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HomeMy WebLinkAboutSOIL REPORT2009 pal I IIIIIII VIII III IIII 23 B E R S F I D IE F/RE ARTM T August 11, 2009 Mr. Jerry Hale D &J Construction 3430 Gilmore Ave suite A Bakersfield, CA 93308 Ronald J. Fraze Fire Chief Re: Underground soil sampling of walker Fuels, 4600 Stine Gary Hutton Road, Bakersfield, CA_(revisiion): Tyler Hartley Douglas Greener Deputy Chiefs Dear Mr. Hale, I have reviewed the soil sampling report for the above site prepared by Advanced Environmental Concepts Inc, dated July 7, 2009, and I am in concurrence with his report. Prior to replacing the old dispensers HOWARD H.WINES,III you will need to over excavate the soil under the former dispensers (4- E and 5) and either treat excavated soil on-site or if unable, remove to DIRECTOR ! a qualified facility. PREVENTION SERVICES Please resubmit a correction action plan to this office within 30 days 1501 Truxtun Ave., I"Floor from receipt this letter. The work plan should follow the guidelines Bakersfield,CA 93301 found in: Appendix A: Reports, Tri-Regional Board Staff VOICE: (661)326-3979 i Recommendations for Preliminary Investigation and Evaluations of FAX: (661)852-2171 Underground Tank Sites: 16 April 2004. If you have any additional questions, please call me at (661) 326-3684. ���ornmen�,�l� Sincerely, S.PE,q%fi,�s ,� Craig P ins REA REA1�08 3Q Via, Hazardous Materials Specialist cc: Jonathan Buck PG Advanced Environmental Concep 1111111IM1111 24 JARrNE R S F I D F/RE T August 4, 2009 Mr. Jerry Hale D `n J Construction 3430 Gilmore Avenue, Suite A Bakersfield, CA 93308 Ronald J. Fraze Fire Chief Re: Under dispenser soil sampling of Walker Fuels, 4600 Stine Road, Bakersfield, CA. Gary Hutton Tyler Hartley Douglas Greener Dear Mr. Hale, Deputy Chiefs have reviewed the soil sampling report for the above site prepared by Advanced Environmental Concepts Inc dated July 7, 2009, and in concurrence with his report. Prior to replacing the old dispensers you will need to over excavate the soil under the former dispensers (4-W and 5) and dispose of it at a qualified facility and replace with clean soil HOWARD H.WINES,III /pee gravel. DIRECTOR i PREVENTION SERVICES ; Please submit a correction action plan to this office within 30 days from receipt this letter..The work plan should follow the guidelines found in: 1501 Tnzxtun Ave., 15L Floor Appendix A: Reports, Tri-Regional Board Staff Recommendations for Bakersfield,CA 93301 Preliminary Investigation and Evaluations of Underground Tank Sites: VOICE: (661)326-3979 16 April 2004. FAX: (661)852-2171 If you have any additional questions, please call me at(661) 326-3684. i Sincerely, S.PER,. Craig Perkins REAo Hazardous Materials Specialist REA i-0 330 Expires I O ,\�, A ---> L DEL ❑ADVANCED ENVIRONMENTAL CONCEPTS INC❑ 0 July 8, 2009 Mr. Craig Perkins Bakersfield Fire Department 1501 Truxtun Avenue, 1st Floor Bakersfield, California 93301 RE: Dispenser Sampling Summary Letter Walker Fuels 4600 Stine Road Bakersfield, California Dear Mr. Perkins, Please find enclosed one (1) copy of the Dispenser Sampling Summary Letter for the above referenced project/location. Should you have any questions or require clarification on any aspects of the enclosed, please do not hesitate to contact our office at(661) 395-1646. Respectfully yours, Advanced Environmental Concepts, Inc. 1 - April SElceaux Office,Manager Enclosure: Report(1) • ENVIRONMENTAL CONCEPTS WITH DESIGN IN MIND 220 E. TRUXTUN AVENUE BAKERSFIELD, CA 93305 661/395-1646 FAX 661/395-1616 nn D ADVANCED ENVIRONMENTAL CONCEPTS INC❑ July 7, 2009 Mr. Jerry Hale D 'n J Construction 3430 Gilmore Avenue, Suite A Bakersfield, California 93008 RE: Dispenser Sampling Walker Fuels 4600 Stine Road Bakersfield, California Dear Mr. Hale; Advanced Environmental Concepts, Inc. (AEC) is pleased to present this summary letter for the collection of soil samples from beneath nine dispenser locations at the Walker Fuels facility, 4600 Stine Road, Bakersfield, California (Figure 1). On June 23, 2009 an AEC geologist mobilized to the Walker Fuels facility to collect discrete soil samples at 2-feet, and 6-feet beneath the nine former dispenser locations (Figure 2). The dispensers, dispenser pans, concrete surfacing, and piping had been removed from the locations to be sampled; native soil was present at each location. AEC used a hand auger to core to the prescribed sampling depths of 2' and 6' beneath the former dispenser locations. Once the requested sampling depth was achieved, AEC brought the hand auger bucket to surface and compressed a new stainless steel sleeve into the undisturbed soil. The ends of the sleeve were sealed with Teflon-lined plastic end caps which were subsequently taped. The sleeves were labeled, then, placed in an ice chest chilled with chipped ice. The soil samples were also recorded on a chain-of-custody. The eighteen discrete soil samples were analyzed for TPH- , gasoline or TPH-diesel, BTXE, and MTBE by EPA Method 8015/8021B by Associated Laboratories, Orange, California(See attached analytical and tabulated results). 1 The soil sample analyses indicated non-detectable concentrations for BTXE and MTBE; however, some detections of TPH as diesel were recorded. Soil samples collected beneath dispenser location 4-E at 2' and exhibited 245 mg/kg and 273 mg/kg of TPH-diesel, respectively. In -'" addition, soil samm q1—A,,V t�6 indicated 0.42 mg/kg and 8.4 mg/kg, respectively.Finally,, soil samples od"Ille0a A from location 5-2-and-6-exhibited991'6 mg/k"g nd 25 mg/kg, respectively;? t Although there are areas-where"the"diesel"appea�s�to-be°in ecr asing with depth(sample 4-E AEC does not recommend a complete subsurface investigation; rather, it is recommended that the area proximal to the sample locations be "over-excavated" until clean soil is visibly, and olfactory, identified and the newly created spoils pile mitigated onsite. r� • ENVIRONMENTAL CONCEPTS WITH DESIGN IN MIND 220 E. TRUXTUN AVENUE BAKERSFIELD, CA 93305 661/395-1646 FAX 661/395-1616 Walker Fuels Advanced Environmental Concepts, Inc. ' AEC appreciates the opportunity to provide our consulting services and should you have any questions please do not hesitate to contact the undersigned. Sincerely, Advanced Environmental Concepts, Inc. E 1 - AIV( B�oc<t� loathan L. Buck RENEW DATE fessional Geologist#7468 � Cc: Mr. Craig Perkins, Fire Protection Services cf'�, N .7468 �Q 1 1 . 1 1 1 1 1 ENVIRONMENTAL CONCEPTS WITH DESIGN IN MIND 2 ' 220 E. TRUXTUN AVENUE BAKERSFIELD, CA 93305 661/395-1646 FAX 661/395-1616 Advanced Environmental Concepts,,Inc. 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SILVER SPRI LN I r - SITE LOCATION MAP - ' FIGURE ' Walker Fuels ADVANCED ENV IRONMENTAL CONCEPTS 4600 Stine Road AV Bakersfield, California ' ADVANCED ENVIRONMENTAL CONCEPTS 220 E. Trudun Avenue Bakersfield,CA 93305 1-W-2',6' 1-E-2',6' Cement • 2-W-2' 6' 2-E-2' 6' ® ® Cement 3-E-2',6' 3-W-2', 6' i00� 00�i Limit of Saw Cut e 4-W-2',6'6' i00 ♦ ® ♦ ♦ � 0 (s �00 oo'ga\\O-1vS NT 4-E-2' 6' Fal-5-2',6' Steel Container ® Soil Sampling Location 0' 10' 20' N W E S Site Map FIGURE Walker Fuels .® �ENWVIL CON CEPTS INC 4600 Stine Road 2 ADVANCED ENVIRONMENTALCONCEPT:S Bakersfield, California P.O.BOX 40872 B4X0?SRELD,CA 83384 Advanced Environmentat Concepts, Inc. ' "Attachment B"' ANALYTICAL RESULTS 1 1 i ASSOCIATED LABORATORIES 806 North Batavia-Orange, California 92868- 7141771-6900 FAX 7141538-1209 CLIENT Advanced Environmental Concepts Inc. (10022) LAB REQUEST 236520 ATTN: Jonathan Buck 220 E.Truxtun Ave. REPORTED 07/02/2009 Bakersfield,CA 93305 RECEIVED 06/25/2009 PROJECT Walker Fuels 4600 Stine Road,Bakersfield ' SUBMITTER Client COMMENTS This laboratory request covers the following listed samples which were analyzed for the parameters indicated on the attached Analytical ' Result Report All analyses were conducted using the appropriate methods as indicated on the report. This cover letter is an integral part of the final report ' Order No. Client Sample Identification 1003622 1-E-2' 1003623 1-E-6' ' 1003624 1-W-2' 1003625 1-W-6' 1003626 2-E-2' 1003627 2-E-6' ' 1003628 2-W-2' 1003629 2-W-6' 1003630 3-E-2' ' 1003631 3-E-6' 1003632 3-W-2' 1003633 3-W-6' Thank you for the opportunity to be of service to your company. Please feel free to call if there are any questions regarding this report or if we can be of further service. ' ASSO TED LABO ORIES by, Edw r ar ,P . Vice resident ' NOTE: Unless notified in writing,all samples will be discarded by appropriate disposalprotoco130 dcTs front date reported. TESTING&CONSULTING The reports of the Associated laboratories are confidential property of our clients and Chemical ' may not be reproduced or used for publication in part or in full without our written Microbiological permission. This is for the mutual protection of the public,our clients,and ourselves. Environmental Lab request 236520 cover,page l of 2 1 1 - LA ASSOCIATED LABORATORIES 806 North Batavia-Orange, California 92868- 7141771-6900 FAX 7141538-1209 ' CLIENT Advanced Environmental Concepts Inc. (10022) LAB REQUEST 236520 ATTN: Jonathan Buck 220 E.Truxtun Ave. REPORTED 07/02/2009 Bakersfield,CA 93305 RECEIVED 06/25/2009 ' PROJECT Walker Fuels 4600 Stine Road,Bakersfield ' SUBMITTER Client COMA ENTS 1 This laboratory request covers the following listed samples which were analyzed for the parameters indicated on the attached Analytical ' Result Report All analyses were conducted using the appropriate methods as indicated on the report This cover letter is an integral part of the final report Order No. Client Sample Identification 1003634 4-E-2' 1003635 4-E-6' 1003636 4-W-2' ' 1003637 4-W-6' 1003638 5-2' 1003639 5-6' 1003640 Laboratory Method Blank 1 ' Thank you for the opportunity to be of service to your company. Please feel free to call if there are any questions regarding this report or if we can be of further service. ' A S TED LAB O S by, ' Edw d re vice resident NOTE: Unless notified in writing, all samples will be discarded by appropriate disposal protocol 30 days from date reported. TESTING&CONSULTING The reports of the Associated Laboratories are confidential property of our clients and Chemical may not be reproduced or used for publication in part or in full without our written Microbiological permission. This is for the mutual protection of the public,our clients,and ourselves. Environmental Lab request 236520 cover,page 2 of 2 Order#: 1003622 Client Sample ID: 1-E-2' ' Matrix: SOLID Sample Description: Northern dispenser Island East dispenser Date Sampled: 06/23/2009 Method Analyte Result DF EQL MDL Units Date/Analyst TPH-DHS Gasoline ND 1 3 0.018 m g/Kg 06/26/09 NZ Surrogates Units Control Limits TPH-DHS p-Bromofluorobenzene(Sur) 91 % 60-140 ' 8260B Benzene ND 1 5 0.18 ug/Kg 06/29/09 LZ 8260B Ethyl benzene ND 1 5 0.23 ug/Kg 06/29/09 LZ ' 8260B Methyl-tert-butylether(MTBE) ND 1 5 0.17 ug/Kg 06/29/09 LZ 8260B Toluene ND 1 5 0.17 ug/Kg 06/29/09 LZ 8260B Xylenes,total ND 1 5 0.38 ug/Kg 06/29/09 LZ ' Surrogates Units Control Limits 8260B Surrl -Dibromofluoromethane 93 % 70- 135 8260B Surr2-1,2-Dichloroethane-14 122 % 70- 135 8260B Surr3-Toluene-d8 108 % 70- 135 8260B Surr4-p-Bromofluorobenzene 98 % 70- 135 1 1 r EQL=Estimated Quantitation Limit, MDL=Method detection limit,DF=Dilution Factor ND=Not detected below indicated MDL,J=Trace,S=Surrogate outside control limits ' ASSOCIATED LABORATORIES Anahrtiral Results Rcnnrt Lab Request 236520 results,page 1 of 19 Order#: 1003623 Client Sample ID: 1-E-6' ' Matrix: SOLID Sample Description: Northern dispenser Island East dispenser Date Sampled: 06/23/2009 Method Analyte Result DF EQL MDL Units Date/Analyst TPH-DHS Gasoline ND 1 3 0.018 mg/Kg 06/26/09 NZ ' Surrogates Units Control Limits TPH-DHS p-Bromofluorobenzene(Sur) 91 % 60-140 ' 8260B Benzene ND 1 5 0.18 ug/Kg 06/29/09 LZ 8260B Ethyl benzene ND 1 5 0.23 ug/Kg 06/29/09 LZ ' 8260B Methyl-tert-butylether(MTBE) ND 1 5 0.17 ug/Kg 06/29/09 LZ 8260B Toluene ND 1 5 0.17 ug/Kg 06/29/09 LZ 8260B Xylenes,total ND 1 5 0.38 ug/Kg 06/29/09 LZ ' Surrogates Units Control Limits 8260B Surrl -Dibromofluoromethane 95 % 70-135 8260B Surr2-1,2-Dichloroethane-d4 121 % 70-135 ' 8260B Surr3-Toluene-d8 102 % 70- 135 8260B Surr4-p-Bromofluorobenzene 97 % 70- 135 r EQL=Estimated Quantitation Limit, MDL=Method detection limit,DF=Dilution Factor ND=Not detected below indicated MDL,J=Trace,S=Surrogate outside control limits ASSOC"TED LABORATOMES Anahituml Results Rannrt Lab Request 236520 results,page 2 of 19 Order#: 1 10036241 Client Sample ID: 1-W-2' ' Matrix:SOLID Sample Description: Northern dispenser Island West dispenser Date Sampled: 06/23/2009 Method Analyte Result DF EQL MDL Units Date/Analyst TPH-DHS Gasoline ND 1 3 0.018 mg/Kg 06/26/09 NZ Surrogates Units Control Limits TPH-DHS p-Bromofluorobenzene(Sur) 89 % 60-140 ' 8260B Benzene ND 1 5 0.18 ug/Kg 06/29/09 LZ 8260B Ethyl benzene ND 1 5 0.23 ug/Kg 06/29/09 LZ 8260B Methyl-tert-butylether(MTBE) ND 1 5 0.17 ug/Kg 06/29/09 LZ 8260B Toluene ND 1 5 0.17 ug/Kg 06/29/09 LZ 8260B Xylenes,total ND 1 5 0.38 ug/Kg 06/29/09 LZ Surrogates Units Control Limits 8260B Surrl-Dibromofluoromethane 99 % 70-135 8260B Surr2- 1,2-Dichloroethane-d4 101 % 70- 135 8260B Surr3-Toluene-d8 103 % 70- 135 8260B Surr4-p-Bromofluorobenzene 102 % 70- 135 1 r i 1 EQL=Estimated Quantitation Limit, MDL=Method detection limit,DF=Dilution Factor ND-Not detected below indicated MDL,J=Trace,S=Surrogate outside control limits ' ASSOCIATED LABORATORIES AnahifiirA Raciilfc Rannrt Lab Request 236520 results,page 3 of 19 Order#: 1003625 Client Sample ID: 1-W-6' Matrix: SOLID Sample Description: Northern dispenser Island West dispenser Date Sampled: 06/23/2009 Method Analyte Result DF EQL MDL Units Date/Analyst ' TPH-DHS Gasoline ND 1 3 0.018 m /K 06/26/09 NZ mg/Kg Surrogates Units Control Limits TPH-DHS p-Bromofluorobenzene(Sur) 90 % 60-140 8260B Benzene ND 1 5 0.18 ug/Kg 06/29/09 LZ 8260B Ethyl benzene ND 1 5 0.23 ug/Kg 06/29/09 LZ 8260B Methyl-tert-butylether(MTBE) ND 1 5 0.17 ug/Kg 06/29/09 LZ 8260B Toluene ND 1 5 0.17 ug/Kg 06/29/09 LZ 8260B Xylenes,total -ND 1 5 0.38 ug/Kg 06/29/09 LZ ' Surrogates Units Control Limits 8260B Surrl -Dibromofluoromethane 102 % 70-135 8260B Surr2-1,2-Dichloroethane-d4 105 % 70-135 ' 8260B Surr3-Toluene-d8 99 % 70-135 8260B Surr4-p-Bromofluorobenzene 101 % 70-135 ' EQL=Estimated Quantitation Limit, MDL=Method detection limit,DF=Dilution Factor ND=Not detected below indicated MDL,7=Trace,S=Surrogate outside control limits ' ASSOCIATED LABORATORIES Anahhiml Roculfc Rannrt ' Lab Request 236520 results,page 4 of 19 Order#: 1003626 Client Sample ID: 2-E-2' Matrix: SOLID Sample Description: Northern dispenser Island West dispenser Date Sampled: 06/23/2009 1 Method Analyte Result DF EQL MDL Units Date/Analyst 1 TPH-DHS Gasoline ND 1 3 0.018 mg/Kg 06/29/09 NZ 1 Surrogates Units Control Limits TPH-DHS p-Bromofluorobenzene(Sur) 85 % 60- 140 ' 8260B Benzene ND 1 5 0.18 ug/Kg 06/29/09 NZ 8260B Ethyl benzene ND l 5 0.23 ug/Kg 06/29/09 NZ 1 8260B Methyl-tert-butylether(MTBE) ND 1 5 0.17 ug/Kg 06/29/09 NZ 8260B Toluene ND 1 5 0.17 ug/Kg 06/29/09 NZ 8260B Xylenes,total ND 1 5 0.38 ug/Kg 06/29/09 NZ 1 Surrogates Units Control Limits 8260B Surrl-Dibromofluoromethane 99 % 70-135 8260B Surr2-1,2-Dichloroethane-d4 99 % 70- 135 1 8260B Surr3-Toluene-d8 102 % 70- 135 8260B Surr4-p-Bromofluorobenzene 97 % 70-135 1 1 i i 1 i 1 EQL=Estimated Quantitation Limit, MDL=Method detection limit,DF=Dilution Factor ND=Not detected below indicated MDL,J=Trace,S=Surrogate outside control limits 1 ASSOCIATED LABORATORIES nabrtiral Results Ronnrfi 1 Lab Request 236520 results,page 5 of 19 Order#: 1003627 Client Sample ID: '2-E-6' Matrix: SOLID Sample Description: Northern dispenser Island West dispenser Date Sampled: 06/23/2009 Method Analyte Result DF EQL MDL Units Date/Analyst TPH-DHS Gasoline ND 1 3 0.018 mg/Kg 06/26/09 NZ Surrogates Units Control Limits TPH-DHS p-Bromofluorobenzene(Sur) 87 % 60- 140 ' 8260B Benzene ND 1 5 0.18 ug/Kg 06/29/09 LZ 8260B Ethyl benzene ND 1 5 0.23 ug/Kg 06/29/09 LZ 8260B Methyl-tert-butylether(MTBE) ND 1 5 0.17 ug/Kg 06/29/09 LZ 8260B Toluene ND 1 5 0.17 ug/Kg 06/29/09 LZ 8260B Xylenes,total ND 1 5" 0.38 ug/Kg 06/29/09 LZ Surrogates Units Control Limits 8260B Surrl-Dibromofluoromethane 102 % 70- 135 8260B Sung-1,2-Dichloroethane-d4 104 % 70- 135 8260B Surr3-Toluene-d8 101 % 70- 135 8260B Surr4-p-Bromofluorobenzene 102 % 70- 135 1 ' EQL=Estimated Quantitation Limit, MDL=Method detection limit,DF=Dilution Factor ND=Not detected below indicated MDL,J=Trace,S=Surrogate outside control limits ASSOCIATED LABORATORIES Analvtiral Rocitltc Rcnnrt ' Lab Request 236520 results,page 6 of 19 Order#: 1003628 Client Sample ID: 2-W-2' Matrix: SOLID Sample Description: Northern dispenser Island West dispenser Date Sampled: 06/23/2009 1 Method Analyte Result DF EQL MDL Units Date/Analyst TPH-DHS Gasoline ND 1 3 0.018 mg/Kg 06/26/09 NZ Surrogates Units Control Limits TPH-DHS p-Bromofluorobenzene(Sur) 95 % 60-140 8260B Benzene ND 1 5 0.18 ug/Kg 06/29/09 LZ 8260B Ethyl benzene ND 1 5 0.23 ug/Kg 06/29/09 LZ 8260B Methyl-tert-butylether(MTBE) ND 1 5 0.17 ug/Kg 06/29/09 LZ 8260B Toluene ND 1 5 0.17 ug/Kg 06/29/09 LZ 8260B Xylenes,total ND 1 5 0.38 ug/Kg 06/29/09 LZ Surrogates Units Control Limits 8260B Surrl -Dibromofluoromethane 101 % 70- 135 9260B Surr2-1,2-Dichloroethane-d4 103 % 70-135 ' 8260B Surr3-Toluene-d8 101 % 70- 135 8260B Surr4-p-Bromofluorobenzene 101 % 70- 135 ,j EQL=Estimated Quantitation Limit, MDL=Method detection limit,DF=Dilution Factor ND=Not detected below indicated MDL,J=Trace,S=Surrogate outside control limits LA\ ' ASSOCIATED LABORATORIES AnalutirPl Rccidfc Rcnnrt ' Lab Request 236520 results,page 7 of 19 Order#: 1003629 Client Sample ID: 2-W-6' Matrix: SOLID Sample Description: Northern dispenser Island West dispenser Date Sampled: 06/23/2009 Method Analyte Result DF EQL MDL Units Date/Analyst TPH-DHS Gasoline ND 1 3 0.018 mg/Kg 06/27/09 NZ Surrogates Units Control Limits, TPH-DHS p-Bromofluorobenzene(Sur) 77 % 60-140 8260B Benzene ND 1 5 0.18 ug/Kg 06/29/09 LZ 8260B Ethyl benzene ND 1 5 0.23 ug/Kg 06/29/09 LZ 8260B Methyl-tert-butylether(MTBE) ND 1 5 0.17 ug/Kg 06/29/09 LZ 8260B Toluene ND 1 5 0.17 ug/Kg 06/29/09 LZ 8260B Xylenes,total ND 1 5 0.38 ug/Kg 06/29/09 LZ Surrogates Units Control Limits 8260B Surr] -Dibromofluoromethane 90 % 70-135 ' 8260B Surr2-1,2-Dichloroethane-d4 121 % 70-1-35 8260B Surr3-Toluene-d8 104 % 70- 135 8260B Surr4-p-Bromofluorobenzene 102 % 70-135 1 EQL=Estimated Quantitation Limit, MDL=Method detection limit,DF=Dilution Factor ND=Not detected below indicated MDL,J=Trace,S=Surrogate outside control limits ASSOCIATED L"01"TOIRMS pnahiticnl Racnitc Rannrt Lab Request 236520 results,page 8 of 19 1 Order#: 1003630 Client Sample ID: 3-E-2' ' Matrix:SOLID Sample Description: Northern dispenser Island West dispenser Date Sampled: 06/23/2009 1 Method Analyte Result DF EQL MDL Units Date/Analyst TPH-DHS Gasoline ND 1 3 0.018 mg/Kg 06/29/09 NZ ' Surrogates Units Control Limits TPH-DHS p-Bromofluorobenzene(Sur) 82 % 60-140 8260B Benzene ND 1 5 0.18 ug/Kg 06/29/09 LZ 8260B Ethyl benzene ND 1 5 0.23 ug/Kg 06/29/09 LZ ' 8260B Methyl-tert-butylether(MTBE) ND 1 5 0.17 ug/Kg 06/29/09 LZ 8260B Toluene ND 1 5 0.17 ug/Kg 06/29/09 LZ 8260B Xylenes,total ND 1 5 0.38 ug/Kg 06/29/09 LZ Surrogates Units Control Limits 8260B Surrl -Dibromofluoromethane 93 % 70-135 8260B Surr2-1,2-Dichloroethane-d4 112 % 70- 135 ' 8260B Surr3-Toluene-d8 106 % 70-135 8260B Surr4-p-Bromofluorobenzene 101 % 70-135 1 ' EQL=Estimated Quantitation Limit, MDL=Method detection limit,DF=Dilution Factor ND=Not detected below indicated MDL,J=Trace,S=Surrogate outside control limits ' ASSOM TED LABORA TORIES Analytical Results Renart ' Lab Request 236520 results,page 9 of 19 Order#: 1663631 Client Sample ID: 3-E-6' Matrix: SOLID Sample Description: Northern dispenser Island West dispenser Date Sampled: 06/23/2009 Method Analyte Result DF EQL MDL Units Date/Analyst TPH-DHS Gasoline ND 1 3 0.018 mg/Kg 06/27/09 NZ Surrogates Units Control Limits TPH-DHS p-Bromofluorobenzene(Sur) 81 % 60-140 ' 8260B Benzene ND 1 5 0.18 ug/Kg 06/29/09 LZ 8260B Ethyl benzene ND 1 5 0.23 ug/Kg 06/29/09 LZ 8260B Methyl-tert-butylether(MTBE) ND 1 5 0.17 ug/Kg 06/29/09 LZ 8260B Toluene ND 1 5 0.17 ug/Kg 06/29/09 LZ 8260B Xylenes,total ND 1 5 0.38 ug/Kg 06/29/09 LZ Surrogates Units Control Limits 8260B Surrl -Dibromofluoromethane 89 % 70-135 1 8260B Surr2-1,2-Dichloroethane-d4 119 % 70-135 8260B Surr3-Toluene-d8 100 % 70-135 8260B Surr4-p-Bromofluorobenzene 96 % 70-135 ,I 1 1 EQL=Estimated Quantitation Limit, MDL=Method detection limit,DF=Dilution Factor 1 ND=Not detected below indicated MDL,J=Trace,S=Surrogate outside control limits ASSOCIATED LABORATORIES Q„a,,,t;,a, Pocu,,tQ Rpnnrt ' Lab Request 236520 results,page 10 of 19 Order#: 10036321 Client Sample ID; 3-fit-2' Matrix: SOLID Sample Description: Northern dispenser Island West dispenser Date Sampled: 06/23/2009 Method Analyte Result DF EQL MDL Units Date/Analyst TPH-DHS Gasoline ND 1 3 0.018 mg/Kg 06/27/09 LZ Surrogates Units Control Limits TPH-DHS p-Bromofluorobenzene(Sur) 80 % 60- 140 8260B Benzene ND 1 5 0.18 ug/Kg 06/28/09 LZ 8260B Ethyl benzene ND 1 5 0.23 ug/Kg 06/28/09 LZ 8260B Methyl-tert-butylether(MTBE) ND 1 5 0.17 ug/Kg 06/28/09 LZ 8260B Toluene ND 1 5 0.17 ug/Kg 06/28/09 LZ 8260B Xylenes,total ND 1 5 0.38 ug/Kg 06/28/09 LZ Surrogates Units Control Limits 8260B Surrl -Dibromofluoromethane 94 % 70-135 8260B Surr2-1,2-Dichloroethane-d4 116 % 70- 135 8260B Surr3-Toluene-d8 107 % 70- 135 8260B Surr4-p-Bromofluorobenzene 99 % 70-135 N 1 EQL=Estimated Quantitation Limit, MDL=Method detection limit,DF=Dilution Factor ND=Not detected below indicated MDL,J=Trace,S=Surrogate outside control limits dA ASSOM TED LABORA TORIES pnahitical Results Ranad ' Lab Request 236520 results,page 11 of 19 Order#: 1003633 Client Sample ID: 3-W-6' Matrix: SOLID Sample Description: Northern dispenser Island West dispenser Date Sampled: 06/23/2009 Method Analyte Result DF EQL MDL Units Date/Analyst TPH-DHS Gasoline ND 1 3 0.018 m g/Kg 06/27/09 NZ Surrogates Units Control Limits TPH-DHS p-Bromofluorobenzene(Sur) 83 % 60-140 8260B Benzene ND 1 5 0.18 ug/Kg 06/28/09 LZ 8260B Ethyl benzene ND 1 5 0.23 ug/Kg 06/28/09 LZ 8260B Methyl-tert-butylether,(MTBE) ND 1 5 0.17 ug/Kg 06/28/09 LZ 8260B Toluene ND 1 5 0.17 ug/Kg 06/28/09 LZ 8260B Xylenes,total ND 1 5 0.38 ug/Kg 06/28/09 LZ Surrogates Units Control Limits 8260B Surrl -Dibromofluoromethane 94 % 70- 135 8260B Surr2-1,2-Dichloroethane-14 115 % 70-135 8260B Surr3-Toluene-d8 106 % 70-135 8260B Surr4 p Bromofluorobenzene 94 % 70-135 i EQL=Estimated Quantitation Limit, MDL=Method detection limit,DF=Dilution Factor ND=Not detected below indicated MDL,)=Trace,S=Surrogate outside control limits LA\ ASSOCIATED LABORATORIES �nahrticai Racnl4c Rpnnrt ' Lab Request 236520 results,page 12 of 19 Order#: 1 10036341 Client Sample ID; 4-E-2' Matrix: SOLID Sample Description: Northern dispenser Island West dispenser Date Sampled: 06/23/2009 Method Analyte Result DF EQL MDL Units Date/Analyst 8260B Benzene ND 1 5 0.18 ug/Kg 06/28/09 LZ 8260B Ethyl benzene ND 1 5 0.23 ug/Kg 06/28/09 LZ 8260B Methyl-teit-butylether(MTBE) ND 1 5 0.17 ug/Kg 06/28/09 LZ 8260B Toluene ND 1 5 0.17 ug(Kg 06/28/09 LZ 8260B Xylenes,total ND 1 5 0.38 ug/Kg 06/28/09 LZ Surrogates Units Control Limits 8260B Surrl-Dibromofluoromethane 93 % 70-135 8260B Surr2-1,2-Dichloroethane-d4 107 % 70-135 8260B Surr3-Toluene-d8 103 % 70-135 8260B Surr4-p-Bromofluorobenzene 106 % 70-135 8015 TEPH Diesel 245 20 20.0 7.4 mg/Kg 07/01/09 AF Surrogates Units Control Limits 8015 Triacontane(Sur) 70 % 60-140 1 1 EQL=Estimated Quantitation Limit, MDL=Method detection limit DF=Dilution Factor ND=Not detected.below indicated MDL,J=Trace,S=Surrogate outside control limits A C SSO IA TED LABORATORIES pnahrtiral Raciiltc Rannrt Lab Request 236520 results,page 13 of 19 Order#: 1 10036351 Client Sample ID: 4-E-6' Matrix:SOLID Sample Description: Northern dispenser Island West dispenser Date Sampled: 06/23/2009 Method Analyte Result DF EQL MDL Units Date/Analyst 1 8260B Benzene ND 1 5 0.18 ug/Kg 06/28/09 LZ I 8260B Ethyl benzene ND 1 5 0.23 ug/Kg 06/28/09 LZ 8260B Methyl-tert-butylether(MTBE) ND 1 5 0.17 ug/Kg 06/28/09 LZ 8260B 'Toluene ND 1 5 0.17 ug/Kg 06/28/09 LZ 8260B Xylenes,total ND 1 5 0.38 ug/Kg 06/28/09 LZ Surrogates Units Control Limits 8260B Surrl -Dibromofluoromethane 92 % 70-135 1 8260B Surr2- 1,2-Dichloroethane-d4 114 % 70- 135 8260B Surr3-Toluene-d8 101 % 70-135 1260B Surr4-p-Bromofluorobenzene 91 % 70-135 8015 TEPH Diesel 273 20 20.0 7.4 mg/Kg 07/01/09 AF Surrogates Units Control Limits 8015 Triacontane(Sur) 64 % 60-140 1 r EQL=Estimated Quantitation Limit, MDL=Method detection limit,DF=Dilution Factor ND=Not detected below indicated MDL,]=Trace,S=Surrogate outside control limits LA\ ASSOCLA TED LABORATORIES Anahitiral Results Rannrr Lab Request 236520 results,page 14 of 19 Order#: 1003636 Client Sample ID: 4-W-2' ' Matrix:SOLID Sample Description: Northern dispenser Island West dispenser Date Sampled: 06/23/2009 Method Analyse Result DF EQL MDL Units Date/Analyst 8260B Benzene ND 1 5 0.18 ug/Kg 06/28/09 LZ 8260B Ethyl benzene ND 1 5 0.23 ug/Kg 06/28/09 LZ 8260B Methyl-tert-butylether(MTBE) ND 1 5 0.17 ug/Kg 06/28/09 LZ 8260B Toluene ND 1 5 0.17 ug/Kg 06/28/09 LZ 8260B Xylenes,total ND 1 5 0.38 ug/Kg 06/28/09 LZ Surrogates Units Control Limits 8260B Surrl -Dibromofluoromethane 97 % 70-135 1 8260B Surr2- 1,2-Dichloroethane-d4 109 % 70- 135 8260B Surr3-Toluene-d8 107 % 70- 135 8260B Surr4-p-Bromofluorobenzene 94 % 70- 135 8015 TEPH Diesel 0.42 J 1 1.0 0.37 mg/Kg 06/30/09 AF Surrogates Units Control Limits 8015 Triacontane(Sur) 103 % 60-140 r EQL=Estimated Quantitation Limit, MDL=Method detection limit,DF=Dilution Factor ND=Not detected below indicated MDL,J=Trace,S=.Surrogate outside control limits ASSOM TED LABORATOAVMS AnahilirM Ractdlfc Rannrt Lab Request 236520 results,page 15 of 19 1 Order#: 1003637 Client Sample ID: 4-W-6' Matrix: SOLID Sample Description: Northern dispenser Island West dispenser Date Sampled: 06/23/2009 Method Analyte Result DF EQL MDL Units Date/Analyst 8260B Benzene ND 1 5 0.18 ug/Kg 06/28/09 LZ ' 8260B Ethyl benzene ND 1 5 0.23 ug/Kg 06/28109 LZ 8260B Methyl-tert-butylether(MTBE) ND 1 5 0.17 ug/Kg 06/28/09 LZ 8260B Toluene ND 1 5 0.17 ug/Kg 06/28/09 LZ 8260B Xylenes,total ND 1 5 0.38 ug/Kg 06/28/09 LZ 1 Surrogates Units Control Limits 8260B Sun I -Dibromofluoromethane 95 % 70-135 8260B Surr2- 1,2-Dichloroethane-d4 115 % 70- 135 8260B Surr3-Toluene-d8 108 % 70- 135 8260B Surr4-p-Bromofluorobenzene 95 % 70- 135 8015 TEPH Diesel 8.4 1 1.0 0.37 mg/Kg 06/30/09 AF Surrogates Units Control Limits 8015 Triacontane(Sur) 128 % 60-140 r t r EQL=Estimated Quantitation Limit, MDL=Method detection limit,DF=Dilution Factor ND=Not detected below indicated MDL,1=Trace,S=Surrogate outside control limits ASSOCIA TED LABORATORIES Anahitee-ni Racuilre Rcnnrt ' Lab Request 236520 results,page 16 of 19 Order#: 1003638 Client Sample ID; 5-2' Matrix: SOLID Date Sampled: 06/23/2009 Method Analyte Result DF EQL MDL Units Date/Analyst 8260B Benzene ND 1 5 0.18 ug/Kg 6/28/09 LZ g 8260B Ethyl benzene ND 1 5 0.23 ug/Kg 06/28/09 LZ 8260B Methyl-tert-butylether(MTBE) ND 1 5 0.17 ug/Kg 06/28/09 LZ 8260B Toluene ND 1 5 0.17 ug/Kg 06/28/09 LZ 8260B Xylenes,total ND 1 5 0.38 ug/Kg 06/28/09 LZ ' Surrogates Units Control Limits 8260B Surrl-Dibromofluoromethane 97 % 70- 135 8260B Surr2-1,2-Dichloroethane-d4 109 % 70-135 8260B Surr3-Toluene=d8 109 % 70-135 8260B Surr4-p-Bromofluorobenzene 99 % 70- 135 8015 TEPH Diesel 916 50 50.0 18.5 mg/Kg K 07/01/09 AF Surrogates Units Control Limits 8015 Triacontane(Sur) 116 % 60- 140 1 1 EQL=Estimated Quantitation Limit, MDL=Method detection limit,DF=Dilution Factor ND=Not detected below indicated MDL,J=Trace,S=Surrogate outside control limits ASSOCIATED LABORATORIES Anandir,l Results Ronnh Lab Request 236520 results,page 17 of 19 r Order#: 1003639 Client Sample ID; 5-6' Matrix: SOLID Date Sampled: 06/23/2009 1 Method Analyte Result DF EQL MDL Units Date/Analyst 1 8260B Benzene ND 1 5 0.18 ug/Kg 06/28/09 LZ 8260B Ethyl benzene ND 1 5 0.23 ug/Kg 06/28/09 LZ 8260B Methyl-tert-butylether(MTBE) ND 1 5 0.17 ug/Kg 06/28/09 LZ 8260B Toluene ND 1 5 0.17 ug/Kg 06/28/09 LZ 8260B Xylenes,total ND 1 5 0.38 ug/Kg 06/28/09 LZ rSurrogates Units Control Limits 8260B Surrl -Dibromofluoromethane 97 % 70- 135 8260B Surr2-1,2-Dichloroethane-d4 124 % 70-135 8260B Surr3-Toluene-d8 110 % 70- 135 8260B Surr4-p-Bromofluorobenzene 93 % 70- 135 1 8015 TEPH Diesel 25 1 1.0 0.37 mg/Kg 07/01/09 AF Surrogates Units Control Limits 8015 Triacontane(Sur) 83 % 60- 140 1 . r r r 1 1 1 , r EQL=Estimated Quantitation Limit, MDL=Method detection limit,DF=Dilution Factor ND=Not detected below indicated MDL,J=Trace,S=Surrogate outside control limits LA r ASSOCIATED LABORATORIES Analutiml Results Rennrt ' Lab Request 236520 results,page 18 of 19 Order#: 1003640 Client Sample ID; Laboratory Method Blank ' Matrix: SOLID Method Analyte Result DF EQL MDL Units Date/Analyst TPH-DHS Gasoline ND •1 3 0.018 mg/Kg 06/26/09 NZ ' Surrogates Units Control Limits TPH-DHS p-Bromofluorobenzene(Sur) 66 % 60-140 8260B Benzene ND 1 5 0.18 ug/Kg 06/28/09 LZ 8260B Ethyl benzene ND 1 5 0.23 ug/Kg 06/28/09 LZ 8260B Methyl-tert-butylether(MTBE) ND 1 5 0.17 ug/Kg 06/28/09 LZ 8260B Toluene ND 1 5 0.17 ug/Kg 06/28/09 LZ 8260B Xylenes,total ND 1 5 0.38 ug/Kg 06/28/09 LZ rSurrogates Units Control Limits 8260B Surrl -Dibromofluoromethane 89 % 70 - 135 8260B Surr2- 1,2-Dichloroethane-d4 107 % 70-135 8260B Surr3-Toluene-d8 107 % 70-135 8260B Surr4-p-Bromofluorobenzene 99 % 70- 135 ' 8015 TEPH Diesel ND 1 1.0 0.37 mg/Kg 06/29/09 AF ' Surrogates Units Control Limits 8015 Triacontane(Sur) 92 % 60- 140 EQL=Estimated Quantitation Limit, MDL=Method detection limit,DF=Dilution Factor ND=Not detected below indicated MDL,J=Trace,S=Surrogate outside control limits jAk ASSOCIATED LABORATORIES o„a,,,ti,,,Qpr,,,tQ Rp,,,,r+ ' Lab Request 236520 results,page 19 of 19 CHAIN-OF-CUSTODY RECORD z gc- 5z° ClientG Dat�//2 I/�3 / LAB Project# G Analysis Requested Project Name Client Project# Page of Project Address Turn Around Requested: a Lab Use Only. O t h p 24-Hour-Rush 00 ,�lr' d Sample Condition , r'A _ 48-Hour-Rush N as received: t7 CJ's ii a pp c Normal Sampler's Signature ��; t� Chlll es No Mobile Lab o ca o Seale /No >�od od m 1- 1 a 'SL- a Sam mple Location Time ontainer Comments zo pie Sa Date IM 5 Alm 031,01 J A V� S Lv �S SPrv' S 3- O Re nqulshed b :(Slgnature D to 2�O ived b ( Date 1Sld y Total Number of Containers Co any: Time Company: Time�� nquish J b .(S g ) Qate 0 Received by Laboratory:(Signature) Date -ADVANCED ENVIRONMENTAL CONCEPTS INc- Oslo , le 661A95-1646 220 E.TRUXTUN AVENUE mpeny Time^� Compan Time q FAX 661M95.1616 BAKERSFIELD.CA 93305 E-mail:aednc®sbcglobal.net CHAIN-OF-CUSTODY RECORD Client Date LAB Project# 2 3 Analysis Requested Pro_ jest N9T8 r � Client Project# � L'� Page ^ of Project g; Turn Around Requested: a l� in Lab Use Only. ❑ 24-Hour-Rush in a jJyl Sample Condition ��QQvV r.5� - ❑ 48-Hour-Rush P i� i as received: Sampler's Signature °�� IS Chilled s/ o 3J Moblle Lab o 1 t Sealed Yes/ o $ EE E9 E Sample • - • • Date �f/lZ tJJfA Z Container Comments -�.'w-6 r� S ✓ f -w-Z' � 5 ✓' I 4-W-6 S 1 5-2 Sys wtv �5�^ 11 Q Re nquishe by Ignature) D t _ e teed by Sign '—"'� Date d S /�Zsl v Total Number of Containers Com Time C mpany: Time 11.h (4 `1'-� Q�IrlinqLds�y- g e) late r Q Received by oratory:(Signature)� � Date q -ADVANCED ENMOONMENTAL CONCEPTS WC- 661/3951646 220 E.TRUXTUN AVENUE C Time CF6 Compart, Time FAX 661)395-1616 BAKERSFIELD.CA 93305 o E-mail:ascinc@sbcglobal.net Advanced Environmental Concepts;Inc. "Attachment C" TABLES 1 ' Walker Fuels 4600 Stine Road Soil Samples June 23, 2009 Sample Ethyl Date TPH-d TPH-q Benzene Benzene MTBE Toluene X lenes Well I.D. 1-E-2' 06/23/2009 NA ND<3 ND<5 ND<5 ND<5 ND<5 ND<5 ' 1-E-6' 06123/2009 NA ND<3 ND<5 ND<5 ND<5 ND<5 ND<5 1-W-2' 06/23/2009 NA ND<3 ND<5 ND<5 ND<5 ND<5 ND<5 1-W-6' 06/23/2009 NA ND<3 ND<5 ND<5 ND<5 ND<5 ND<5 2-E-2' 06/23/2009 NA ND<3 ND<5 ND<5 ND<5 ND<5 ND<5 ' 2-E-6' 06/23/2009 NA ND<3 ND<5 ND<5 ND<5 ND<5 ND<5 2-W-2' 06/23/2009 NA ND<3 ND<5 ND<5 ND<5 ND<5 ND<5 2-W-6' 06/23/2009 NA ND<3 ND<5 ND<5 ND<5 ND<5 ND<5 ' 3-E-2' 06/23/2009 NA ND<3 ND<5 ND<5 ND<5 ND<5 ND<5 3-E-6' 06/23/2009 NA ND<3 ND<5 ND<5 ND<5 ND<5 ND<5 ' 3-W-2' 06/23/2009 NA ND<3 ND<5 ND<5 ND<5 ND<5 ND<5 3-W-6' 06/23/2009 NA ND<3 ND<5 ND<5 ND<5 ND<5 ND<5 4-E-2' 06/23/2009 245 NA ND<5 ND<5 ND<5 ND<5 ND<5 ' 4-E-6' 06/23/2009 273 NA ND<5 ND<5 ND<5 ND<5 ND<5 4-W-2' 06/23/2009 0.42 J NA ND<5 ND<5 ND<5 ND<5 ND<5 4-W-6' 06/23/2009 8.4 NA ND<5 ND<5 ND<5 ND<5 ND<5 5-2' 06/23/2009 916 NA ND<5 ND<5 ND<5 ND<5 ND<5 5-6' 06/23/2009 1 26 NA ND<5 ND<5 ND<5 ND<5 ND<5