HomeMy WebLinkAbout1620 BRUNDAGE LN 27
IE
Oilfield Environmental&Compliance, Inc. Phone: 805-922-4772 INVOICE
307 Roemer Way, Suite 300 Fax: 805-925-3376
Santa Maria, CA 93454 Email: AR @oecusa.com
FID# 77-0498914
Client PO Number Invoice Number
Dereck Johnson 1002014
Coles Services Inc.
Proiect Manager Date:
Invoice To:
Lisa Race. 23-Jun-10
Dereck Johnson Proiect Terms
Coles Services Inc. Cole Services NET 30
1620 E.Brundage Lane
Bakersfield,CA 93307
_Work Order(s)
1001938
Proiect Number
Ceramic West
Quantity Analysis/Description Matrix Unit Cost Extended Cost
Oilfield Environmental and Compliance
6 STLC Metals Extraction [5 day] Solid $60.00 $360.00
6 Chromium STLC EPA 6020[5 day] Solid $30.00 $180.00
Invoice Total: $540.00
All invoices are due and payable net 30 days upon the date of the invoice noted above.If payment is not received in full by Oilfield Environmental&
Compliance,Inc.("OEC"),within seven(7)days of the due date,then Customer shall pay OEC interest at the rate of one and a half percent(1.5%)
per month until the full amount of the invoice is paid or the highest rate allowed by law.Customer further agrees that by receiving this invoice and
asking OEC to perform any services for it,Customer is agreeing to all the terms noted herein for any and all services that OEC has,is,and/or will
perform for Customer at any time.Furthermore,if OEC is required to take any action,including but not limited to,retaining an attorney or filing a
lawsuit to collect payment of any invoice,Customer shall pay to OEC all reasonable expenses OEC may incur,including but not limited to,
reasonable attorney's fees,court costs and expert witness fees.Customer further agrees that this Agreement shall be construed in accordance with
the laws of the State of California and that the exclusive venue for any litigation arising under this Agreement shall be the Superior Court of the
State of California in and for the County of Santa Barbara,Santa Maria Branch-Cook Division.Customer(s)agrees that even if it is a business
entity,he/she is personally a party to this Agreement.
IIIIIII VIII III IIII 28
IE _ Page 1 of 1
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Analysis Requeste6
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Client Sample ID
FARE �IIEE
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Oilfield Environmental and Compliance CHAIN OF CUSTODY
307 Roemer Way Suite 300,Santa Maria CA 93454 Highway 33,McKittrick CA
,%� phone: (805)922-4772 fax: (805)925.3376 www.oscusa.com phone: (661)762-9143 Page of
company, ,4t:5 �V --�V/ y�G• Project Name/#:
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Send report via- FAX- PDF-tK Colt(LUFT EDF- ❑ EDD- ❑
Turnaround Time 10 Days-❑ 5 Days- 72 hr-❑ 48 hr-❑ 24 hr- ❑ ASAP-❑
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ReUn.Mshed By Date: Time:
Received By: Date: Time:
EQ40RSAMPLE RECEIPT CLIENT: Ooleg 5&OCe'-< OEC ID#: Temp: *C
RN.01/15/10 Acceptable Range: 0°C to 6°C
COC RECEIVED RECEIPT LOGIN
DATKi7IME: .7 5415 DATE/TIME: 6-7-10 ISS'3 REFRIGERATOR(s):
SAMPLE TRANSPORT,RECEIPT,CONDITION& PRESERVATION: Yes No N/A (*)PROBLEM CHAIN FORMED
11 WOEC Courier/Sampler COC document(s)received with samples A ❑* Custody Seals(circle): Present
❑Delivery(Other than OEC Courier) Correct containers for analysis requested CK ❑* ❑ Samples/Coolers
3gmples Received on Ice Container(s)intact and in good condition of ❑* ❑ Intact/Broken*
95amples Received Outside Temp.Rang * Container label(s)consistent with COC ❑* ❑ Method of Shipment&Tracking#tifappiwable):
❑Samples Direct from field(Outside Temp) OEC preservative added (**note std ID) *" ❑
❑After-Hours Outside Drop-off[Brought Inside] Proper preservation on sample label(s) ❑ ❑ (**)OEC Preservative ID:
(Initials/Date/Time): VOA containers free of headspace ❑ ❑* Dissolved Metals Filtration:(DatelinitlPmerve ID)
Tedlar Bas free of condensation ❑ ❑*
CONTAINERS,COC CHANGES AND/OR CORRECTIONS CHANGES AUTHORIZED BY:
OEC ID Client ID***If blank,refer to CoC Container Description Preservative ResCI Matrix Date/Tlme Comments/Remarks/
/ H Sampled*** Condition Notes Etc.
?oz e-ot - So Lot is
RECEIPT LOGIN BY: RECEIPT REVIEWED BY: Page of
Oilfield Environmental and Compliance, INC.
Dereck Johnson
Coles Services Inc.
1620 E. Brundage Lane
Bakersfield, CA 93307
23 June 2010
RE: Cole Services Work Order: 1001938
Dear Client:
Enclosed is an analytical report for the above referenced project. The samples included in this report
were received on 07-Jun-10.15:45 and analyzed in accordance with the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines
established in our Quality Assurance Manual, applicable standard operating procedures, and other
related documentation. The results in this analytical report are limited to the samples tested and any
reproduction thereof must be made in its entirety.
If you have any questions regarding this report, please do not hesitate to contact the undersigned.
Sincerely,
Lisa Race
Laboratory Manager
TEL: (805)922-4772
307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805)925-3376
Oilfield Environmental and Compliance, INC.
Coles Services Inc. Project:Cole Services
1620 E.Brundage Lane Project Number: Ceramic West Reported:
Bakersfield CA,93307 Project Manager: Dereck Johnson 23-Jun-10 11:19
ANALYTICAL REPORT FOR SAMPLES
Sample ID Laboratory ID Matrix Date Sampled Date Received
Bin#I Front Outside Bin 1001938-01 Solid 04-Jun-10 13:00 07-Jun-10 15:45
Bin#1 Middle Outside Bin 1001938-02 Solid 04-Jun-10 13:05 07-Jun-10 15:45
Bin 41 Back Outside Bin 1001938-03 Solid 04-Jun-10 13:10 07-Jun-10 15:45
Bin#2 Front Inside Bin 1001938-04 Solid 04-Jun-10 13:15 07-Jun-10 15:45
Bin#2 Middle Inside Bin 1001938-05 Solid 04-Jun-10 13:20 67-Jun-10 15:45
Bin#2 Back Inside Bin 1001938-06 Solid 04-Jun-10 13:25 07-Jun-10 15:45
Oilfield Environmental and Compliance The results in this report apply to the samples analyzed in accordance with the chain of
custody document.This analytical report must be reproduced in its entirety.
TEL: (805)922-4772
307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805)925-3376
Page 2 of 14
Oilfield Environmental and Compliance, INC.
Coles Services Inc. Project:Cole Services
1620 E.Brundage Lane Project Number: Ceramic West Reported:
Bakersfield CA,93307 Project Manager: Dereck Johnson 23-Jun-10 11:19
Bin#1 Front Outside Bin
1001938-01 (Solid)
Analyte Result Reporting Units Dilution Batch Prepared Analyzed Method Note
Lima
Total Metals by EPA 6000/7000 Series Methods
Antimony ND 5.0 mg/kg 5 A006156 09-Jun-10 11-Jun-10 EPA 6020
Arsenic 6.6 0.99 "
Barium 79 0.50 "
Beryllium ND 2.5 "
Cadmium 5.0 0.99 "
Chromium 55 0.99 N-02
Cobalt 4.5 0.99 "
Copper 10 0.99
Lead 13 0.99 "
Mercury ND 0.10 1 A006166 10-Jun-10 10-Jun-10 EPA 7471A
Molybdenum 2.3 0.99 5 A006156 09-Jun-10 11-Jun-10 EPA 6020
Nickel 27 0.99 "
Selenium ND 5.0 "
Silver ND 0.99 "
Thallium ND 5.0 "
Vanadium 42 5.0 "
Zinc 64 2.5 "
STLC Metals by 6000/7000 Series Methods
Chromium 2.1 0.020 mg/L 10 A006362 21-Jun-10 22-Jun-10 STLC/EPA
6020
Oilfield Environmental and Compliance The results in this report apply to the samples analysed in accordance with the chain of
custody document.This analytical report must be reproduced in its entirety.
TEL: (805) 922-4772
307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376
Page 3 of 14
r A
Oilfield Environmental and Compliance, INC.
Coles Services Inc. Project:Cole Services
1620 E.Brundage Lane Project Number: Ceramic West Reported:
Bakersfield CA,93307 Project Manager: Dereck Johnson 23-Jun-10 11:19
Bin#1 Middle Outside Bin
1001938-02(Solid)
Analyte Result Reporting Units Dilution Batch Prepared Analyzed Method Note
Limit
Total Metals by EPA 6000/7000 Series Methods
Antimony ND 4.9 mg/kg 5 A006156 09-Jun-10 I I-Jun-10 EPA 6020
Arsenic 4.0 0.99 "
Barium 62 0.49 "
Beryllium ND 2.5 "
Cadmium 6.5 0.99 "
Chromium 55 0.99 N-02
Cobalt 3.7 0.99 "
Copper 14 0.99 "
Lead 14 0.99 "
Mercury ND 0.090 1 A006166 10-Jun-10 10-Jun-10 EPA 7471A
Molybdenum 7.3 0.99 5 A006156 09-Jun-10 11-Jun-]0 EPA 6020
Nickel 24 0.99 "
Selenium ND 4.9 "
Silver ND 0.99 "
Thallium ND 4.9 "
Vanadium 43 4.9 "
Zinc 84 2.5 "
STLC Metals by 6000/7000 Series Methods
Chromium 4.0 0.040 mg/L 20 A006362 21-Jun-10 22-Jun-10 STLC/EPA
6020
Oilfield Environmental and Compliance The results in this report apply to the samples analyzed in accordance with the chain of
custody document.This analytical report must be reproduced in its entirety.
307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com TEL: (805) 922-4772 FAX: (805) 925-3376
Page 4 of 14
Oilfield Environmental and Compliance, INC.
Coles Services Inc. Project:Cole Services
1620 E.Brundage Lane Project Number: Ceramic West Reported:
Bakersfield CA,93307 Project Manager: Dereck Johnson 23-Jun-10 11:19
Bin#1 Back Outside Bin
1001938-03(Solid)
Analyte Result Reporting Units Dilution Batch Prepared Analyzed Method Note
Limit
Total Metals by EPA 6000/7000 Series Methods
Antimony ND 4.8 mg/kg 5 A006156, 09-Jun-10 11-Jun-10 EPA 6020
Arsenic 3.3 0.95 "
Barium 100 0.48 "
Beryllium ND 2.4 "
Cadmium 1.8 0.95 "
Chromium 51 0.95 N-02
Cobalt 6.6 0.95 "
Copper 14 0.95 "
Lead 16 0.95 "
Mercury ND 0.095 1 A006166 10-Jun-10 10-Jun-10 EPA 7471A
Molybdenum 5.9 0.95 5 A006156 09-Jun-10, 11-Jun-]0 EPA 6020
Nickel 19 0.95 "
Selenium ND 4.8 "
Silver ND 0.95 "
Thallium ND 4.8 "
Vanadium 69 4.8 "
Zinc 27 2.4 "
STLC Metals by 6000/7000 Series Methods
Chromium 1.2 0.020 mg/L 10 A006362 21-Jun-10 22-Jun-10 STLC/EPA
6020
Oilfield Environmental and Compliance The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
TEL: (805) 922-4772
307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376
Page 5 of 14
Oilfield Environmental and Compliance, INC.
Coles Services Inc. Project:Cole Services
1620 E.Brundage Lane Project Number: Ceramic West Reported:
Bakersfield CA,93307 Project Manager: Dereck Johnson 23-Jun-10 11:19
Bin#2 Front Inside Bin
1001938-04(Solid)
Analyte Result Reporting Units Dilution Batch Prepared Analyzed Method Note
Limit
Total Metals by EPA 6000/7000 Series Methods
Antimony ND 4.8 mg/kg 5 A006156 09-Jun-10 11-Jun-10 EPA 6020
Arsenic 1.7 0.97 "
Barium 63 0.48 "
Beryllium ND 2.4 "
Cadmium 5.0 0.97 "
Chromium 89 0.97 N-02
Cobalt 5.6 0.97
Copper 15 0.97
Lead 6.8 0.97 "
Mercury ND 0.098 1 A006166 10-Jun-10 10-Jun-10 EPA7471A
Molybdenum ND 0.97 5 A006156 09-Jun-10 11-Jun-10 EPA 6020
Nickel 21 0.97 "
Selenium ND 4.8 "
Silver ND 097 "
Thallium ND 4.8 "
Vanadium 110 4.8 "
Zinc 36 2.4 "
STLC Metals by 6000/7000 Series Methods
Chromium 2.6 0.040 mg/L 20 A006362 21-Jun-10 22-Jun-10 STLC/EPA
6020
Oilfield Environmental and Compliance The results in this report apply to the samples analyzed in accordance with the chain of
custody document.This analytical report must be reproduced in its entirety.
TEL: (805)922-4772
307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805)925-3376
Page 6 of 14
Oilfield Environmental and Compliance, INC.
Coles Services Inc. Project:Cole Services
1620 E.Brundage Lane Project Number: Ceramic West Reported:
Bakersfield CA,93307 Project Manager: Dereck Johnson 23-Jun-10 11:19
Bin#2 Middle Inside Bin
1001938-05(Solid)
Analyte Result Reporting Units Dilution Batch Prepared Analyzed Method Note
Limit
Total Metals by EPA 6000/7000 Series Methods
Antimony ND 5.0 mg/kg 5 A006156 09-Jun-10 11-Jun-10 EPA 6020
Arsenic 13 1.0 "
Barium 130 0.50 "
Beryllium ND 2.5 "
Cadmium 13 1.0 N-02
Chromium 120 1.0 N-02,N-03
Cobalt 13 1.0 "
Copper 7.3 1.0 "
Lead 9.4 1.0 "
Mercury ND 0.098 1 A006166 10-Jun-10 10-Jun-10 EPA 7471A
Molybdenum 35 1.0 5 A006156 09-Jun-10 11-Jun-10 EPA 6020
Nickel 76 1.0
Selenium ND 5.0 "
Silver ND 1.0 "
Thallium 6.2 5.0 "
Vanadium 130 5.0 "
Zinc 280 10 20 14-Jun-10 "
STLC Metals by 6000/7000 Series Methods
Chromium 4.5 0.040 mg/L 20 A006362 21-Jun-10 22-Jun-10 STLC/EPA
6020
Oilfield Environmental and Compliance The results in this report apply to the samples analyzed in accordance with the chain of
custody document.77tis analytical report must be reproduced in its entirety.
TEL: (805) 922-4772
307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376
Page 7 of 14
Oilfield Environmental and Compliance, INC.
Coles Services Inc. Project:Cole Services
1620 E.Brundage Lane Project Number: Ceramic West Reported:
Bakersfield CA,93307 Project Manager: Dereck Johnson 23-Jun-10 11:19
Bin#2 Back Inside Bin
1001938-06(Solid)
Analyte Result Reporting Units Dilution Batch Prepared Analyzed Method Note
Limit
Total Metals by EPA 6000/7000 Series Methods
Antimony ND 4.8 mg/kg 5 A006156 09-Jun-10 11-Jun-10 EPA 6020
Arsenic 17 0.97 " " " "
Barium 160 0.97 10 14-Jun-10
Beryllium ND 2.4 5 11-Jun-10 "
Cadmium 11 0.97 N-02
Chromium 130 0.97 N-02,N-03
Cobalt 11 0.97 "
Copper 11 0.97 "
Lead 13 0.97 "
Mercury ND 0.099 1 A006166 10-Jun-10 10-Jun-10 EPA 7471A
Molybdenum 33 0.97 5 A006156 09-Jun-10 11-Jun-10 EPA 6020
Nickel 73 0.97 "
Selenium ND 4.8 "
Silver ND 0.97 "
Thallium 7.0 4.8 "
Vanadium 120 4.8 "
Zinc 290 9.7 20 14-Jun-10 "
STLC Metals by 6000/7000 Series Methods
Chromium 2.4 0.020 mg/L 10 A006362 21-Jun-10 22-Jun-10 STLC/EPA
6020
Oilfield Environmental and Compliance The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com TEL: (805) 922-4772 FAX: (805) 925-3376
Page 8 of 14
WAR-
Oilfield Environmental and Compliance, INC.
Coles Services Inc. Project:Cole Services
1620 E.Brundage Lane Project Number: Ceramic West Reported:
Bakersfield CA,93307 Project Manager: Dereck Johnson 23-Jun-10 11:19
Total Metals by EPA 6000/7000 Series Methods -Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch A006156-EPA 3050B
Blank(A006156-BLKI) Prepared:09-Jun-10 Analyzed: I I-Jun-10
Antimony ND 1.0 mg/kg
Arsenic ND 0.20
Barium ND 0.10 "
Beryllium ND 0.50 "
Cadmium ND 0.20 "
Chromium ND 0.20 "
Cobalt ND 0.20 "
Copper ND 0.20
Lead ND 0.20 "
Molybdenum ND 0.20
Nickel ND 0.20 "
Selenium ND 1.0 "
Silver ND 0.20
Thallium ND 1.0 "
Vanadium ND 1.0 "
Zinc 0.710 0.50 QB-01
LCS(A006156-BSI) Prepared:09-Jun-10 Analyzed: 11-Jun-10
Antimony 15.8 1.0 mg/kg 15.0 105 85-115 20
Arsenic 17.9 0.20 15.0 119 85-115 20 QM-11
Barium 15.4 0.10 15.0 102 85-115 20
Beryllium 17.8 0.50 15.0 118 85-115 20 QM-11
Cadmium 16.0 0.20 15.0 107 85-115 20
Chromium 15.2 0.20 15.0 101 85-115 20
Cobalt 15.0 0.20 15.0 100 85-115 20
Copper 15.4 0.20 15.0 102 85-115 20
Lead 14.6 0.20 15.0 97.6 85-115 20
Molybdenum 14.5 0.20 15.0 96.4 85-115 20
Nickel 15.0 0.20 15.0 100 85-115 20
Selenium 18.6 1.0 15.0 124 85-115 20 QM-I1
Silver 16.5 0.20 15.0 110 85-115 20
Thallium 14.2 1.0 15.0 94.8 85-115 20
Vanadium 15.1 1.0 15.0 101 85-115 20
Zinc 17.5 0.50 15.0 117 85-115 20 QM-11
Oilfield Environmental and Compliance The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
TEL: (805)922-4772
307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376
Page 9 of 14
Oilfield Environmental and Compliance, INC.
Coles Services Inc. Project:Cole Services
1620 E.Brundage Lane Project Number: Ceramic West Reported:
Bakersfield CA,93307 Project Manager: Dereck Johnson 23-Jun-10 11:19
Total Metals by EPA 6000/7000 Series Methods -Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch A006156-EPA 3050B
LCS Dup(A006156-BSDI) Prepared:09-Jun-10 Analyzed: 11-Jun-10
Antimony 16.5 1.0 mg/kg 15.0 110 85-115 4.63 20
Arsenic 16.0 0.20 15.0 107 85-115 11.3 20
Barium 14.6 0.10 15.0 97.4 85-115 4.95 20
Beryllium 16.2 0.50 15.0 108 85-115 9.29 20
Cadmium 16.4 0.20 15.0 109 85-115 2.56 20
Chromium 15.0 0.20 15.0 100 85-115 1.12 20
Cobalt 15.1 0.20 15.0 101 85-115 0.676 20
Copper 14.8 0.20 15.0 98.7 85-115 3.65 20
Lead 14.4 0.20 15.0 96.3 85-115 1.33 20
Molybdenum 13.7 0.20 15.0 91.0 85-115 5.78 20
Nickel 14.6 0.20 " 15.0 97.4 85-115 2.63 20
Selenium 16.1 1.0 15.0 107 85-115 14.3 20
Silver 16.3 0.20 15.0 108 85-115 1.43 20
Thallium 15.8 1.0 15.0 105 85-115 10.6 20
Vanadium 15.3 1.0 15.0 102 85-115 1.60 20
Zinc 16.3 0.50 15.0 109 85-115 6.94 20
Duplicate(A006156-DUP1) Source: 1001925-01 Prepared:09-Jun-10 Analyzed: 11-Jun-10
Antimony ND 4.8 mg/kg ND 20
Arsenic 2.34 0.96 2.13 9.24 20
Barium 68.8 0.48 73.5 6.55 20
Beryllium ND 2.4 ND 20
Cadmium 0.948 0.96 0.935 1.33 20
Chromium 12.3 0.96 10.9 12.2 20
Cobalt 5.18 0.96 5.58 7.49 20
Copper 12.4 0.96 14.1 13.0 20
Lead 68.5 0.96 41.1 49.9 20 QR-04
Molybdenum ND 0.96 ND 20
Nickel 13.6 0.96 13.6 0.410 20
Selenium ND 4.8 ND 20
Silver ND 0.96 ND 20
Thallium ND 4.8 ND 20
Vanadium 27.8 4.8 29.2 4.72 20
Zinc 31.4 2.4 33.4 6.16 20
Oilfield Environmental and Compliance The results in this report apply to the samples analysed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
TEL: (805) 922-4772
307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376
Page 10 of 14
Oilfield Environmental and Compliance, INC.
Coles Services Inc. Project:Cole Services
1620 E.Brundage Lane Project Number: Ceramic West Reported:
Bakersfield CA,93307 Project Manager: Dereck Johnson 23-Jun-10 11:19
Total Metals by EPA 6000/7000 Series Methods -Quality Control
Reporting Spike Source %REC RPD
lAnalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch A006156-EPA 3050B
Matrix Spike(A006156-MSI) Source:1001925-01 Prepared:09-Jun-10 Analyzed: 11-Jun-10
Antimony 29.7 19 mg/kg 291 ND 10.2 0-88 20
Arsenic 270 3.9 291 2.13 92.1 73-124 20
Barium 345 1.9 291 73.5 93.5 18-166 20
Beryllium 311 9.7 291 ND 107 76-132 20
Cadmium 279 3.9 291 0.935 95.8 82-118 20
Chromium 300 3.9 291 10.9 99.6 58-139 20
Cobalt 288 3.9 291 5.58 97.1 85-114 20
Copper 286 3.9 291 14.1 93.4 64-138 20
Lead 339 3.9 291 41.1 102 61-138 20
Molybdenum 186 3.9 291 ND 63.8 67-112 20 QM-05
Nickel 288 3.9 291 13.6 94.3 68-132 20
Selenium 268 19 291 ND 92.0 66-132 20
Silver 289 3.9 291 ND 99.3 18-153 20
Thallium 280 19 291 ND 96.2 78-114 20
Vanadium 326 19 291 29.2 102 80-119 20
Zinc 307 9.7 291 33.4 94.1 40-153 20
Matrix Spike Dup(A006156-MSDI) Source: 1001925-01 Prepared:09-Jun-10 Analyzed: 11-Jun-10
Antimony 22.1 20 mg/kg 293 ND 7.53 0-88 30.3 20 QR-02
Arsenic 276 3.9 293 2.13 93.4 73-124 1.41 20
Barium 372 2.0 293 73.5 102 18-166 8.46 20
Beryllium 315 9.8 293 ND 107 76-132 0.583 20
Cadmium 285 3.9 293 0.935 97.1 82-118 1.32 20
Chromium 310 3.9 293 10.9 102 58-139 2.63 20
Cobalt 294 3.9 293 5.58 98.6 85-114 1.49 20
Copper 296 3.9 293 14.1 96.1 64-138 2.88 20
Lead 333 3.9 293 41.1 99.7 61-138 2.63 20
Molybdenum 188 3.9 293 ND 64.1 67-112 0.362 20 QM-05
Nickel 296 3.9 293 13.6 96.4 68-132 2.20 20
Selenium 278 20 293 ND 95.0 66-132 3.18 20
Silver 292 3.9 293 ND 99.8 18-153 0.475 20
Thallium 281 20 293 ND 95.8 78-114 0.449 20
Vanadium 330 20 293 29.2 103 80-119 0.722 20
Zinc 320 9.8 293 33.4 98.0 40-153 4.05 20
Oilfield Environmental and Compliance The results in this report apply to the samples analyzed in accordance with the chain of
custody document.This analytical report must be reproduced in its entirety.
TEL: (805) 922-4772
307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376
Page 11 of 14
Oilfield Environmental and Compliance, INC.
Coles Services Inc. Project:Cole Services
1620 E.Brundage Lane Project Number: Ceramic West Reported:
Bakersfield CA,93307 Project Manager: Dereck Johnson 23-Jun-10 11:19
Total Metals by EPA 6000/7000 Series Methods -Quality Control
Reporting Spike Source %REC RPD
lAnalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch A006166-EPA 7471A Prep
Blank(A006166-BLKI) Prepared&Analyzed: 10-Jun-10
Mercury ND 0.10 mg/kg
LCS(A006166-BSI) Prepared&Analyzed: 10-Jun-10
Mercury 1.71 0.10 mg/kg 1.67 103 85-115 20
LCS Dup(A006166-BSDI) Prepared&Analyzed: 10-Jun-10
Mercury 1.71 0.10 mg/kg 1.67 102 85-115 0.244 20
Duplicate(A006166-DUPI) Source:1001925-01 Prepared&Analyzed: 10-Jun-10
Mercury 0.0168 0.096 mg/kg 0.0197 15.9 20
Matrix Spike(A006166-MS1) Source:1001925-01 Prepared&Analyzed: 10-Jun-10
Mercury 1.56 0.090 mg/kg 1.51 0.0197 103 75-125 20
Matrix Spike Dup(A006166-MSDI) Source: 1001925-01 Prepared&Analyzed: 10-Jun-10
Mercury 1.72 0.099 mg/kg 1.66 0.0197 103 75-125 0.0308 20
Oilfield Environmental and Compliance The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com TEL: (805) 922-4772 FAX: (805) 925-3376
Page 12 of 14
Oilfield Environmental and Compliance, INC.
Coles Services Inc. Project:Cole Services
1620 E.Brundage Lane Project Number: Ceramic West Reported:
Bakersfield CA,93307 Project Manager: Dereck Johnson 23-Jun-10 11:19
STLC Metals by 6000/7000 Series Methods-Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch A006362-EPA 3005A Leachate
Blank(A006362-BLKI) Prepared:21-Jun-10 Analyzed:22-Jun-10
Chromium ND 0.0020 mg/L
LCS(A006362-BSI) Prepared:21-Jun-10 Analyzed:22-Jun-10
Chromium 0.160 0.0020 mg/L 0.150 107 85-115 20
LCS Dup(A006362-BSDI) Prepared:21-Jun-10 Analyzed:22-Jun-10
Chromium 0.156 0.0020 mg/L 0.150 104 85-115 2.68 20
Duplicate(A006362-DUPI) Source:1001938-01 Prepared:21-Jun-10 Analyzed:22-Jun-10
Chromium 2.18 0.020 mg/L 2.13 2.36 20
Matrix Spike(A006362-MSI) Source: 1001938-01 Prepared:21-Jun-10 Analyzed:22-Jun-10
Chromium 9.68 0.080 mg/L 6.00 2.13 126 67-130 20
Matrix Spike Dup(A006362-MSD1) Source: 1001938-01 Prepared:21-Jun-10 Analyzed:22-Jun-10
Chromium 8.15 0.080 mg/L 6.00 2.13 100 67-130 22.6 20 QR-02
Oilfield Environmental and Compliance The results in this report apply to the samples analyzed in accordance with the chain of
custody document.This analytical report must be reproduced in its entirety.
TEL: (805) 922-4772
307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376
Page 13 of 14
Oilfield Environmental and Compliance, INC.
Coles Services Inc. Project:Cole Services
1620 E.Brundage Lane Project Number: Ceramic West Reported:
Bakersfield CA,93307 Project Manager: Dereck Johnson 23-Jun-10 11:19
Notes and Definitions
QR-04 The RPD exceeded the QC control limits.
QR-02 The RPD result exceeded the QC control limits;however,both percent recoveries were acceptable.Sample results for the QC batch
were accepted based on percent recoveries and completeness of QC data.
QM-I 1 The spike recovery was outside acceptance limits for the LCS.The batch was accepted based on acceptable LCSD recovery.
QM-05 The spike recovery was outside acceptance limits for the MS and/or MSD due to matrix interference.The LCS and/or LCSD were
within acceptance limits showing that the laboratory is in control and the data is acceptable.
QB-01 The method blank contains analyte at a concentration above the RLIPQL;however,concentration is less than 10%of the sample result,
which is negligible according to method criteria.
N-03 Analyte concentration above 20 X TCLP.
N-02 Analyte concentration below TTLC but above 10 X STLC.
DEf Analyte DETECTED
ND Analyte NOT DETECTED at or above the reporting limit
NR Not Reported
dry Sample results reported on adry weight basis
RPD Relative Percent Difference
Oilfield Environmental and Compliance The results in this report apply to the samples analyzed in accordance with the chain of
custody document.This analytical report must be reproduced in its entirely.
TEL: (805) 922-4772
307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805)925-3376
Page 14 of 14
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Oilfield Environmental and Compliance CHAIN OF CUSTODY
307 Roemer Way Suite 300,Santa Maria CA 93454 Highway 33,McKittrick CA
phone: (805)9224772 fax: (805)925.3376 www.oecusa.com phone: (661)762-9143 Page of
Company., V�" G��/ G• Project Namely:
Address: rAy X1 �? site:
04 /������ Analysis Requested special Insbuctions:
PhonejAll'Y 2�A %S v Fax �s�� � -mail:
Report To Sampler:
Send report via- FAX- PDF-jK Colt/LUFT EDF- ❑ EDD- ❑
Turnaround Time 10 Days-❑ 5 Days- 72 hr-[-] 48 hr-❑ 24 hr- ❑ ASAP-❑
DatelTime Sampled Mai CoM Client Sample ID
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Received By: Date: Time: S-�5
Relinquished By ------------------Date: ----Time_---------------
Received By Date: Time:
SAMPLE RECEIPT CLIENT: &/" 5&VlCe-C OEC ID#: 1&0J'?3 Q0 Temp: � °C
nry.01/15/10 Acceptable Range: 0°C to 6°C
COC RECEIVED RECEIPT LOGIN
DATE/TIME: (p ..7 Sics DATE/TIME: 6-7-10 ISS3 REFRIGERATOR(s):
SAMPLE TRANSPORT,RECEIPT,CONDITION&PRESERVATION: Yes No N/A (*)PROBLEM CHAIN FORM> DED
�OEC Courier/Sampler COC document(s)received with samples X . ❑* 11 Custody Seals(circle): Present d ,��,
❑Delivery(Other than OEC Courier) Correct containers for analysis requested ❑* ❑ Samples/Coolers
0Samples Received on Ice Container(s)intact and in good condition ❑* ❑ Intact/Broken*
9Samples Received Outside Temp.Rang *V Container label(s)consistent with COC 0 ❑* ❑ Method of Shipment&Tracking#tif applicablel:
❑Samples Direct from field(Outside Temp) OEC preservative added (**note std ID) 0** ❑ 9
❑After-Hours Outside Drop-off[Brought Inside] Proper preservation on sample label(s) ❑ ❑ (**)OEC Preservative ID:
(Initials/Date/Time): VOA containers free of headspace ❑ ❑* Dissolved Metals Filtration:(DatellnitlPreserwv ID)
Tedlar Bas free of condensation ❑ ❑*
CONTAINERS,COC CHANGES AND/OR CORRECTIONS CHANGES AUTHORIZED BY:
OEC ID Client ID***lf blank,refer to CoC Container Description Preservative ResCl Matrix Date/Time Comments/Remarks/
/ H Sampled*** Condition Notes Etc.
�A
RECEIPT LOGIN BY: RECEIPT REVIEWED BY: Page j of
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