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LABORATORIES, INC.
`:Date of Report: 11 /08/2006
jJerry Hale
`D & J Construction
,''3534-A Gilmore Ave
'~Bakers~eld, CA 93308
RE: Soil Samples -'D'
BC Lab Number: 0611114
Enclosed are the results of analyses for samples received by the laboratory on 10/24/06 12:20. If you have any
:questions concerning this report, please feel free to contact me.
Sincerely,
Person: Linda Phoudamneun
Authorized Signature
Al! results listed in this report nre for the exclusive use of the submitting party. BC Laboratories, inc. assumes no responsibility for report alteration, separation„ detachment or third party interpretation.
4100 Atlas Court • Bakersfield, CA 93308 • (661) 327-4911 • FAX (661) 327-1918 • www.bclabs.com
,Client Service Rep.
Laboratories, Inc. Chain of Custody Farm p e~QUO~ ~~°
t 2613
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Tn: ,~.
;nt: 1-~" ~,.~ (~,UC.~ IW\
Pro'ect #: _
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Page of
~: P Pro ect Name: rt r ,~1t Tom- l.-n Comments:
et:Address• 3;3~-IQ t A-/~' Pro ect Code: ~ ^ ~,~ :.~~ ~~~~ , a , e~: ~
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State Zi u~ 33'1 Sam ler s v ~ ,.A ~ ~ ,,,.,~ ~ t ~" ., ~~
e: Fax: t;.~! ~.. ~.~ ~ ,, ; ~~~~T ~ ~~ ~ ~
~il AddreSS:
-( etA ~ i*.ja~ i~'v.~,~
v Sample Matrix
~ w .p ~',
a ~ nre there any tests with holding times less than
or equal to 48 hours?
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' ittal #• '' ~ ~ ~ ~1 vv ~
7
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3 3 ~ ox
~ ^ Yes ^. No
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* Standard Turnaround =15 work days
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Notes
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^ Same as above Report Drinking
Waters on State Form?
Sampl Disposal
^ urn to Client ^ Disposal by lab ^ Archive: Mo s_~~_
Special Reporting
QC IP ^ Raw Data
Date
Time
1. elan uished By i. Received By i Date Time
^ Yes ^ NO nn ~/ -
State Zip Send Copy to State of
cA, 2. Re n uished y Date Time 2. Received"By Date Time
^
^ 3. R uished By Date Time 3. Received By Date Time
NO
Yes
BC Laboratories, Inc. - 4100 Atlas Ct. -Bak ersfield, CA 93308 - 661.327.4911- Fax: 661.327.1918 - www.bclabs.com
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Assigned to: ~ ~'1 ~ ~~
Field Service
Sampling Request. Form
Today's Date: ~~ } ~~~~Y (~~-~.
Client Code: Project Name or #:~
Company: ~~ G~~ l~l [G`~- Office #:
Address:
Cell #:
Contact: Completed by:
( )Sample P/U ()Bottle D/O ()Pick up & Drop off ()Sampling ()Other
Date Needed:
Information:
Time Needed:
-Siti~L
] ,
Sampling Information:
Quantity of Samples:
Matrix:
Supplies -__.._ ____
Needed:
Analysis:,
Take bottle order #:
f~ .di j
Billing Charges for Courier/Field Time: `~-t'' ram , /~-~''
Time: Bottle order Delivery:
Miles: Flat Rate:
Equipment:
Return with Chain of Custody for billing parposes. Field service Request rami.aoc
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BC LABORATORIES INC. SAMPLE RECEIPT FORM Rev. No. 10 ot/2t/oa Page ~ Of J
Submission #: ~o"' l 1 ~ Pro'ect Code: TB Batch #
SHIPPING INFORMATION
Federal Express ^ UPS ^ Hand Delivery ^
BC Lab Field Service ~ Other O (Specify) HIPPING CONTAINER
Ice Chest None ^
Box ^ Other ^ (Specify)
Refrigerant: Ice Blue Ice D None ^ Other ^ Comments:
Custody Seals: Ice Chest D
Intact? Yes D No D Containers D
I tact? Yes D No None Comments:
All samples received? Yes o t7 All samples containers intact? Y o O Descriptionls) match COG? Ye~ No O
COC Received tt:e Chest ID Emissivity C~ DatelTime !~ %~t
Temperature: I °C Container 0. ~
YES ~ NO Analyst mit ~,1~ .
SAMPLE CONTAINERS t 2 3 a 6 6 7 a 9 it
l1T GENERAL INERAL/ GENERAL PHYSICAL
PT PE UNPRESERVED
T INORGANIC CHEMICA METALS
P'i' INORGANIC CHEMICAL ME
PT CYANIDE
PT NITROGEN FORMS
PT TO AL SULFIDE
2oz ITRATE / NITRIT
I OOmI TOTAL ORGANIC CARBON
T TOX
PT CHEMICAL OXYGEN DERIAND
P A PHENOLICS
40m1 VOA VIAL TRAVEL BLANK
40m1 VOA VIAL ' ' ' ' ' ' ' ~ ' ~ ' ~ ' ~ '
T EPA 413.1 41 JZ 418.1
PT ODOR
RADIOLOGICAL
BACTERIOLOGICAL
40 m VOA VIAL- 504 i
T EPA 508/608/8080
EPA SI5.1 5
T EPA 525
T EPA 525 TRAVEL BLANK
{90m1 EPA 547
100m1 EPA 531.1
EPA 548
T EPA 549
T EP 632
T EP 8015h1
T A/ C
T AMDER
8 Z. JAR
32 02. JAR -
OILSI,EEVE ,
PcB vlAl.
PLASTIC DAC
FERROUSIRUN
ENCORE
Comments: ~.o fla+-c_ r3y~~. i°"t"~Q
Sample Numbering Completed Bv: C ~~ Dete/Time: w/ Gt't Z.,.a~ a
LABORATORIES, INC.
D & J Construction Project: Soii Samples - D'
3534-A Gilmore Ave Project Number: Shell Station on White Lane
Bakersfield CA, 93308 Project Manager: Jerry Hale Reported: 11/08/06 13:02
Laboratory /Client Sample Cross Reference
Laboratory Client Sample Information
0611114.01 COC Number: 28613 Receive Date: 10/24!06 12:20 Waste Type:
Project Number: --- Sampling Date: 10/24/06 10:20
Sampling Location: --- Sample Depth: --
Sampling Point: Waste Oil Tank 2 Ft Sample Matrix: Solids
Sampled By: Jerry Mason
0611114.02 COC Number: 28613 Receive Date: 10/24/06 12:20 Waste Type:
Project Number: --- Sampling Date: 10!24!06 10:50
Sampling Location: --- Sampee Depth: ---
Sampling Point: Waste Oil Tank Eft Sample Matrix: Solids
Sampled By: Mike Graham
0611114-03 COC Number: 28613 Receive Date: 10/24/06 12:20 Waste Type:
Project Number: --- Sampling Date: 10/24/06 10:25
Sampling Locatian: -- Sample Depth: ---
Sampling Point: East Dispenser 2ft Sample Matrix: Solids
Sampled By: Jerry Mason
0611114-04 COC Number: 28613 Receive Date: 10/24/06 12:20 Waste Type:
Project Number: --- Sampling Date: 10/24/06 10:45
Sampling Location: --- Sample Depth: ---
Sampling Point: East Dispenser Eft Sample Matrix: Solids
Sampled By: Jerry Mason
0611114-05 COC Number: 28613 Receive Date: 10/24/06 12:20 Waste Type:
Project Number: --- Sampling Date: 10/24/06 11:05
Sampling Location: --- Sample Depth: ---
Sampling. Point: South Dispenser 2ft Sample Matrix: Solids
Sampled By: Mike Graham
BC Laboratories The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entire
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation„ detachment or third party interpretation.
4100 Atlas Court • Bakersfield, CA 93308 • (661) 327-4911 • FAX (661 } 327-1918 • www.bclabs.com Page 1 of
'' ~~ LABORATORIES, INC.
D & J Construction Project: Soii Samples -'D'
3534-A Gilmore Ave Project Number: Shell Station on White Lane
Bakersfield CA, 93308 Project Manager: Jerry Hale Reported: 11/08/06 13:02
Laboratory /Client Sample Cross Reference
iraboratory Client Sample Information
0611114.06 COC Number: 28613 Receive Date: 10/24/06 12:20 Waste Type:
Project Number: --- Sampling Date: 10/24/05 11:15
Sampling Location: --- Sample Depth: ---
Sampling Point: South Dispenser Eft Sample Matrix: Solids
Sampled By: Mike Graham
0611114A7 COC Number: 28613 Receive Date: 10/24/06 12:20 Waste Type:
Project Number: --- Sampling Date: 10/24/06 10:55
Sampling Location: --- Sample Depth: ---
Sampling Point: North Dispenser 2ft Sample Matrix: Solids
Sampled By: Jerry Mason
0611114.08
i COC Number: 28613 Receive Date: 10/24/06 12:20 Waste Type:
~ Project Number: -- Sampling Date: 10/24/06 11:00
Sampling Location: --- Sample Depth: ---
Sampling Point: North Dispenser Eft Sample Matrix: Solids
Sampled By: Mike Graham
BC Laboratories The results fn this report apply to the samples analyzed in accordance with the chain of custody document. This ana[ytica! report must be reproduced !n i!s a»tirery.
' All results listed in this report aze for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation„ detachment or third party interpretation.
4100 Atlas Court • Bakersfield, CA 93308 • (661) 327-4911 • FAX (661) 327-1918 • www.bclabs.eom Pege 2 of 23
~.. LABORATORIES, INC.
D & J Construction Project: Soil Samples -'D'
3534-A Gilmore Ave Project Number: Shep Station on White Lane
Bakersfield CA, 93308 Project Manager: Jerry Hale Reported: 11/08/06 13:02
- ~ EPA Method 1664
BCL Sam le ID: 0611114-01 Client Sample Name: Waste Oil Tank 2 Ft, 10/24/2006 10:20:OOAM, Jerry Mason
rep un nstru-
Constituent Result Units PQL MDL Method Date Date/Ttme Analyst ment ID Dilution Batch 1D Bias Quais
Oil and Grease ND mg/kg 50 EPA-1664H 11/06/06 11/06/08 08:30 JAK MAN-SV - 1 BPK0256 ND
BC Laboratories The results in this report apply to the samples analyzed in accordance tvith the chain of custody document.- This analytlca! report must be reproduced in its enure
Atl results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation„ detachment or third party interpretation.
4100 Atlas Court • Bakersfield, CA 93308 • (661) 327-4911 • FAX (661) 327-1918 • www.bciabs.com Page3 0.
~. LABORATORIES, INC.
D & J Construction Project: Soil Samples -'D'
3534-A Gilmore Ave Project Number: Shell Station on White Lane
Bakersfield CA, 93308 Project Manager: Jerry Hale Reported: 11/08/06 13:02
Total Concentrations (TTLC}
BCL• Sam le ID: 0611114-01 Client Sample Name: Waste Oil Tank 2 Ft, 10/24/2006 10:20:OOAM, Jerry Mason
rep Run nstru- a
Constituent Result Units PQL MDL Method Date Date/Tlme Analyst ment ID Dilution Batch ID Btas Quaffs
Antimony ND mglkg 5.0 EPA-6010811/02/06 11/06/06 17:03 JCC TJA61E 0.98 BPK0095 ND
Arsenic 3.6 mg/kg 0.50 EPA-60108 11/02/06 11/02/06 23:57 JCC TJA61E 0.98 BPK0095 ND
Barium 95 mg/kg 0.50 EPA-60108 11/02/06 11/02/06 23:57 JCC TJA61E 0.98 BPK0095 ND
Beryllium ND mg/kg 0.50 EPA-60108 11/02/06 11/02/06 23:57 JCC TJA61E 0.98 BPK0095 ND
Cadmium ND mg/kg 0.50 EPA-60108 11/02/06 11/02/06 23:57 JCC TJA61E 0.98 BPK0095 ND
Chromium 8.2 mg/kg 0.50 EPA-60108 11/02/06 11/02/06 23:57 JCC TJA61E 0.88 BPK0095 ND
Cobalt 5.4 mg/kg 2.5 EPA-60108 11/02/06 11/02/06 23:57 JCC TJA61E 0.98 BPK0095 ND
Copper 5.6 mg/kg 1.0 EPA-60108 11/02/06 11/02/06 23:57 JCC TJA61E 0.98 BPK0095 ND
Lead 3.3 mg/kg 2.5 EPA-60108 11/02/06 11/02/06 23:57 JCC TJA61E 0.98 BPK0095 ND
Mercury ND mg/kg 0.16 EPA-7471A 10/31/06 11/02/06 10:12 PRA CETACI 1.01 BPJ1785 ND
Molybdenum ND mg/kg 2.5 EPA-60108 11/02/06 11/02/06 23:57 JCC TJA61E 0.98 BPK0095 ND
Nickel 4.9 mg/kg 0.50 EPA-60108 11/02/06 11/02/06 23:57 JCC TJA61E 0.98 BPK0095 ND
Selenium ND mglkg 0.50 EPA-6010811/02/06 11/06/0617:03 JCC TJA61E 0.98 BPK0095 ND
Silver ND mg/kg 0.50 EPA-60108 11/02/06 11/02/06 23:57 JCC TJA61E 0.98 BPK0095 ND
Thallium ND mg/kg 5.0 EPA-60108 11/02/06 11/02/06 23:57 JCC TJA61E 0.98 BPK0095 ND
Vanadium 30 mg/kg 0.50 EPA-60108 11/02/06 11/02/06 23:57 JCC TJA61E 0.98 BPK0095 ND
Zinc 40 mg/kg 2.5 EPA-60108 11/02/06 11/02/06 23:57 JCC TJA61E 0.98 BPK0095 ND
BC Laboratories The results in this report apply to the samples analyzed in accordance with [he chain of custody document. This analytical report must be reproduced in its entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation,, detachment or third party interpretation.
4100 Atlas Court • Bakersfield, CA 93308 ~ (661) 327-4911 • FAX (661) 327-1918 • www.bclabs.com Page4 of23
~, LABORATORIES, INC.
D & J Construction Project: Soil Samples -'D'
3534-A Gilmore Ave Project Number: Shell Station on White Lane
Bakersfield CA, 93308 Project Manager: Jerry Hale Reported: 11/08/06 13:0:
EPA Method 1664
BCL Sample ID: 0611114-02 Client Sample Name: Waste Oil Tank Eft, 10/24/2006 10:50:OOAM, Mike Graham
' Prep Run nstru- Q a
COnStitUent ReSUIt Units PQL MDL Method Date Date/Time Analyst ment ID Dilution Batch ID Bias Quals
Oil and Grease ND mg/kg 50 EPA-1664H 11/06/06 11106/06 08:30 JAK MAN-SV 1 BPK0256 ND
BC Laboratories The results in this report apply to the samples analyzed in accordance tvith the chain oJcustody document. This analytical report muss be reproduced in !ts entin
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation„ detachment or third party interpretation.
4100 Atlas Court • Bakersfield, CA 93308 • (661) 327-4911 • FAX (661) 327-1918 • www,bclabs.com Page 5 0
LABORATORIES, INC.
D & J Construction Project: ,Soil Samples -'D'
3534-A Gilmore Ave Project Number: Shell Station on White Lane
Bakersfield CA, 93308 Project Manager: Jerry Hale Reported: 11/08/06 13:02
. Total Concentrations (TTLC)
ICL Sample ID: 0611114-02 Client Sample Name: Waste Oil Tank Eft, 10/24/2006 10:50:OOAM, Mike Graham
• rep Run nstru- B a
:OnStitUent ReSUIt Units PQL MDL Method Date Date/Tlme Analyst ment tD Dllutlon Batch ID Blas Quals
Antimony ND mg/kg 5.0 EPA-6010811/02/06 11/06/0617:27 JCC TJA61E 0.97 BPK0095 ND
Arsenic 1.6 mg/kg 0.50 EPA-60108 11/02/06 11/03/06 00:21 JCC TJA61E = 0.97 BPK0095 ND
Barium 43 mg/kg 0.50 EPA-60108 11/02/06 11/03/06 00:21 JCC TJA61E 0.97 BPK0095 ND
Beryllium ND mglkg 0.50 EPA-60108 11/02/06 11!03!06 00:21 JCC TJA61 E 0.97 BPK0095 ND
~ Cadmium ND mg/kg 0.50 EPA-60108 11/02/06 11/03/06 00:21 JCC TJA61E 0.97 BPK0095 ND
Chromium 4.3 mglkg 0.50 EPA-60108 11/02/06 11!03/06 00:21 JCC TJA61E 0.97 BPK0095 ND
Cobalt 3.3 mg/kg 2.5 EPA-60108 11/02/06 11/03/06 00:21 JCC TJA61E 0.97 BPK0095 ND
Copper 3.0 mg/kg 1.0 EPA-60108 11/02/06 11!03/06 00:21 JCC TJA61E 0.97 BPK0095 ND
', Leatl ND mg/kg 2.5 EPA-60108 19/02/06 11/03/08 00:21 JCC TJA61E 0.97 BPK0095 ND
' Mercury
1~ ND mg/kg 0.16 EPA-7471A 10/31!06 11/02/06 10:14 PRA CETACI 1.01 BPJ1785 ND
' Morybdenum ND mgikg 2.5 EPA-60108 11/02/06 11/03/06 00:21 JCC TJA61E 0.97 BPK0095 ND
'~ Nickel 2.6 mg/kg 0.50 EPA-60108 11/02/06 11/03/06 00:21 JCC TJA61E 0.97 BPK0095 ND
Selenium ND mg/kg 0.50 EPA~010811/02/06 11/06/0617:27 JCC TJA61E 0.97 BPK0095 ND
'~ S(iver ND mglkg 0.50 EPA-60108 11/02/06 11/03/06 00:21 JCC TJA61E 0.97 BPKQ095 ND
Thallium ND mg/kg 5.0 EPA-60108 11/02/06 11/03/06 00:21 JCC TJA61E 0.97 BPK0095 ND
' Vanadium 18 mg/kg 0.50 EPA-60108 11/02/06 11/03!06 00:21 JCC TJA61E 0.97 BPK0095 ND
Zinc 22 mg/kg 2.5 EPA-60108 11/02/06 11/03/06 00:21 JCC TJA61E 0.97 BPK0095 ND
BC Laboratories The results in this report apply Jo the samples analyzed rn accordance with the chain of custody document. This analytical report must be reproduced in l~s entirety.
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, sepazation„ detachment or third party interpretation.
4100 Atlas Court • Bakersfield, CA 93308 • (661) 327-4911 • FAX (661) 327-1918 • www.bclabs.com Page 6 of23
~. LABORATORIES, INC.
D & J Construction
3534-A Gilmore Ave
Bakersfield CA, 93308 Project:
Project Number:
Project Manager: Soil Samples -'D'
Shell Station on White Lane
Jerry Hale
Reported: 11/08/06 13:02
Volatile Organic Analysis (EPA Method 8260)
BCL Sample ID: 0611114-03 Client Sample Name: East Dispenser 2ft, 10/24/2006 10:25:OOAM, Jerry Mason
COtlStitUent
ReSUit
Units
PQL MDL
Method rep un
Date DatelTime
Analyst nstru-
ment ID Dilution
Batch ID a
Bias 4uals
Benzene ND mg/kg 0.0050 EPA-8260 10/24/06 10/25/06 07:57 DRS MS-V3 1 BPJ1423 ND
Ethylbenzene ND mg/kg 0.0050 EPA-8260 10/24/06 10/25/06 07:57 DRS MS-V3 1 BPJ1423 ND
Methyl t-butyl ether ND mg/kg 0.0050' EPA-8260 10/24!06 10/25/06 07:57 DRS MS-V3 1 ~ BPJ1423 ND
Toluene ND mg/kg 0.0050 EPA-8260 10/24/06 10/25/06 07:57 DRS MS-V3 1 BPJ1423 ND
Total Xylenes ND mg/kg 0.010 EPA-8260 10/24/06 10/25/06 07:57 DRS MS-V3 1 BPJ1423 ND
p- & m-Xylenes ND mg/kg 0.0050 EPA-8260 .10/24/06 10!25/06 07:57 DRS MS-V3 1 BPJ1423 ND
o-Xylene ND mg/kg 0.0050 EPA-8260 10/24/06 10/25/06 07:57 DRS MS-V3 1 BPJ1423 ND
Totat Purgeabie Petroleum
Hydrocarbons 23 mg/kg 5.0 EPA-8260 10/25/06 10/26/06 05:04 DRS MS-V3 25 BPJ1423 ND A01
1,2-Dichloroethane-d4 (Surrogate) 96.9 % 70 -121 (LCL -UCL) EPA-8260 10/25/06 10/26/06 05:04 DRS MS-V3 25 BPJ1423
1,2-Dichloroethane-d4 (Surrogate) 98.5 % 70 -121 (LCL -UCL) EPA-8260 10/24/06 10/25/06 07:57 DRS MS-V3 1 BPJ1423
Toluene-d8 (Surrogate) 97.4 % 81 -117 (LCL -UCL) EPA-8260 10/25!06 10/26/06 05:04 DRS MS-V3 25 BPJ1423
Toluene-d8 (Surrogate) 96.8 % 81 -117 (LCL -UCL) EPA-8260 10/24/06 10/25/06 07:57 DRS MS-V3 1 BP,11423
4-Btomofluorobenzene (Surrogate) 93.3 % 74 -121 (LCL -UCL) EPA-8260 10/24/06 10/25/06 07:57 DRS MS-V3 1 BPJ1423
4-Bromofluorobenzene (Surrogate) 89.0 % 74 -121 (LCL -UCL) EPA-8260 10/25!06 10/26/06 05:04 DRS MS-V3 25 BPJ1423
BC Laboratories The resu/~s in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in fts entire
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation„ detachment or third party interpretation.
4100 Attas Court • Bakersfield, CA 93308 • (661) 327-4911 • FAX (661) 327-1918 • www.bclabs.com Page 7 of
LABORATORIES, INC.
D & J Construction
3534-A Gilmore Ave
Bakersfield CA, 93308 ~ Project:
Project Number:
Project Manager: Soil Samples -'D'
Shell Station on White Lane
Jerry Hale
Reported: 1 t/08/06 13:02
Volatile Organic Analysis (EPA Method 8260)
BCL Sample ID: 0611114-04 Client Sample Name: -East Dispenser Eft, 10/24/2006 10:45:OOAM, Jerry Mason
Constituent
Result
Units
PQL MDL Method rep un
Date DateiTime
Analyst nstru-
meat ID Dilution
Batch ID B a
Bias Quals
Benzene ND mg/kg 0.0050 EPA-8260 10/24/06 10/25/06 07:30 DRS MS-V3 1 BPJ1423 ND
Ethylbenzene ND mg/kg 0.0050 EPA-8260 10/24/06 10/25/06 07:30 DRS MS-V3 1 BPJ1423 ND
Methyl t-butyl ether ND mg/kg 0:0050 EPA-8260 10/24/06 10/25/06 07:30 ORS MS-V3 1 ~ BPJ1423 ND
Toluene ND mg/kg 0.0050 EPA-8260 10!24/06 10/25/06 07:30 DRS MS-V3 1 BPJ1423 ND
Total Xylenes ND mglkg 0.010 EPA-8280 10/24/06 10/25/06 07:30 DRS MS-V3 1 BPJ1423 ND
p- 8~ m-Xylenes ND mg/kg 0.0050 EPA-8260 10/24/06 10/25/06 07:30 DRS MS-V3 1 BPJ1423 ND
o-Xylene ND mg/kg 0.0050 EPA-8260 10/24/06 10/25/06 07:30 DRS MS-V3 1 BPJ1423 ND
Total Purgeable Petroleum
Hydrocarbons 1.4 mg/kg 0.20 EPA-8260 10!24/06 10/25/06 07:30 DRS MS-V3 1 BPJ1423 ND
1,2-Dichloroethane-d4 (Surrogate) _
101
%
70 -121 (LCL -UCL) EPA-8260
10/24/06 10/25/06 07:30
DRS
MS-V3
1
BPJ1423
Toluene-d8 (Surrogate) 91.0 % 81 -117 (LCL -UCL) EPA-8260 10/24/06 10/25/06 07:30 DRS MS-V3 1 BPJ1423
4-Bromofluorobenzene (Surrogate) 92.7 % 74 -121 (LCL -UCL) EPA-8260 10/24/06 10/25/06 07:30 DRS MS-V3 1 BPJ1423
BC Laboratories The results in this report apply to the samples analyzed in accordance with the chain of custody documenl. This analytical report muse be reproduced in its entire
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, sepazation„ detachment or third party interpretation.
4100 Atlas Court • Bakersfield, CA 93308 • (661) 327-4911 • FAX (661) 327-1918 • www.bclabs.com Page 8 of
~. LABORATORIES, INC.
D & J Construction
3534-A Gilmore Ave
Bakersfield CA, 93308 Project:
Project Number:
Project Manager: Soil Samples -'D'
Shell Station on White Lane
Jerry Hale
Reported: l 1/08/06 13:
Volatile Organic Analysis (EPA Method 8260)
BCL Sample.ID: 0611114-05 Client Sample Name: South Dispenser 2ft, 1.0/24/2006 11:05:OOAM, Mike Graham
Constituent
Result
Units
PQL MDL Method nap un
Date Date/Time
Analyst Instru-
meet ID Dllutlon
Batch ID
Blas Quals
Benzene ND mg/kg 0.0050 EPA-8260 10/24/06 10/25/06 07:04 DRS MS-V3 1 BPJ1423 ND
Ethylbenzene ND mg/kg 0.0050 EPA-8260 10/24/06 10/25/06 07:04 DRS MS-V3 1 BPJ1423 ND
Methyl t-butyl ether ND mg/kg 0.0050 EPA-8260 10/24/06 10/25/06 07:04 DR5 MS-V3 1 BPJ1423 ND "
Toluene ND " mg/kg 0.0050 EPA-8260 10/24/06 10/25/06 07:04 DRS MS-V3 1 BPJ1423 ND
Total Xylenes ND mg/kg 0.010 EPA-8260 10/24/06 10/25/06 07:04 DRS MS-V3 1 BPJ1423 ND
p- 8 m-Xylenes ND mg/kg 0.0050 EPA-8260 10124/06 10/25/Q6 07:04 DRS MS-V3 1 BPJ1423 ND
o-Xylene ND mg/kg 0.0050 EPA-8260 10/24/06 10/25/06 07:04 , DRS MS-V3 1 BPJ1423 ND
Total Purgeable Petroleum
Hydrocarbons ND mg/kg 0.20 EPA-8260 10124/06 10/25/06 07:04 DRS MS-V3 1 BPJ1423 ND
_ __
1,2-Dlchloroethane-d4 (Surrogate} 106 % 70 -121 (LCL -UCL} EPA-8260 10/24/06 10/25/06 07:04 DRS MS-V3 1 BPJ1423
Toluene-d8 (Surrogate) 96.4 % 81 • 117 (LCL -UCL) EPA-8260 10/24/06 10/25/06 07:04 DRS MS-V3 1 BPJ1423
4-Bromofluorobenzene (Surrogate) 95.6 % 74 -121 (LCL -UCL) EPA-8260 10/24/06 10/25/06 07:04 DRS MS-V3 1 BPJ1423
BC Laboratories The resu/~s in thts report apply to the samples analyzed in accordance wtth the chain of custody document. This arralyllcal report must be reproduced in tts er
All results listed in this report are for the exclusive use of the submitting party. BC [,aboratories, lnc. assumes no responsibility for report alteration, separation„ detachment or third parry interpretation.
4100 Atlas Court • Bakersfield, CA 93308 • (661) 327-4911 • FAX (661) 327-1918 • www.bclabs.com Page
~, LABORATORIES, INC.
D & J Construction
3534-A Gilmore Ave
Bakersfield CA, 93308 Project:
Project Number:
Project Manager: Soil Samples -'D'
Shell Station on White Lane
Jerry Hale
Reported: 11 /08/06 13:~
Volatile Organic Analysis (EPA Method 8260)
BCL Sam le ID: 0611114-06 Client Sample Name: South Dispenser Eft, 10/24/2006 11:15:OOAM, Mike Graham
COnstituent
Result
UnItS
PQL MDL Method rep un
Date DatelTime
Analyst ns ru-
ment iD Dilution
Batch iD
Bias Quals
Beniene ND mglkg 0.0050 EPA-8260 10/24/06 10!25/06 06:37 DRS MS-V3 1 BPJ1423 ND
Ethyibenzene ND mglkg 0.0050 EPA-8260 10/24/06 10/25/06 06:37 DRS MS-V3 1 BPJ1423 ND
Methyl t-butyl ether ND mg/kg 0.0050 EPA-8260 10/24/06 10/25/06 06:37 DRS MS-V3 1 BPJ1423 ND
Toluene ND mg/kg 0.0050 EPA-8260 10!24/06 10/25/06 06:37 DRS MS-V3 1 BPJ1423 ND
Total Xylenes ND mg/kg 0.010 EPA-8260 10/24/06 10!25/06 06:37 DRS MS-V3 1 BPJ1423 ND
p- 8 m-Xylenes ND mg/kg 0.0050 EPA-8260 10!24106 10!25!06 06:37 DRS MS-V3 1 BPJ1423 ND
o-Xylene ND mg/kg 0.0050 .EPA-8260 10/24/06 10/25/06 06:37 DRS MS-V3 1 BPJ1423 ND
Total Purgeable Petroleum
Hydrocarbons ND mg/kg 0.20 EPA-8260 10/24/06 10/25/06 06:37 DRS MS-V3 1 BPJ1423 ND
1,2•Dichloroethane-d4 (Surrogate) 107 % 70 -121 (LCL -UCL) EPA-8260 10!24/06 10/25/06 06:37 DRS MS-V3 1 BPJ1423
Toluene-d8 (Surrogate) 103 % 81 -117 (LCL -UCL) EPA-8260 10!24/06 10/25!06 06:37 DRS MS-V3 1 BPJ1423
4-Bromofluorobenzene {Surrogate) 93.0 % 74 -121 (LCL -UCL) EPA-8260 10/24/06 10/25/06 06:37 DRS MS-V3 1 BPJ1423
BC Laboratories The results in this report apply to the samples analyzed in accordance tvith the chain of custody document. This analytical report must be reproduced in its entire
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation„ detachment or third party interpretation.
4100 Atlas Court • Bakersfield, CA 93308 • (661) 327-4911 • FAX (661) 327-1918 • www.bclabs.com Page 10 of
~. LABORATORIES, INC.
D & J Construction
3534-A Gilmore Ave
Bakersfield CA, 93308 Project:
Project Number:
Project Manager: Soil Samples -'D'
Shell Station on White Lane
Berry Hale
Reported: 11/08/06 13:0:
Volatile Organic Analysis EPA Method 8260)
BCL Sample ID: 0611114-07 Client Sample Name: North Dispenser 2ft, 10/24/2006 10:55:OOAM, Jerry Mason
Constituent
Result
Units
PQL MDL Method rep un
~~ Date/Tlme
Analyst nstru-
ment ID Dltutlon
Batch ID B
Blas quals
Benzene ND mg/kg 0.0050 EPA-8260 10/24/06 10/25!06 06:11 DRS MS-V3 1 BPJ1423 ND
Ethylbenzene ND mg/kg 0.0050 EPA-8260 10/24/06 10/25/06 06:11 DRS MS-V3 1 BPJ1423 ND
Methyl t-butyl ether ND mg/kg 0.0050 EPA-8260 10/24/06 10/25/06 06:11 DRS MS-V3 1' BPJ1423 ND
Toluene ND mglkg 0.0050 EPA-8260 10/24/06 10/25/08 06:11 _ DRS MS-V3 1 BPJ1423 ND
Total Xylenes ND mg/kg 0.010 EPA-8260 10/24!06 10/25/06 06:11 DRS MS-V3 1 BPJ1423 ND
p- & m-Xylenes ND mg/kg 0.0050 EPA-8260 10/24/06 10/25/06 06:11 DRS MS-V3 1 BPJ1423 ND
o-Xylene ND mg/kg 0.0050 EPA-8260 10/24/06 10/25/06 06:11 DRS MS-V3 1 BPJ1423 ND
Total Purgeable Petroleum
Hydrocarbons ND mg/kg 0.20 EPA-8260 10/24/06 10/25/06 06:11 DRS MS-V3 1 BPJ1423 ND
1,2=Dichloroethane-d4 (Surrogate) 101 % 70 -121 (LCL -UCL) EPA-8260 10/24/06 10/25!06 06:11 DRS MS-V3 1 BPJ1423
Toluene-d8 (Surrogate) 95.7 % 81 -117 (LCL -UCL) EPA-8260 10/24/06 10/25/06 06:11 DRS MS-V3 1 BPJ1423
4-Bromofluorobenzene (Surrogate} 88.4 % 74 -121 (LCL -UCL) EPA-8260 10/24/06 10/25/06 06:11 DRS MS-V3 1 BPJ1423
BC Laboratories The results to this report apply to the samples analyzed in accordance with the chain of custody document. This analyttcaJ report must be reproduced in its entirE
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation„ detachment or third party interpretation.
4100 Atlas Court • Bakersfield, CA 93308 • (66t) 327-4911 • FAX (661) 327-1918 • www.bclabs.com page 1 I o.
LABORATORIES, INC.
D & J Construction Project: Soil Samp}es -'D'
3534-A Gilmore Ave Project Number: Shell Station on White Lane
Bakersfield CA, 93308 Project Manager: Jerry Hale Reported: 11/08/06 13:02
Volatile Organic Analysis (EPA Method 8260)
Benzene ND mg/kg 0.0050 EPA-8260 10/24!06 10!25/06 05:45 DRS MS-V3 1 BPJ1423 ND
Ethylbenzene ND mg/kg 0.0050 EPA-8260 10/24/06 10/25/08 05:45 DRS MS-V3 1 BPJ1423 ND
Methyl t-butyl ether ND mg/kg 0.0050 EPA-8260 10/24/06 14/25106 05:45 DRS MS-V3 1 BPJ1423 ND
Toluene ND mg/kg 0.0050 EPA-8260 10/24/06 10/25/06 05:45 DRS MS-V3 1 BPJ1423 ND
Total Xylenes ND mglkg 0.010 EPA-8260 10/24/06 10/25/06 05:45 DRS MS-V3 1 BPJ1423 ND
p- & m-Xylenes ND mglkg 0.0050 EPA-8260 10/24/06 10/25/06 05:45 DRS MS-V3 1 BPJ1423 ND
o-Xylene ND mg/kg 0.0050 EPA-8260 10124/06 10/25/06 05:45 DRS MS-V3 1 BPJ1423 ND
Total Purgeable Petroleum
Hydrocarbons ND mg/kg 0.20 EPA-8260 10/24/06 10/25/06 05:45 DRS MS-V3 1 BPJ1423 ND
1,2-Dichloroethane-d4 (Surrogate) 101 % 70 -121 (LCL -UCL) EPA-8260 10/24/06 10!25/06 05:45 DRS MS-V3 1 BPJ1423
Toluene-d8 (Surrogate) 99.6 % 81 -117 (LCL -UCL) EPA-8260 10/24/06 10/25/06 05:45 DRS MS-V3 1 BPJ1423
4-Bromoftuorobenzene (Surrogate) 86.9 % 74 -121 (LCL -UCL) EPA-8260 10/24/06 10/25/06 05:45 DRS MS-V3 1 BPJ1423
BC Laboratories The results in this report apply to the samples analyzed in accordance tvJ1h the chain of custody document. This analytical report must be reproduced in Its enllrery.
All resits listed in this report are for the exclusive use of the submitting party. BC Laboratories, inc. assumes no responsibility for report alicrtttion, separation„ detachment or third party interpretation.
. LABORATORIES, INC.
D & J Construction Project: Soil Samples -'D'
3534-A Gilmore Ave Project Number: Shell Station on White Lane
Bakersfield CA, 93308 Project Manager: Jeny Hale Reported: 11/08/06 13:0:
Volatile Organic Analysis (EPA Method 8260)
Quality Control Report -Precision & Acc uracy
Control Limits
Source Source Spike Percent Percent
Constituent Batch ID QC Sam le T Sam le ID Result Result Added Units RPD Recove RPD Recove Lab Qua
Benzene BPJ1423 Matrix Spike 0610676-20 ND 0.12362 0.12500 mg/kg 98.9 70 -130
Matrix Spike Duplicate 061,0676-20 ~ ND 0.12010 0.12500 mg/kg 2.87 96.1 20 70 -130
Toluene BPJ1423 Matrix Spike 0610676-20 ND 0.11844 0.12500 mglkg 94.8 70 -130
Matrix Spike Duplicate 0610676-20 ND 0.12385 0.12500 mg/kg 4.44 99.1 20 70 -130 .
1,2-Dichloroethane-d4 (Surrogate) BPJ1423 Matrix Spike 0610676-20 ND 0.049780 0.050000 mg/kg 99.6 70 -121
Matrix Spike Duplicate 0610676-20 ND 0.048580 0.050000 mglkg 97.2 70 - i21
Toluene-d8 (Surrogate) BPJ1423 Matrix Spike 0610676-20 ND 0.048930 0.050000 mg/kg 97.9 81 -117
Matrix Spike Duplicate 0610676-20 ND 0.049410 0.050000 mg/kg 98.8 81 -117
4-Bromofluorobenzene (Surrogate) BPJ1423 Matrix Spike 0610676-20 ND 0.048550 0.050000 mg/kg 97.1 74 -121
Matrix Spike Duplicate 0610676-20 ND 0.049430 0.050000 mg/kg 98.9 74 - 121
BC Laboratories The results in this repot( apply to the samples analyzed to accordance with the chain of etrstody document. Thfs analytical report must be reproduced in its entire
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation„ detachment or third party interpretation.
4100 Atlas Ctiurt • Bakersfield, CA 93308 • (661) 327-4911 • FAX (661) 327-1918 • www.bclabs.com Page 13 of
LABORATORIES, INC.
D & J Construction Project: Soil Samples -'D'
3534-A Gilmore Ave Project Number: Shell Station on White Lane
Bakersfield CA, 93308 Project Manager: Jerry Hale Reported: 11/08/06 13:02
EPA Method 1664
Quality Control Report -Precision & Accuracy
Control Limits
Source Source Spike Percent Percent
Constituent Batch ID QC Sam le T e Sam le ID Result Result Added Units RPD Recove RPD ~ Recove Lab Quals
Oil and Grease BPK0256 Duplicate 0811114-02 ND ND mg/kg 30
Matrix Spike 0610676-34 ND 598.00 784.00 mglkg 76.3 56 -111
Matrix Spike Duplicate 0610676.34 ND 820.00 784.00 mg/kg 31.7 105 30 56 -111 Q02
BC Laboratories 77te results in lhts report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
ett .ec,arc NSrFd .n this re»or< gre fnr rhr exclusive use nrthe submitting narly. AC Laboratories. Inc. assumes no responsibility for report alteration, separation„ detachment or third party interpretation.
~. LABORATORIES, INC.
D & J Construction Project: Soil Samples -'D'
3534-A Gilmore Ave Project Number: Shell Station on White Lane
Bakersfield CA, 93308 Project Manager: Jerry Hale Reported: 11/08/06 13:0
Total Concentrations (TTLC)
Quality Control Report -Precision & Accu racy
Control Limits
Source Source Spike Percent Peroent
Constituent Batch ID QC Sam le T e Sam le ID Result Result Added Units RPD Recove RPD ~ Recove Lab Qu:
Mercury BPJ1785 Duplicate 0611102-01 ND ND mg/kg 20
Matrix Spike 0611102-01 ND 0.83650 0.83333 mg/kg 100 85 -115
Matrix Spike Duplicate 0611102-01 ND 0.73633 0.83333 mg/kg 12.3 88.4 20 85 -115
Antimony BPK0095 Duplicate 0611114-01 0.92157 0.66176 mg/kg 32.8 20 A02
Matrix Spike 0611114-01 0.92157 57.304 98.039 mg/kg 57.5 16 -119
Matrix Spike Duplicate 0611114-01 0.92157 53.529 98.039 mg/kg 6.83 53.7 20 16 -119
Arsenic BPK0095 Duplicate 0611114-01 3.5931 3.7647 mg/kg 4.66 20
Matrix Spike 0611114-01 3.5931 7.9020 4.9020 mg/kg 87.9 75 -125
Matrix Spike Duplicate 0611114-01 3.5931 7.7059 4.9020 mg/kg 4.66 83.9 20 75 -125
Barium BPK0095 Duplicate 0611114-01 95.147 93.088 mg/kg 2.19 20
Matrix Spike 0611114-01 95.147 195.44 98.039 mg/kg 102 75 -125
Matrix Spike Duplicate 0611114-01 95.147 188.97 98.039 mg/kg 6.37 95.7 20 75 -125
Beryllium BPK0095 Duplicate 0611114-01 0.24510 0.25000 mg/kg 1.98 20
Matrix Spike 0611114-01 0.24510 10.642 9.8039 mg/kg 106 75 -125
Matrix Spike Duplicate 0611114-01 0.24510 10.578 9.8039 mg/kg 0.948 105 20 75 -125
Cadmium BPK0095 Duplicate 0611114-01 ND ND mg/kg 20
Matrix Spike 0611114-01 ND 9.9510 9.8039 mg/kg 102 75 -125
Matrix Spike Duplicate 0611114-01 ND 9.9216 9.8039 mg/kg 0.985 101 20 75 -125
Chromium BPK0095 Duplicate 0611114-01 8.2402 8.3039 mg/kg 0.770 20'
Matrix Spike 0611114-01 8.2402 103.87 98.039 mg/kg 97.5 75 -125
Matrix Spike Duplicate 0611114-01 8.2402 103.77 98.039 mg/kg 0.103 97.4 20 75 -125
Cobalt BPK0095 Duplicate 0611114-01 5.3873 5.3676 mg/kg 0.366 20
Matrix Spike 0611114-01 5.3873 106.91 98.039 mg/kg 104 75 - 125
Matrix Spike Duplicate 0611114-01 5.3873 106.42 98.039 mglkg 0.966 103 20 75 -125
Copper BPK0095 Duplicate 0611114-01 5.5735 5.2402 mg/kg 6.16- 20
Matrix Spike 0611114-01 5.5735 106.81 98.039 mg/kg _ 103 75 -125
Matrix Spike Duplicate 0611114-01 5.5735 105.93 98.039 mg/kg 0.976 102 20 75 - 125
BC Laboratories The results to rhts report apply ro the samples analyzed in accordance tvJrh the chain of custody document. Th1s analytical report must be reproduced 1n lJS enlrn
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation„ detachment or third party interpretation.
4100 Atlas Court • Bakersfield, CA 93308 • (661) 327-4911 • FAX (661) 327-1918 • www.bclabs.com Page 15 0
~. LABORATORIES, INC.
D & J Construction Project: Soil Samples -'D'
3534-A Gilmore Ave Project Number: Shell Station on White Lane
Bakersfield CA, 93308 Project Manager: Jeny Hale Reported: 11/08/06 13:02
Total Concentrations (TTLC)
Quality Control Report -Precision & Accuracy
Control Limits
Source Source Spike Percent ~ Percent
Constituent Batch ID QC Sam 1e T e Sam le ID Result Result Added Units RPD Recove RPD Recove Lab Qua
Lead BPK0095 Duplicate 0611114-01 3.2598 3.0784 mglkg 5.72 20
Matrix Spike 061,1114-01 3.2598 98.333 98.039 mg/kg 97.0 75 -125
Matrix' Spike Duplicate 0611114-01 3.2598 99.853 98.039 mg/kg 1.53 98.5 20 75 -125
Molybdenum BPK0095 Duplicate 0611114-01 0.47549 0.47059 mg/kg 1.04 20
~
Matrix Spike 0611114-01 0.47549 96.324 98.039 mg/kg 97.8 75 -125
Matrix Spike Duplicate 0611114-01 0.47549 95.490 98.039 mg/kg 0.925 96.9 20 75 -125
Nickel BPK0095 Duplicate 0611114-01 4.8873 4.6765 mg/kg 4.41 20
Matrix Spike 0611114-01 4.8873 106.27 98.039 mgikg 103 75 -125
Matrix Spike Duplicate 0611114-01 4.8873 105.64 98.039 mg/kg 0.00 103 20 75 - 125
Selenium BPK0095 Duplicate 0611114-01 ND 0.68627 mg/kg 20
Matrix Spike 0611114-01 ND 5.3137 4.9020 mg/kg 108 ~ 75 -125
Matrix Spike Duplicate 0611114-01 NO 5.6127 4.9020 mg/kg 5.41 114 20 75 -125
Silver BPK0095 Duplicate 0611114-01 ND ND mgikg 20
Matrix Spike 0811114-01 ND 10.078 9.8039 mglkg 103 75 -125
Matrix Spike Duplicate 0611114-01 ND 9.9265 9.8039 mg/kg 1.96 101 20 75 - 125
Thallium BPK0095 Duplicate 0611114-01 ND 0.84804 mg/kg 20
Matrix Spike 0611114-01 ND 99.510 98.039 mg/kg 102 75 -125
Matrix Spike Duplicate 0611114-01 ND 98.725 98.039 mg/kg 0.985 101 20 75 -125
Vanadium BPK0095 Duplicate 0611114-01 29.863 29.613 mglkg 0.841 20
Matrix Spike 0611114-01 29.863 130.00 98.039 mg/kg 102 75 -125
Matrix Spike Duplicate 0611114-01 29.863 128.43 98.039 mg/kg 0.985 101 20 75 -125
Zinc BPK0095 Duplicate 0611114-01 40.500 38.917 mg/kg 3.99 20
Matrix Spike 0611114-01 40.500 137.50 98.039 mg/kg 98.9 75 -125
Matrix Spike Duplicate 0611114-01 40.500 136.47 98.039 mg/kg 1.02 97.9 20 75 - 125
BC Laboratories The results to lhls report apply to the samples analyzed in accordance tvfth the chain of custody document. This analytical report must be reproduced rn its entire
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation„ detachment or third party interpretation.
4100 Atlas Court • Bakersfield, CA 93308 • (661) 327-4911 • FAX (661) 327-1918 • www.bclabs.com Page 16 01
~, LABORATORIES, INC.
D & J Construction Project: Soil Samples -'D'
3534-A Gilmore Ave Project Number: Shell Station on White Lane
Bakersfield CA, 93308 Project Manager: Jerry Hale Reported: 11/08/06 13:02
Volatile Organic Analysis (EPA Method 8260)
Quality Control Report -Laboratory Control Sample
Control Limits
' Spike Percent Percent
Constituent Batch ID QC Sam le ID QC T Result Level PQL Units Recove RPD Recove RPD Lab Quals
Benzene BPJ1423 BPJ1423-BS1 LCS 0.11844 0.12500 0.0050 mg/kg 94.8 70 -130
Toluene BPJ1423 BPJ1423-BS1 LCS 0.12108 0.12500 0.0050 mg/kg 98.9 70 -130
1,2-Dichtoroethane-d4 (Surrogate) BPJ1423 BPJ1423-BS1 LCS 0.047810 0.050000 mg/kg 95.8 70.121
Toluene-d8 (Surrogate) BPJ1423 BPJ1423-BS1 LCS 0.048530 0.050000 mg/kg 97.1 81 -117
4-Bromofluorobenzene (Surrogate) BPJ1423 BPJ1423-BS1 LCS 0.049370 0.050000 mg/kg 98.7 74 -121
BC Laboratories The results in rhrs report apply to the samples analyzed in accordance tvith the chain of custody document. Thls analytical report mtrs! be reproduced in its entirety.
AIi results listed in this report are for the exclusive use of the submitting party. BC Laboratories, [nc. assumes no responsibility for report alteration, separation„ detachment or third party interpretation.
4100 Atlas Court • Bakersfield, CA 93308 • (661) 327-4911 • FAX (661) 327-1918 • www.bclabs.com Page 17 of23
~. LABQRATORIES, INC.
D & J Construction Project: Soil Samples -'D'
3534-A Gilmore Ave Project Number: Shell Station on White Lane
Bakersfield CA, 93308 Project Manager: Jerry Hale ~ Reported: 11/08/06 13:02
EPA Method 1664
Quality Control Report -Laboratory Control Sample
Control Limits
Spike Percent Percent
Constituent Batch ID QC Sam le ID QC T e Result Level PQL Units Recove RPD Recove RPD Lab Quals
OII and Grease BPK0256 BPK0256-BS1 LCS 727.00 784,00 50 mgfkg 92.7 59 -117
BC Laboratories The results in this report apply to the samples analyzed in accordance tvtth the chain of custody document. This analytical report must be reproduced in its entire
All results listed in this report aze for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, sepazation„ detachment or third party interpretation.
4100 Atlas Court • Bakersfield, CA 93308 • (661) 327-4911 • FAX (661) 327-1918 • wv<~w.bclabs.com Page 18 0l
~. LABORATORIES, INC.
D & J Construction Project: Soil Samples -'D' _
3534-A Gilmore Ave -- Project Number: Shell Station on White Lane
Bakersfietd CA, 93308 Project Manager: Jeny Hale Reported 11!08/06 13:02
Total Concentrations (TTLC)
Quality Control Report -Laboratory Control Sample
~_ Control Limits
Spike Percent Percent
Constituent Batch ID QC Sam le ID QC T e Result Level PQL Units Recove RPD Recove RPD Lab Quals
Mercury BPJ1785 BPJ1785-BSi tCS 1.2700 1.5000 0.16 mg/kg 84.7 75-125
Antimony BPK0095 BPK0095-BS2 LCS 1.4450. 1.6362 5.0 mg/kg 88.3 75 -125
Arsenic BPK0095 BPK0095-BS1 LCS 10.710 10.260 0.50 mg/kg 104 75 -125
Barium BPK0095 BPK0095-BS1 LCS 90.850 92.340 0.50 mgikg 98.4 75 -125
Beryllium BPK0095 BPK0095-BS1 LCS 5.7850 5.9400 0.50 mg/kg 97.4 75 -125
Cadmium BPK0095 BPK0095-BS1 LCS 5.5450 5.4540 0.50 mg/kg 102 75 -125
Chromium BPK0095 BPK0095-BS1 LCS 12.760 13.808 0.50 mg/kg 93.8 75 -125
Cobalt BPK0095 BPK0095-BS1 LCS 9.4700 8.8020 2.5 mg/kg 108 75 -125
Copper BPK0095 BPK0095-BS1 LCS 12.465 13.986 1.0 mg/kg 89.1 75 -125
Lead BPK0095 BPK0095-BS1 LCS 11.270 9.5580 2.5 mg/kg 118 75 -125
Molybdenum BPK0095 BPK0095-BS1 LCS 5:6350 5.9400 2.5 mg/kg 94.9 75 -125
Nickel BPK0095 BPK0095-BS1 LCS 11.080 11.394 0.50 mg/kg 97.2 75 -125
Selenium BPK0095 BPK0095-BS2 LCS 5.3300 4.7628 0.50 mg/kg 112 75 -125
Silver BPK0095 BPK0095-BS1 LCS 5.3000 5.2218 0.50 mg/kg 101 75 -125
Thallium BPK0095 BPK0095-BS1 LCS 5.6700 5.0706 5.0 mg/kg 112 75 -125,
Vanadium BPK0095 BPK0095-BS1 LCS 28.590 28.782 0.50 mg/kg 99.3 75 -125
Zinc BPK0095 BPK0095-BS1 LCS 36.130 34.938 2.5 mg/kg 103 75 -125
BC Laboratories The results !n this report apply to the samples analyzed to accordance ivtth the chattt of custody document. This analytical report must be reproduced 1n Its endrery.
en ~rcuUc licrpd in i6ip rPDPA ere for the eXcinaive uce of the snhmittinn nartv. AC L.ahoratnries. inc. assumes no responsibility for report alteration, separation„ detachment or third party interpretation.
_~, LABORATORIES, INC.
D & J Construction Project: Soil Samples -'D'
3534-A Gilmore Ave Project Number: Shell Station on White Lane
Bakersfield CA, 93308 Project Manager: Jerry Hale Reported: 11/08/06 13:'
Volatile Organic Analysis (EPA. Method 8260)
Quality Control Report -Method Blank Analysis
`Constituent Batch ID QC Sample ID MB Result Units PQL MDL Lab Qual
Benzene BPJ1423 BPJ1423-BLK1 ND mglkg 0.0050 0.0015
Ethylbenzene BPJ1423 BPJ1423-BLK1 ND mg/kg 0.0050 0.0012
Methyl t-butyi ether BPJ1423 BPJ1423-BLK1 ND mg/kg 0.0050 0.00051
Toluene BPJ1423 BPJ1423-BLK1 NO mglkg 0.0050 0.0016
Total Xylanes BPJ1423 BPJ1423-BLK1 ND mglkg 0.010 0.0031
p-&m-Xylenes BPJ1423 BPJ1423-BLK1 ND mg/kg 0.0050 0.0022
o-Xylene BPJ1423 BPJ1423-BLK1 ND mg/kg 0.0050 0.00091
Total Purgeable Petroleum Hydrocarbons BPJ1423 BPJ1423-BLK1 ND mg/kg 0.20 0.14
1,2-Dichloroethane-d4 (Surrogate) BPJ1423 BPJ1423-BLK1 105 % 70 -121 (LCL -UCL)
Toluene-d8 (Surrogate) BPJ1423 BPJ1423-BLK1 97.2 °~ 81 -117 (LCL -UCL)
4-Bromofluorobenzene (Surrogate) BPJ1423 BPJ1423-BLK1 90.8 % 74 -121 (LCL -UCL)
BC Laboratories The results fn this report apply 1o the samples analyzed in accordance with the chain ojcuslody document. This analytical report must be reproduced in its entire
All results listed in this report are for the exclusive use of the submitting parry. BC Laboratories, inc. assumes no responsibility for report alteration, separation„ detachment or third party interpretation.
4100 Atlas Court • Bakersfield, CA 93308 • (661) 327-4911 • FAX (661) 327-1918 • www.bclabs.com Page 20 of
~. LABORATORIES, INC.
D & J Construction Project: Soil Samples -'D'
3534A Gilmore Ave Project Number: Sheil Station on White Lane
Bakersfield CA, 93308 Project Manager: Jerry Hale Reported: 11/08/46 13:02
EPA Method 1664
Quality Con#rol Report -Method Blank Analysis
Constituent Batch ID QC Sample ID MB Result Units PQL MDL Lab Quals
Oil and Grease BPK0256 BPK0256-BLK1 ND mglkg 50 27
BC Laboratories The results in this report apply to the samples analyzed rn accordance lvtth the churn of custody document 77rfs analytical report must be reproduced in tts enJiret
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation„ detachment or third party interpretation.
4100 Atlas Court • Bakersfield, CA 93308 • (661) 327-4911 • FAX (661) 327-1918 • www.bclabs.com Page 210£
'~~ ,LABORATORIES, INC.
D & J Construction
3534-A Gilmore Ave
Bakersfield CA, 93308 Project: Soil Samples -'D'
Project Number: Shell Station on White Lane
Project Manager: Jerry Hale
Reported: 1(/08/06 13:02
Total Concentrations (TTLC)
Quality Control Report -Method Blank Analysis
Constituent Batch ID QC Sample ID MB Result Units PQL MDL Lab Quals
Mercury BPJ1785 BPJ1785-BLK1 ND mg/kg 0.16 0.014 .
Antimony BPK0095 BPK0095-BLK2 ND mg/kg 5.0 0.34
Arsenic BPKQ095 BPK0095-BLK1 ND mg/kg 0.50 0.44
Barium BPK0095 BPK0095-BLK1 ND mg/kg 0.50 0.067
Beryllium BPK0095 BPK0095-BLK1 ND mg/kg 0.50 0.039
Cadmium BPK0095 BPK0095-BLK1 ND mg/kg 0.50 0.073
Chromium BPK0095 BPK0095-BLK1 ND mglkg 0.50 0.17
Cobalt BPK0095 BPK0095-BLK1 ND mg/kg 2.5 0.13
Copper BPK0095 BPK0095-BLK1 ND mg/kg 1.0 0.090
Lead BPK0095 BPK0095-BLK1 ND mg/kg 2.5 0.29
Molybdenum BPK0095 BPK0095-BLK1 ND mglkg 2.5 0.12
Nickel BPK0095 8PK0095-BLK1 ND mg/kg 0.50 0.25
Selenium BPK0095 BPK0095-BLK2 ND mg/kg 0.50 0.40
Silver BPK0095 BPK0095-BLK1 ND mg/kg 0.50 0.059
Thallium BPK0095 BPK0095-BLK1 ND mg/kg 5.0 0.83
Vanadium BPK0095 BPK0095-BLK1 ND mg/kg 0.50 0.065
Zinc BPK0095 BPK0095-BLK1 ND mg/kg 2.5 0.31
BC Laboratories The results in this report apply to fhe samples analyzed in accordance tvJth the chain of custody document. 77ris analytical report must be reproduced rn ifs entire
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc. assumes no responsibility for report alteration, separation„ detachment or third party interpretation.
4100 Atlas Court • Bakersfield, CA 93308 • (661) 327-4911 • FAX (661) 327-1918 • www.bclabs.com Page 22 of
LABORATORIES, INC.
D & J Construction Project: Soil Samples -'D'
3534-A Gilmore Ave Project Number: Shell Station on White Lane
Bakersfield CA, 93308 Project Manager: Jerry Hale Reported: 11/08/06 13:02
Notes and Definitions
Q02
J
A02
A01
ND
dry
RPD
Matrix spike precision is not within the control limits.
Estimated value
The difference between duplicate readings is less than the PQL.
PQL's and MDL's are raised due to sample dilution.
Analyte NOT DETECTED at or above the reporting limit
Sample results reported on a dry weight basis
Relative Percent Difference
BC Laboratories The results in this report apply to the samples analyzed in accosdance with the chain of custody document. This analytical report must be reproduced to its enlire~
All results listed in this report are for the exclusive use of the submitting party. BC Laboratories, Inc, assumes no responsibility for report alteration, separation„ detachment or third party interpretation.
4100 Atlas Court • Bakersfield, CA 93308 • (661) 327-49i 1 • FAX (661) 327-1918 • www.bclabs.com Page 23 of
L ARCHITECTURE • ENGINEERING • E N V I R O N M E N T A L S E R V I C E S
~ GROUP INC. 1137 North McDowell Boulevard, Petaluma, CA 94954-1110 Telephone: (707) 765-1660 Facsimile: (707) 765-9908
June 6, 2006
John W. Johnson Prevention Services
Co-President Bakersfield Fire Department
Architect 900 Truxtun Avenue, Suite 210
Bakersfield, CA 93301
Brian F. Zita
Co-President RE: Shell Station Closure/Sale
Architect
Dear Prevention Services:
John B. Hicks This letter is to inform you that the Shell Station located at 2600 White Lane in Bakersfield
Vice President (Customer No. 2907) has been sold to the operator effective 03/03/2005. Shell Oil Products
no longer operates this business. All future correspondences regarding this facility, the
Regional Managers hazardous materials permit and the underground storage tanks should be directed to:
Brad A. Gubser Steve Yang -Yang's Oil Corporation
Jesse E. Macias White Lane Shell 135068
Roy W. Pedro 2600 White Lane
Alan K. Shimabukuro Bakersfield, CA 93304
805 831-0502
John W. Strobel
If you have any questions, please feel to contact me at the number above.
Respectfully,
RHL DESIGN GROUP, INC.
I
~~--
Steve Skanderson
Project Manager
Off ces Cc: Shell Oil Products US
ANAHEIM, CA
BELLEVUE, WA
CAMAS, WA
DENVER, CO
MARTINEZ, CA
PETALUMA, CA
ROSEVILLE, CA
SCOTTSDALE, AZ
\\rhI-haz\hazmat\HAZMAT\Shell\zFORMSWgency SOLD HMMP Letter Merge.doc
www.rhldesign.com