66L:i'J6 0576 ~~_-----_£ _-C----!~-HAZ-M~Tr-D~~ __ Ii!J002 ~k~. ~~ðC\.' ~ pcrrnU No. ,., 13 CITY OF BAKERSFIELD ? Á ,¡h 17;.,(,,4 OFFICE OF ENVIRONMENTAL SERVICES t 71 5 Chester Ave., Bakersfield, CA (805) 326-3979 PERMIT APPLICATION FOR REMOV AL OF AN UNDERGROUND STORAGE TANK SHE IN.'ORMATION SITE~ ~*,dì ADDRESS \0\ S ',)D\ür::\ _ZIPCODE~?0U APN fACILITY NAME -. - CROSS STREET i¥\J(\cI ~ç T ANK OWNER!OPER~OR &f\J1'- rj ~I~ =". ~ PHON ~t l' ~ ~ "t ') ~ ~ QU> !$i¡ LI,., ,- MAILING ADDRESS _ 0 L _~ lO _ __ '5 ~ CITY _ . bn ' ~ ~ ZIP:!') z¡ 01 - -, '-':::. CONTRACTOR INFORMATION ~~:~~;Jz; ~~~~~~\ ¿ INSURANCE CARRIER 4~ y=JV\ PHONE NO.3'3'1 ~ ~ ~ \Î 30 L.ICENSE NO.1J "I L~ h .L CITY T:--11-:--sf'lO ZIP ~ 3 ' z.. _ wo1U<MENS COMP NO. I')\Jl~q I ~ 4 ~ PREUMIN",RY ~~MENT INFOKM!.TION . COMPANY~:' ;~+_ ÐWII'TmllélllQ.\~ p!l0NE NO~ q1..Q ~ L.ICENSE NO, _1 L.\o <;~ 2- fl ADDRESS I." .<;1-, :">\>0, f) ~ cITY ~ Jt"\ ð ~ ~ ZIP "')'1 \ ß ( INSURANCE C A.mER ~ TV V\Ò _ woRKMENS COMP NO, ~~2.. - 2.''1 ~ oQ~ ~ TANK CLEANING INFORMATION CQMPA.NY=E..L \:;: _PHONENO ~'S\()"'no -î'1.U'L. ADDRESS '2. =;«> V;;;>v<: V, \ \! ë\ ' : cITtJ2. ,c1IV1\()ro ßP .3 '-\ ~') ¡: W A.SíE TRANSPORTER IDENTlFICA TlON NUMBER _ c· Ab~ Ý\:? n qo \'1 ~ NAME Of RINSA.n DlSPOSAt.. F¡\Cll-ITY .~\C- -.~' ~ - Þ.DDRESS 2G«' 1:><1 ,~y\ ' a CITY IS. ~ \<3 P \ \'\, - ZIP :BYD ~:S FACILITY ïDENT(flCA Tl0 NtJMBER =- C-fÀ ,,0 ov¡ ~52.J Q-C::;'î «\X) 'Î \.9 \.¡¡ 4 z.. L\ ~ 1'~' 16Y'µ" \ S 3 '3 'T.....NK TRANSPORTER INFORMATION COMPANY ",C" \ - , PHoNE N05'J. \) 2.'3'5 \ ,,¡q '3 uq¡NSE NO, ,4 ~ ~n ADDRESS -= 2 ~ ~'<.'L \?\\)(\ c¡Ti.Il. ,( ýIrI\..'YYj. ZIP ~ 1I'ö1 TANK DEST\NAT10N - ~<:::) ~NK INFORMATION CHEMICAL STORED \\ÝÌ6' ..9. \ Vì~ ~ \ r)ç DATES STORED --Q ? 1 1 CHEMICAL PREV10USL Y STORED T A.NK NO. \ '2.. ---~~ AGE VOLUME \O.l1.')n j" lÌ (':Jl') " -, lú I--U~ ) ---- ~~ flJl' oniçjø.\ \J~ Qat AJ'PUCA.TIOl< OÅii /~' ,. .,·...\:.:W;;Fi\~f.Å~~~~ž"i)j!;i¡;:$@;'1ï~~(åi:1j4¡ì<ãr,¿!¥i¿"/}1~J~\ TIIF. ^"I'I.ICAN1' liAS RI'CfNED. UNDI'RST ANDS. AND W1Ll. COMPI,Y WITII'l11E ^ Tt ACIII'U CON1)\'IlONS Of 1111" I'rRMIT AN ) ANY 0'11 IER ST^TL, \.O(.:Al, AND FEDERAL REGULATIONS, llllS "()~ IIA.' IIE(;N COMPl.KrEi> !IN )(;1( p"NAerY OF PßI\JtIRY. AND TO 'l1IE úr-»'T 0\' MY I<NOWI.\'.IXm IS TR \I F. ANI)ccßI {Fer. ;/ APPLICANT g ìNA 11JRE _...~ .. nOI IrATION BECOME A PERMIT WHEN APPROVED .... .. FIRE CHIEF RON FRAZE ADMINISTRATIVE SERVICES 2101 "H" Street Bakersfield. CA 93301 VOICE (661) 326-3941 FAX (661) 395·1349 SUPPRESSION SERVICES 2101 "H" Street , Bakersfield. CA 93301 VOICE (661) 326-3941 FAX (661) 395-1349 PREVENTION SERVICES 1715 Chester Ave. Bakersfield. CA 93301 VOICE (661) 326-3951 FAX (661) 326-0576 ENVIRONMENTAL SERVICES 1715 Chester Ave. Bakersfield. CA 93301 VOICE (661) 326·3979 FAX (661) 326,0576 TRAINING DIVISION 5642 Victor Ave. . Bakersfield. CA 93308 VOICE (661) 399-4697 FAX (661) 399-5763 '- e December 13,2000 Equiva Services Larry Turner PMB #368 2060 D Avenue Los Rarboles, Thousand Oaks Ca 91362 RE: Expiration of Temporary Closure Permit for Shell Service Station, 101 South Union Avenue, Bakersfield, Ca 93305 NOTICE OF EXPIRATION OF TEMPORARY CLOSURE PERMIT Dear Mr. Turner: The temporary closure permit for the above mentioned facility will expire on December 31, 2000. Accordingly, no further extension can be granted as outlined in our previous correspondence of May 31, 2000. You are required, under section 7902.1.7.2.3 U.F.C. (97 Edition) to remove those tanks or put them back into service. "Underground tanks which have been out of service for a period of one year shall be removed from the ground and the site shall be restored in an approved manner." ¡,¡,...r~ áe CCOnl/~ 37'0P ~0P6 .o/~ A W~" e . Recent phone conversations indicate a time table for removal set for January 2001. This is agreeable, provided that the removal pennit be submitted prior to December 31, 2000. Should you have additional questions, please do no hesitate to call me at 661-326-3979. Sincerely, Ralph E. Huey, Director Office of Environmental Services by: /L rMmo Steve Underwood, Inspector Office of Environmental Services SBU/dm cc: Feryal Sarrafian Georgina Davila-Dimario SENDER: · Complete items 1 and;..r additional services. · Complete items 3, and b. · Print your name and adar ss on the reverse of this form so that we can return this card to you. __ -:'~~ · Attach this form to the front of the mailpiec~, or on the back if space does not permit. · Write "Return Receipt Requested" on the mailpiece below the article number. · The Return Receipt will show to whom the article was delivered and the date delivered. 3. Article Addressed to: 4a. CARLTON E HOWELL EQUIVA SERVICES LLC 13105 MEADOW LANE LEAWOOD, KS 66209 I also _1:\ to receive the followingWices (for an extra 8 fee): '; .. 1. 0 Addressee's Address Æ Õ. "ã) u II) II: EI ~I II) II: 2. 0 Restricted Delivery Consult postmaster for fee. Article Number Z 410 286 914 4b. Service Type o Registered ~ Certified o ExpreBs Mail CI c: ïii :I 7. 8. I I I ! .. o ... trU.S. GPO: 1993-352-714 DOMESTIC RETURN RÉCEIPT UNITED STATES _AL SERVICE Official Business "'" l e ~. -' U.S. MAil . Print your name, address and ZIP Code here . I I I I I r: - - . ¡.- - . - . .. ", -.:.' '0:" :....:.;_:.\0.. "='::'.\0 :..t , , I PENALTY FOR PRIVATE USE TO AVOID PAYMENT OF POSTAGE, $300 BAK[;~SFiELD FiRE DEPARTMENT ()t=!=u .' ~B ... II II" I· ., \ i ·/11 'IIII'¡ I lid,,!; UIIl\illIHl1 1II.Iìllllll\ld \\111;1 1.1 I 11,1,11 '. .. " . '..' . '. . . . ~ .'. . . . . " .... . . '" . . . . . . . . '. .' '. . . Z 410 28_14 ~ US Postal Service . Receipt for Certified Mail No Insurance Coverage Provided. tr.-.;-,· Il') m m ..... Do not use for Intemational Mail (See rliverse) ~. Senlto CARLTON E HOWELL Street & Number 13105 MEADOW LANE Post Office, State. & ZIP Code LEA WOOD KS 66209 Postage $ .32 Certified Fee 1.10 Special Delivery Fee Restricted Delivery Fee Return Receipt Showing to 1.10 Whom & Date Delivered Return Receipt Showing to Whom, Date, & Addressee's Address TOTAL Postage & Fees $ 2.52 Postmark or Date 5- « c:i o CO C') E o u. C/) a. ~ Stick postage stamps to article to cover First-Class postage, certified mail fee, and charges for any selected optional services (See front). . 1. If you want this receipt postmarked, stick the gummed stub to the right of,the return address leaving the receipt attached, and present the article at a post office service window or hand it to your rural carrier (no extra charge). 2. If you do not want this receipt postmarked, stick the gummed stub to the right of the return address of the article, date, detach, and retain the receipt, and mail the article. 3. If you want a return receipt, write the certified mail number and your name and address on a return receipt card, Form 3811, and attach ~ to the front of the article by means of the gummed ends if space perm~s. Otherwise, affix to back of article. Endorse front of article RETURN RECEIPT REQUESTED adjacent to the number. 4. If you want delivery restricted to the addressee, or to an authorized agent of the addressee, endorse RESTRICTED DELIVERY on the front of the article. 5. Enter fees for the services requested in the appropriate spaces on the front of this receipt If return receipt is requested, check the applicable blocks in item 1 of Form 3811. 6. Save this receipt and present ~ if you make an inquiry. 102595,9S-M-054S ~ t 0..; ~ ( ) f:£ a. < Õ g CO M E o u. (J) a.. FIRE CHIEF RON FRAZE ADMINISTRATIVE SERVICES 2101 "H" Street Bakersßeld, CA 93301 VOICE (661) 328-3941 FAX (661) 395-1349 SUPPRESSION SERVICES 2101 "H" Street Bakersfield. CA 93301 VOICE (661) 328-3941 FAX (661) 395-1349 PREVENTION SERVICES 1715 Chester Ave. Bakersßeld, CA 93301 VOICE (661) 326-3951 FAX (661) 32s.œ78 EN~RONMENTALSERVlCES 1715 Chester Ave. Bakersfield, CA 93301 VOICE (661) 326-3979 FAX (661) 32s.œ76 TRAINING DMSION 5642 Victor Ave. Bakersßekl, CA 93308 VOICE (661) 399-4697 FAX (661) 399-5783 *.-.' '- ,......../. ~....!"'. 'I \ <> ,. () () hø-t ~ ~ t/JÆJ ~~Jb ,.., q' "', $~C~~ w 6-4t, T q) a tA.~f ~vtlt¿ , August 9,2000 ~(f e-~UðO@~ fS OS'. 4 ~3 b fJ'1 ÞJ lø ¡::A~ t@~o €:,t'ì~ <i> @ 1;) 0 Carlton E. Howell Equiva Services LLC 13105 Meadow Lane Leawood, KS 66209 CERTIFIED MAIL NOTICE OF VIOLATION SCHEDULE FOR COMPLIANCE RE: Improper Housekeeping and Maintenance at (2) Shell Facilities: 101 South Union Avenue & 3130 24th Street in Bakersfield, Ca. Dear Mr. Howell: A request for extension of temporary closure for the above mentioned fàcilities was granted on May 31,2000. As part of that agreement, you were to assure, on a regular basis, that proper housekeeping is maintained. A personal inspection was performed on August 9, 2000 at both fàcilities to insure proper housekeeping was maintained. Both fàcilities are currently unacceotable. Combustible weeds are 2' & 3' high in planter box area with weeds I' tall in parking lot. This letter is to advise you that you are in danger of losing your temporary closure permit if this weed abatement problem is not handled immediately. You have fifteen (15) days (August 23,2000) to properly abate weeds accumulated at property. Failure to coinply will result in revocation of your temporary closure permits. Should you have any questions, please feel free to contact me at 326-3190. Sincerely, ...: Ralph E. Huey, Director Office of Environmental Services ~~~ Steve Underwood, Inspector Office of Environmental Services SBU/dm cc: Terry Runnels ~~7~~ g:'~ ~ ~~ §,~.A g:'~" ... ---...- --.... -- -.. -...---.....-.. \ .:.J...j ~ ,.,..... 0¡¡¡ICE OF ENVIRONMENTAL" RVICES 13::>t:J.,f- 1715 ~ster Ave., Bakersfield, CA 933 . (661) 326-3979 UNDERGROUND STORAGE TANKS - UST FACILITY . OF ACTION " . ex OM t/em only) 0 1. NEW SITE PERMIT j2S,1. F,:NEWAL PERMIT 0 5. CHANGE OF INFORMATION (Specify chenge. o 4. AMENDED PERMIT Ioce/ use only) .. ._.__. ...,.__"._. ____..'___________..' .__,__ ._.. _.___.~MPORARY SITE CLOSURE .JQ_Lt::o I~ On.~ôI\ I. FACILITY I SITE INFORMATION '"S~S """ ,.... æ ""'ITY """ a OBA . """' ,-- '" , , ""'N". l' (I N~ ~o~;¡;:k À Ac. \ A.o ~ '-'¿"L::: I ""UN 0,,"" NeE L LL / "'\ . (),. ,... ,.. - fv1 1. CORPORATION "-'~\. ~ \...:.J -.0~ \':::> \Âo¿ a> C' Po - E!ÜŠiÑÈsŠ---";;;'- 0 0 I 0 2. INDIVIDUAL TYPE ¡,o. 1. GAS STATION 3. FARM 5. COMMERCIAL 0 3. PARTNERSHIP o 2. DISTRIBUTOR 0 4. PROCESSOR 0 6. OTHER TOTAL NUMBER OF TANKS Is fadllty on Indian Reservailon or REMAINING AT SITE lrusllands? 404. ~NO I 405. I 'If owner of UST a public agency: name of supervisor of dl\iÍslon. section Q( office whid1 operates the UST. (This is the contact person for the lank records.) Dyes Page L of !:l o 7. PERMANENTLY CLOSED SITE o 6. TANK REMOVED 400. _._._-'-------~-----_._----.. I I I I i o 4. LOCAL AGENCY/DISTRICr o 5. COUNTY AGENCY' o 6. STATE AGENCY' o 7. FEDERAL AGENCY' 402. 406. II. PROPERTY OWNER INFORMATION LLC. 407. PHONE 408. 6Iß-"1~"- 507B PROPERTY OWNER NAME -- - ,.__ t:::::: Q V ~ "- 0 ~ E::::: ~ -r .::--R, ..p R. \ S ¿-..5 MAILING OR STREET ADORESS Po 60>' 7~C¡ CITY 0Û-'<.\~A'Ñ.C- PROPERTŸ- OWNER TYPE !8!: 1. CORPORATION 410. I STATE i GA I D 4. LOCAL AGENCY / DISTRICT o 5. COUNTY AGENCY D 2. INDIVIDUAL o 3. PARTNERSHIP 409. 411. I ZIP CODE I q,Slo - ~8b9 D 6. STATE AGENCY o 7. FEDERAL AGENCY 413. 412. III. TANK OWNER INFORMATION 414. PHONE 415. 6\E3- ~ ~fe?-5078 OWNER NAME ....- E:::::. V\ '-0 ~ c:::: '\....l T ¿ € ..p \ ð c ..!ff> MAILIN.G~ STREET,-4DDRESS 'r"O QOX 1f 8~q 'CITY 12>""~0A N \C.. TANK OWNER TYPE L L c.... 417. ¡STATE 416. i OA o 4. LOCAL AGENCY I DISTRICT D 5. COUNTY AGENCY ~ 1. CORPORATION o 2. INDIVIDUAL o 3. PARTNERSHIP IV. BOARD OF EQUALIZATION UST STORAGE FEE ACCOUNT NUMBER TY (TK) HQ Call (916) 322-9669 if questions arise V. PETROLEUM UST FINANCIAL RESPONSIBILITY 416. ZIP CODE c:¡ I S\ 0 - 76b9 419. o 6. STATE AGENCY o 7. FEDERAL AGENCY 420. 421. INDICATE METHOD(S) ~ 1. SELF-INSURED D 2. GUARANTEE .0 3. INSURANCE o 4. SURETY BOND o 5. LETTER OF CREDIT o 6. EXEMPTION o 7. STATE FUND o 6. STATE FUND & CFO LETTER o 9. STATE FUND & CD o 10. LOCAL GOV'T MECHANISM D 99. OTHER: VI. LEGAL NOTIFICATION AND MAILING ADDRESS 422. :hed< one box to indicate which address should be used for legal nollficatlons and mailing. _egal nollfications and mailings will be sent to the lank owner unless box 1 or 2 is d1ecked. o 1. FACILITY .B( 3. TANK OWNER 423. D 2. PROPERTY OWNER VII. APPLICANT SIGNATURE :ertlficatlon: I certify that the In/ormation provided herein Is true nd accurate to the besl of my knOY<1edge. ) GÑÃTÜRË.~~~~:~NT __,_ - ] DATE :5 / L~l ~ _._:~.r~~~~,.'7~~~~~;·.. jAME OF APPliCANT (print) 426'1 TITLE OF APPLICANT 427. .~ ~::{-~~__,_;2_~R.f.:\_£J Ab-I.._~___._____.____ :5 \-\_ª,cÇ _a~,~\"'J.ß.N5'-:::~_ aog,º,-~~'I<?~ / ¡TATE UST FACILITY NUMBER (Forloce! use only) 429. 428. 1996 UPGRAOE CERTIFICA TE NUMBER (For /ocal use only) 'CF (7)99) s:\CU P AFORMSlswrcb-a. wpd ';' /A" /(, ' II , . II.. !LLL1 " "". All'. ~ ...... '-- - e.E OF ACTION IClleck one ,Iem only) ~ CITY OF BAKERSFIELD . \ ~'::)O'1<t-(ó OFAE OF ENVIRONl\tIENT AL SeVICES .. · .. 1715 Chester Ave., Bakersfield, CA 93301 (661) 326-3979 . ~> UNDERGROUND STORAGE TANKS - TANK PAGE 1 Page L ot 7 ~. TEMPORARY SITE CLOSURE - o 7. PERMANENTLY CLOSED ON SITE o B. TANK REMOVED o 1. NEW SITE PERMIT 0 4. AMENDED PERMIT o 5. CHANGE OF IN FORMA TION) o 3. RENEWAL PERMIT 43C {Specdy reason· lor local use only} (Specify change' lor local use only) BUSIÑESS NAME'{säñi~ãšï=Äëíí.ïiYÑÃME ë; DåÃ': öö¡;;g'šûši;;ëšš-Ä:ï)'''''' " ..,., .-.,--., -3-: FACIU1Y ID # - I \-0 R -t\¿ R. ,,-"'1 \....1\ .A- c. \,~..5 5\-\cl..\- I · LoéÃriõÑ"WITHiÑSITE (OptionaÏj---.---- ..-----'-.- ----. I :]--¡ ¡-'I---:-i ~ -- .--,.--...-.-------- 1, _'_ __.U,_ --.------ - -, .......-.-.-..-. 431 432 TANK MANÙ-FACTURER O....¡..¡~ .> TANK CAPACI1Y IN GAllÕNS ~ 433 , COMPARTMENTALIZED'~~Ö Yes ---:if No 434 ' ~ A.. t-.\ \~,,,' If "Yes", complete ooe page (0( eaCh compar1ment. I --43ë-TÑ-UMãËR OF COMPARTMENTS . -.-'---..-----¡jj , ! , I. TANK DESCRIPTION -t ÀÑI< ID # "ÖÄTÊïÑsi'ÃlLED (YEAR/MO) 435 \O\ODO 438 :-ÃDDITIONAl DESCRIPTION (For local USa only) I TANK USE 439 : )::j. MOTOR VEHICLE FUEL : (If markad, complete Petroleum Type) o 2. NON-FUEL PETROLEUM o 3. CHEMICAL PRODUCT o 4. HAZARDOUS WASTE (Includes Used Oil) o 95. UNKNOWN PE OF TANK : (Check one ~em only) · TANK MATERIAL - primary tank · (Check one ~em only) II. TANK CONTENTS 44C PETROLEUM TYPE )(., a. REGULAR UNLEADED o 1 b. PREMIUM UNLEADED o Ic. MJDGRADE UNLEADED o 5. JET FUEL o 6. AVIATION FUEL o 99. OTHER o 2. LEADED o 3. DIESEL o 4. GASOHOL 441 CAS # (from HazardOus Materials Inventory page) 44:< COMMON NAME (from HazardOus Materials Inventory page) \..J~R QA~~'-\.~c::.'- III. TANK CONSTRUCTION o ,. SINGLE WALL ~2. DOUBLE WALL o 3. SINGLE WALL WITH EXTERIOR MEMBRANE LINER o 4. SINGLE WAll IN A VAULT o 5. SINGLE WALL WITH INTERNAL BLADDER SYSTEM 095. UNKNOWN o 99. OTHER o 5. CONCRETE o 8. FRP COMPATIBLE W/100% METHANOL 443 o 1. BARE STEEL o 2. STAINLESS STEEL 3. FIBERGLASS I PLASTIC o 4. STEEL CLAD W/FIBERGLASS REINFORCED PLASTIC FRP 3. FIBERGLASS I PLASTIC o 4. STEEL CLAD WIFIBERGLASS REINFORCED PLASTIC (FRP) o 5. CONCRETE o 3. EPOXY LINING o 4. PHENOLIC LINING o 95. UNKNOWN o 99. OTHER 444 o 95. UNKNOWN o 99. OTHER 445 TANK MATERIAL - secondary tank 0 ¡ ,. BARE STEEL · (Check one item only) 0 2. STAINLESS STEEL o 8. FRP COMPATIBLE WII00% METHANOL o 9. FRP NON-CORRODIBlE JACKET 0,0. COATED STEEL o ,. MANUFACTURED CATHODIC PROTECTION o 2. SACRIFICIAL ANODE YEAR INSTALLED 450 1YPE (For local use only)" 451 ~1. SPill CONTAINMENT ~ r567A.... G?.o.'Ñ IE 2. DROP TUBE ì '6 ç,- Af'(,,ø{¿, }š. 3. STRIKER PLATE ð A.:>",¿-T C'À<ñé . :'; ;; :.;.9~i : \W¡;"{'$:'. :~1. i~;~ S,: ,1t::g··¿;~{~:Þi~'{,·';~T0'!)iy~~t.Ãij,çL~ Òi:.:tEëT1ÇN·-.'~~~~"¡:·· t~~:':¡¡~~r¡.f!if;~.;~;>t<:i~'?;l ~~.' ,c. c...,.>. ..;;. .c'::':~f +;:&.~~;':¡:~:< IF SINGLE WALL TANK (Check all thet epply): 453 IF DOUBLE WALL TANK OR TANK WITH BLADDER (Check one item only): 4~ o I, VISUAL (EXPOSED PORTION ONLY) 0 5. MANUAL TANK GAUGING (MTG) 0 ,. VISUAL (SINGLE WALL IN VAULT ONLY) 02. AUTOMATIC TANK GAUGING (ATG) 06, VADOSE ZONE ~ 2. CONTINUOUS INTERSTITIAL MONITORING o 3. CONTINUOUS ATG 0 7. GROUND~ATER I 0 3. MANUAL MONITORING AD 4. STATISTICAL INVENTORY RECONCILlATlDN (SIR)" 0 B. TANK TESTING I ~..___~NIAL TANK TESTING 099. OTHER I V. TANK CLOSURE INFORMATION / PERMANENT CLOSURE IN PLACE I I· TANK INTERIOR liNING I OR COATING I UCheck one item only} : OTHER CORROSION i PROTECTION IF APPLICABLE I : ~c.~eck ~,,-e item only) SPill AND OVERFill I : {Check all that apply} ¡- ! i ,- .--...--- I , 446 DA TE INSTALLED 447 .3'95. UNKNOWN o 99. OTHER o 5. GLASS LINING o 6. UNLINED o 1. RUBBER LINED o 2. ALKYD liNING (For local use only) DATE INSTALLED 449 ~ 3. FIBERGLASS REINFORCED PLASTIC o 4. IMPRESSED CURRENT o 95. UNKNOWN o 99. OTHER 44B (For local use only) OVERFILL PROTECTION EQUIPMENT: YEAR INSTAllED .. J ,.::2 o 1. ALARM J:r 3. Fill TUBE SHUT OFF VALVE .1C1.L o 2. BALL FLOAT 0 4. EXEMPT 456 TANK FILLED WITH INERT MATERIAL? 45 455 - ESTIMATED QUANTITY OF SU~NCE REMAINING ø _ gallons .____.__ __._____._ _________. ___._..__...... .. .__.n._._---L- ..--.-------.-'--..--- --------- .... .......--...----.- UPCF (7/99) DYes ONe S:\CUPAFORMS\SWRCB-B.WI _ CJìY OF BAKERSFIELD _OFFICE OF ENVIRONMENTAL SERViCe. 1715 Chesler Ave.. Bakersfield. CA 93301 (661) 3!11!979 I ~ :5"' 0 ...., q:. / ·t- . UST. TANK P4¿t ._~------- --~~- .:ö.._~~.,!1- ---ABõÏtËÖROUND PiPiÑã--' .,- -.---'-- VI. PIPING CONSTRUCTION (eMck./I that .pp/'¡) ... ., -.. -. -'---'ÜNÕËRGROUND PIPING .. . ... 'YS rEM TYPE )( 1. PRESSURE' 0 .2. SUC::TI?N.. 0 3. GRAVITY 458 U:J I. PRESSU~E_ . CONSTRUCTION/ 0 1. SINGLE WALL 0 3. LINED TRENCH 0 99. OTHER 460; 0 1. SINGLE WALL MANUFACTURER~ 2. DOUBLE WALL 0 95. UNKNOWN ! 0 2. DOUBLE WALL , MANUFACTURER 461 ! MANUFACTURER ....- ~[j" ~.'~-;';~' š~-;i;:-- Ö 6. F~P COMPA it;(e :;'~I00%'~~THANOL '-'rb -;-;~~È STE~~·-··_" '" ., ..., MATERIALS AND '0 2. STAINLESS STEEL 0 7 GALVANIZED STEEL I 0 2. STAINLESS STEEL CORROSION I , . . PROTECTION i 0 3. PLASTIC COMPATIBLE WITH CONTENTS 0 95. UNKNOWN I 0 3. PLASTIC COMPATIBLE WITH CONTENTS !~4. FIBERGLASS 0 8. FLEXIBLE (HDPE) 099. OTHER ,. 0 4. FIBERGLASS !O 5. STEEL WI COATING 09. CATHODIC PROTECTION 464 ,05. STEEL WI COATING VII. PIPING LEAK DETECTION (CMck all Ìhat apply) . ' I 466 EMERGENCY GENERATORS ONLY (Check all1hat apply) ] 14. CONTINUOUS SUMP SENSOR WITHOUT AUTO PUMP SHUT OFF + AUDIBLE AND VISUAL AlARMS - ] 15. AUTOMATIC LINE lEAK DETECTOR (3.0 GPH TEST) WITHOUT FLOW SHUT OFF OR RESTRICTION ] 16. ANNUALlNTEGRITY TEST (0.1 GPH) 0 16., ANNUALlNTEGRITYTEST(O.1 GPH) ] 17. DAJLYVISUALCHECK 0 17. DAilY VISUAL CHECK ...; ,:~.:.,:;; {-:-;' '·";:1~(.~ ·..Of;. ':'~.~;;;'~:~"~'tW:~~~.?~~:~·'f§:ii~1I ';blS.~~~~E~' C()~TAt~~WNT" :..,,;. )ISPENSER CONTAINMENT 1. FLOAT MECHANISM THAT SHUTS OFF SHEAR VALVE DATE INST LLEPJ 468 0 2. CONTINUOUS DISPENSER PAN SENSOR + AUDIBLE AND VISUAL AlARMS " ,C8:3. CONTINUOUS DISPENSER PAN SENSOR WITH AUTO SHUT OFF FOR DISPENSER + AUDIBLE AND VISUAL ALARMS IX. OWNER/OPERA TOR SIGNATURE ..._._.____.__,_._.. UNDERGROUND PIPING -ŠiNGlE WALL PIPING ~RESSURIZED PIP1NG (Check all that apply): :J 1. ELECTRONIC LINE LEAK DETECTOR 3.0 GPH TESTYill!;j AUTO PUMP SHUT OFF FOR LEAK, SYSTEM FAilURE, AND SYSTEM DISCONNECTION + AUDIBLE AND VISUAL AlARMS :J 2. MONTHLY 0.2 GPH TEST :J 3. ANNUAL INTEGRITY TEST (0.1 GPH) :ONVENTIONAL SUCTION SYSTEMS: :J 5. DAILY VISUAL MONITORING OF PUMPING SYSTEM + TRIENNIAL PIPING INTEGRITY TEST (0.1 GPH) 5AFE SUCTION SYSTEMS (NO VALVES IN BELOW GROUND PIPING): ] 7. SELF MONITORING 3RAVITY FLOW: . 9. BIENNIAL INTEGRITY TEST (0.1 GPH) SECONDARILY CONTAINED PIPING 'RESSURIZED PIPING (Check all that apply): 10. CONTINUOUS TURBINE SUMP SENSOR WITH AUDIBLE AND VISUAL ALARMS AND (Chedl one) - o a, AUTO PUMP SHUT OFF WHEN A LEAK OCCURS .9. b. AUTO PUMP SHUT OFF FOR lEAKS, SYSTEM FAILURE AND SYSTEM DISCONNECTION o c. NO AUTO PUMP SHUT OFF ~ 11. ~\~W~~g~INE LEAK DETECTOR (3.0 GPH TEST) ~ FLOW SHUT OFF OR J 12. ANNUAL INTEGRITY TEST (0.1 GPH) ìUCTION/GRAVITY SYSTEM: ] 13. CONTINUOUS SUMP SENSOR + AUDIBLE AND VISUAL AlARMS o 2. SUCTION o 95. UNKNOWN o 99. OTHER . [J 3. GRAVITY 45' 46: _ ., .._ ___ ___ 46, o 6. FRP COMPATIBLE WI ~-~~ANO-;:-'" o 1. GALVANIZED STEEL o 8. FLEXIBLE (HOPE) 0 99. OTHER o 9. CATHODIC PROTECTION 095. UNKNOWN 465 ABOVEGROUND PIPING SiÑGlE WALL PIPING PRESSURIZED PIPING (Check aI/that apply): o 1. ELECTRONIC LINE LEAK DETECTOR 3.0 GPH TEST!Y!I!:2 AUTO PUMP SHUT OFF FOR LEAK. SYSTEM FAILURE, AND SYSTEM DISCONNECTION + AUDIBLE AND VISUAL AlARMS o 2. MONTHLY 0.2 GPH TEST o 3. ANNUAL INTEGRITY TEST (0.1 GPH) i 0 4. DAfl.. Y VISUAL CHECK I CONVENTIONAL SUCTION SYSTEMS (CheCk aI/that apply): I 0 5. DAilY VISUAL MONITORING OF PIPING AND PUMPING SYSTEM I 0 6. TRIENNIAL INTEGRITY TEST (0.1 GPH) 467 SAFE SUCTION SYSTEMS (NO VALVES IN BELOW GROUND PIPING): o 1. SELF MONITORING GRAVITY FLOW (Check aI/that apply): o 8. DAILY VISUAL MONITORING o 9. BIENNIAL INTEGRITY TEST (0.1 GPH) SECONDARILY CONTAINED PIPING I PRESSURIZED PIPING (Check all that apply): 10. CONTINUOUS TURBINE SUMP SENSOR ~ AUDIBLE AND VISUAL ALARMS AND (check one) lOa. AUTO PUMP SHUT OFF WHEN A LEAK OCCURS o b. AUTO PUMP SHUT OFF FOR LEAKS. SYSTEM FAILURE AND SYSTEM DISCONNECTION o c. NO AUTO PUMP SHUT OFF o 11. AUTOMATIC LEAK DETECTOR o 12. ANNUAL INTEGRITY TEST (0.1 GPH) SUCTION/GRAVITY SYSTEM: o 13. CONTINUOUS SUMP SENSOR + AUDIBLE AND VISUAL ALARMS EMERGENCY GENERATORS ONLY (Check all that apply) o 14. CONTINUOUS SUMP SENSOR~ AUTO PUMP SHUT OFF + AUDIBLE AND VISUAL AlARMS o 15. AUTOMATIC LINE LEAK DETECTOR (3.0 GPH TEST) ~..." ': :"·('."·;·C '. o 4. DAilY VISUAL CHECK o 5. TRENCH LINER I MONITORING o 6. NONE 469 ._--~.- I certify Ihat Ihe information provided herein Is lrue and accurate to Ihe best of _GNATUf¡'É òï= ÖWNERJOPERATOR -- W!.MË OF ÔWNEÃÏoPËAArOR (print) J~ -B..'-(~,=-__ 5' A ~~A_E-Lß~ 474 Permll expiration Dale (For local uss only) 475 P8ITI11 Number (For locs/ use only) 473 Permit Approved (For local use only) S:\CUPAFORMS\SWRCB-BWPD· PCF (7/99) ---{ÕA'T{---'T-- --- ~--.., ... --'--·-----41Õ '" - ,ifu-Ôi~'~eb---- -------- -- ---- -----.¡, ._., _~ \-\- ~~..__,___.~\~'--_\A.."t::i(...L-aDQ OU~,!.è ...~,. (Specify reason' lor local use only) (Specify change ,lor !ccal use only) BUSIÑESS NAME(Säm..-ã; i=ÄëiLi-ï-Ÿ ÑÃME orDéÃ: ôÖin¡ éúš.;;;Ü-Ãs)·--· - -' ---' -3"1 FACIUlY ID # - I _ ,..__..,_!:::-O R ~¿ R '- ~ ~ 1\ ~S--,~ ~..s .__.?\-',\.'- I LOCATION W1THIN SITE (Optional) - - . NPE OF ACTION (Check one I/em only) .. CITY OF BAK.El{~t1J:;LU \ :;J:::JD ~/'+- I OFWCE OF ENVIRONMENTAL "VICES œ: 1715 Chester Ave., Bakersfield, CA 93301 (661) 326-3979 " ~ .'. UNDERGROUND STORAGE TANKS· TANK PAGE 1 Page j- 01 7. : ~. TEMPORARY SITE CLOSURE o 7. PERMANENTLY CLOSED ON SITE o 8. TANK REMOVED I íI-; ¡-I--ï'¡' ~ : ¡ i :: I ' _---- _.----.:...-.- __~_l.-__ ~...;... ....,.--...--.-.--- 4 o I. NEW SITE PERMIT 0 4. AMENDED PERMIT o 5. CHANGE OF INFORMATION) o 3. RENEWAL PERMIT 41 ....;--.-..--.----.' I ! I I. TANK DESCRIPTION 433 : COMPARTME~TAN;--Õ Yes -:if No I If "Yes". complete one page for each companment. 4:36(ÑÜMBÈROFëõMPARTMENTS' ---.--.-----:¡ . i , I I . 432:TANK WlNUFACi1JRER I -f ÄÑI< ID # "ÖÄfËiNSfAL:LED (YEAR/MO) a A.. ~ \~'" 435 O...¡..¡~ ~ TANK CAPACITY IN GALLÕNS \O\ODO 4, :-ÃDDITIONAL DESCRIPTION (For local use only) I TANK USE 439 : ~. MOTOR VEHICLE FUEL , (If marked. ClJmplete Petroleum Type) · 0 2. NON,FUEL PETROLEUM o 3. CHEMICAL PRODUCT D 4. HAZARDOUS WASTE (Includes Used On) o 95. UNKNOWN - T ANK MATERIAL - secondary lank 0 I 1. BARE STEEL ; (Check one #em only) D 2. STAINLESS STEEL o 1. MANUFACTURED CATHODIC ~3. FIBERGLASS REINFORCED ?\.ASTIC 095. UNKNOWN PROTECTION 0 4. IMPRESSED CURRENT 0 99. OTHER o 2. SACRIFICIAL ANODE (For locallJse only) YEAR INSTALLED 450 1YPE (Forlocal use only)" 451 OVERFill PROTECTION EQUIPMENT: YEAR INSTALLED 4 ~. '"'' ",,,,,,"M'''' ~ 15 é?...~ 0....... 0 L MARM )!:r um'''''""' 0", '"'' d I rg 2. DROP TUBE ~ Ç".... Af'(þ'¿-Q. 02. 8ALLFLOAT 04. EXEMPT )&3. STRIKER PLATE ~ 0A:>~'" CPrvté i '.::; ;;. ." ;.i_4h~;Iþ~;~g:. '~:~;.; J!~~' Si. ·1~:r5.f~~±~:~~.'~~';~'!!)X~··'fAij¡{~ E~ D~èqt1C?N.-~':::iift:'!·~~ \~'3:;'o/¡t ",!{if!A:4~,,~>~~j',;;'f i~. ::.. ;",;" ..,;·e~~:f.':;¿~i~i~¡~ 1 IF SINGLE WALL TANK (Check all that apply): 453 IF DOUBLE WALL TANK OR TANK WITH BLADDER (Check one item only): ' VISUAL (EXPOSED PORTION ONLY) 05. MANUAL TANK GAUGING (MTG) 0 1. VISUAL(SINGLEWALLINVAULTONLY) AUTOMATIC TANK GAUGING (ATG) 06. VADOSE ZONE BJ 2. CONTINUOUS INTERSTITIAL MONITORING CONTINUOUS ATG 0 1. GROUNDWATER 0 3. MANl)AL MONITORING STATISTICAL INVENTORY RECONCILIATION (SIR) + 0 B. TANK TESTING BIENNIAL TANK TESTING D 99. OTHER \ V. TANK CLOSURE INFORMATION I PERMANENT CLOSURE IN PLACE TYPE OF TANK i : (Check one #em only) · TANK MATERIAL· primary tank · (Check one item only) \. TANK INTERIOR LINING lOR COATING I ~Check one item onl · OTHER CORROSION : PROTECTION IF APPLICABLE I ; ~~~~ck ~ne ilem only) · SPILL AND OVERFILL ! ; (Check all/hat apply) 01. D 2. i D 3. .:04. \-,---- ; r·"--·~ , II. TANK CONTENTS I 41 PETROLEUM TYPE o la. REGULAR UNLEADED ~b. PREMIUM UNLEADED Ole. MIDGRADE UNLEADED o 5. JET FUEL o 6. AVIATION FUEL o 99. OTHER o 2. LEADED o 3. DIESEL o 4. GASOHOL 441 CAS # (from Hazardous Materials Inventory page) COMMON NAME (from HazardouS Materials Inventory page) o 1. SINGLE WAll ~2. DOUBLE WAll \- 1\0"'\0 R... Q\¡so,-~~é III. TAN ( CONSTRUCT1ON o 3. SINGLE WALL WITH EXTERIOR MEMBRANE LINER o 4. SINGLE WALL IN A VAULT J I I I 4-' ¡ o 5, SINGLE WALL W1TH INTERNAL BLADDER SYSTEM D 95. UNKNOWN o 99. OTHER o 5. CONCRETE o 8. FRP COMPATIBLE WI100% METHANOL o 95. UNKNOWN D 99. OTHER o 1. BARE STEEL D 2. STAINLESS STEEL 3. FIBERGLASS I PLASTIC D 4. STEEL CLAD W/FIBERGLASS REINFORCED PLASTIC FRP ~ 3. FIBERGLASS / PLASTIC o 4. STEEL CLAD WIFIBERGLASS REINFORCED PLASTIC (FRP) o 5. CONCRETE o 3. EPOXY LINING o 4. PHENOLIC LINING 4-' o 95. UNKNOWN o 99. OTHER o 8. FRP COMPATIBLE W/100% METHANOL o 9. FR? NON-CORRODlBlE JACKET 010. COATED STEEL I 41 41 446 DATE INSTALLED 3"95. UNKNOWN o 99. OTHER D 5. GLASS UNING o 6. UNLINED o 1. RUBBER LINED o 2. ALKYD LINING (For local use only) DATE INSTAllED 448 456 TANK FILLED W1TH INERT MATERIAL? ð 455' . E~TIMA TED QUANTllY~UBST ANCE REWlINING ' ~_ gallons /' -- --~-------'---"---- I S:\CUP AFORMS\SWRCB-B.\ DYes 0 No __----. ..~ .,....__.M__--·- UPCF (7199) ..-..-.-- -_.~-_._..._------_.-._,.__._.- :- CI¡Y OF BAKERSFIELD ~ OFFICE OF ENVIRONMENTAL SERVI 1715 Chester Ave" Bakersfield, CA 93301 (661) 26-3979 " ." . I ~.. I UST. TANK PA,,¡ I . Page ~ ( ....-:: --------- ---- =---.·....!!--4 I ~ :)O'lq::.. .M____.... --:"eõvËGRõüÑÕPiPiÑõ--- -.- -.------ . '.... ..0. _ . ------ÜÑÕËRCROUND PIPING VI. PIPING CONST~UCT10N (Chock an that apply) SYS rEM TYPE \./' .' 0 .RSJ 1. PRESSURE 0 _2. SUC::TI~N.. 0 3. GRAVITY 45e ~... 1. PRESSU~E_. CONSTRUCTION! 0 1. SINGLE WALL 0 3. LINED TRENCH 0 99. OTHER 460 i 0 1. SINGLE WALL MANUFACTURER:R 2. DOUBLE WALL 0 95. UNKNOWN : 0 2. DOUBLE WALL , MANUFACTURER 461 ~ MANUFACTURER , ¡j" ~.··~;;Ê· ~:;;~~_. ··-O~. F;P COMPA TI;~É ';'/1 OO~'~ETIiANOL -'! 0 "7.-~~~E STE;;:-·------ -- .. ... ., - MATERIALS AND '0 2. STAINLESS STEEL 0 7 GALVANIZED STEEL I 0 2. STAINLESS STEEL CORROSION ' . PROTECTION iO 3. PLASTIC COMPATIBLE WITH CONTENTS 095. UNKNOWN 10 3. PLASTIC COMPATIBLE WITH CONTENTS i8:"4. FIBERGLASS 0 e. FLEXIBLE (HDPE) 099. OTHER I 0 4. FIBERGLASS :0 5. STEEL WI COATING 0 9. CATIiODIC PROTECTION 464 0 5. STEEL WI COATING VJI. PIPING LEAK DETECTION (Check aU ihat apply) . .. , 466 EMERGENCY GENERATORS ONLY (Check aU /hat epply) ] 14. CONTINUOUS SUMP SENSOR WITHOUT AUTO PUMP SHUT OFF + AUDIBLE AND VISUAL ALARMS - ] 15. AUTOMATIC LINE LEAK DETECTOR (3.0 GPH TEST) WITHOUT FLOW SHUTOFF OR RESTRICTION ] 16. ANNUAL INTEGRITY TEST (0.1 GPH) 0 16.. ANNUALlNTEGRITY TEST (0.1 GPH) ] 17. DAILY VISUAL CHECK 017. DAILY VISUAL CHECK .-. . ~.-; ::.,~.::/~' ~i:1J~"'1~~j~~~:>:::Yei~¡j;;¡_~~;;'~i-#:ti;Yj't!.bJs.~~~~EF!,·C()~r.Ai~~,¢NT",:;;; , )ISPENSER CONTAINMENT 1. FLOAT MECHANISM THAT SHUTS OFF SHEAR VALVE DATE N A 468 0 2. CONTINUOUS DISPENSER PAN SENSOR + AUDIBLE AND VISUAL AlARMS ]:8:.3. CONTINUOUS DISPENSER PAN SENSOR WlTIi AUTO SHUT OFF FOR DISPENSER + AUDIBLE AND VISUAL ALARMS IX. OWNER/OPERA TOR SIGNATURE ..,____.____._,_ UNDERGROUND PIPING -·----Šï~WALL PIPING "RESSURIZED PIPING (Check all that apply): ::J 1. ELECTRONIC UNE LEAK DETECTOR 3.0 GPHTEST~AUTO PUMP SHUT OFF FOR LEAK, SYSTEM FAILURE, AND SYSTEM DISCONNECTION + AUDIBLE AND VISUAL ALARMS 2. MONTHLY 0.2 GPH TEST ::J :J 3. ANNUAL INTEGRITY TEST (O.1 GPH) ::ONVENTIONAL SUCTION SYSTEMS: :J 5. DAILY VISUAL MONITORING OF PUMPING SYSTEM + TRIENNIAL PIPING INTEGRITY TEST (0.1 GPH) 5AFE SUCTION SYSTEMS (NO VALVES IN BELOW GROUND PIPING): ] 7. SELF MONITORING . 3RAVITY FLOW: ] 9. BIENNIAL INTEGRITY TEST (O.1 GPH) SECONDARILY CDNTAlNED PIPING 'RESSURIZED PIPING (Check a/l thet apply): 10. CONTINUOUS TURBINE SUMP SENSOR W1TIi AUDIBLE AND VISUAL ALARMS AND (Check one) - o a. AUTO PUMP SHUT OFF WHEN A LEAK OCCURS .B. b. AUTO PUMP SHUT OFF FOR LEAKS, SYSTEM FAILURE AND SYSTEM DISCONNECTION o c. NO AUTO PUMP SHUT OFF ~ 11. AUTOMATIC LINE LEAK DETECTOR (3.0 GpH TEST) WITH FLOW SHUT OFF OR RESTRICTION - ] 12. ANNUAL INTEGRITY TEST (O.1 GPH) jUCTION!GRAVITY SYSTEM: ] 13. CONTINUOUS SUMP SENSOR + AUDIBLE AND VISUAL ALARMS I certify Ihal (he Information proVIded herein Is true and accurate 10 lhe best of my know1edge. . "....nj'Éó'_"',¡;ffi:,~~ NAMÉ OF òÌNN-ËRJOPERÞ.rOR (print) __~ß..,-{~__5A~~A_F' ~~ o 2. SUCTION o 95. UNKNOWN o 99. OTHER . [;1 3.. GRAVITY o 6. FRP COMPAT;B~ ~/1-~¡'-~TIiAN~~ o 7. GALVANIZED STEEL o 6. FLEXIBLE (HDPE) 0 99. OTHER I o 9. CATHODIC PROTECTION o 95. UNKNOWN ABOVEGROUND PIPING ŠÎÑ'GLE WALl. PIPING PRESSURIZED PIPING (CheCk aU /hat apply): o 1. ELECTRONIC UNE LEAK DETECTOR 3.0 GPH TEST~ AUTO PUMP SHUT OFF FOR LEA SYSTEM FAILURE. AND SYSTEM DISCONNECTION + AUDIBLE AND VISUAL ALARMS 2. MONTHLY 0.2 GPH TEST o o 3. ANNUAL INTEGRITY TEST (O.1 GPH) i 0 4. DAILY VISUAL CHECK I CONVENTIONAL SUCTION SYSTEMS (Check aU /hat apply): ,0 5. DAILY VISUAL MONITORING OF PIPING AND PUMPING SYSTEM ¡ 0 6. TRIENNIAL INTEGRITY TEST (0.1 GPH) SAFE SUCTION SYSTEMS (NO VALVES IN BELOW GROUND PIPING): o 7. SELF MONITORING GRAVITY FLOW (Check all that apply): o B. DAILY VISUAL MONITORING o 9. BIENNIAL INTEGRITY TEST (O.1 GPH) SECONDARILY CONT AJNED PIPING I PRESSURIZED PIPING (Check all that apply): 10. CONTINUOUS TURBINE SUMP SENSOR ~ AUDIBLE AND VISUAL ALARMS AND {check OJ ,. 0 a. AUTO PUMP SHUT OFF WHEN A LEAK OCCURS o b. AUTO PUMP SHUT OFF FOR LEAKS. SYSTEM FAILURE AND SYSTEM OISCONNECTIC o Co NO AUTO PUMP SHUT OFF o 11. AUTOMATIC LEAK DETECTOR o 12. ANNUAL INTEGRITY TEST (0.1 GPH) SUCTION/GRAVITY SYSTEM: o 13. CONTINUOUS SUMP SENSOR + AUDIBLE AND VISUAL ALARMS EMERGENCY GENERATORS ONLY (Check all that apply)' o 14. CONTINUOUS SUMP SENSOR~ AUTO PUMP SHUT OFF + AUDIBLE AND VISUAL ALARMS o 15. AUTOMATIC LINE LEAK DETECTOR (3.0 GPH TEST) ~..... . '-:r~,':i:'r'"' ': o;.,t:, ~'::'C '. o 4. CAlLY VISUAL CHECK o 5. TRENCH LINER I MONITORING o 6. NONE 4õ 47~.J-_--_:::'ÕF~~l0~~=: .~~~_:~~~=.,:: -,-=~ =~ :: ~ ~~.:::..__~_t:A\-'?!o,.,_,~_aDQ OL~II2.f 474 Perm ( ,exPiration Dale (Por local use only) 47 Perm" Number (Por loca/ use only) 473 I Permll Approved (For local use only) nf""'t: 1*7,,,n\ S:\CUP AFORMS\SWRCB-B.W Page 1.? 01 ~. TEMPORARY SITE CLOSURE o 7. PERMANENTLY CLOSED ON SITE (Specify reason . lor local use only) (Specify change . lor lOcal use only) 0 B. TANK REMOVED 43 BUSIÑES'S NAME '¡"Šå'me'ãš-FÃèÜï-V ÑÃME ói DM- ~ 00;;,"9- ã~s.;;;;;Ãs)'---' -- - ---' --3-îFAëiLïrnõïl-I-II-' -;-. --(, -_.~ -- . - - - ; -- -..---.------- -" _ ¡:I II;' 'r-O R ~¿: R. ,-"'1 \....1\ A- c. \.~..s S\-\¿-~'- I : i i :: i' , · 'LõëÄriõN"wITHIN SITE (Opüona-¡¡------ .----.---.- .-.- , -- ,-- .-.--'-.. -.-.-"-,--. - -'--. _.. -.". - - ---45 I I ." . rYPE OF ACTION (Check one Ilem only) ¡;> CITY OF BAKERSFIELU I ~::::JO 7q..- i O~E OF ENVIRONMENTAL .VICES Œ 1715 Chester Ave., Bakersfield, CA 93301 (661) 326-3979 " ~> UNDERGROUND STORAGE TANKS - TANK PAGE 1 ' I ':11 o 1. NEW SITE PERMIT 0 4. AMENDED PERMIT o 5. CHANGE OF INFORMATION) o 3. RENEWAL PERMIT I. TANK DESCRIPTION -fMfK ID # 432 TANK W.NUFACTURER O-..J.J é"N ~ TANK CAPACITY IN GAlLÓÑS rl 433 : COMPARTMENTALIZED ~;---Õ Yes '-:xr- No 43- Ló ~ ~ \~, q ~ If 'Yes". complete one page lor each compa"ment. '-43ST'ÑÚMãË'R OF COMPARTMENTS' _.._,- I , "ÖÄfËiNSfÃLCED (YEAR/MO) 431 435 \0\000 43å I ;"ÃDDITIONAL DESCRIPTION (For lOcal use only) I TANK USE 439 : ):::,. MOTOR VEHICLE FUEL , (II marlced. complete Petroleum Type) · 0 2. NON·FUEL PETROLEUM o 3. CHEMICAL PRODUCT o 4. HAZARDOUS WASTE (Includes Used Oil) o 95. UNKNOWN PE OF TANK ¡ (Check one flem only) · TANK MATERIAL· primary lank · (Check one flem only) II. TANK CONTENTS 441 PETROLEUM TYPE o 1 a. REGULAR UNLEADED o 1 b. PREMIUM UNLEADED );::(1C. MIDGRADE UNLEADED o 2. LEADED o 3. DIESEL o 4. GASOHOL o 5. JET FUEL o 6. AVIATION FUEL o 99. OTHER 441 CAS # (Irom Hazerdous Materials Invenrory page) 44 COMMON NAME (Irom Hazardous Materials Inventory page) \:-1\0 -roO ~ C;:\~'o.o '- , ~J 111. TANK CONSTRUCTION o 1. SINGLE WALL :>'t2. DOUBLE WALL o 3. SINGLE WALL WITH EXTERIOR MEMBRANE LINER o 4. SINGLE WALLIN A VAULT o 5. SINGLE WALL WITH INTERNAL BLADDER SYSTEM o 95. UNKNOWN o 99. OTHER o 5. CONCRETE o B. FRP COMPATIBLE W/100% METHANOL 44: o 1. BARE STEEL o 2. STAINLESS STEEL 3. FIBERGLASS I PLASTIC o 4. STEEL CLAD WIFIBERGLASS REINFORCED PLASTIC (FRP) }(3. FIBERGLASS I PLASTIC o 4. STEEL CLAD W/FIBERGLASS REINFORCED PLASTIC (FRP) o 5. CONCRETE o 3. EPOXY LINING o 4. PHENOLIC LINING 095. UNKNOWN o 99. OTHER 44< o 95. UNKNOWN o 99. OTHER 44! TANK MATERIAL· secondary lank 0 ¡ 1. BARE STEEL : (Check one ¡¡em only) 0 2. STAINLESS STEEL o 8. FRP COMPAT1BLE W/100% METHANOL o 9. FRP NON-GORROOIBLE JACKET 010. COATED STEEL o 1. MANUFACTURED CATHODIC PROTECTION o 2. SACRIFICIAL ANODE YEAR INSTALLED 450 TYPE (For/ocel use only¡- 451 ~1. SPILL CONTAINMENT ~ 15674<... ~'Ñ ~ 2. DROP TUBE ~ -\-.... Ai>f>'¿-{2. .1813. STRIKER PLATE ì (? A:>~T CPrrné .. ':~:' . ~~;:l'~';A~~;:"if.'; &~ X<f':::~~;~~£;:?r~.'{~¡:Þ1:',:iy:···tAijKi:~ D~EC:tl~.·..'~d¥r,:::~ to:~18~::,,\f;;:.If;~f-;~;,+;:!J>~ii~!;1 ~~.," ~: i':;,.:-:;., ·"::'~.;:;:~~i1'~¡~· IF SINGLE WALL TANK (Check alllhat apply): 453 IF DOUBLE WALL TANK OR TANI< WITH BLADDER (Check one item only): 45 o 1. VISUAL(EXPOSEDPORTIONONLY) 05. MANUAL TANK GAUGING (MTG) 01. VISUAL (SINGLE WALLIN VAULT ONLY) o 2. AUTOMATIC TANK GAUGING (ATG) 0 6. VADOSE ZONE }S: 2. CONTINUOUS INTERSTITIAL MONITORING o 3. CONTINUOUS ATG 0 7. GROUNDWATER 0 3. MANUAL MONITORING .. 0 4. STATISTICAL INVENTORY RECONCILIATION {SIR) + 0 8. TANK TESTING BIENNIAL TANK TESTING 0 99, OTHER \ f--.---..- V. TANK CLOSURE INFORMATION I PERMANENT CLOSURE IN PLÞ.CE 'I TANK INTERIOR LINING I OR COATING !iCheck one item only) ! OTHER CORROSION : PROTECTION IF APPLICABLE ; : (_~h_eck ~'!..e item only) SPILL AND OVERFill I : (Check all Iher epply) r 1 ~ 446 DATE INSTALLED <\.4: I .3'95. UNKNOWN o 99. OTHER o 5. GLASS LINING o 6. UNLINED o 1. RUBBER LINED o 2. ALKYD LINING {For toealuse only} DATE INSTALLED 44' .8r 3. FIBERGLASS REINFORCED PLASTIC o 4. IMPRESSED CURRENT o 95. UNKNOWN o 99. OTHER <\.48 (For local use only) OVERFILL PROTECTION EQUIPMENT; YEAR INSTAllED 45 o 1. ALARM ;gr 3. FILL TUBE SHUT OFF VALVE 'ìf'1 f o 2. BALL FLOAT 0 4. EXEMPT 41 TANK FILLED WITH INERT MATERIAL? IDAY) €:> 455 . . E~TIW. TED QUANTITY OF SUBSTANCE REMAINING 456 ~ gallons . .----.- -,-~--~-----_._-_.._~-- o Yes 0 No --.--..-.-- .." ...........----.- '-'" , , UPCF (7199) S :\CUPAFORMS\SWRCB-B.v-. ... e .. CITY OF BAKERSFIELD OFFICE OF ENVIRONMENTAL SERVlcA 1715 Chester Ave., Bakersfield, CA 93301 (66~6-3979 ,. I !> ::>0 '-1 cr- " UST· TANK PÄ¿ .-:-------- _...!:~- 4-~~..!; ..__._.,... H'_ ---Aã'övËõRõüÑÕPiPiÑã-- ..- -.---.-- ..-- VI. PIPING CONSTRUCT10N (Check eJ/ that apply) . ..... ,.-. -. -.----..-..- UNDERGROUND PIPING .. ..; SYSTEM TYPE )¡(1. PRESSURE 0 .2. S~~TI~N.. 0 3. GRAVITY 458 u;¡ I. PRESSU~E... CONSTRUCTION/ 0 1. SINGLE WALL 0 3. LINED TRENCH 0 99. OTHER 460; 0 1. SINGLE WALL MANUFACTURER:R 2. DOUBLE WALL 0 95. UNKNOWN : 0 2. DOUBLE WALL : MANUFACTURER 461 ~ MANUFACTURER .---. ~d ~.··~~~·Š~~L 0;. F;' COMPATI;:e '~1100%'~-ETHANOL "', Ö -;';~~E STE;~""--' ... . .. .- MATERIALS AND '0 2. STAINLESS STEEL 0 7 GALVANIZED STEEL I 0 2. STAINLESS STEEL CORROSION I . . PROTECTION [03. PLASTIC COMPATIBLE WiTH CONTENTS 095. UNKNOWN ,0 3. PLASTIC COMPATIBLE WITH CONTENTS ¡~4. FIBERGLASS 0 8. FLEXIBLE (HDPE) 099. OTHER I 0 4. FIBERGLASS ;0 5. STEEL WI COATING 0 9. CATHODIC PROTECTION 464 0 5. STEEL WI COATING VB. PIPING LEAK DETECT10N (ChÐck sO iha/ apply) . .. I 466 EMERGENCY GENERATORS ONLY (Check all that apply) J 14. CONTINUOUS SUMP SENSOR WITHOUT AUTO PUMP SHUT OFF + AUDIBLE AND VISUAL ALARMS - ] 15. AUTOMATIC LINE LEAK DETECTOR (3.0 GPH TEST) WITHOUT FLOW SHUTOFF OR RESTRICTION ] 16. ANNUALlNTEGRITYTEST(0.1 GPH) 0 16.. ANNUALlNTEGRITYTEST(0.1 GPH) J 17. DAILY VISUAL CHECK 017. DAJLYVISUALCHECK . .. ;'.. ,..,."........ - ., >"."," . .,,' .,'<r:'~,~;<,,,¡&.;:._."": ·l:·;¡;··Virl·:bISPENSER'CONTAiNMENT··'·' _. .... , '..... ::: ~:;..,.;./~ .' ~~·::¿:J~~:~,{;~.,_~,;-:.~~:~...'~f::~~~·~~~~~,~r~~r.~~..~;~;~....'.. "'~"" "r.·-'· .,' '. .of.,:' ~,,' ~-.,~. '....::~~.. ,f. JlSPENSER CONTAINMENT 1. FLOAT MECHANISM THAT SHUTS OFF SHEAR VALVE DATE INS L 468 0 2. CONTINUOUS DISPENSER PAN SENSOR + AUDIBLE AND VISUAL ALARMS ~ ~3. CONTINUOUS DISPENSER PAN SENSOR WITH AUTO SHUT OFF FOR DISPENSER + AUDIBLE AND VISUAL ALARMS IX. OWNER/OPERA TOR SIGNATURE 'œ""~,..~",~,,,~~~~.....~.myM""'''''' .~________________ __ . ________ _ . :::::::,:: - _ --- ~ on L:ä~l,~!Y ---- ---------------=~---:; .J~ ß......(~__5 ~Q~A_E 1 A.~ .,L;S 'r-\B' -=,_~_~~~_,..ð:tl"_S;;__aDQOL\~~.è'ÏQ.f ..,____.___.__,_ UNDERGROUND PIPING . -----šiNGLE WALL PIPING PRESSURIZED PIPING (Check all Ina/apply): :J ,. ELECTRONIC LINE LEAK DETECTOR 3.0 GPH TEST Y!!]:! AUTO PUMP SHUT OFF FOR LEAK. SYSTEM FAILURE. AND SYSTEM DISCONNECTION + AUDIBLE AND VISUAL ALARMS :J 2. MONTHLY 0.2 GPH TEST :J 3. ANNUAL INTEGRITY TEST (0.1 GPH) ::ONVENTIONAL SUCTION SYSTEMS: :J 5. DAILY VISUAL MONITORING OF PUMPING SYSTEM + TRIENNIAL PIPING INTEGRITY TEST (0.' GPH) òAFE SUCTION SYSTEMS (NO VALVES IN BELOW GROUND PIPING): ] 7. SELF MONITORING 3RAVITY FLOW: . ] 9. BIENNIALlNTEGRITY TEST (0,1 GPH) SECONDARILY CONTAINED PIPING 'RESSURIZED PIPING (Check sl//na/apply): 10. CONTINUOUS TURBINE SUMP SENSOR WITH AUDIBLE AND VISUAL ALARMS AND (Check one) - o a. AUTO PUMP SHUT OFF WHEN A LEAK OCCURS ~ b. AUTO PUMP SHUT OFF FOR LEAKS. SYSTEM FAILURE AND SYSTEM DISCONNECTION o c. NO AUTO PUMP SHUT OFF ). 11. AUTOMATIC LINE LEAK DETECTOR (3.0 GPH TEST) WITH FLOW SHUT OFF OR RESTRICTION - ] 12. ANNUAL INTEGRITY TEST (0.1 GPH) ¡UCTION/GRAVITY SYSTEM: ] 13. CONTJNUOUS SUMP SENSOR + AUDIBLE ANO VISUAL ALARMS 02. ..9 J,. GRAVITY SUCTION o 95. UNKNOWN o 99. OTHER --·--õ 6~'~;~-ë;~~ATIBLE ~71-~""%-~THAN~Z o 7. GALVANIZEO STEEL o 8. FLEXIBLE (HOPE) 0 99. OTHEF o 9. CATHODIC PROTECTION o 95. UNKNOWN ABOVEGROUND PIPING šiÑGLE WALL PIPJNG PRESSURIZED PIPING (Check al/tha/ apply): o 1. ELECTRONIC LINE LEAK DETECTOR 3.0 GPH TEST ~ AUTO PUMP SHUT OFF FOR LEI SYSTEM FAILURE, AND SYSTEM DISCONNECTION + AUDIBLE AND VISUAL ALARMS o 2. MONTHLY 0.2 GPH TEST o 3. ANNUAL INTEGRITY TEST (0.1 GPH) ¡ 0 4. DAILY VISUAL CHECK I CONVENTIONAL SUCTION SYSTEMS (Check aI/that apply): I 0 5, DAILY VISUAL MONITORING OF PIPING AND PUMPING SYSTEM ) 0 8. TRJENNIAL INTEGRITY TEST (0.1 GPH) , SAFE SUCTION SYSTEMS (NO VALVES IN BELOW GROUND PIPING~ o 7. SELF MONITORING GRAVITY FLOW (Check aI/that apply): o 6, DAILY VISUAL MONITORING o 9. BIENNIAL INTEGRITY TEST (0.' GPH) SECONDARJL Y CONTAINED PIPING I PRESSURIZED PIPING (Check all that apply): 10. CONTINUOUS TURBINE SUMP SENSOR ~ AUDIBLE ANO VISUAL ALARMS AND (ct>eek c o a. AUTO PUMP SHUT OFF WHEN A LEAK OCCURS o b. AUTO PUMP SHUT OFF FOR LEAKS. SYSTEM FAILURE AND SYSTEM DISCONNECTI( o c. NO AUTO PUMP SHUT OFF o 11. AUTOMATIC LEAK DETECTOR o 12. ANNUAL INTEGRITY TEST (0.1 GPH) SUCTION/GRAVITY SYSTEM: o 13. CONTINUOUS SUMP SENSOR + AUDIBLE AND VISUAL ALARMS EMERG ENCY GENERATORS ONLY (Check a/l thaI apply) o 14. CONTINUOUS SUMP SENSOR ~ AUTO PUMP SHUT OFF + AUDIBLE AND VISUAL ALARMS o 15. AUTOMATIC LINE LEAK DETECTOR (3.0 GPH TEST) ~....., . .. . ·~,~r,..:·· .,' :.,l:, '~':,r o 4. DAILY VISUAL CHECK o 5, TRENCH LINER I MONITORING o 6. NONE M: Penn It Number (For local use only) 473 I Perml! Approved (For local use only) 474 I Permll7xPlrauon Dale (For local use only) 471 I PCF 17/99\ S:\CUPAFORMS\SWRCS-SW FIRE CHIEF RON FRAZE ADMINISTRATIVE SERVICES 2101 ·H· Street Bakersfield, CA 93301 VOICE (661) 326-3941 FAX (661) 395-1349 SUPPRESSION SERVICES 2101 "H· Street Bakersfield, CA 93301 VOICE (661) 326-3941 FAX (661) 395·1349 PREVENTION SERVICES 1715 Chester Ave. Bakersfield, CA 93301 VOICE (661) 326-3951 FAX (661) 326-D576 ENVIRONMENTAL SERVICES 1715 Chester Ave. Bakersfield, CA 93301 VOICE (661) 326-3979 FAX (661) 326-D576 TRAINING DIVISION 5642 Victor Ave. Bakersfield, CA 93308 VOICE (661) 399-4697 FAX (661) 399-5763 - e May 31,2000 Carlton E. Howell Equiva Services LLC 13105 Meadow Lane Leawood, KS 66209 RE: Request for extension of temporary closure of (2) Shell facilities, 101 S. Union Ave. and 3130 24th S1. r Dear Mr. Howell Please be advised, that the Bakersfield Fire Department has approved your request for an extension of temporary closure for the above mentioned facilities, through 12-31-00. This extension is subject to proper housekeeping and maintenance of each facility. Should you have any questions, please feel free to contact me at (661) 326-~979. Sincerely, Ralph Huey, Director Office of Environmental Services bY:~~ Steve Underwood, Inspector Office of Environmental Services cc: Terry Runnels ""7~ de W~ ~ .A0Pe ffbt, A Wedu~" j. FIRE CHIEF RON FRAZE ADMINISTRATIVE SERVICES 2101 .H" Street Bakersfield. CA 93301 VOICE (805) 326-3941 FAX (805) 395-1349 SUPPRESSION SERVICES 2101 "H. Street Bakersfield. CA 93301 VOICE (805) 32~941 FAX (805) 395-1349 PREVENT10N SERVICES 1715 Chester Ave. Bakersfield. CA 93301 VOICE (805) 326-3951 FAX (805) 326-0576 ENVIRONMENTAL SERVICES 1715 Chester Ave. Bakersfield. CA 93301 VOICE (805) 326-3979 FAX (805) 326-0576 TRAINING DMSION 5642 Victor Ave, Bakersfield, CA 93308 VOICE (805) 399-4697 FAX (805) 399-5763 .- . April 4, 2000 Equilon Enterprises LLC Ms. F eryal Sarrafian 255 N. Ontario St #208A Burbank CA 91504 Dear Ms. Sarrafian: You have been identified as the compliance coordinator for the facility/facilities referenced in the attachment. The pennits to operate this facility/facilities will expire on June 30, 2000. However, in order for this office to renew your pennit, updated fonns A, B, & C must \>e filled out and returned prior to the issuanceof a new' pennit. Please make sure that you are sending the updated fonns which are indicated by the date 7/99 in the lower left hand comer. Please complete and return to this office by May 15,2000. Failure to comply, will result in a delay of issuance of your new pennit to operate. Should you have any questions, please feel tree to call me at 661-326-3979. Sincerely, ~rIÆv Steve Underwood, Inspector Office of Environmental Services SU/dam attachment ~~7~de ~~ ~ ~~.r~.A ~~p" ~ .# Í"" e ..:\ . , . Facility California Ave Shell Cleo Reyes Shell White Lane Shell Fonnerly Macias Shell Ming Ave Shell Shell Service Station Stockdale Texaco Texaco Gas ' Texaco Texaco Texaco Star Mart Texaco Star Mart - Address 3623 California Ave, Bakersfield, Ca 93301 3605 Rosedale Hwy, Bakersfield, Ca 93308 2600 White Lane, Bakersfield, Ca 93309 çlØ-I-&-T:fuiotr~ Bakersfield, Ca 93305 3700 Ming Ave, Bakersfield, Ca 93309 3130 24th Street, Bakersfield, Ca 93301 5321 Stockdale Hwy, Bakersfield Ca 93309 2401 Oak Street, Bakersfield, Ca 93301 3698 Ming Avenue, Bakersfield, Ca 93309 4050 Gosford Lane, Bakersfield, Ca 93309 3621 CalifomiaAve, Bakersfield, Ca 93301 2601 White Lane, Bakersfield, Ca 93304 - - STATEOFCAUFORNlA STATE WATER RESOURCES CONTROL BOARD UNDERGROUND STORAGE TANK PERMIT APPLICATION· FORM A COMPLETE THIS FORM FOR EACH FACILITY/SITE MARK ONLY ONE ITEM o 1 NEW PERMIT o 2 INTERIM PERMIT o 3 RENEWAL PERMIT o 4 AMENDED PERMIT 5 CHANGE OF INFORMATION 0 7 PERMANENTLY CLOSED SITE o 8 TEMPORARY SITE CLOSURE I. FACILITY/SITE INFORMATION & ADDRESS· (MUST BE COMPLETED) DBA OR FACILITY NAME NAME OF OPERATOR Macias Shell Adrian Hacias ADDRESS NEAREST CROSS STREET PARCEL. (OPTIONA~ STATE . ZIP CODE CA SITE PHONE. WITH AREA CODE TO INDICATE fVi}'CORPORATlON 0 INDIVIDUAL 0 PARTNERSHIP 0 LOCAL·AGENCY 0 COUNTY-AGENCY' 0 STATE·AGENCY· 0 FEDERAL-AGENCY' '-o\-Aj¡" DISTRICTS' . ~ owner 01 UST Is a public agency, colT1>letethe following: name of Supervisor of division, section, or office which operates the UST TYPE OF BUSINESS rTYY 1 GAS STATION D 2 DISTRIBUTOR 0 ./ IF INDIAN . OF TANKS AT SITE E. P. A. '- D.' (opliOflal) L.!!.ill' RESERVATION D 3 FARM 0 4 PROCESSOR 0 5 OTHER OR TRUST LANDS 3 EMERGENCY CO NT ACT PERSON (PRIMARY) EMERGENCY CO NT ACT PERSON (SECONDARY)· optional DAYS: NAME (LAST, FIRS~ PHONE. WITH AREA CODE DAYS: NAME (LAST, FIRST) PHONE. WITH AREA CODE Adrian acias 805 322-0792 Hike Hurray 805 322-0792 NIGHTS: NAME (LAST, FIRST) PHONE. WITH AREA CODE NIGHTS: NAME (lAST, FIRST) PHONE. WITH AREA CODE Adrian Hacias 805-323-1824 Hike Hurrav 805-861-1862 II. PROPERTY OWNER INFORMATION· MUST BE COMPLETED NAME SHELL OIL COMPANY Ct~,O~A~D~En~'ti~~'Wr MAILING OR STREET ADDRESS P.O, BOX 4023 CITY NAME CONCORD III. TANK OWNER INFORMATION· (MUST BE COMPLETED) NAME OF OWNER SHELL OIL COftPANY MAILING OR STREET ADDRESS ./ box Ð Indicate 0 INDIVIDUAL iXXJ CORPORATION 0 PARTNERSHIP STATE ZIP CODE C o LOCAL,AGENCY 0 STATE·AGENCY o COUNTY,AGENCY 0 FEDERAL·AGENCY PHONE. WITH AREA CODE 0- 75-6100 P.O. BOX 4023 CITY NAME CARE OF ADDRESS INFORMATION H,S, & E REPRESENTATIVE ./ box Ð indicate 0 INDIVIDUAL W CORPORATION 0 PARTNERSHIP STATE ZIP CODE o LOCAL·AGENCY 0 STATE·AGENCY o COUNTY-AGENCY 0 FEDERAL·AGENCY PHONE. WITH AREA CODE IV. BOARD OF EQUALIZATION UST STORAGE FEE ACCOUNT NUMBER· Call (916) 322·9669 if questions arise. TY(TK) HQ @]j-~ V. PETROLEUM UST FINANCIAL RESPONSIBILITY· (MUST BE COMPLETED) -IDENTIFY THE METHOD(S) USED ./ box Ð Indicate SELF,INSURED o 5 LETTER OF CREDIT D 2 GUARANTEE o 6 EXEMPTION D 3 INSURANCE o 99 OTHER o 4 SURETY BOND VI. LEGAL NOTIFICATION AND BILLING ADDRESS Legal notification and billing will be sent to the tank owner unless box I or II is checked, '-0 11·0 111·0 OWNER'S T~E \) \ÞJ'\} ~ DATE MONTHlDAYIYEAR COUNTY # CD JURISDICTION # ITD FACilITY # ITIIIIJ LOCATION CODE - OPTIONAL I CENSUS TRACU - OPTIONAL I SUPVISOR· DISTRICT CODE . OPTIONAL THIS FORM MUST BE ACCOMPANIED BY ATLEAST (1) OR MORE PERMIT APPUCATJON· FORM 8, UNLESSTHIS IS A CHANGE OF SITE INFORMATION ONl. Y. OWNER MUST FILE THIS FORM WITH THE LOCAL AGENCY IMPLEIENTING THE UNDERGROUND STORAGE TANK REGULAT10NS FORM A (3193) FaIOO33A-R7 TIN§ll)i:~G~C::ON§ }aR COMIPILE1LJING 1891fì¿M cc ACC GENERAL INSTRUCTIONS: SECT1U." '7,1 UF TiTL,¡: OJ, C' .!\:'TER 16, CAT.ì:~"SI/::-()DE OF REGULA110}:S AND SECTIOl'\S 25286, 25287, Al'\D 25289 OF CHAPTER 6,7, Df"iS10Y 20, C;\] ,ll()R>: L\ IIC,\LTH /'.':1:::",' i 1,1''/ ,~, ,OE REQUilŒ OWIŒRS TO APPLY FOR AN UST OPERA11NG PE~'\i1IT. 1. {)nç :<Ji{~\i_ "n" shdl ~.:-: C0Pl:;i2!.C,} :'0. 2, Sl:B:,ilT O:<1-V OS:: (i) [();<.'; 3. This forrl1 shol.'id b~ Ct;mp1c.IC'G hy ~:tJle¡- ~~I~' 4. Pk.ar.2 '\", 1.'~;(~-.-\ 5. u~;:; - ¡';'~1'~ ~~ r::::: 6. 'T\J.l1!c C"'ll ,7" !(Jl.~t :,~IG,n~' :.;. f¿cJi!' Chl 1':G£5 o. 1:11Y Fi,DUTY/SITE INFORMATION CHANGES. :-~;;3rdkss of tfJc numb2"!' Of t2"J1~CS located. üt the site. i,:'I'UCJ\Kf oïîhe LCCl,L AGEI-:CY UNDERGROUND TANK INSPECTOR. , -", bu~lÔí~l;:<~: rr.,-~ l¿,Tìur,',', ':, i:::~c¡.ic·\ , _" 1121' 8.:; :J2Xî. ú; ¡l¡iJ 2'}'1Iiic::~io:.-"( ßf'!OV/Î.ng thclocf.1ion of the USTs with respzct to ,C'),G:;~ì, 7< T~'n~::: :'::'·'·.1~C'¡- ',""'.1::-: :Ubï,ìÎt Cb::::'lìl'l nUli ,:r ~"(J\'·;I' so:n:, pJi ~_ su~t<.: fii1~nci_1i 1·c.~p0ü:;¡b;lity rcqvircInen.ts to the lo<:al agency L;S part of the êpp1iG'¡i,,,¡ "'Jrc""r'h.uPl ',1ST; ¡,:~:¡i," '/1 , 1), ,:>",:, TOP OF FO!Ü:í: "j"=i\¡~;~ O>:L': O:<E ffUi" 7\1.1],': ::..n (X) Ü"( Ih:-;. ho··. p·:::.zL Lo 1~1::;' it.:n' th';, l~'_;'~ ,:k:SCJ1Îl-C:J·J ',,::;:>,;;on Lh~ {'ora) is bd.nj. cOTnplcted, 1. FACHJT'I/SJTE [-.FO¡'j'iÍ!\T'OX [>, }d)lXI;:5~ (.\.ili:,T 11E CŒ:iPLETED) L Record ¡,,,mc and "dðrl,":; (phy,iç¡:ll')~21 í('~) é,é Ihe ¡¡',nk(¡;). 1\OI:B: /' ddrc<;;" ~\'lCS'r ¡H~-:(~ [' v::iliti P;lyslca) k'::-::;Iion Ci1Y, state! and zip cod~. P.O. ßO;~ l'_ CÅ','l E LkS J\~~ E ",«if ¡\ t ~CEr"'¡\,I?t"E. TT'!\,:hh..1e l1C.:¡"':'S~ cro<;s .--;lrcd 8J)(J !l(',Tnl: (~f t·le op·::r:: lr}L 2. Phuru:~ nl!.mhc!" 111U:;t ;'él:"; /I.r: H~:' (~,,3 .í.~"l t.j...: f1 î:'f1! nun<:: t i:. t;¡è ::;ZTJ1~ v,'ïttc.: !'SA"I\1Et' in proper h.:,.~~tto'1. 3, Crce', Ih, "p]J,ùr";f.i~ h". !u, T',,'~ ~,F I~;;,''' :::~~; C.,'-."j'<ER51HP (~x. CORPORATlOI':, L~DIVIDUAL, etc.). 4. Che(;i-:' ttìl~ 'Jf'p¡()priak b'"I~, [U(".I""·I' ;)L 01.'" !~ I~.\'r'·~" 5. If ¡':;:"clHl~-/Í~)i~c IS lo('.'·;'\cd \,;i']~:n ~L!: In,JI.II~ i~·S,·,-,!:'l!(~;J..x uther lnJi:ul tnlgt lands, dlCC~( the bo)~ mar!çe(,.~ '·YES". 6, Indicz.!c the :-:Ll.iEU{ of T;\Y;~S ,ell"i" "..' ,L 7. RcconJ the; J:~.P.A.ID # (y¡, \\Titt..: ":\O~\Et" iL1 t:l:: :;rJl"~ p1'0vidcd. II. PROPERTY OW:<ER L"'FOR.ViAno:" & ¡\DDRES:I (:"'iUST dE COMPLETED) Complete aJl ilcms in this sccliun. tmlc,,' aU iLcms arc the same as SECTiON 1; If t,he same, write "SAME AS SITE" across this section, Be sure to cheek PROPERTY OWNERSI ill' T~(!'E t.û~. lIt TA:\K O\v:-:m ]);FOI\\1AT10:-< 8,. ,\ I) DiUS: (:"llSr BE Cm.lPLETED) ;J!l iterm in lhis sClti,)r" uilkss ~!I i".ms arc the S:¡[,jC as SECI10;-..I 1; if the same, write "5A;I,1E AS SITE" across this section, Be sme to TA:\K ()\'«U~~: TYPE hJ~.. lV, BOARD OJ: EQl'ALJ/,', :m:" LS! ~;I( II, ,\ CF ¡'::E ¡\('~COLXT :<iJ\iBER Ç"iL:ST BE CO:V1PLETED, SEE ARTICLE 5, CHAPTER (;,75, 1)1\,151(;:\ 2U, C\UHJR'\;,\ flEAI 'j Ii ,. \D '.,;¡:ijTY CUU1õ.) Enter Y"tJr ij,)Jrd 01 (B(J[; lIS' ",)[J,~e fee accuunt !lumber which is required !Kfore your pennit ,¡pplícalÍp!l e:m he proccssed. Rcgj,.;¡ ral lun \\ i lh lhl; \', in CJ:-..Uf't Ü1dl ) l'\1 \.\ ì!J reci.? ivC' (1 \.lU~H"tcrly sturagc fee return in n:porÜng the 50.0U6 (bmilL) per gJlh>n fee flue un the. numh..:r of g;Ül¡)fls p1.1C;,.;d in t'S] s" 'Ill"': BOl~ \\ ill code persons cxcn1pt fforn the stor.1gt; feG 50 return~ \vij¡ f}('L bt~ sent. HUt) not h:l\:c an ¡¡<XOdnt nun,D,r VI the no;.: ur Ii )('lJ have ;>11)' qucstitJ!!S rq;¡¡rding the or çal1lhc BUE JI of \'<TJle to tlle HOE Jt Üh~ fl)i!uWLI1f .1 1J[I:" d,¡Jf.l E:'¡;'l..!i¿¡¡iu:l, Fuel 'Ta;.;.cs Division, 1'.0, Box CA Q..12'/q·.(juo:. V. PI:TROLEL::-1 LST 1'1:\A\(,[AI. }(¡:Sl'í),'j\-llHUTY C,;¡SI BE Cm¡lPLETED FOR PETROLU;:"¡ CST, O.\L'{, SEE SEC'] ]O:\S 271 ¡ (a)(8) 01- TJTEE 23. CHAPTER j (I, C\U ['OR\lA CODE OF jŒGLL·\ TIOXS.) Identify thc rl1l:thDJV,) u,e:cl by tJ,e owner anäor ,)peralof. in meeting the: FeJe:raI and Stale fimnciaj responsibility teqlJircnwnts. 1.:51's owned by any Fedeli]1 or Sl4te agenlY 8' weB as ntJI1T,:tr(JklJm CSTs are exempt from this requirement. VI. LEGAL J\OT!FJCATIO'\ A:'\D B1LUJ\G ADD!ŒSS Check 0;\[ BOX Ù'r ¡he addrcs< ¡h.,t will be used for BOll! LEGAL A:\D BlLLI\'G ;\OT1F1CAT10:\S. T ¡\l\K OW:<ER OR Í\ UTI \UR\/':\) ¡U:1'IŒSE:--iTlI.l1VE fv¡LST SIG:-J A;-..ID DATE THE FOR\l AS l:\DJC\TED. ¡SEE SECJJ!);"'·) 271 I (a) (I 3) OF TnLE 23 C1 \'\Pll,R 16. C¡\ l.1]'()I(":l/\ CODE OF REGULAT!Ü\'S.] INS'HWCTIO:\ !·OR·j lIE LOCi' I. .\C !.::':CiL:; The county an jurisdlc¡i,m I'UII'I:,.[\ c,,; l,,,:,kterrnincd and c¡¡n be obtained by calling the State Board (9]6) 227,4303. The fauiily numher may be assigned hy the luc" 1 ag"'"lY; ¡w,\ ever, thi:; j)lIJnb~r rnLlst be numeric,,1 and cannot contain any alphabetica] characters, If thc local agency prefers the St(.!k BC1ard t(\ ;.:.sSÍ":.;n tJll~ f..lt!li!/ .1LJflJblcf, plc;.i.~:c l·-~;.:ve ìt bhmk. IT IS TlIl: ELSl'i,)j\~)II\Ii.il'i ()¡; JIIE LOC~,L i\CfCj\C: THAT INSPECTS THE FACiUTY TO VEg¡¡·y THE ACCC:RACY OF 'HIE L'FOR:-1ATl(J'\, TI II S ^ 1'1' ¡ JCi'T1CF (~,\;:;.:crr HE PROCESSED IF TUE BOE ACCOIJI\T I\UMBER IS ;-..IOT FILLED L"i. THE LOCAL AGE:\CY IS IŒSI'O:\S!BU: I·OK T!!I~ C:O:>iPLETJO;\J OF THE "LOCAL AGEI\CY USE O;-..ILY" II\FOR.IVíATION BOX AND FOR FOR W AIWL\'C; 0\ E H)f(\i "X' ;\>:D i\SSOCIA TED FORM "B"(s) TO THE FOLLOWL'\'G ADDRESS. T1IE LOCAL AGEJ\CY SHOULD RETAI:'\ T11I, ORlc;j:\AI_S ASD FURWA!W THE YELLOW COPIES TO THE FOLLOWL'\G ADDRESS. THE PINK COPY SHOULD BE RETAL'\'I]) BY THE TA:'\K OWl\ER. ST i\lE OF CALlFORXiA Sli, 1 E \.'! /','ŒR RESOt:RCES CONTROL BOARD C/O :J"'N..r2,I::.p.~~. DA1/', l'ROCESSC<G CÙHER P.O. Bœ~ 527 PARA.\10UNT, CA 90723 3;93 F0R0120R1 e e STATE OFCAUFORNlA STATE WATER RESOURCES CONTROL BOARD UNDERGROUND STORAGE TANK PERMIT APPLICATION· FORM B COMPLETE A SEPARATE FORM FOR EACH TANK SYSTEM. MARK ONLY ONE ITEM o ' NEW PERMIT o 2 INTERIM PERMIT o 3 RENEWAl PERMIT o 4 AMENDED PERMIT ~ 5 CHANGE OF INFORMATION o 8 TEMPORARY TANK CLOSURE o 7 PERMANENTLY CLOSED ON SITE D 8 TANK REMOVED DBA OR FACILITY NAME WHERE TANK IS INST ALlED: MAGI AÇ S H--G I L.. I. TANK DESCRIPTION COMPLETE ALL ITEMS - SPECIFY IF UNKNOWN A. OWNER'S TANK I.D.' O1J.102-- Z. - r<r:; C. DATE INSTALLED (MOIOAYIYEAR) 'f ß B. MANUFACTURED BY:O¡,J¡; '5 Ca2.11 JAl6 D. TANK CAPACllY IN GAlLONS: I '2. 00 0 II. TANK CONTENTS IFA-' IS MARKED. COMPLETE ITEM C. ~ ' MOTOR VEHICLE FUEL o 4 OIL B. C. ß ,. REGULAR B 3 DIESEL D 6 AVIATION GAS A. UNLEADED o 2 PETROLEUM 080 ß, PRODUCT D 'b PREMIUM 4 GASAHOL o 7 METHANOL EMPlY o 5 JET FUEL UNLEADED o 3 CHEMICAL PRODUCT o 95 UNKNOWN o 2 WASTE D 2 LEADED o 99 OTHER (DESCRIBE IN ITEM D. BELOW) D. IF (A.1) IS NOT MARKED. ENTER NAME OF SUBSTANCE STORED C.A.S..: III. TANK CONSTRUCTION MARK ONE ITEM ONLY IN BOXES A, B, AND C, AND ALL THAT APPLIES IN BOX D AND E A, TYPE OF ~ ' DOUBLE WALL 0 3 SINGLE WALL WITH EXTERIOR LINER 0 95 UNKNOWN SYSTEM 0 2 SINGLE WALL 0 4 SECONDARY CONTAINMENT (VAULTED TANK) 0 99 OTHER 0' BARE STEEL 0 2 STAINLESS STEEL g 3 FIBERGlASS 0 4 STEEL CLAD WI FIBERGLASS REINFORCED PlASTIC 8, TANK MATERIAL 0 5 CONCRETE 0 6 POLYVINYL CHLORIDE 0 7 AlUMINUM 0 8 100% METHANOL COMPATIBLE WIFRP (Primary Tank) 09 BRONZE 0 10 GALVANIZED STEEL 0 95 UNKNOWN 0 99 OTHER 0' RUBBER LINED 0 2 AlKYD LINING 0 3 EPOXY LINING 0 4 PHENOLIC LINING C. INTERIOI:¡ 0 5 GLASS LINING Q6 UNLINED 0 95 UNKNOWN D 99 OTHER LINING IS LINING MATERIAL COMPATIBLE WITH '00% METHANOL? YES_ NO_ D. CORROSION 0' POLYETHYLENE WRAP D 2 COATING o 3 VINYL WRAP ~ 4 FIBERGLASS REINFORCED PLASTIC PROTECTION 05 CATHODIC PROTECTION 0 91 NONE o 95 UNKNOWN D 99 OTHER E. SPill AND OVERFILL SPILL CONTAINMENT INSTALLED (YEAR) /9f3~ OVERFILL PREVENTION EQUIPMENT INSTAlLED (YEAR) - IV. PIPING INFORMATION CIRCLE A IF ABOVE GROUND OR U IF UNDERGROUND, BOTH IF APPLICABLE A. SYSTEM TYPE A U 1 SUCTION A@ 2 PRESSURE A U 3 GRAVllY A U 99 OTHER B. CONSTRUCTION Ad>, SINGLE WALL A U 2 OOUBLE WALL A U 3 LINED TRENCH A U 95 UNKNOWN A U 99 OTHER C. MATERIAL AND A U , BARE STEEL A U 2 STAINLESS STEEL A U 3 POLYVINYL CHLORIDE (pvC)AdD4 FIBERGlASS PIPE CORROSION A U 5 AlUMINUM A U 6 CONCRETE A U 7 STEEL WI COATING A U 8 '00% METHANOL COMPATIBLE WiFRP PROTECTION A U 9 GALVANIZED STEEL A U '0 CATHODIC PROTECTION A U 95 UNKNOWN A U 99 OTHER D, LEAK DETECTION '5š 1 AUTOMATIC LINE LEAK DETECTOR o 2 LINE TIGHTNESS TESTING o 3 MONITORING 099 OTHER V. TANK LEAK DETECTION o ' VISUAL CHECK g 2 o 6 TANK TESTING ~ 7 INVENTORY RECONCILIATION 0 3 VAOOZE MONITORING D 4 AUTOMATIC TANK GAUGING D 5 GROUND WATER MONITORING INTERSTITIAL MONITORING 0 91 NONE 0 95 UNKNOWN D 99 OTHER VI. TANK CLOSURE INFORMATION ,. ESTIMATED DATE LAST USED (MO/DAYIYR) 3. WAS TANK FILLED WITH GALLONS INERT MATERIAL? YES 0 NO 0 R PENAL TY OF PER URY, A~D TO THE BESTpF MY KNOWLEDGE, IS TRUE AND CORRECT ~ DAT~ ~ ~ --1...- î -<1 \ PERMIT NUMBER I PERMIT APPROVED BYiDATE T PERMIT EXPIRATION DATE THIS FORM MUST BE ACCOMPANIED BY A PERMIT APPLICATION· FORM A, UNLESS A CURRENT FORM A HAS BEEN FILED. FILE THIS FORM WITH THE LOCAL AGENCY IMPLEMENTING THE UNDERGROUND STORAGE TANK REGULATIONS COUNTY # OJ JURISDICTION # LID FACILITY # ITIIIIJ TANK # CIIIITJ STATE 1.0.# FORM B (12-91) FOROO348-!16 I -;- e e INSTRUCTIONS FOR COMPLETING FORM "B" GENERAL INSTRUCTIONS: 1. One FORM "B" shall be completed for each tank for all NEW PERMITS. PÈRMIT CHANGES. REMOVALS and lor any other TANK INFORMATION CHANGE. 2. This form should be completed by either the PERMIT APPLICANT or the LOCAL AGENCY UNDERGROUND TANK INSPECTOR. 3. Please type or print clearly all requested information. 4. Use a hard point writing instrument. you are making 3 copies. TOP OF FORM: 'MARK ONLY ONE ITEM" 1. Mark an (X) in the box next to the item that best descri bes the reason the form is bei ng completed 2. Indicate the DBA or Facility name where the tank is installed. I. TANK DESCRIPTION· COMPLETE ALL ITEMS· IF UNKNOWN· SO SPECIFY A. Indi cate owners tank 10 # - I f there is a tank number that is used by the owner to i dent Hy the tank (ex AB70189). B. Indicate the name of the company that manufactured the tank (ex. ACME TANK MFG). C. Indicate the year the tank was installed (ex. 1987). D. Indicate the tank capacity in gallons (ex. 25.000 or 10.000 etc.) II. TANK CONTENTS A. ß. C. D. III. 1. 2. 1. IF MOTOR VEHICLE FUEL. check box 1 and comDlete items B & C. 2. If not MOTOR VEHICLE FUEL. check the appropriate box in section A and complete items B & D. Check the appropriate box. Check the type of MOTOR VEHICLE FUEL (if box 1 is checked in A). Print the chemical name of the hazardous substance stored in the tank and the C.A.S.'. (Chemical Abstract Service number), if box 1 is NOT checked in A. TANK CONSTRUCTION . MARK ONE ITEM ONLY IN BOX A, B, C & D Check only one item in TYPE OF SYSTEM. TANK MATERIAL. INTERIOR LINING and CORROSION PROTECTION. If OTHER. print 1n the space provided. IV. PIPING INFORMATION 1. Circle A if above ground circle U if underground. and circle both if applicable. 2. If UNKNOWN circle: or if OTHER. print in space provided 3. Indicate the LEAK DETECTION system(s) used to comply with the monitoring requirement for the piping.· V. TANK LEAK DETECTION 1. I ncji cate the LEAK DETECTION system( s) used to camp 1 y with the monitor'i ng requi rement s for the tank. VI. INFORMATION ON TANK PERMANENTLY CLOSED IN PLACE 1. ESTIMATED DATE LAST USED - MONTHlY EAR (January. 1988 or 01/88) 2. ESTIMATED QUANTITY of HAZARDOUS SUBSTANCE remaining in the tank (in Gallons). 3 WAS TANK FILLED WITH INERT MATERIAL? Check 'Yes' or 'NO' APPLICANT MUST SIGN AND DATE THE FORM AS INDICATED. INSTRUCTION FOR THE LOCAL AGENCIES The state underground storage tank identification number is composed of the two digit county number. the three digit jurisdiction number. the six digit facility number and the six digit tank number. The county and JL;;'isdictiuiì nWilbers òr'e ¡:,redeterm1f1ed and can be obtained by calling the State Board (916) 227-4303. The facil ity number must be the same as shown inform "A". The tank number may be ass i gned by the 1 oca 1 agency. however. this number must be numerical and cannot contain an alphabet. If the local agency prefers the State Board to assign the tank number. please leave it blank. IT IS TJ,.¡ :' Dt:<:,om'<:'TI3ILTTV f)r T!'':: :..CC",~. AGEhlCY -:-H;',-;- :;::~S?EC7S THE FACILïrY TO VERIFY THE ACCURACY OF THE ", JR~h, lVI'1. Ir,,: ~OCAL ¡.\GtiJCY IS RESPONSIBLE FOR THE COMPLETION OF THE "LOCAL AGENCY USE ONLY" INFORMATION BOX AND FOR FORWARDING ONE FORM "A" AND ASSOCIATED FORM "B"(s) TO THE FOLLOWING ADDRESS. e e MARK ONLY ONE ITEM o 3 RENEWAL PERMIT o 4 AMENDED PERMIT STATE OFCAUFORNlA STATE WATER RESOURCES CONTROL BOARD UNDERGROUND STORAGE TANK PERMIT APPLICATION· FORM B COMPLETE A SEPARATE FORM FOR EACH TANK SYSTEM. o 1 NEW PERMIT o 2 INTERIM PERMIT 5 CHANGE OF INFORMATION 0 7 PERMANENTLY CLOSED ON SITE 8 TEMPORARY TANK CLOSURE 0 8 TANK REMOVED DBA OR FACILITY NAME WHERE TANK IS INSTALLED: SL/- I. TANK DESCRIPTION COMPLETE ALL ITEMS - SPECIFY IF UNKNOWN A. OWNER'S TANK I.D.' O'/IPZ...1..I. C. DATE INSTALLED (MOiDAYIYEAR) I q D. TANK CAPACITY IN GALLONS: II. TANK CONTENTS IF A-1IS MARKED. COMPLETE ITEM C. ~1 MOTOR VEHICLE FUEL 0 4 OIL B. C. o 1a REGULAR E! 3 DIESEL o 8 AVIATION GAS A. UNLEADED 02 PETROLEUM 0 80 EMPTY ~1 PRODUCT ~ 1b PREMIUM 4 GASAHOL o 7 METHANOL UNLEADED o 5 JET FUEL 03 CHEMICAL PRODUCT 0 95 UNKNOWN 02 WASTE o 2 LEADED o 99 OTHER (DESCRIBE IN ITEM D. BELOW) D. IF (A.1) IS NOT MARKED, ENTER NAME OF SUBSTANCE STORED C.A.S.': III. TANK CONSTRUCTION MARK ONE ITEM ONLY IN BOXES A. B. AND C, AND ALL THAT APPLIES IN BOX D AND E A. TYPE OF ~1 DOUBLE WALL 0 3 SINGLE WALL WITH EXTERIOR LINER 0 95 UNKNOWN SYSTEM 0 2 SINGLE WALL 0 4 SECONDARY CONTAINMENT (VAULTED TANK) 0 99 OTHER 01 BARE STEEL 0 2 STAINLESS STEEL ~ 3 FIBERGLASS 0 4 STEEL CLAD WI FIBERGLASS REINFORCED PLASTIC B. TANK MATERIAL 0 5 CONCRETE D 6 POLYVINYL CHLORIDE o 7 ALUMINUM 0 8 100'f. METHANOL COMPATIBLE WiFRP (Primary Tank) D 9 BRONZE 0 10 GALVANIZED STEEL 0 95 UNKNOWN 0 99 OTHER 01 RUBBE R LINED 0 2 ALKYD LINING 0 3 EPOXY LINING 0 4 PHENOLIC LINING C. INTERIOI~ 0 5 GLASS LINING ~ 6 UNLINED 0 95 UNKNOWN 0 99 OTHER LINING IS LINING MATERIAL COMPATIBLE WITH '00'f. METHANOL? YES_ NO_ D. CORROSION D 1 POLYETHYLENE WRAP D 2 COATING D 3 VINYL WRAP ~ 4 FIBERGLASS REINFORCED PlASTIC PROTECTION D 5 CATHODIC PROTECTION 0 91 NONE o 95 UNKNOWN o 99 OTHER E. SPILL AND OVERFILL SPILL CONTAINMENT INSTALLED (YEAR) /986 OVERFILL PREVENTION EOUIPMENT INSTALLED (YEAR) - IV. PIPING INFORMATION CIRCLE A IF ABOVE GROUND OR U IF UNDERGROUND. BOTH IF APPLICABLE A. SYSTEM TYPE A U 1 SUCTION A -d)2 PRESSURE A U 3 GRAVITY A U 99 OTHER B. CONSTRUCTION AV, SINGLE WALL A U 2 DOUBLE WALL A U 3 LINED TRENCH A U 95 UNKNOWN A U 99 OTHER C. MATERIAL AND A U , BARE STEEL A U 2 STAINLESS STEEL A U 3 POLYVINYL CHLORIDE (PVC) A d)4 FIBERGLASS PIPE CORROSION A U 5 AlUMINUM A U 6 CONCRETE A U 7 STEEL WI COATING A U 8 100'f. METHANOL COMPATIBLE WiFRP PROTECTION A U 9 GALVANIZED STEEL A U 10 CATHODIC PROTECTION A U 95 UNKNOWN A U 99 OTHER D. LEAK DETECTION ~ 1 AUTOMATIC LINE LEAK DETECTOR o 2 LINE TIGHTNESS TESTING o 3 MONITORING o 99 OTHER V. TANK LEAK DETECTION D 1 VISUAL CHECK ~ 2 INVENTORY RECONCILIATION D 3 VADOZE MONITORING 0 4 AUTOMATIC TANK GAUGING 0 5 GROUND WATER MONITORING D 6 TANK TESTING ~ 7 INTERSTITIAL MONITORING D 91 NONE 0 95 UNKNOWN 0 99 OTHER VI. TANK CLOSURE INFORMATION 2. ESTIMATED OUANTITY OF SUBSTANCE REMAINING 3. WAS TANK FILLED WITH GALLONS INERT MATERIAL? YES 0 NO 0 PENAL TY OF PERJURY, AND TO THE BEST OF MY KNOWLEDGE, IS TRUE AND CORRECT DATE. . NUMBER IS COMPOSED OF THE FOUR NUMBERS BELOW STATE 1.0.# COUNTY # CD JURISDICTION # ITIJ FACILITY # ITIIIIJ TANK # ITITIIJ PERMIT NUMBER I PERMIT APPROVED BYiDATE I PERMIT EXPIRATION DATE THIS FORM MUST BE ACCOMPANIED BY A PERMIT APPLICATION· FORM A, UNLESS A CURRENT FORM A HAS BEEN FILED. FILE THIS FORM WITH THE LOCAL AGENCY IMPLEMENTING THE UNDERGROUND STORAGE TANK REGULATIONS FORM B (12·91) FOROO:MB-R6 e e INSTRUCTIONS FOR COMPLETING FORM "B" GENERAL INSTRUCTIONS: 1. One FORM "S" sha 11 be completed for each tank for all NEt-J PERMITS. PERMIT CHANGES. REMOVALS and/or any other TANK INFORMATION CHANGE. 2. Th'¡ s for'm should be completed by either the PERMIT APPLICANT or the LOCAL AGENCY UNDERGROUND TANK INSPECTOR. 3. Please type or print clearly all requested information. 4. Use a hard point writing instrument, you are making 3 copies. TOP OF FORM: . MARK ONLY ONE ITEM" 1. Mark an (X) in the box next to the item that best descri bes the reason the form is bei ng completed 2. Indicate the DBA or Facility name where the tank is installed. I. TANK DESCRIPTION· COMPLETE ALL ITEMS - IF UNKNOWN - SO SPECIFY A. Indicate owners tank 10 # - If there is a tank number that is used by the owner to identify the tank (ex. AB70789). B. Indicate the name of the company that manufactured the tank (ex. ACME TANK MFG). C. Indicate the year the tank was installed (ex. 1987). D. Indicate the tank capacity in gallons (ex. 25,000 or 10,000 etc.) II. TANK CONTENTS A. 8. C. D. III. 1. 2. 1. IF MOTOR VEHICLE FUEL, check box 1 and complete items B & C. 2. If not MOTOR VEHICLE FUEL, check the appropriate box in section A and complete items ß & D. Check the appropriate box. Check the type of MOTOR VEHICLE FUEL (if box 1 is checked in A). Print the chemical name of the hazardous substance stored in the tank and the C.A.S.'. (Chemical Abstract Service number), if box 1 is NOT checked in A. TANK CONSTRUCTION - MARK ONE ITEM ONLY IN BOX A. B. C & D Check only one item in TYPE OF SYSTEM, TANK MATERIÞ.L, INTERIOR LINING and CORROSION PROTECTION. If OTHER, print in the space provided. IV. PIPING INFORMATION 1. Circle A if above ground circle U if underground, and circle both if applicable. 2. If UNKNOWN circle: or if OTHER, print in space provided 3. Indicate the LEAK DETECTION system(s) used to comply with the monitoring requirement for the piping. V. TANK LEAK DETECTION 1. Indicate the LEAK DETECTION system(s) used to comply with the monitoring requirements for the tank. VI. INFORMATION ON TANK PERMANENTLY CLOSED IN PLACE 1. ESTH1ATFD DATE LAST USED, MONTH/YEAR (January. 1988 or 01/88) 2. ESTIMATED QUANTITY of HAZARDOUS SUBSTANCE remaining in the tank (in Gallons). 3. WAS TANK FILLED WITH INERT MATERIAL? Check 'Yes' or 'NO' APPLICANT MUST SIGN AND DATE THE FORM AS INDICATED. INSTRUCTION FOR THE LOCAL AGENCIES The state underground storage tank identification number is composed of the two digit county number, the three digit jurisdiction number, the six digit faCllity number and the six digit tank number. The county and JUf'isdictí0ï¡ r:ur,ibers die predeterrnHled and can be obtained by calling the State Board (916) 227-4303. The facility number must be the same as shown in form "A". The tank number may be assigned by the local agency. however, this number must be numerical and cannot contain an alphabet. If the local agency prefers the State Board to assign the tank number, please leave it blank. IT IS TI-!¡:" [) :"CDnMCTSIU"Ty 0F ~[ !_OCA,L AGENCY THS-:- INS:'ECTS THE FACIUTY TO VERIFY THE ACCURACY OF THE ~,,¡ùR~Ih, .Ul'L ìhi: LOCAL Þ.GEi~CY IS RESPONSIBLE FOR THE COMPLETION OF THE "LOCAL AGENCY USE ONLY" INFORMATION BOX AND FOR FORWARDING ONE FORM "A" AND ASSOCIATED FORM "B"(s) TO THE FOLLOWING ADDRESS. e e Sf ATE OF CAUFORNlA STATE WATER RESOURCES CONTROL BOARD UNDERGROUND STORAGE TANK PERMIT APPLICATION· FORM B COMPLETE A SEPARATE FORM FOR EACH TANK SYSTEM. MARK ONLY ONE ITEM o 1 NEW PERMIT o 2 INTERIM PERMIT o 7 PERMANENTLY CLOSED ON SITE o 8 TANK REMOVED o 3 RENEWAL PERMIT o 4 AMENDED PERMIT ~ 5 CHANGE OF INFORMATON o 8 TEMPORARY TANK CLOSURE I. TANK DESCRIPTION DBA OR FACILITY NAME WHERE TANK IS INSTALLED: ÞfALJA.-~ S'H£U- COMPLETE ALL ITEMS - SPECIFY IF UNKNOWN A. OWNER'S TANK I. D.' Otj C. DATE INSTALLED (MOiDAYIVEAR) II. TANK CONTENTS PI.- B. MANUFACiURED BY:e>NI:A.)S Co/Z.NIM D. TANK CAPACITY IN GALLONS: I Z. 000 IF A,11S MARKED. COMPLETE ITEM C. J2!] 1 MOTOR VEHICLE FUEL o 4 OIL B. C. S 1. REGULAR B 3 DIESEL o 8 AVIATION GAS A. UNLEADED o 2 PETROLEUM 080 EMPTY r23' 1 PRODUCT o 1bPREMIUM 4 GASAHOL o 7 METHANOL UNLEADED D 5 JET FUEL o 3 CHEMICAL PRODUCT o 95 UNKNOWN 02 WASTE o 2 LEADED o 99 OTHER (DESCRIBE IN ITEM D. BELOW) D. IF (A.1) IS NOT MARKED. ENTER NAME OF SUBSTANCE STORED C,A.S,.: III. TANK CONSTRUCTION MARK ONE ITEM ONLY IN BOXES A, B. AND C, AND ALL THAT APPLIES IN BOX D AND E A, TYPE OF SYSTEM ~ 1 DOUBLE WALL tJ 2 SINGLE WALL B. TANK MATERIAL (Primary Tank) D 1 BARE STEEL o 5 CONCRETE D 9 BRONZE o 1 RUBBER LINED o 5 GLASS LINING C. INTERIOF~ LINING D 3 SINGLE WAll WITH EXTERIOR LINER o 4 SECONDARY CONTAINMENT (VAULTED TANK) o 2 STAINLESS STEEL o 6 POLYVINYL CHLORIDE o 10 GALVANIZED STEEL o 2 ALKYD LINING ~ 6 UNLINED I)? 3 FIBERGLASS o 7 ALUMINUM o 95 UNKNOWN o 3 EPOXY LINING o 95 UNKNOWN IS LINING MATERIAL COMPATIBLE WITH 100% METHANOL? YES_ NO_ D. CORROSION PROTECTION o 1 POLYETHYLENE WRAP 0 2 COATING o 5 CATHODIC PROTECTION 0 91 NONE o 3 VINYL WRAP o 95 UNKNOWN 1'1& o 95 UNKNOWN D 99 OTHER D 4 STEEL CLAD WI FIBERGLASS REINFORCED PlASTIC D 8 100% METHANOL COMPATIBLE WIFRP o 99 OTHER o 4 PHENOLIC LINING D 99 OTHER ~ 4 FIBERGLASS REINFORCED PLASTIC o 99 OTHER IV, PIPING INFORMATION SPILL CONTAINMENT INSTALLED (YEAR) OVERFILL PREVENTION EQUIPMENT INSTALLED (YEAR) - E, SPILL AND OVERFILL CIRCLE A IF ABOVE GROUND OR U IF UNDERGROUND. BOTH IF APPLICABLE A. SYSTEM TYPE A U 1 SUCTION A t:)z PRESSURE A U 3 GRAVITY A U 99 OTHER B. CONSTRUCTION A df), SINGLE WALL A U 2 DOUBLE WALL A U 3 LINED TRENCH A U 95 UNKNOWN A U 99 OTHER C. MATERIAL AND A U 1 BARE STEEL A U 2 STAINLESS STEEL A U :3 POLYVINYL CHLORIDE (PVC)A¡jfJ4 FIBERGlASS PIPE CORROSION A U 5 ALUMINUM A U 6 CONCRETE A U 7 STEEL WI COATING A U 8 100% METHANOL COMPATIBLE W/FRP PROTECTION A U 9 GALVANIZED STEEL A U 10 CATHODIC PROTECTION A U 95 UNKNOWN A U 99 OTHER D, LEAK DETECTION ~ 1 AUTOMATIC LINE LEAK DETECTOR o 2 LINE TIGHTNESS TESTING o 3 MONITORING 099 OTHER V. TANK LEAK DETECTION o 1 VISUAL CHECK ~ 2 INVENTORY RECONCILIATION 0:3 VADOZE MONITORING 0 4 AUTOMATIC TANK GAUGING 0 5 GROUND WATER MONITORING o 6 TANK TESTING ~ 7 INTERSTITIAL MONITORING 0 91 NONE 0 95 UNKNOWN 0 99 OTHER VI. TANK CLOSURE INFORMATION 2. ESTIMATED OUANTITY OF SUBSTANCE REMAINING 3. WAS TANK FillED WITH GALLONS INERT MATERIAL? YES 0 NO 0 ~ ....... LOCAL AGENCY USE ONLY THE STATE I.D. NUMBER IS COMPOSED OFTHE FOUR NUMBERS BELOW STATE 1.0,# TANK # ITIIIIJ COUNTY # CD JURISDICTION # OTI FACilITY # ITIIIIJ I PERMIT APPROVED BYiDATE I PERMIT EXPIRATION DATE THIS FORM MUST BE ACCOMPANIED BY A PERMIT APPLICATION· FORM A, UNLESS A CURRENT FORM A HAS BEEN FILED. FILE THIS FORM WITH THE lOCAL AGENCY IMPLEMENTING THE UNDERGROUND STORAGE TANK REGULATIONS PERMIT NUMBER FORM B (12-91) FOROO:M~R6 e e INSTRUCTIONS FOR COMPLETING FORM "B" GENERAL INSTRUCTIONS: 1. One FORM "B" sha 11 be completed for each tank for all NEW PERMITS. PERMIT CHANGES. REMOVALS and/or any other TANK INFORMATION CHANGE. 2. This form should be completed by either the PERMIT APPLICANT or the LOCAL AGENCY UNDERGROUND TANK INSPECTOR. 3. Please type or print clearly all requested information. 4. Use a hard point writing instrument. you are making 3 copies. TOP OF FORM: ' MARK ONLY ONE ITEM" 1. Mark an (X) in the box next to the item that best describes the reason the form is being completed. 2. Indicate the DBA or Facility name where the tank is installed. T. TANK DESCRIPTION· COMPLETE ALL ITEMS· IF UNKNOWN· SO SPECIFY A. Indi cate o\omers tank ID # - If there is a tank number that is used by the owner to i dent ify the tank (ex. AB70789). B. Indicate the name of the company that manufactured the tank (ex. ACME TANK MFG). C Indicate the year the tank was installed (ex. 1987). D. Indicate the tank capacity in gallons (ex. 25.000 or 10,000 etc.) II. TANK CONTENTS A. 1. IF MOTOR VEHICLE FUEL. check box 1 and complete items B & C. 2. If not MOTOR VEHICLE FUEL, check the appropriate box in section A and complete items B & D. B. Check the appropriate box. C. Check the type of MOTOR VEHICLE FUEL (if box 1 is checked in A). D. Print the chemical name of the hazardous substance stored in the tank and the C.A.S.#. (Chemical Abstract Service number), if box 1 is NOT checked in A. III. TANK CONSTRUCTION· MARK ONE ITEM ONLY IN BOX A. B. C & D 1. Check only one item in TYPE OF SYSTEM. TANK MATERIAL, INTERIOR LINING and CORROSION PROTECTION 2. If OTHER, print ln the space provided. IV. PIPING INFORMATION 1. Circle A if above ground circle U if underground. and circle both if applicable. 2. If UNKNOWN circle; or if OTHER. print in space provided 3. Indlcate the LEAK DETECTION system(s) used to comply wlth the monitoring requirement for the piping. V, TANK LE~< DETECTION 1. Indicate the LEAK DETECTION system(s) used to comply with the monitoring requirements for the tank. VI. INFORMATION ON TANK PERMANENTLY CLOSED IN PLACE 1. ESTIMATED DATE LAST USED - MONTH/YEl,R (January. 1988 or 01/88) 2. ESTIr1,1\TED QUA.NTITY of HAZARDOUS SUBSTANCE remaining in the tank (in Gallons). 3. WAS TANK FILLED WITH INERT MATERIAL? Check 'Yes' or 'NO' APPLICANT MUST SIGN AND DATE THE FORM AS INDICATED. INSTRUCTION FOR THE LOCAL AGENCIES The state underground storage tank identification number is composed of the two digit county number, the three digit jurisdictlon number, the six digit facility number and the six digit tank number. The county and Jüri Sdl cti 0" "U¡ilOèrS åí'e predetermi ned and can be obtai ned by ca 11 i ng the State Board (916) 227 -4303. The facil i ty number must be the same as shown inform "A". The tank number may be assigned by the 1 oca 1 agency. however. this number must be numerical and cannot contain an alphabet. If the local agency prefers the State Board to assign the tank number. please leave it blank. IT IS -rnl=' Dr:cP()MCTI3ILTTV f)r T1Ji.: ~.,OC~,!... AGENCY TH;\-;- ¡~]SPECTS THE FACiLITY TO VERIFY THE ACCURACY OF THE ~.,ùR~IJ-..li.)¡~. ¡r¡i: LOCAL Þ.GEI~CY IS RESPONSIBLE FOR THE COMPLETION OF THE "LOCAL AGENCY USE ONLY" INFORMATION BOX AND FOR FORWARDING ONE FORM "A" AND ASSOCIATED FORM "B"(5) TO THE FOLLOWING ADDRESS. - e / STATE OF CALIFORNIA STATE WATER RESOURCES CONTROL BOARD UNDERGROUND STORAGE TANK PERMIT APPLICATION - FORM A COMPLETE THIS FORM FOR EACH FACILITY/SITE MARK ONLY ONE ITEM o 1 NEW PERMIT o 2 INTERIM PERMIT o 3 RENEWAL PERMIT D 4 AMENDED PERMIT KX 5 CHANGE OF INFORMATION 0 7 PERMANENTLY CLOSED. SITE o 6 TEMPORARY SITE CLOSURE I. FACILITY/SITE INFORMATION & ADDRESS - (MUST BE COMPLETED) DBA OR FACILITY NAME NAME OF OPERATOR tv\,þçC\ AS S\-\ E:::: LL k\)12Æ AN \./lA-C tA-'S ADORESS NEAREST CROSS STREET PARCEL # (OPTIONAL) \Q\ ~. uN\ùN~, CITY NAME STATE I Z'PÓt°3:S bl SITE PHONE # WITH AREA CODE 'ßA-~sÇ-\ f:::l, \) CA UòóS) 322-Dì9 2 II BOX 00 CORPORATION o INDIVIDUAL o PARTNERSHIP o LOCAL,AGENCY o COUNTY,AGENCY' o STATE·AGENCY· o FEDERAL·AGENCY· TO INDICATE DISTRICTS . "owner of UST is a public agency, complete the following: name of supervisor of division, section or office which operates the UST TYPE OF BUSINESS !XX 1 GAS STATION D 2 DISTRIBUTOR D II IF INDIAN 1# OF TANKS AT SITE E. P.A. L D. # (optional) RESERVATION 3 D 3 FARM D 4 PROCESSOR D 5 OTHER OR TRUST LANDS N/A EMERGENCY CONTACT PERSON (PRIMARY) DAYS: NAME (LAST, FIRST) PHONE # WITH AREA CODE MACA ~ AíJ l'òCS) 32..-"2--0' L NIGHTS: NAME (l:AST, FIRST) P\,ONE # WITH AREA CODE \J\ACAPf3 M:>'\&\ ~ L~o'5) 62-5- i ß2L. - II. PROPERTY OWNER INFORMATION - (MUST BE COMPLETED) EMERGENCY CONTACT PERSON (SECONDARY) - optional DAYS: NAME (LAST, FIRST) PHON # WITH AREA CODE V\lJ12e-N'í !vi I \l/£ L öS 3"2-2--61 2- NIGHTS: NAME (LAST, FIRST) PHONE # WITH AREA CODE Hu1Z.eN'1 K\\L..E (13oS) 30¡3-S'ß96 NAME CARE OF ADDRESS INFORMATION EQUILLON ENTERPRISES LLC MAILING OR STREET ADDRESS 01 box to indicate o INDIVIDUAL o LOCAL·AGENCY o STATE,AGENCY P.O. BOX 8080 CXi CORPORATION D PARTNERSHIP o COUNTY,AGENCY o FEDERAL·AGENCY CITY NAME STATE I ZIP CODE I PHONE # WITH AREA CODE l'I"illRTINEZ, CA 94553 III. TANK OWNER INFORMATION - (MUST BE COMPLETED) NAME OF OWNER CARE OF ADDRESS INFORMATION EQUILLON ENTERPRISES LLC MAILING OR STREET ADDRESS II box to indicale o INDIViDUAL o LOCAL-AGENCY o STATE·AGENCY P.O. BOX 8080 [Xi CORPORATION o PARTNERSHIP o COUNTY·AGENCY o FEDERAL·AGENCY CITY NAME STATE I ZIP CODE I PHONE # WITH AREA CODE MARTINEZ, CA 94553 IV. BOARD OF EQUALIZATION UST STORAGE FEE ACCOUNT NUMBER - Call (916) 322-9669 if questions arise. TY(TK) HQ @K]-~ V. PETROLEUM UST FINANCIAL RESPONSIBILITY - (MUST BE COMPLETED) -IDENTIFY THE METHOD(S) USED '" box 10 indicale CXl1 SELF,INSURED 0 2 GUARANTEE 0 3 INSURANCE D 4 SURETY BOND 0 5 LETTER OF CREDIT 0 6 EXEMPTION 0 7 STATE FUND 08 STATE FUND & CHIEF FINANCIAL OFFICER LETTER 09 STATE FUND & CERTIFICATE OF DEPOSIT D 10 LOCAL GOVT. MECHANISM 0 99 OTHER VI. LEGAL NOTIFICATION AND BILLING ADDRESS Legal notification and billing will be sent to the tank owner unless box I or 1\ is checked. CHECK ONE BOX INDICATING WHICH ABOVE ADDRESS SHOULD BE USED FOR LEGAL NOTIFICATIONS AND BILLING: '-0 II. [X] III. IX] f:I LOCAL AGENCY USE ONLY COUNTY # CD FACILITY # ITITITI LOCATION COOE . OPTIONAL CENSUS TRACT # - OPTIONAL SUPVISOR ' DISTRICT CODE ' OPTIONAL THIS FORM MUST BE ACCOMPANIED BY AT LEAST (1) OR MORE PERMIT APPLICATION - FORM B, UNLESS THIS IS A CHANGE OF SITE INFORMATION ONLY, OWNER MUST FILE THIS FORM WITH THE LOCAL AGENCY IMPLEMENTING THE UNDERGROUND STORAGE TANK REGULATIONS FORM A (6'95) ~ ~ --~...., ---. p -..,.~-..,...- <---..:.. ~ ,- - ---~--~ ~- ~- e . p- H GENERAL CHAPTER ;;¡! z~, AGENCY IJNDERGROUND TANK JNS1'ECTOIt ù1pie~ plot plan to lhe loz:al agcHi :,< as pa.n. of the 3pphuQi.on sh(nJ..'¡n:~ and iündmarks [Scondon t j (a)(3L rnu:;t docurncH{.ation ~tah: appiic;i1wn for pC1mkum CST, [St;uion 271 ¡ (aj( ¡ 1). lG(:t~tion of rhe CST.;; \v\th respect to Íoç::d 2.gcncy ;1~ pJ..rt the FORM: "\<1ARK ONt Y OM] ¡TEl',, ,' r....1ark an (X) in the. hox ne:<t 10 _~Ü;w that the bcí çnmpktccL L ere} b(¡x r¡;ark~~d 7. this B~ sure 111. tLlS 1\. BOARD OF EQUALIZATION UST STORAGE FEE COMPLETED. SEE ARTICLE 5. GiAPTER 6. DIVISION 20, CAUFORNI¡\ HEALTH AND SAFETY CODE) Enter )'our BO:1fd (HOE) CST fc~ aCC1JW1t nurnbcr 'xhich is required before your pennìt c:m be precessed, Rcgistra1ion wÍ!h (be \ViIi en~ure thm recc;ve n 1.pJ:lrtcdy feç f(:wrn reporting the per fee duc en the nmnbcr of gallons pJaced Ín your USTs, The BOE \viH code ç);e!npt ffU1l1 so returns win nOt be :\cnL If you do not. h8VC an account nun~ber "-xith the. HOE if you hJve any questions HOE ~t 916~J22-,9669 or to the ROE:¡t the fOnOìvÍng ~kh.ln.~ss Boa.rd of Fud 94:79~n001 V, PETnOLEUM liST F¡~,ANCIAL fŒSPONSm¡UTY OrTJTLE 23. CHMYfER 16. CALIfORNIA CODE OF nEC;ULATJm:Sì Ickm¡ry the methodes) used hy the owner ;lDdior oper::nor. in Federd agcu:y \\'dl CST, y, SEE SECTJONS 271 ¡ h)(J I) USTs owned by VI. LEGAL N011F1CAT10N AND BILUN(, Check ONE BOX for the address Om wíII be u:;cd for BOTH LEGAL TANK OWNEF OR ,-\UT!IOIUZED (a)(13) or TITLE 23 CHAPTER Hi. CALIFORNiA CODE OF REGULATiONS] JND!C\TED. [SEE SECTIONS 271 J fNSTRCCTJON FOR THE LOCAL t\GENCIES The county tl.'ld numbers are prdetermined and can be obtained by be by locai agçnçy~ ho\vever, thi$: ournber b:; nurnenc:11 prefers SEtte Board tn assign the fadEty numbeL pIca;;::: k;¡ve It th;; State Board (916) 227,4303. The facility rmrnbcrmay alph:1h(~tic;11 chn.r~h-:!Crs, If tbe i0C::~j agency TO VERIFY THE ACCURACY THE ~;UMBEE IS NOT FILLED IN. THE LOCAL ONLY" INFORMATJON BOX. THE LOCAL COPY SW)ULD BE RETAINED BY THE TANK rrIS THE RESPONSmJUTY OF THE LOCAL ,\GENCY THiS APPUCATION AGENCY IS RESPONSIBLE FOR THE CŒv!FLETION AGENCY SHOULD RETAl>: THE OWNER. 9 PACIFIC ENVIRONMENTAL GROUP, INC. . . - I , AN [i] COMPANY March 15,2000 , Project No. 705-131.1B i I I I Mr. Howard Wines 'Office of Environmental Services Bakersfield Fire Department 1715 Chester Avenue Bakersfield, California 93301 Re: New Landowner Notification 'Former Shell Station 101 S. Union Avenue Bakersfield, California DearMr. Wines: Pacific Environmental Group, Inc. (PEG), on behalf of Equiva Services LLC, (Equiva), respectfully request an extension on submittal ofthè New Landowner Notification Form for the àbove-referenced site. PEG requests a 60-day extension beyond the Bakersfield Fire Department original submittal date (March 16, 2000) to obtain the landowner information. i . i , ' If you have any questions, please call me at (626) 351-4814. Sincerely, . " Jci, I' C, Env,ironm~nt, Group, Inc. I p . ~ r.. ~,' " ' Gary P. Pestana, R.G. ' , Senior Geologist G:Project\ 7 40\008\ 1 a \Extension.doc 650 Sierra Madre Villa, Suite 204 . Pasadena, California 91107-2013 (626) 351-4814 FAX(626) 351-4822 FIRE CHIEF RON FRAZE ADMINISTRATIVE SERVICES 2101 "Hn Street Bakersfield. CA 93301 VOICE (661) 326-3941 FAX (661) 395-1349 SUPPRESSION SERVICES 2101 "H· Street Bakersfield. CA 93301 VOICE (661) 326-3941 FAX (661) 395·1349 PREVENTION SERVICES 1715 Chester Ave. Bakersfield. CA 93301 VOICE (661) 326-3951 FAX (661) 326-0576 ENVIRONMENTAL SERVICES 1715 Chester Ave. Bakersfield. CA 93301 VOICE (661) 326-3979 FAX (661) 326-0576 TRAINING DIVISION 5642 Victor Ave. Bakersfield. CA 93308 VOICE (661) 399-4697 FAX (661) 399-5763 . - February 25, 2000 Mr. Gary Pestana, R.G. Pacific Environmental Group 650 Sierra Madre Villa, Suite 204 Pasadena, CA 91107-2013 RE: New Landowner Notification and Participation Requirements Fonner Shell Station, 101 South Union Avenue in Bakersfield Dear Mr. Pestana: This letter is to infonn you of new legislative requirements pertaining to cleanup and closure of sites where an unauthorized release of hazardous substance, including petroleum, has occurred from an underground storage tank (UST). Section 25297. 15(a) ofCh. 6.7 of the Health & Safety Code requires the primary or active responsible party to notify all current record owners of fee title to the site of: I) a site cleanup proposal, 2) a site closure proposal, 3) a local agency intention to make a detennination that no further action is required, and 4) a local agency intention to issue a closure letter. Section 25297.15(b) requires the local agency to take all responsible steps to accommodate responsible landowners' participation in the cleanup or site closure process and to consider their input and recommendations. For purposes of implementing these sections, you have been identified as the primary or active responsible party. Please provide to this agency, within twenty (20) calendar days of receipt of this notice, a complete mailing list of all current record owners of fee title to the site. You may use the enclosed list of landowners fonn (sample letter 2) to comply with this requirement. If the list of current record owners of fee title to the site changes, you must notify the local agency of the change within twenty (20) calendar days from when you are notified of the change. ""Y~ de W~ .¥OP .j~0P6 .!7~ .A Wedu~"" .::.I'< -. .. e e Landowner Notification Page 2 If you are the sole landowner, please indicate that on the landowner list fonn. The following notice requirements do not apply to responsible parties who are the sole landowner for the site. In accordance with Section 25297.15(a) ofCh 6.7 of the Health & Safety Code, you must certify to the local agency that all current record owners of fee title to the site have been infonned of the proposed action before the local agency may do any of the following: 1) consider a cleanup proposal (corrective action plan) 2) consider a site closure proposal 3) make a detennination that no further action is required 4) issue a closure letter You may use the enclosed notice of proposed action fonn (sample letter 3) to comply with this requirement. Before approving a cleanup proposal or site closure proposal, detennining that no further action is required, or issuing a closure letter, the local agency will take all reasonable steps necessary to accommodate responsible landowner participation in the cleanup and site closure process and will consider all input and recommendations from any responsible landowner. Sincerely, 4J4t-J---- Howard H. Wines, III Hazardous Materials Specialist Office of Environmental Services HHW/dm enclosures S:IUSTFORMSIUST.L4 -;. ~~ e Sample Letter (2): List of Landowners Form - "" Date: City of Bakersfield Fire Department Office of Environmental Services c/o Howard H. Wines, III 1715 Chester Avenue, Suite 300 Bakersfield, CA 93301 RE: Certified List of Record Fee Title Owners for Site name Site address Fill out item 1 ifthere are multiple site landowners. If you are the sole site landowner, skip item 1 and fill out item 2. 1. In accordance with section 25297.15(a) of Chapter 6.7 of the Health & Safety Code, I, Name of primary responsible party certify that the following is a complete list of current record fee title owners and their mailing addresses for the above site: 2. In accordance with section 25297. 15(a) ofCh. 6.7 of the Health & Safety Code, I, Name of primary responsible party certify that I am the sole landowner for the above site. Sincerely, Signature of primary responsible party Name of primary responsible party --,...,j.... . Sample Letter (3) Notice of Proposed Action Submitted to Local Agency . Date: City of Bakersfield Fire Department Office of Environmental Services c/o Howard H. Wines, III 1715 Chester Avenue, Suite 300 Bakersfield, CA 93301 RE: Notice of Proposed Action Submitted to Local Agency for Site name Site address In accordance with section 25297.15(a) ofCh. 6.7 of the Health & Safety Code, I, , certify that I have notified all Name of primary responsible party responsible landowners of the enclosed proposed action. Check space for applicable action(s): _ cleanup proposal (corrective action plan) _ site closure proposal _ local agency intention to make a detennination that no further action is required. local agency intention to issue a closure letter. Sincerely, Signature of primary responsible party Name of primary responsible party CC: (Names and addresses of all record fee title owners) . r~U~'~¡ ~"i{l@ ~Q,.""... ill w ~ "., SEA V ICE S L L C Shell. "Texaco & SeudI Aramco Working To¡;¡ether Carlton E. Howell Senior Area Real Estate Manager May 10,2000 1 1- ------ I Mr. Steve Underwood Bakersfield Fire Department Dept. of Environmental Services 1715 Chester Avenue Bakersfield, CA. 93301 .,~c ~ ~~ ~, ~/' ~~ ,,.t?~ 6' 'J. 041 <"ddd . .s'~ ~t?c ~.s' Via Telecopier: 805-326-0576 and Regular Mail Re: 101 South Union, Bakersfield CA. CUP Temporary Closure Permit Expiration Date: 6-1-00 3130 24th Street, Bakersfield, CA CUP Temporary Closure Permit Expiration Date: 7-1-00 Dear Mr. Underwood; Confirming our telephone conversation today, I am pleased that you have found our recent clean-up efforts to be satisfactory at the captioned closed properties. Once again, I apologize for the condition that occurred and I assure you that steps have been taken to review these sites on a regular basis to insure that proper housekeeping is maintained. If yoú or your staff find any item that needs correcting, please contact me either via fax at 913-498-2026 or voice at 913-498-2024. Please also copy our Sales Manager Mr. Terry Runnels, whose fax number is 714-993-2284. In the event you need to speak with Mr. Runnels, he can be reached at 818-736-5420. i____ I With respect to the temporary closure permits which expire as shown above, I respectfully request an extension thereof thru December 31, 200:0. As we discussed, we are negotiating a multi station sales package which inctudes-these two properties, anë:finsrny öeliãnhât a rean~stãte-ëlošingonhis paCKage will occur prioTtotfie enClof this year. Thank you in advance for your consideration and assistance in this matter. YOUrS~IY' carlto~iCW Senior Area Real Estate Manager CEH:mw cc: Mr. Terry Runnels 13105 Meadow Lane, L.eawoOO, 1<5. 66209 Phone: (913) 498-2024 Fax: (913) 498-2026 SE~"~l C~!JA,.PL~TE TH. /S SECT/ON · Complete items 1, 2, and 3. Also complete item 4 if Restricted Delivery is desired. · Print your name and address on the reverse so that we can return the card to you. · Attach this,card to the back of the mailpiece, or on the fWQt if space permits. 1. Article Addressed to: PAUL SCHOENFELD EQUILON'ENTERPRISES LLC 5200 StOCKDALE HWY MI0 103 BAKERSFIELD CA 93311 ì RE: 101 S. UNION AVE o Agent o Addressee I o Yes I o No I I I 3. Service Type ~ertified Mail o Registered o Insured Mail o Express Mail o Return Receipt for Merchandise o C.O.D. 4. Restricted Delivery? (Extra Fee) DYes 2. JA. Number (Copy from service label) Jlllrl0 286 893 PS Form 3811, July 1999 Domestic Return Receipt' 102595,99-M-1789 I UNITED STATES POSTAL SERVICE First-Class M' I 'Þõstage-Kfêe... al ~ -== ~ttSPS==-== --- - ~Permit"No:,,~ë'"fO=~ -.. ~--=- '---~-~.~-- Co. ~===== 55, and Z~~ BAKERSFIELD FIRE DEPARTMENT OFFICE OF ENVIRONMENTAL SERVICES 1715 Chester Avenue, Suite 300 ~ Bakersfield, CA93301 ~:":,":.~-: ,. .....:.-.-:. -.: ... .040.0. ........ ;.. - - - - - . - - .. 0_" III \ 1III \1111\\ I \\ 1111111\ 1\ 1111"/111111 n 111111111'111111/1111111'1' II, ,I III/ Z 410 286 .3 "- US Postal Service ~..~ -:.-;.- Receipt for Certified Mail No Insurance Coverage Provided. LO C» C» ,.... Do not use for International Mail (See reverse) Sent to PAUL SCHOENFELD Street & Number 5200 STOCKDALE HWY M10 fJ1 Post Office, State, & ZIP Code BAKERSFIELD CA 93311 Postage $ .32 Certified Fee 1.10 Special Delivery Fee Restricted Delivery Fee Return Receipt Showing to 1.10 Whom & Date Delivered Return Receipt Showing to Whom, Date, & Addressee's Address TOTAL Postage & Fees $ 2.52 Postmark or Date 3 "§.. < ci o CIO C') E (; u. (J) a.. 1 t~ Stick postage stamps to article to cover First-Class postage, certified mail fee, and' charges for any selected optional services (See front). J 1. If you want this receipt postmarked, stick the gummed stub to the right of the returrt address leaving the receipt attached, and present the article at a post office service window or hand it to your rural carrier (no extra charge). 2. If you do not want this receipt postmarked, stick the gummed stub to the right of the retum address of the article, date, detach, and retain the receipt, and mail the article. 3. If you want a retum receipt, write the certijjed mail number and your name and address on a retum receipt card, Form 3811, and attach ~ to the front of the article by means of the gummed ends if space permits. Otherwise, affix to back of article. Endorse front of article RETURN RECEIPT REQUESTED adjacent to the number. 4. If you want delivery restricted to the addressee, or to an authorized agent of the addressee, endorse RESTRICTED DEUVERY on the front of the article. 5. Enter fees for the services requested in the appropriate spaces on the front of this receipt If retum receipt is requested, check the applicable blocks in item 1 of Form 3811. 6. Savet/lis receipt and present ~ if you make an inquiry. 102595-98-M-0548 Q) !!? ~ CI) . en en .... "§. « Ô (;) w tv) E (; u.. en a.. ·/ FIRE CHIEF RON FRAZE ADMINISTRATIVE SERVICES 2101 ·W Street Bakersfield. CA 93301 VOICE (805) 326-3941 FAX (805) 395-1349 SUPPRESSION SERVICES 2101 oW Street Bakersfield. CA 93301 VOICE (805) 326-3941 FAX (805) 395-1349 PREVENTION SERVICES 1715 Chester Ave. Bakersfield. CA 93301 VOICE (805) 326-3951 FAX (805) 326-0576 ENVIRONMENTAL SERVICES 1715 Chester Ave. Bakersfield. CA 93301 VOICE (805) 326-3979 FAX (805) 326-0576 TRAINING DMSION 5642 Victor Ave. Bakersfield. CA 93308 VOICE (805) 399-4697 FAX(805)3~5763 /. . '';; .. f' '__ December 27, 1999 Paul Schoenfeld Equilon Enterprises LLC 5200 Stockdale Hwy, M10 #103 Bakersfield, Ca 93311 CERTIFIED MAIL RE: Extension of Temporary Closure Until June 1,2000 at 101 South Union Avenue Bakersfield CA. NOTICE OF EXTENSION OF TEMPORARY CLOSURE Dear Mr. Schoenfeld: Please be advised that pending receipt of your letter outlining marketing action for Shell stations in Kern County, this office will grant an extension to your temporary closure, which expires January 7, 2000. This extension is subject to receiving your marketing plan on or before January 7, 2000. This office will require quarterly updates starting in March of 2000. Should you have any questions, please feel free to call me at 661-326- 3979. Sincerely, Ralph E. Huey, Director Office of Environmental Services bY:~ d/kv Steve Underwood, Inspector Office of Environmental Services SBU\dm "'-. --..9'~ ~ W~ ~.A~ g--~ A W~'I'I ;\ _t' <- .- EQ.UIVA _ SERVICES LLC Shell. Texeco & Seudi Aremco Working Togethel" Deni, Gallonio Real Estate Manager !)~; -: ...... ) , December 15,1999 í9>g Captain Steve Underwood Bakersfield Fire Department Environmental Services 1715 Chester Ave. 3rd Floor Bakersfield, CA 93301 ....... ,. ':~" . - ......, ~, Re: Shell!fexaco service stations in Bakersfield Bid Package Dear Steve: It has been a pleasure speaking with you on the phone for the last several weeks. As we had discussed, Equilon, successor in interest to Shell and Texaco, is receiving bids for the sale of the entire Bakersfield package of stations. This package consists ofa total of twenty-three locations. Bids will continue to be received through the <:nd of this year. Once all bids have been received, each one will be analyzed for terms and conditions. The best bid will be chosen and the due diligence process by successful bidder will begin. During this process, each of the dealers at the above locations will be notified of the sale and given their right of first refusal. Once the rights of first refusal are satisfied, we will move into the negotiations, underground storage tank issues, contracts, escrow and final transition phases. Our timeline to cover these major phases as well as a substantial number of lesser phases is projected to run through the fifth of May next year. Some items in this bid process can and will be processed simultaneously to save time. This is a major market sale for Equilon that is being spearheaded by executive management They have given me a directive to complete this bid process and close the sale of the twenty-three properties on or before the May fifth date. I will be happy to keep you informed of my progress. The Conditional Use Permits at various Bakersfield sites are very important to our business and this sale in particular. The value of the sale would be diminished by the loss of these permits. Equilon will work with your agency to retain the permits through the entire bid process. Thank you for your understanding. Please feel free to call with questions. ~a Denis Gallonio Real Estate Manager .... 713 W. Duarte Rd. Box G·562 Arcadia. CA 91007 9 PACIFIC ENVIRONMENTAL GRO~P,INC. - .~ e ,. .""''':'' Lìì.t'>.".", "".,'" .", A . ''''1/ if" Ihn ~ÍÍ'j\ 'V' ! y ~, /';'. t, .J. ilfJn ¡:;·:L [f V¡jt; 17.19 I. ~'():",If . :, l" t:Jff:'- . . . -::tflt!r";' ·""¿:S (. AN rn COMPANY August 10, 1999 Project 705-131.7B Mr. Ralph Huey Bakersfield Fire Department - EnviroIimental Services 1715 Chester A venùe . Bakersfield, California 93301 Re:. Quarterly Status Report (2nd Quarter 1999) Shell-Branded Service Station (WIC No. 204-4262-2100) ~~~~~~t~~~:~~u~ ~, a Dear'Mr. Huey: . . Pacific Environmental Group, Inc. (PEG), on behalf of Equiva Services LLC _ (EQUIV A), is pleased to submit this second quarter 1999 status report for the site . refer~nced above. ) . On Marcþ 16, 1999, the Bakersfield Fire Department - Environmental Services Division (BFDESD) issued a: letter which requested a work plan for further site assessment. On April 16, 1999, PEG submitted the work plan to the BFDESD. On May20, 1999, the BFDESD approved the work plan. During the third quarter of 1999, PEG will perform site assessment activities and submit a report documenting the field activijies. If you have any questions, please call either of the two undersigmid at (626)'351·'-4814 or Mr. Ed Paden, Equiva Services LLC, (310) 816-2075. Sincerely, Pacific E~nmcntal Group A1ex~ou, P.E. , Project Engineer cc: Mr. Edward Paden - Equiva Services LLC r Gary P. P stana, R.G. Senior Project Geologist 650 Sierra Madre Villa, Suite 204 . Pasadena, Califòrnia 91107-2013 (626) 351-4814 FAX (6'26) 351-4822 · ..( RECORD OF TELEPHONE. CONVERSATION Location: lOt ~. U,rJ'(~ Business Name: Ei&} L on..J Contact Name: ÔJ3rèv .p~rANA ~ PAC... Ef\lv" ú;;P, ID# Business Phone: <3 '2.<ó < ~ ~ I, 48 ( 4 FAX: Inspeètor's Name: Time of Call: Date: ff-J <6/1- / C1q , Time: <g' ~v :# Min: /ð Returned.·k:}:: Type of Call: Incoming [ ] Outgoing [~ Content of Call: 'f:c:Ç-TùfùJC-r;> JVt5G. ~ ç:¡¿,~ ~V s.Ä-rD ~LE5 1-'05,,> 1l~ (0{) ff~ (PH ~. Nbrc cr-Cl3'(,. cÇ G-t\-$ cJYl.·O(C$E~ ~I <..~ £..J1 tL- (LuN y:iXU{)f6fL ~rc ~ ÖIÙ <;~PLé Hft-. 10, ArID 'L f\.I-' ~p t (..J G- ¿,J'ÞÒ ,J 10 f¥2-cJ.-f'tV^0 0 (sp. A2-ðA \ Actions Required: Aov1s(5/) ~v -¡V $'c..rirO /vté cæ(£5-c;P IZEfbYlJ,S ~ <'fG CcMl'J';::.,.y <\1-ks rNFd "[0' -(2ùv<;J Å'1 CAe...... LJ'A4C-1L Time Required to Complete Activity # Mln: ~ Mi OF "- F0R PHONE CALL ) TIME = fë) :5~ TELEPHONED RETURNED YOUR CALL PLEASE CALL WILL CALL AGAIN CAME TO SEE YOU WANTS TO SEE YOU i~~ .l A ~ !!_~KERSF[ELD . e Haz Mat Emerg e Spill Report Complaint ~ Environmental Services o o s- Date Haz Mat Incident I Spill Report I Complaint Follow Up <0 (!)-O 7 lIS- )9 Time I ¿) . F f2 u r:> if (CkL W'V\.<IC~) Reporting Party Address Telephone No. Environmental Services Contact g3~ - 32-'3 g Location of the incident lJ N (OAJ ~ ~c.J,JùA<3c- Description of the incident ( Chemical name and Quantity) G-A50\../~ ~~'N4-TL-J) ,$.b/£-C-.A.JCCJJ,.J'C.J2.C.-.D f}I<I--K.- Ckc -LJA-'l~'S Co---fì"tê.A:-L1ðt'L ,e)C('J\v4-'í1a~ (~tZòV'M-L' Dæl LV..t~) ~ A./'C-<-J t.-J\A-'rC"L L( Af é Responding to Incident Œ)N Observations J\-.. ') !) Ace.,f 'ï ßEcÄN'E t,J7-fC--¡J &.s'fl-,rJG- RC4-CuC-I) S w <:~~z eJ>f=.. 1~-rc./è::J Ec-'Tlc:Y"/ '1'0 AßA-vDahlC-D Sff(?L(... . ~rYt-T1cJrJ I 10 (, s ~ UN(ótV / So, (.. C v(ï/ .....t;..s ÑcJ1ìGlßt..~ I;'VI f' 4-e TC-I) ~y ?~C>LEvN\.. ~_o-n ......"..-u'L " Special Conditions and / or health risks Haz Mat Team Dispatched Y N Van Cellular No. 332-7865 OES Number Required Y N Number Poss Exposure Victims Medical Attention Required or Obtained Probable Hazardous Waste Clean Up (i) N Discussion and Disposition ~ ð '11 Ft C:of) PM'- S:.#::i:~évD (J'C-- EQ()¡UJ,J öP S'"TVl.\--l1cVV_ ,VI cl\- v(){cé l^-t.Ã-tL, f\I() (2C~ (ALt ~ <:>r yC-.,- rAul rN~ll\=J CAL<"'~ í\.ßC~ 7!:t..! ¡cpo¡, Referral ? FIRE CHIEF RON FRAZE ADMINISTRATIVE SERVICES 2101 "H· Street Bakersfield. CA 93301 VOICE (805) 326-3941 FAX (805) 395-1349 SUPPRESSION SERVICES 2101 "H" Street Bakersfield. CA 93301 VOICE (805) 326-3941 FAX (805) 395-1349 PREVENTION SERVICES 1715 Chester Ave. Bakersfield. CA 93301 VOICE (805) 326-3951 FAX (805) 326-0576 E~RONMENTALSERVlCES 1715 Chester Ave. Bakersfield. CA 93301 VOICE (805) 326-3979 FAX (805) 32eµQ576 TRAINING DMSION 5642 Victor Ave. Bakersfield. CA 93308 VOICE (805) 399-4697 FAX(805)3~5763 . - January 26, 1999 Mr. Tim Hargraves, HS&E Representative Equillon Enterprises LLC P.O. Box 8080 Martinez, CA 94553 RE: Laboratory results from preliminary site assessment conducted at the Macias Shell Station, 101 South Union Avenue in Bakersfield. Permit #BI-0116. Dear Mr. Hargraves: Upon review of the recently submitted laboratory results from your facility, this office has determined that the extent of the contamination plume, associated with the dispenser island upgrade activities located on your property, has not been adequately defmed. This office requires (in accordance with Chapter 6.7 of the California Health and Safety Code and Chapter 16, Title 23 of the California Code of Regulations) that further assessment be done to define the vertical and horizontal extent of the contamination plume. Please submit a work plan for further assessment, to this office, within 30 days from receipt of this letter. The workplan should follow guidelines found in: Appendix A -Reports. Tri - Regional Board Staff Recommendations for Preliminary evaluation and Investigation of Under~round Tank Sites; July 6, 1990. Additionally, be advised that oversight cost for this project will be billed to you at a rate of $75.00 per hour. If you have any questions, please call me at (805) 326-3979. Sincerely, ~(¢b~ ~ Howard H. Wines, III Hazardous Materials Specialist Office of Environmental Services ""Y~ ~ ~on~ ..¥OP uØ60P6 y~ A W~p" FIRE CHIEF RON FRAZE ADMINISTRATIVE SERVICES 2101 "H' Street Bakersfield. CA 93301 VOICE (805) 326-3941 FAX (805) 395-1349 SUPPRESSION SERVICES 2101 "H" Street Bakersfield, CA 93301 VOICE (805) 326-3941 FAX (805) 395-1349 PREVENTION SERVICES 1715 Chester Ave. Bakersfield, CA 93301 VOICE (805) 326-3951 FAX (805) 326-0576 E~RONMENTALSERVlCES 1715 Chester Ave. Bakersfield. CA 93301 VOICE (805) 326-3979 FAX (805) 326-0576 TRAINING DMSION 5642 Victor Ave. Bakersfield, CA 93308 VOICE (805) 399-4697 FAX (805) 399-5763 . . June 8, 1999 Paul Schoenfeld Equillon Enterprises LLC 8200 Stockdale Hwy., Suite MIO #103 Bakersfield, CA 93311 RE: Temporary Closure of Former Macias Shell, 101 South Union A venue Dear Mr. Schoenfeld: Our records indicate that the above mentioned address has been closed for more than 90 days. At this time, you are required to either remove the tanks or request a temporary closure in writing. It is noted that on March 5, 1999, K.E. Curtis performed the necessary requirements as outlined in Section 2671 of Title 23 CCR for temporary closure. So that the facility will stay in compliance, it is necessary for Equillon to request a temporary closure. Please note that a temporary closure cannot be extended past January 1, 2000. Please submit your request within 15 days (June 18, 1999)" Should you have any questions, please feel free to call me. S)~ Steve Underwood Underground Storage Tank Inspector Office of Environmental Services ~~7~ de W~ ~.A0Pe.r~ A W~" FIRE CHIEF RON FRAZE ADMINISTRATIVE SERVICES 2101 "H" Street Bakersfield, CA 93301 VOICE (661) 326-3941 FAJ< (661) 395-1349 SUPPRESSION SERVICES 2101 "H· Street Bakersfield, CA 93301 VOICE (661) 326-3941 FAJ< (661) 395-1349 PREVENTION SERVICES 1715 Chester Ave. Bakersfield, CA 93301 VOICE (661) 326-3951 FAJ«661)326-o576 ENVIRONMENTAL SERVICES 1715 Chester Ave. Bakersfield, CA 93301 VOICE (661) 326-3979 FAJ< (661) 326-0576 TRAINING DIVISION 5642 Victor Ave. Bakersfield, CA 93308 VOICE (661) 399-4697 FAJ< (661) 399-5763 - . ,~ .. ;(,1 c, ",,' I 'I. October 19, 1999 Paul Schoenfeld Equilon Enterprises LLC 8200 Stockdale Hwy, M10 #103 Bakersfield, CA 93311 CERTIFIED MAIL RE: Temporary Closure at 101 South Union Avenue, Bakersfield, CA Dear Mr. Schoenfeld: This letter is a reminder that temporary closure at the above mentioned site will expire on January 7, 2000. Accordingly, this office requests an update on the status of this facility within 30 days, November 18, 1999. Sincerely, ~~ Steve Underwood, Inspector Office of Environmental Services SBU/dm ""7~~ W~ ~.Aon? ff'~.Æ W~'I'I FIRE CHIEF RON FRAZE ADMINISTRATIVE SERVICES 2101 "H· Street Bakersfield, CA 93301 VOICE (805) 326-3941 FAX (805) 395-1349 SUPPRESSION SERVICES 2101 "H" Street Bakersfield, CA 93301 VOICE (805) 326-3941 FAX (805) 395-1349 PREVENTION SERVICES 1715 Chester Ave. Bakersfield, CA 93301 VOICE (805) 326-3951 FAX (805) 326-0576 ENVIRONMENTAL SERVICES 1715 Chester Ave. Bakersfield. CA 93301 VOICE (805) 326-3979 FAX (805) 326-0576 TRAINING DMSION 5642 Victor Ave. Bakersfield, CA 93308 VOICE (805) 399-4697 FAX(805)3~5763 - - May 20, 1999 Patrick McCullough Pacific Environmental Group 650 Sierra Madre Villa, Suite 650 Pasadena, Ca 91107-2013 RE: .Macias Shell Station (WIC No. 204-4262-2100) Located at 101 S. Union Avenue, Bakersfield CA. Dear Mr. McCullough: This is to notify you that the work plan for the above stated address is satisfactory. Please give this office 5 working days notice prior to the commencement of work. Please be advised that any work done that is not performed under direct oversight by this office will not be accepted, unless previously approved. If you have any questions, please call me at (661) 326-3979. Sincerely, P E. uey, Director Office of Environmental Services REH/dlm cc: Paul Schoenfeld, Equilon Services S:IUSTFORMSIUST.L3 "..9'~ de W~ ~ ~~ g--~ .A W~" ·' '.9>. PACIFIC· ENVIRONMENTAL GRQUP,INC. e e AN rn COMPANÝ May 3, 1999 Project 705-131.1B Mr. Ralph Huey Bakersfield Fire Department - Environmental SerVices 1715 Chester Avenue Bakersfield, California 93301 Re: Work Plan for Additional Site Assessment Shell-Branded Service Station (WIC No. 204-4262-2100) , Marcias Shell Station 101 South Union Avenue Bakersfield, California Dear Mr. Huey: Pacific Environmental Group, Inc. (PEG), on behalf of Equiva Services LLC - (EQUN A), is pleased to present this work plan for the site referenced above. PEG prepared this workplan in response to a letter dated March 16, 1999, ftom the . Bakersfield Fire Department - Environmèntal Services Division, requestiIlga work plan for further assessment. BACKGROUND -, Site Description The Site is locàted at the intersection of South Union Avenue and Brundage Lane in Bakersfield" California (Figure 1). The Site operates as a Shell-branded service station that has recently undergone upgrade activities to the dispensers and sump containment around turbines. ( Previous Environmental Activities Prior environmental activities are ~umníarized as follows: · July 1998 - upgrade activities included secondary containment to the existing dispensers and gasoline turbines. Analytical results areinèluded as Table 1. On July 10, 1998, Cambria Environmental Technology, Inc. (Cambria) obset;Ved upgrade activities on dispensers and gasoline turbines. Cambria subsequently collected . - 650 Sierra Madre Villa, Suite 204- Pasadena; California 91107-2013 (626) 351-4814 FAX (626) 351-4822 ; e e May 3, 1999 Page 2 soil samples from beneath all dispensers (Figure 2). Ofthese samples, the highest detected hydrocarbon concentrations [D-4 (2')] occurred at two feet beneath dispenser 4. The analytical results were reported as 2,600 milligr$TIs per kilogram (mg/kg) total petroleum hydrocarbons as gasoline (TPH-g) [Table 1]. PROPOSED SCOPE OF WORK - SUBSURFACE ASSESSMENT PEG proposes' to conduct additional subsurface assessment,to evaluate soil conditions surrounding areas of known hydrocarbon impacts to soil. Pre-field Activities. PEG will visit the site to mark the boring locations, contact Underground Services Alert 48 hours prior to drilling, arrange the drilling schedule, and mobilize drilling equipment and materials. PEG will prepare a site-specific health and safety plan prior to initiating field activities. Notifications regarding the field activities' will be made in advance to the appropriate agencies, current property owner, and tenants. Field Activities. Two exploratory soil borings (GP-1 and GP-2) will be drilled in the vicinity of dispensers 4 and 5 (Figure 2). The borings will be drilled to 15 feet bgs utilizing a direct-push probe equipped truck. Total depth of borings will ,be extended if field, observations (i.e. staining, smell, PID readings) indicate impacted soils. Prior to drilling,. the exploratory boring locations will be 'cleared by hand-auger equipment to a depth of 5-feet bgs. Soil samples will be collected at five-foot depth intervals. Soil will be logged and sampled using a 1- to 2-inch diameter direct-push sampler. Soil' samples will be retained in I-inch diameter tubes or brass rings. The containers'wîll be sealed at each end with Teflon®-lined plastic end caps, labeled, and stored on ice for transport to a California state certified analytical laboratory with the appropriate chain- . of-custody documentation. A field geologist, under the direction of a Registered Geologist, will m~e geologic interpretations and field observations of all sampling intervals. All soil samples will be field screened for the presence of volatile organic compounds (VOCs) by headspace analysis using a photo-ionization detector (pID)'calibrated to 100 parts per million by volume (ppmv) of isobutylene. The borings will be backfilled with bentonite chips and plugged with asphalt patch, concret~, or soil to match the existing sUrface. Laboratory Analysis. All soil samples will be analyzed for the presence ofTPH-g using Environmental Protection Agency (EPA) Method 8015 (modified), and BTEX compounds and methyl tert-butyl ether (MtBE) using EP A Method 8021. Thesoil sample with the hIghest MtBE concentration from each boring will be confinned using , EP A 8260A. G:Projet\705\!3!\! B\WORKPLAN.DOC ..f. : e . May 3, 1999 Page'3 Equipment Decontamination. All down-hole sampling equipment will be washed between samples in a non-phosphate detergent" and triple-rinsed with potable water. ' Water/Soil Disposal. Soil and rinsate generated during drilling and sampling activities will be left temporarily onsite in labeled Department of Transportation (DOT)-approved 55-gallon drums pending analytical results and coordination of disposal or recycling. Report Preparation. After completing all field activities ~nd upon receipt of analytical, data; PEG will prepare a written report describing prefeild and sample collection activities. The réport will also include analytical sòil results and findings of subsurface ~onditions. SCHEDULE This work will be initiated upon approval from the Bakersfield Fire Department- Environmental Services Division.- Upon receiving written approval of this work plan, PEG will obtain the necessary pennits and commence drilling. We will submit our investigation report approximately four to six weeks after completing the fieldwork. Should you have any quéstions or need any further assistance, pleasè contact Patrick McCullough at (626) 351-4814. ~~~ a~k Sincerely, PEG/The IT Group Patrick T. McCùllough, R.E.A. Project Manager Attachments: . Table l'~ Soil Results Collected Beneath Fonner USTs (Cambria, 1998) Figure 1 - Site Location Map Figure 2 - Site Map , Kì2. Y'A'L <31 Zs-. 13" . 501g rs\O . ~'.6. ~ò7Ç cc: Mr. Edward Paden - Equiva Services LLC ----,.-----.., . -----.. G:Projet\ 705\131 \IB\ WORKPLAN.DOC " ,,~ ~:" CAMBRIA Table 1. Dispenser Sample Analytical Data - Shell-branded Service Station - WIC #204-0462-2100, 101 S. Union Avenue, Bakersfield, California Date Sample ID Depth TPHg MTBE Benzene Tolu~ne Ethylbenzene Xylenes (feet) . (Concentrations reported in milligrams per kilogram) ~ 7/10/98 D-1(2') 2,0 <20 30( 19) <0.1 <0.1 <0.1 <0.1 7/10/98 D-2(2') 2.0 <1.0 0,21 <0,0050 <0.0050 <0,0050 <0.0050 7/10/98 D-4(2') 2.0 ,2,600 <6.2 <1.2 2.3 1.3 70 e 7/10/98 D-5(2') 2,0 '58 3.2 <0,050 <0.050 <0.050 1.4 Abbreviations nnd Notes: TPHg = TOlal petroleum hydrocarbons as gasoline by modified EPA Melhod 8015. MTBE = Methyl tert-butyl ether by EPA Method 8020. Result in parentheses represents MTBE by EPA Method 8260. Benzene, ethylbenzene, toluene, and tolal xylenes by EPA Method 8020. <n= Below detection limit of n milligrams per kilograms e G:lßakcrsficld IOIlUpgrodcs\Dispc:nscrs.XLS Page I of I " ~')·Ir--tr 11····-11 . ~ ~....I ,-~ ~.. 1/ ~:.I:!;sc!l . RNI . I Yi ~T L1T '... I"'~~ . 1== ; BM4p~ ~~~~Qb¡ ~Ll ./I./~~(I!!f¿j o _1 ì I 1~Þ!JOG~~øJ!}~ H 1r- II 71 ~ """ J · fi}"'~ O/MU/I""l<' I I]~ ¡ .. 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Wl:= .....>, ..-,,' í~~)~'<':i,' , . - . 1',.\'\:·,:'.'./',': n·' r ..- tl,\ . 11·>/·..·, % QUADRANGLE LOCATION REFERENCES: USGS 7.5 MIN. TOPOGRAPHIC MAP TITLED: GOSFORD, CALIFORNIA; LAMONT, CALIFORNIA DATED: 1954 REVISED: 1973 I 2000 SCALE IN FEET I o I 2000 ~ PACIFIC ENVIRONMENTAL GROUP, INC. SHELL SERVICE STATION 101 South Union Avenue Bakersfield, California SITE LOCATION MAP FIGURE: 1 PROJECT: 705-131.1 B · BRUNDAGE LANE I ------- ------ I I 1 I 1 I 1 I I I 1 I I I 1 f- I~ S I..J ~ I~ ð IW 10... -< 0 :> e::; 10... I 1 I I I 1 I I I 1 1 I I I I I I I ------------------------------------' ------- UNDERGROUND STORAGE TANKS /-__1__- { ~ \ .....-______1 ---........ r- ..., I I<{ ! I I I ! I I I DISPENSER ISLAND --"-- -- /------- { \ ,-______1 /------- I \ .....-______1 D DISPENSER ISLANDS I I I \ \ \_._-,--,--,- B-2 ~ 400 GAL. PROP ANE ü < o e::; 0... 0... 1< HIGHWAY 58 C- 10 ::¡: 2' ~ ..... '" ..... G) o ..... éí5 C) z ~ o ¡::::: ü UJ --, o c:: a.. LEGEND B-1-+- PROPOSED SOIL BORING LOCATION AND DESIGNATION N ....... U ..,.. Ò e::; 0... 0... -< ¡;..J ;-.. ¡...J Z ¡;,.,; >- ~ Z o .... z ~ ~ :;: ~ W o (/) I o APPROXIMATE SCALE I I 30 60 FEET ~ SHELL SERVICE STATION 101 South Union Avenue Bakersfield, California FIGURE: 2 PROJECT: 705-131.1 B PACIFIC ENVIRONMENTAL GROUP, INC. SITE MAP ~ ~ .......-. -: .' M1f'i 1 0 99 1 1 : 09 a Paul Schoenfeld (805)587-7866 p.2 it - EQ.UILDN - ENTERPRISES LLC Shell Ii< Te:uco Working Together May 10,1999 Mr. Steve Underwood UST Inspector Office of Environmental Services 1715 Chester Ave Bakersfiel~ CA 93301 I am requesting temporary closure status for the Shell station located at 101 Union Ave in the city of Bakersfield. The station was involved in a fire earlier this year and has been closed ever since. In accordance with the city fire department, all necessary measures were taken within reason to insure the safety of the facility and its premises. Currently, our company is undergoing a review of several options to take in regards to the future direction of the subject Shell station. As soon as any decision is made, I will be sure to contact your department in order to keep the flow of communication timely. Q;~J Paw Schoenfeld Sales Consuhant Equilon Enterprises L.L.C. ~~M~~ 10 99 11:09a Paul SchoenFeld . Attention: Ms, Steve Underwood Company: Fax Number: 3260576 Voice Number: From: Paul Schoenfeld Company: Shell Oil Products Company Fax Number: (805)587 -7866 Voice Number: (805)587 -7466 Subject: 101 Union Ave Comments: (805)587-7866 p. 1 e Date: 5/10/99 Number of Pages: 1 Steve, . Per your request. ,'. FIRE CHIEF RON FRAZE ADMINISTRATIVE SERVICES 2101 'W Street Bakersfield, CA 93301 VOICE (805) 326-3941 FAX (805) 395-1349 SUPPRESSION SERVICES 2101 "H" Street Bakersfield, CA 93301 VOICE (805) 326-3941 FAX (805) 395-1349 PREVENTION SERVICES 1715 Chester Ave. Bakersfield. CA 93301 VOICE (805) 326-3951 FAX (805) 326-0576 ENVIRONMENTAL SERVICES 1715 Chester Ave. Bakersfield, CA 93301 VOICE (805) 326-3979 FAX (805) 326-0576 TRAINING DIVISION 5642 Victor Ave. Bakersfield, CA 93308 VOICE (805) 399-4697 FAX (805) 399-5763 .... ~ e April 21, 1999 Patrick McCullough, Project Geologist Pacific Environmental Group Inc. 650 Sierra Madre Villa, Suite 650 Pasadena, CA 91107-2013 RE: Request for Extension for Work Plan Submitted fOJ:: 101 South Union Avenue, Bakersfield, CA Dear Mr. McCullough: I have received your letter requesting an extension for the work plan submitted at 101 South Union. In a telephone conversation with Mr. Raul Schoenfeld of Equilon Services, we have already granted a fifteen (15) day extension on this submittal. You are requesting an additional extension, until May 16, 1999. That extension request is also granted. I will expect the work plan on or before May 16, 1999. If you have any questions, please call me at 326-3979. Sincerely, d~ Ralph E. Huey, Director Office of Environmental Services REH/dm cc: Paul Schoenfeld, Equilon Services ··7~ de W~ .970P uØ60Pe .r~ A W~" "~9 . PACIFIC ENVIRONMENTAL GROUP, INC. AN rn COMPANY April 16, 1999 Project No. 705-131.1B Mr. Ralph E. Huey Bakersfield Fire Department Environmental Services 1715 Chester Avenue . Bakersfield, California 93301 Fax(805)-~26-0576 Re: Extension Request for Work Plan Submittal Marcias Shell Station 101 South Union Avenue Bakersfield, CA ' WIC# 204-0462-2100 Dear Mr. Huey: . I , On behalf of Equiva ServicesLLC (Equiva), Pacific Environmental Group, Inc, (PÈG) is requesting ~ extension for wor~plan submittal for the site referenced,above. In a letter dated March 16, 1999, the Bakersfield Fire Department - Environmental Services requested a work plan be submitted 30 days from receipt of the letter. PEG requests an . extension for work plan submittal through May 16, 1999. If you have any questions regarding ,this request or need additional infonnation regarding this site, please call the undersigned at (626) 351-481'4. . Sincerely, Pacific Environmental Group, Inc. ~~ ~c~ . , Patrick McCullough Project Geologist Cc: Mr. Edward Paden, Equiva Services,LLC ., . G:Project\705\131\BFDLTR I FAX (626) 351-4822 650 Sierra Madre Villa, Suite 204· Pasadena, California 91107-2013 (626) 351-4814 ~. .~ March 16, 1999 FIRE CHIEF RON FRAZE Paul Schoenfeld Equilon Services LLC 8200 Stockdale Hwy, Suite M-lO #103 Bakersfield, CA 93311 ADMINISTRATIVE SERVICES 2101 ·H· Street Bakersfield, CA 93301 VOICE (805) 326-3941 FAX (805) 395-1349 RE: Laboratory results from preliminary site assessment conducted at the Macias Shell Station, 101 South Union Avenue. SUPPRESSION SERVICES 2101 ·W Street Bakersfield, CA 93301 VOICE (805) 326-3941 FAX (805) 395-1349 Dear Mr. Schoenfeld: PREVENTION SERVICES 1715 Chester Ave. Bakersfield, CA 93301 VOICE (805) 326-3951 FAX (805) 326-0576 Upon review of the recently submitted laboratory results from your facility, this office has determined that the extent of the contamination plume, associated with the dispenser soil samples located on your property, has not been adequately defined. ENVIRONMENTAL SERVICES 1715 Chester Ave. Bakersfield, CA 93301 VOICE (805) 326-3979 FAX (805) 326-0576 This office requires (in accordance with Chapter 6.7 of the California Health and Safety Code and Chapter 16, Title 23 of the California Code of Regulations) that further assessment be done to define the vertical and horizontal extent of the contamination plume. TRAINING DIVISION 5642 Victor Ave. Bakersfield, CA 93308 VOICE (805) 399-4697 FAX (805) 399-5763 Please submit a work plan for further assessment, to this office, within 30 days from receipt of this letter. The workplan should follow uidelines found in: Appendix A -Reports. Tri - Regional Board Staff Recommendations for Preliminary evaluation and Investigation of Underground Tank Sites; July 6, 1990. Additionally, be advised that oversight cost for this project will be billed to you at a rate of $75.00 per hour. If you have any questions, please call me at (661) 326-3979. Sincerely, REH/dlm ~~7~ de Wonv~ .¥eve .A0P6 y~ A W~" Mar 05 99 10:42a paU'SChoenfe 1 d (805)587-7866 -- p. 1 i ~....~ Attention: Mr. Sreve UndeIWood Date: 3/5/99 Company: Number of Pages: 1 Fax Number: 3260576 Voice Number: From: Paul Schoenfeld Company: Shell Oil Products Company f9 ;)-00 Sf-vc.~Ct-lL- -thu'11 ~~ k )i1-1 D 6MPI / C A c¡ =3~1 I ..tI:-l 0 ? Fax Number: (805)587 -7866 Voice Number: (805)587-7466 Subject: Shell station - 101 Union Comments: Steve, Here is the document as requested. Please call me with any questions or concerns. Thanks! Mar 05 99 10:42a =Feb 26 99 02:08p Pau.SChoenfe 1 d I<E~urt is Canst. (805)587-7866 805-.-0409 02/26/99 FAX To: Equilon Services LLC Attn: Paul Schoenfdd Fax: 661-587-7866 No. ofp32es J From: K.E. Curtis Const CO. Griffin Williamson 9SO Orcutt Rd. I#B San Luis Obispo, Ca. 93406 Phone: 805-S9~405 Fax: 805-593-0409 Re2ardin¡:: Shell at 101 S. Union I Brundage in Bakersfield. The fill eaps have been locked. A secured cbain link fence closes off the lot. The site will remain in this condition until further notice by Equilon. Thank You, Griffin W ìJliamson p.2 p.l